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Journal articles on the topic 'N-Methylphenyl thiourea'

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Published: 5 June 2025

Last updated: 1 August 2025

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1

Zhang, Bin, Bi-Quan Su, and Liang Xian. "N-Benzoyl-N′-(2-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 62, no. 9 (2006): o4024—o4026. http://dx.doi.org/10.1107/s1600536806032740.

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2

Lin, Qi, You-Ming Zhang, Tai-bao Wei, and Hai Wang. "N-Ethoxycarbonyl-N′-(2-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 60, no. 4 (2004): o580—o582. http://dx.doi.org/10.1107/s1600536804005161.

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3

Yusof, M. Sukeri M., A. Sahali Mardi, and Bohari M. Yamin. "N-(4-Methoxybenzoyl)-N′-(4-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 61, no. 10 (2005): o3357—o3358. http://dx.doi.org/10.1107/s1600536805029478.

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4

Razis, S. Aminah A., M. Sukeri M. Yusof, A. Maisara Kadir, and Bohari M. Yamin. "N-(4-Methylbenzoyl)-N′-(4-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 63, no. 11 (2007): o4395. http://dx.doi.org/10.1107/s1600536807049720.

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The title compound, C16H16N2OS, adopts a trans–cis configuration of the 4-methylbenzoyl and 4-methylphenyl groups, with respect to the thiono S atom across the thiourea C—N bonds. The dihedral angle between the two groups is 10.36 (8)°. The structure is stabilized by intermolecular hydrogen bonds which form dimers. There are also intramolecular hydrogen bonds.

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5

Xian, Liang. "N-(3-Methylphenyl)-N′-(4-nitrobenzoyl)thiourea." Acta Crystallographica Section E Structure Reports Online 64, no. 10 (2008): o1969. http://dx.doi.org/10.1107/s1600536808029425.

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6

Semwal, Amit, Amit Nigam, and D. C. P. Singh. "Synthesis, Characterization and Biological Activity of Novel N-p-methylbenzoyl-N’ substituted thiourea." International Journal of Drug Design and Discovery 2, no. 4 (2011): 654–58. https://doi.org/10.37285/ijddd.2.4.7.

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A series of N-p-methylbenzoyl-N’ thiourea derivatives bearing different substituents have been synthesized and screened in order to evaluate for their antibacterial and antifungal activity. Antibacterial and antifungal activity of the title compounds has been evaluated by varying the substituents in the thiourea moiety. Reaction of p-methylbenzoyl chloride with ammonium thiocynate followed by the addition of various aromatic amines afforded N-p-methylbenzoyl-N’ substituted thiourea. The structures of newly synthesized compounds has been supported by IR and 1HNMR spectral analysis. Among the sy

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7

Zhang, You-Ming, Liang Xian та Tai-Bao Wei. "Chlorobis[N′-ethoxycarbonyl-N-(4-methylphenyl)thiourea-κS]copper(I)". Acta Crystallographica Section C Crystal Structure Communications 59, № 11 (2003): m473—m474. http://dx.doi.org/10.1107/s0108270103022285.

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The title complex, chlorobis{ethyl N-[(4-methylanilino)thiocarbonyl]carbamate-κS}copper(I), [CuCl(C11H14N2O2S)2], was synthesized by the reaction of cupric chloride with the corresponding thiourea derivative. The complex has imposed crystallographic m symmetry and the CuI coordination environment is trigonal planar, formed by two S atoms and one Cl atom. The formation of intramolecular hydrogen bonds promotes the stability of the complex.

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8

Yeo, Chien, and Edward Tiekink. "1-[N-Methyl-N-(Phenyl)amino]-3- (4-Methylphenyl)Thiourea." Molbank 2019, no. 1 (2019): M1052. http://dx.doi.org/10.3390/m1052.

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The title compound, 1-[N-methyl-N-(phenyl)amino]-3-(4-methylphenyl)thiourea (1), was synthesized by the reaction of 1-methyl-1-phenyl hydrazine and 4-tolyl isothiocyanate, and was characterized by spectroscopy (1H and 13C{1H} NMR, IR, and UV), elemental analysis as well as by single crystal X-ray crystallography. In the solid state, the molecule exists as the thioamide tautomer and features an anti-disposition of the thioamide–N–H atoms; an intramolecular N–H⋯N hydrogen bond is noted. The molecular conformation resembles that of the letter L. In the molecular packing, thioamide-N1–H⋯S1(thione)

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9

Dolzhenko, Anton V., Geok Kheng Tan, Lip Lin Koh, Anna V. Dolzhenko, and Wai Keung Chui. "N-Carbethoxy-N′-[3-(4-methylphenyl)-1H-1,2,4-triazol-5-yl]thiourea." Acta Crystallographica Section E Structure Reports Online 66, no. 3 (2010): o549—o550. http://dx.doi.org/10.1107/s1600536810004289.

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10

Du, Hai-Tang, Ming Lu, Wei-Yi Zhou, and Li-Li Sun. "N-(5-Chloro-3-methyl-1-phenylpyrazol-4-ylcarbonyl)-N′-(4-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 63, no. 11 (2007): o4287. http://dx.doi.org/10.1107/s1600536807043541.

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The crystal structure of the title compound, C19H17ClN4OS, has been determined in order to elucidate the molecular conformation. The pyrazole ring makes dihedral angles of 74.3 (3)° and 2.9 (3)° with the phenyl and tolyl rings, respectively; these two six-membered rings are twisted by 71.6 (3)° with respect to each other. The crystal packing of the title compound is stabilized by intramolcular N—H...O and intermolcular N—H...S hydrogen bonds.

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11

Touadjine, A. M., A. Mostefai, A. Rahmouni, S. Humbel та A. Krallafa. "A theoretical study of atropisomerism in N-(2-methylphenyl)-N′-(2-methylphenyl) thiourea and its inclusion in the β-cyclodextrin". Journal of Inclusion Phenomena and Macrocyclic Chemistry 88, № 3-4 (2017): 199–207. http://dx.doi.org/10.1007/s10847-017-0719-3.

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12

Uckun, Fatih M., Chen Mao, Sharon Pendergrass, et al. "N-[2-(4-Methylphenyl)Ethyl]-N′-[2-(5-Bromopyridyl)]-Thiourea as a Potent Inhibitor of NNRTI-Resistant and Multidrug-Resistant Human Immunodeficiency Virus Type 1." Antiviral Chemistry and Chemotherapy 11, no. 2 (2000): 135–40. http://dx.doi.org/10.1177/095632020001100205.

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The composite non-nucleoside reverse transcriptase inhibitor (NNRTI) binding pocket model was used to study a number of thiourea analogues with different substitutions at the 4-phenyl position including N-[2-(4-methylphenyl)ethyl]-N′-[2-(5-bromopyridyl)]-thiourea (compound HI-244), which inhibited recombinant RT better than trovirdine or compound HI-275 with an unsubstituted phenyl ring. HI-244 effectively inhibited the replication of HIV-1 strain HTLVIIIB in human peripheral blood mononuclear cells with an IC50 value of 0.007 μM, which is equal to the IC50 value of trovirdine. Notably, HI-244

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13

ZHANG, Lei, Donglan MA, Jianping LI, and Yulu WANG. "Synthesis of N-o-Methylphenyl-N′-(sodium p-aminobenzene-sulfonate) thiourea and Its Chromogenic Reaction with Palladium(II)." Analytical Sciences 22, no. 7 (2006): 989–92. http://dx.doi.org/10.2116/analsci.22.989.

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14

Yardily, Dr A. "Molecular structure, Vibrational assignment, HOMO-LUMO and Mulliken analysis of 2-[4-amino-2-(4-methylphenylamino) thiazol-5-oyl]benzothiazole(AMPATOB)." Green Chemistry & Technology Letters 2, no. 1 (2016): 38. http://dx.doi.org/10.18510/gctl.2016.218.

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The compound 2-[4-amino-2-(4-methylphenylamino) thiazol-5-oyl]benzothiazole (AMPATOB) was prepared from 1-(4-methylphenyl)-3-(N-nitroamidino)thiourea and 2-(2-bromoacetyl)benzothiazole in the presence of triethylamine and characterised by FTIR, NMR and mass spectra. The geometry of the molecule was investigated and optimized with the help of B3LYP/ 6-31G density functional theory (DFT) method using Gaussian 09 software package.The calculated geometries such as bond lengths, bond angles, dihedral angles, atomic charges, harmonic vibrational wave numbers and intensities of vibrational bonds of t

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15

Mohamad Nasri, Nur Ain, and Juliana Jumal. "A PRELIMINARY STUDY ON DETECTION OF CADMIUM (II) ION USING BENZOYL PHENYLTHIOUREA." Journal of Wastes and Biomass Management 2, no. 1 (2020): 09–14. http://dx.doi.org/10.26480/jwbm.01.2020.09.14.

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Two benzoyl phenylthiourea derivatives namely: 1-benzoyl-3-(4-bromophenyl)-2- thiourea (M) and 1-(4-chlorobenzoyl)-3-(4-methylphenyl)-2-thiourea (MI) were successfully synthesized and characterized by using Carbon, Hydrogen and Nitrogen (CHN) micro elemental analysis, Fourier Transform Infra-Red (FTIR) and Nuclear Magnetic Resonance (NMR) spectroscopy methods. Elemental analysis for M (C14H11N2SOBr) and MI (C15H13N2SOCl) were compatible with the expected theoretical calculation. The FTIR spectrum obtained for M and MI compounds show the presence of four important functional groups; ʋ(N-H), ʋ(C

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16

Sardohan-Koseoglu, Tugba, Ulviye Beyza Ogul, Esengul Kır, and Fatma Karipcin. "Chemical modification of expanded glass aggregate with N-Benzoyl-N′-(4-methylphenyl) thiourea (TTU) for the adsorptive removal of Cr(III) ion." Arabian Journal of Chemistry 12, no. 6 (2019): 772–79. http://dx.doi.org/10.1016/j.arabjc.2015.11.009.

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17

Stevens, Gregory J., Karen Hitchcock, Y. Karen Wang, et al. "In VitroMetabolism ofN-(5-Chloro-2-methylphenyl)-N‘-(2-methylpropyl)thiourea: Species Comparison and Identification of a Novel Thiocarbamide−Glutathione Adduct." Chemical Research in Toxicology 10, no. 7 (1997): 733–41. http://dx.doi.org/10.1021/tx9700230.

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18

Abosadiya, Hamza M., El Hassane Anouar, Siti Aishah Hasbullah, and Bohari M. Yamin. "Synthesis, X-ray, NMR, FT-IR, UV/vis, DFT and TD-DFT studies of N-(4-chlorobutanoyl)-N′-(2-, 3- and 4-methylphenyl)thiourea derivatives." Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 144 (June 2015): 115–24. http://dx.doi.org/10.1016/j.saa.2015.01.092.

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19

Gowda, B. Thimme, Sabine Foro, and Sharatha Kumar. "3-Acetyl-1-(3-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 68, no. 8 (2012): o2574. http://dx.doi.org/10.1107/s1600536812032825.

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In the crystal structure of the title compound, C10H12N2OS, the conformation of the two N—H bonds areantito each other. The amide C=O and the C=S are are alsoantito each other. The N—H bond adjacent to the benzene ring issynto them-methyl groups. The dihedral angle between the benzene ring and the side chain [mean plane of atoms C—C(O)N—C—N; maximum deviation 0.029 (2) Å] is 14.30 (7)°. There is an intramolecular N—H...O hydrogen bond generating anS(6) ring motif. In the crystal, the molecules are linkedviaN—H...) hydrogen bonds, forming chains propagating along [001]. The S atom is disordered

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20

Shahwar, Durre, M. Nawaz Tahir, Muhammad Mansha Chohan, Naeem Ahmad, and M. Asam Raza. "3-Acetyl-1-(2-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 68, no. 4 (2012): o1160. http://dx.doi.org/10.1107/s1600536812011658.

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In the title compound, C10H12N2OS, the toluene and theN-carbamothioylacetamide units are oriented at dihedral angle of 78.75 (5)°. An intramolecular N—H...O hydrogen bond generates anS(6) ring. In the crystal, molecules are linked into [101] chains by pairs of N—H...S hydrogen bonds [which generateR22(8) loops] and pairs of O—H...O hydrogen bonds [which generateR22(4) loops]. The two motifs alternate in the chain.

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21

Saeed, Aamer, and Ulrich Flörke. "1-(3-Methylbenzoyl)-3-(2-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 63, no. 3 (2007): o1390—o1392. http://dx.doi.org/10.1107/s1600536807007519.

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In the structure of the title compound, C16H16N2OS, the dihedral angle between the two aromatic ring planes is 68.08 (9)°. Intermolecular N—H...S hydrogen bonds link the molecules into dimeric units which are stacked along [100].

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22

Jotani, Mukesh M., Chien Ing Yeo, and Edward R. T. Tiekink. "Crystal structure of 1-(4-methylphenyl)-3-(propan-2-ylideneamino)thiourea." Acta Crystallographica Section E Crystallographic Communications 71, no. 10 (2015): 1236–41. http://dx.doi.org/10.1107/s2056989015017624.

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In the title thiosemicarbazone, C11H15N3S, thep-tolyl-N—H and imino-N—H groups areantiandsyn, respectively, to the central thione-S atom. This allows for the formation of an intramolecularp-tolyl-N—H...N(imino) hydrogen bond. The molecule is twisted with the dihedral angle between thep-tolyl ring and the non-hydrogen atoms of the N=CMe2residue being 29.27 (8)°. The crystal packing features supramolecular layers lying in thebcplane whereby centrosymmetric aggregates sustained by eight-membered thioamide {...HNCS}2synthons are linked by further N—H...S hydrogen bonds. Layers are connectedviameth

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23

Abdel-Wahab, Bakr F., Ehab Abdel-Latif, Seik Weng Ng, and Edward R. T. Tiekink. "5-(4-Fluorophenyl)-3-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazol-4-yl]-4,5-dihydro-1H-pyrazole-1-carbothioamide." Acta Crystallographica Section E Structure Reports Online 68, no. 6 (2012): o1954—o1955. http://dx.doi.org/10.1107/s1600536812024245.

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In the title compound, C20H19FN6S, the pyrazole ring has an envelope conformation, with the methine C atom being the flap atom. The dihedral angle between the least-squares plane through the pyrazole and triazole rings is 7.59 (9)°, and the triazole and attached benzene ring form a dihedral angle of 74.79 (9)°. The thiourea group is coplanar with the pyrazole ring [N—N—C—S torsion angle = −179.93 (11)°], which enables the formation of an intramolecular N—H...N hydrogen bond. In the crystal, inversion-related molecules associate via N—H...S hydrogen bonds and eight-membered {...HNCS}2 synthons

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24

Satheesh, Sandhya, Akhila Radha, Krishnapriya Girija, Kallikat Rajasekharan та Priya Maheswari. "Hindered phenolic aminothiazoles - synthesis, α-glucosidase, α-amylase inhibitory and antioxidant activities". Journal of the Serbian Chemical Society 82, № 10 (2017): 1087–95. http://dx.doi.org/10.2298/jsc161005084s.

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Base-catalysed heterocyclization of either N-aryl-N'-[imino(nitroamino) methyl]thioureas or N-aryl-N'-cyanothioureas by reaction with 2-bromo- 1-(2,6-di-t-butyl-4-hydroxyphenyl)ethanone afforded 4-amino-2-(arylamino)- -5-(3,5-di-t-butyl-4-hydroxybenzoyl)thiazoles, designed as molecular hybrids of hindered phenolic and 2-aminothiazole moieties. These compounds were screened for their inhibition activity on carbohydrate hydrolyzing enzymes. Thus, [4-amino-2-(phenylamino)-5-thiazolyl](3,5-di-t-butyl-4-hydroxyphenyl)- methanone exhibited ?-glucosidase inhibition activity with an IC50 value of 117

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