Dissertations / Theses: 'NbC composite'

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SANTOS, THAIS da S. "Micro-nanocompósitos de Al2O3/ NbC/ WC e Al2O3/ NbC/ TaC." reponame:Repositório Institucional do IPEN, 2014. http://repositorio.ipen.br:8080/xmlui/handle/123456789/23599.

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Dissertação (Mestrado em Tecnologia Nuclear)
IPEN/D
Instituto de Pesquisas Energeticas e Nucleares - IPEN-CNEN/SP

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FERREIRA, VANDERLEI. "Processamento, caracterizacao mecanica e tribologica do composito Alsub(2)Osub(3)-Nbc." reponame:Repositório Institucional do IPEN, 2001. http://repositorio.ipen.br:8080/xmlui/handle/123456789/10894.

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Dissertacao (Mestrado)
IPEN/D
Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP

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TONELLO, KAROLINA P. dos S. "Compositos a base de Alsub(2)Osub(3) com adicoes de NbC e de MgO." reponame:Repositório Institucional do IPEN, 2009. http://repositorio.ipen.br:8080/xmlui/handle/123456789/11780.

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Dissertação (Mestrado)
IPEN/D
Instituto de Pesquisas Energeticas e Nucleares - IPEN-CNEN/SP

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PANELLI, RENATO. "Processamento do aco AISI M2 com adicao de 10 porcento vol. NbC utilizando a tecnica de mechanical alloying." reponame:Repositório Institucional do IPEN, 1999. http://repositorio.ipen.br:8080/xmlui/handle/123456789/10748.

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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
Dissertacao (Mestrado)
IPEN/D
Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP
FAPESP:96/08958-1

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Salem, Raphael Euclides Prestes. "Desenvolvimento de ZrO2/Al2O3 e ZrO2/Al2O3-NbC usando sinterização convencional e não convencional." Universidade de São Paulo, 2017. http://www.teses.usp.br/teses/disponiveis/74/74133/tde-26022018-094441/.

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Os compósitos cerâmicos de alto desempenho têm sido objeto de frequentes estudos nas últimas décadas, visando à melhora das propriedades mecânicas e ao aumento da sua gama de aplicações em produtos tecnológicos. Este trabalho consistiu em estudar a preparação, a sinterização convencional e não convencional e as propriedades mecânicas e tribológicas resultantes de dois sistemas compósitos: t-ZrO2/Al2O3 e t-ZrO2/Al2O3-NbC. No sistema t-ZrO2/Al2O3 foram estudadas as composições de 0, 5 e 15% em volume de Al2O3 usando pós comerciais. No sistema t-ZrO2/Al2O3-NbC, foi usado um pó nanocristalino de Al2O3-NbC, obtido por moagem reativa de alta energia e adicionado na proporção de 5% em volume à matriz de t-ZrO2. Os pós foram prensados uniaxial e isostaticamente e sinterizados em forno convencional e pelas técnicas de flash sintering (FS) (t-ZrO2/Al2O3) e spark plasma sintering (SPS) (t-ZrO2/Al2O3-NbC). Os compósitos t-ZrO2/Al2O3 sinterizados convencionalmente e t-ZrO2/Al2O3-NbC sinterizados convencionalmente e por SPS foram caracterizados por medidas de densidade aparente, dilatometria, microscopia eletrônica de varredura (MEV), e medidas de propriedades mecânicas: dureza, módulo de Young e tenacidade à fratura. Os compósitos t-ZrO2/Al2O3 sinterizados por FS foram caracterizados por medidas de densidade aparente, dilatometria in situ e MEV. Os nanocompósitos de t-ZrO2/Al2O3-NbC foram também caracterizados quanto à resistência ao desgaste pelo método esfera-no-disco, utilizando esferas de Al2O3 e WC-6%Co como contramateriais. Os resultados mostraram que a moagem reativa de alta energia foi completa e efetiva na obtenção de pós nanométricos de Al2O3-NbC, com tamanhos de cristalito de 9,1 nm para Al2O3 e 9,7 nm para o NbC. A desaglomeração posterior à moagem de alta energia foi eficaz na redução do tamanho de aglomerados. Os compósitos t-ZrO2/Al2O3 e t-ZrO2/Al2O3-NbC sinterizados convencionalmente e ZrO2/Al2O3-NbC sinterizados por SPS mostraram alta densificação (>97% DT e boas propriedades mecânicas. Os nanocompósitos de t-ZrO2/Al2O3 sinterizados por FS apresentaram uma densificação ultrarrápida (< 1 min) com retração linear superior às amostras sinterizadas em forno convencional, ocorrente a temperaturas inferiores a 1000°C, com densidades relativas superiores a 90% DT em algumas composições. Os nanocompósitos de t-ZrO2/Al2O3-NbC apresentaram propriedades competitivas entre os compósitos sinterizados convencionalmente e por SPS, com dureza e tenacidade à fratura superiores às da t-ZrO2 monolítica. A resistência ao desgaste desses nanocompósitos sinterizados convencionalmente, no entanto, foi notadamente superior à dos sinterizados por SPS. A oxidação do NbC nos compósitos sinterizados convencionalmente influiu negativamente nas propriedades, levando à sugestão de uma \"janela\" de temperaturas em que a sinterização do nanocompósito de t-ZrO2/Al2O3-NbC seja interessante sem a degradação das propriedades mecânicas. Os resultados permitiram concluir que os materiais estudados apresentam potencial para aplicações industriais que requerem cerâmicas de alto desempenho mecânico e de resistência ao desgaste.
High performance ceramic composites have been the subject of frequent studies in recent decades, aiming at improving mechanical properties and increasing their range of applications in technological products. This work consisted in studying the preparation, the conventional and non-conventional sintering and the mechanical properties resulting from two t-ZrO2 matrix composites: the t-ZrO2/Al2O3 system and the t-ZrO2/Al2O3-NbC system. In the t-ZrO2/Al2O3 system, the compositions of 0, 5 and 15% by volume of Al2O3 using commercial powders were studied, while in the t-ZrO2/Al2O3-NbC system, an Al2O3-NbC nanocrystalline powder obtained by high energy reactive milling, deagglomerated, leached in HCl and added in the proportion of 5% by volume to the t-ZrO2 matrix. The obtained powders were uniaxially and isostatically pressed and sintered in conventional furnace and using flash sintering (t-ZrO2/Al2O3) and spark plasma sintering (SPS) (t-ZrO2/Al2O3-NbC). Conventionally sintered t-ZrO2/Al2O3 and conventionally sintered t-ZrO2/Al2O3-NbC composites were characterized by measurements of apparent density, dilatometry, SEM, and mechanical properties: hardness, Young\'s modulus and fracture toughness. The t-ZrO2/Al2O3 composites sintered by FS were characterized by measurements of apparent density, in situ dilatometry and SEM. t-ZrO2/Al2O3-NbC nanocomposites were also characterized for wear strength by the ball-in-disc method, using Al2O3 and WC-6%Co beads as countermaterials. The results showed that the high energy reactive milling was complete and effective in obtaining nanometric powders of Al2O3-NbC, with crystallite sizes equal to 9.1 and 9.7 nm, for Al2O3 and NbC, respectively. The deagglomeration after high energy reactive milling was effective in reducing the size of agglomerates. Conventionally sintered t-ZrO2/Al2O3 and t-ZrO2/Al2O3-NbC composites and SPS-sintered t-ZrO2/Al2O3-NbC showed high densification (> 97% TD), good dispersion of the inclusions in the matrix and good mechanical properties. The t-ZrO2/Al2O3 nanocomposites sintered by FS presented an ultrafast densification (<1 min) with linear shrinkage superior to the sintered samples in conventional furnace, occurring at temperatures lower than 1000°C, with relative densities higher than 90% TD in some compositions. The t-ZrO2/Al2O3-NbC nanocomposites presented competitive properties between conventionally sintered and SPS-sintered composites with higher hardness and fracture toughness than monolithic t-ZrO2. The wear resistance of these conventionally sintered nanocomposites, however, was markedly higher than those of SPS-sintered ones. The oxidation of NbC in the composites sintered conventionally influenced negatively the properties, leading to the suggestion of a \"window\" of temperatures in which the sintering of the t-ZrO2/Al2O3-NbC nanocomposite is interesting without the degradation of the mechanical properties. The results allowed concluding that the studied materials present potential for industrial applications that require high mechanical performance and wear resistance ceramics.

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COUTINHO, ANA C. de S. "Influência da adição de carbetos (NbC,TaC, SiC e TiC) na sinterização de cerâmicas à base de Sisub(3)Nsub(4)." reponame:Repositório Institucional do IPEN, 2005. http://repositorio.ipen.br:8080/xmlui/handle/123456789/11351.

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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
Tese (Doutoramento)
IPEN/T
Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP
FAPESP:01/01889-4

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PASOTTI, ROSA M. da R. "Obtencao e caracterizacao do composito Alsub2 Osub3-NbC e o efeito da adicao de Ysub2 Osub3 na sua sinterizacao." reponame:Repositório Institucional do IPEN, 1999. http://repositorio.ipen.br:8080/xmlui/handle/123456789/10745.

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Dissertacao (Mestrado)
IPEN/D
Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP

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TONELLO, KAROLINA P. dos S. "Compósitos de alumina com adições de NbC, TaC e TiC para aplicação em ferramentas de corte." reponame:Repositório Institucional do IPEN, 2013. http://repositorio.ipen.br:8080/xmlui/handle/123456789/10206.

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Tese (Doutoramento)
IPEN/T
Instituto de Pesquisas Energeticas e Nucleares - IPEN-CNEN/SP

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RUMBAO, ALEXANDRE H. "Influência da ítria nas propriedades mecânicas e térmicas do compósito Al sub(2) O sub(3) - 20 porcento NbC." reponame:Repositório Institucional do IPEN, 2002. http://repositorio.ipen.br:8080/xmlui/handle/123456789/11032.

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Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
Dissertação (Mestrado)
IPEN/D
Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP
FAPESP:00/03079-7

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Silva, J?nior Jos? Ferreira da. "Comportamento da adi??o do carbeto de ni?bio (nBC) na matriz met?lica do a?o ferr?tico 15kH2mfa." Universidade Federal do Rio Grande do Norte, 2012. http://repositorio.ufrn.br:8080/jspui/handle/123456789/12804.

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Conselho Nacional de Desenvolvimento Cient?fico e Tecnol?gico
The 15Kh2MFA steel is a kind of Cr-Mo-V family steels and can be used in turbines for energy generation, pressure vessels, nuclear reactors or applications where the range of temperature that the material works is between 250 to 450?C. To improve the properties of these steels increasing the service temperature and the thermal stability is add a second particle phase. These particles can be oxides, carbides, nitrites or even solid solution of some chemical elements. On this way, this work aim to study the effect of addition of 3wt% of niobium carbide in the metallic matrix of 15Kh2MFA steel. Powder metallurgy was the route employed to produce this metallic matrix composite. Two different milling conditions were performed. Condition 1: milling of pure 15Kh2MFA steel and condition 2: milling of 15Kh2MFA steel with addition of niobium carbide. A high energy milling was carried out during 5 hours. Then, these two powders were sintered in a vacuum furnace (10-4torr) at 1150 and 1250?C during 60 minutes. After sintering the samples were normalized at 950?C per 3 minutes followed by air cooling to obtain a desired microstructure. Results show that the addition of niobium carbide helps to mill faster the particles during the milling when compared with that steel without carbide. At the sintering, the niobium carbide helps to sinter increasing the density of the samples reaching a maximum density of 7.86g/cm?, better than the melted steel as received that was 7,81g/cm?. In spite this good densification, after normalizing, the niobium carbide don t contributed to increase the microhardness. The best microhardness obtained to the steel with niobium carbide was 156HV and to pure 15Kh2MFA steel was 212HV. It happened due when the niobium carbide is added to the steel a pearlitic structure was formed, and the steel without niobium carbide submitted to the same conditions reached a bainitic structure
O a?o 15Kh2MFA, da fam?lia dos a?os CrMoV, pode ser utilizado em turbinas para gera??o de energia, vasos de press?o, reatores nuclear ou aplica??es, onde o material ? submetido a temperaturas de servi?o entre 250 e 450?C. Uma forma de melhorar as propriedades do a?o, para que ele trabalhe a temperaturas mais altas ou que se torne mais est?vel ? adicionar part?culas de segunda fase na sua matriz. Estas part?culas podem estar na forma de ?xidos, carbetos, nitretos ou at? mesmo em solu??o s?lida quando alguns elementos qu?micos s?o adicionados ao material. Neste contexto, este trabalho objetiva estudar o efeito da adi??o de 3% de carbeto de ni?bio na matriz met?lica do a?o 15Kh2MFA. Para isto a metalurgia do p? foi a rota empregada para a produ??o deste comp?sito de matriz met?lica. Para tal, duas moagens distintas foram realizadas. A primeira com o a?o 15Kh2MFA e a segunda com o a?o 15Kh2MFA com adi??o de 3% de carbeto de ni?bio. A moagem de alta energia foi realizada durante 5 horas. Em seguida, os dois p?s produzidos foram sinterizados em um forno a v?cuo (10-4torr) a temperaturas de 1150?C e 1250?C durante 60 minutos. Ap?s a sinteriza??o as amostras foram submetidas ao tratamento t?rmico de normaliza??o a 950?C. Os resultados mostraram que a adi??o do carbeto de ni?bio ajuda o processo de cominui??o das part?culas, quando comparado com o a?o sem o carbeto de ni?bio. O carbeto de ni?bio tem um papel fundamental na densifica??o das amostras durante a sinteriza??o, levando a densidade 7,86g/cm?, que ? maior do que a densidade do a?o fundido recebido que era de 7,81g/cm?. Apesar desta boa densifica??o, ap?s a normaliza??o, o NbC n?o contribuiu de forma significativa para aumento da dureza, onde a melhor dureza obtida para o a?o com NbC foi de 156HV e para o a?o puro foi de 212HV. Isto se deve ao fato de que, quando o NbC foi adicionado ao a?o, formou-se uma estrutura perl?tica, enquanto que, com o a?o sem adi??o de NbC, submetido as mesmas condi??es, obteve-se uma estrutura bain?tica

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Valdes, Serra Juan Carlos. "Caracterização mecanico-metalurgica de compositos A1-Nbc, produzidos por metalurgia do po." [s.n.], 1998. http://repositorio.unicamp.br/jspui/handle/REPOSIP/263655.

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Orientadores: Maria Helena Robert, Jesualdo Luiz Rossi
Dissertação (mestrado) - Universidade Estadual de Campinas, Faculdade de Engenharia Mecanica
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Resumo: o presente trabalho apresenta a caracterização mecânico-metalúrgica de compósitos constituídos de Al reforçado com 5, 10 e 15%vol de partículas NbC, fabricados por metalurgia do pó, e no estado extrudado. A caracterização metalúrgica envolveu a análise do efeito do processamento na estabilidade das partículas de NbC, a análise de sua distribuição macroscópica na estrutura dos compósitos e a análise de interfaces reforço/matriz por MEV. Os resultados obtidos mostraram que as partículas de NbC podem soffer ffatura durante processamento, mas não têm alteradas suas dimensões; reações de interface não foram observadas e uma homogênea distribuição macroscópica das partículas de reforço foram obtidas nos compósitos, embora microscópicamente tenha sido observada tendência à aglomeração de partículas com o aumento do teor de reforço utilizado. Os compósitos foram também caracterizados quanto à expansão térmica e densidade aparente. Os resultados obtidos indicam redução do coeficiente de dilatação linear do Al da ordem de 17. a 26.% com a adição de teores de NbC de 5 a 15%vol, respectivamente; e aumento na densidade aparente da ordem de 15 a 20% para as mesmas adições...Observação: O resumo, na íntegra, poderá ser visualizado no texto completo da tese digital
Abstract: The work deals with the metalIurgicaland mechanical characterization of composites Al-NbC containing 5, 10 and 15% vol of NbC particles, in the extruded condition. Composites were produced from Al 1100 and NbC powders (average powder diameter 25 and 2,3 um, respectively), and subsequently extruded to bars. MetalIurgical characterization involved the analysis of the stability of reinforcement particles and their macroscopic distribution within the matrix as welI as the analysis of particles/matrix interface by MEY. Results showed that fracture can occurs in the particles of NbC at some extent; no interface reactions and changes in particles dimensions were observed. Homogeneous macroscopic distribution of NbC particles was obtained in all cases; therefore, microscopically it could be observed agglomeration of NbC as its vol fraction increases. It was also characterized thermal expansion and apparent density. Results showed decrease in the coefficient of linear thermal expansion in the order of 17 to 26% related to Al alone, as NbC content increases from 5 to 15% vol, respectively; and an increase of 15 to 20% in apparent density, for the same conditions...Note: The complete abstract is available with the full electronic digital thesis or dissertations
Mestrado
Materiais e Processos de Fabricação
Mestre em Engenharia Mecânica

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Damerval, Claire. "Contributions à l'étude du comportement mécanique des composites cotac γ /γ'-NbC à moyenne et haute température." Paris 11, 1986. http://www.theses.fr/1986PA112034.

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Cette thèse présente une étude du comportement des composites à fibres Cotac δ / δ’-NbC sous divers types de sollicitations mécaniques : fluage, traction transversale, cyclage thermique sous charge et fatigue oligo-cyclique. En fluage, nous avons montré que le transfert de charge de la matrice dans les fibres s'accompagne, dans le Cotac 784, d'un changement de mécanisme de déformation plastique de la matrice au cours d'un essai. D'autre part, nous avons étudié l'influence du mode de rupture des fibres sur l'allure des courbes de fluage, et mis en évidence l'influence de la résistance mécanique de la matrice sur les propriétés du composite. En traction transversale, l'analyse des mécanismes de rupture des Cotac 744 et 784 permet d'interpréter qualitativement l'évolution de leur ductilité avec la température, en terme de trois contraintes la limite élastique de la matrice, la contrainte de cohésion des joints de grains et la contrainte de clivage des lamelles de NbC. Une interprétation de l'augmentation de ductilité transversale obtenue grâce à une addition mineure de bore et à la formation d'un film de phase δ' aux joints de grains est proposée. En cyclage thermique sous charge, la chute de durée de vie provoquée par la superposition au fluage d'un cyclage de température s'élève à un facteur 3 environ à 1100°C ; ce phénomène s'est avéré non spécifique aux composites. En fatigue oligocyclique, le Cotac 784 a été caractérisé à 650°C en traction_compression à déformation imposée et une analyse succincte (phénoménologique et fractographique) de son comportement a été effectuée.

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Spirandeli, Bruno Roberto. "Influência da adição de NbC e Al2O3+TiO2 nos desempenhos de revestimentos a base de Ni-Al produzidos por aspersão térmica." Universidade de São Paulo, 2014. http://www.teses.usp.br/teses/disponiveis/18/18158/tde-12032015-151858/.

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Aspersão térmica é um processo de produção de revestimentos metálicos, poliméricos, cerâmicos ou compósitos sobre superfícies previamente preparadas que objetiva na maioria das vezes a prevenção contra o desgaste e/ou corrosão e também a recuperação dimensional de superfícies desgastadas. Ligas de Ni-Al são extensivamente empregadas na aspersão térmica para reconstrução dimensional e como camada de ligação como materiais que não se ligam adequadamente à superfície a ser revestida. A baixa dureza e resistência ao desgaste (principalmente em aplicações de reconstrução dimensional) desta liga poderiam ser contornadas pela adição de partículas ou compostos de altas durezas na matéria prima em pó antes da aspersão. Neste trabalho avaliou-se a influência da adição de NbC e do composto cerâmico Al2O3+TiO2 no desempenho ao desgaste de revestimentos de Ni-Al, bem como verificou-se as alterações microestruturais, químicas, e mecânicas decorrentes. Para tanto se adicionou 25%p de NbC ou 25%p do composto Al2O3+TiO2 à liga base de Ni-Al, formando-se dois materiais compósitos: Ni-Al + NbC e Ni-Al + (Al2O3+TiO2). Utilizou-se microscópio eletrônico de varredura com EDS para caracterizar as matérias primas e os revestimentos produzidos, assim como determinar o mecanismo de desgaste nos ensaios de micro-abrasão tipo \"esfera-livre\" e \"esfera-fixa\". Mediram-se as durezas superficiais e as microdurezas das fases por meio dos ensaios Rockwell Superficial e microdureza Vickers. Avaliou-se a resistência ao desgaste por meio de ensaios de micro-abrasão nas modalidades \"esfera-livre\" e \"esfera-fixa\". As adições dos materiais citados na liga a base de níquel alteraram características microestruturais importantes, como aumento do percentual de óxidos, bem como a composição química e distribuição dos elementos nas camadas formadas; ocorreram também aumentos significativos das durezas e nas resistências ao desgaste dos revestimentos.
Thermo Spray is a metallic, polymeric, ceramic and composite coating process applied over a previously prepared surface usually seeking to improve wear and/or corrosion resistance. It is also used to repair worn surfaces restoring the original dimensions. Ni-Al alloys are used as a primer coating to promote the adhesion between surface and incompatible coatings and also extensively in the reconstruction of worn surfaces. The low hardness and wear resistance (when used in reconstruction applications) of this alloy could be improved by the addition of hard particles/composites to the powdered raw material prior to the spray operation. In this work the influence of NbC and Al2O3+TiO2 additions to Ni-Al alloys were evaluated concerning wear performance and the resulting changes in microstructure, chemical and mechanical behavior. The experimental procedure included the preparation of samples of the Ni-Al base alloy with additions of 25wt% of NbC or 25wt% of Al2O3+TiO2, what resulted in two different sprayed composite materials: Ni-Al + NbC e Ni-Al + (Al2O3+TiO2). SEM with EDS microprobe was used to characterize the raw materials, the sprayed coating samples and the type of wear mechanism occurring in the wear tests of the type \"free sphere\" and \"fixed sphere\" micro abrasion that were used to evaluate the wear resistance of the samples. Surface hardness and micro hardness of the different phases in the coatings were evaluated using Rockwell and Vickers micro hardness testing machines respectively. The addition of the hard phases promoted important changes in the Ni-Al base alloy, decreasing the porosity level and increasing the percentage of oxides. Hardness were significantly increased as well as the wear resistance of the coatings.

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Rydén, Michaéla. "Impact of different concrete types on the LCA of NCC Composite bridge." Thesis, KTH, Bro- och stålbyggnad, 2015. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-177861.

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Traditionell betong används i majoriteten av broar som byggmaterial. Om byggnadsmaterialet skulle kunna ersättas av en betong med mindre miljöpåverkan, kan stora delar av miljöpåverkan minskas. I denna avhandling, ska NCC:s samverkansbro utredas, där tre olika betongtyper ska testas i dess olika konstruktionsdelar. Samverkansbron kommer att jämföras i tre olika scenarier av byggmaterial: traditionell betong, traditionell betong innehållande 5 % slagg och injekteringsbetong. Jämförelsen kommer att utföras genom en livscykelanalys (LCA) med hjälp av programvaran GaBi 6.5. Resultatet av modelleringen i GaBi presenteras på samma sätt som i en miljövarudeklaration (EPD). I presentationen av resultatet kommer diagram och tabeller visualisera de resultat som erhållits i livscykelanalysen. Det erhållna resultatet visar att vid jämförelse av de tre scenarierna ger injekteringsbetong en mindre klimatpåverkan i majoritet av resultaten.
Traditional concrete is used in the majority of bridges as a building material. If the building material could be replaced by a concrete with less environmental impact, large parts of the environmental impact could be reduced. In this dissertation, NCC Composite Bridge is to be investigated, where three different concrete types are to be tested in its various design elements. The composite bridge will be compared in three scenarios: traditional concrete, traditional concrete with slag as part of binder and prepact concrete. The comparison will be carried out by a Life Cycle Assessment (LCA) using the software GaBi. The outcome will be in form of an Environmental Product Declaration (EPD) table. (NCC has implemented the EPD system into the company with the ambition to easier and more thorough provide a legit evaluation of the environmental impact.) In the presentation of the result, diagrams and tables visualizes the results obtained in the EPD. The result obtained has shown that comparing the three scenarios; prepact concrete provides a less environmental impact and if replacing traditional concrete with prepact, savings of the environment can be made.

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Tonello, Karolina Pereira dos Santos. "Compósitos de alumina com adições de NbC, TaC e TiC para aplicação em ferramentas de corte." Universidade de São Paulo, 2013. http://www.teses.usp.br/teses/disponiveis/85/85134/tde-29052013-092205/.

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No presente trabalho foram desenvolvidos compósitos à base de alumina, com adição de carbetos de metais de transição, NbC, TaC e TiC, como reforço. Os carbetos, na forma de partículas, foram adicionados em 1,5% em volume à matriz de alumina durante a moagem em attritor. O processamento foi realizado por moagem em attritor, secagem em rotoevaporadora e desaglomeração em peneira. A dinâmica de oxidação dos carbetos e das composições dos compósitos foi estudada para a definição de parâmetros de sinterização e processamento dos compósitos. A cinética de sinterização foi estudada por dilatometria, com taxa de 10°C/min. até 1600°C em atmosfera de ar sintético, e até 1800°C, em atmosfera de argônio, com esta etapa foi possível verificar que o NbC e o TiC dificultaram a sinterização da alumina e que o TaC auxiliou nos processos de retração. Nas amostras que foram sinterizadas em dilatômetro ao ar foram detectadas fases resultantes de fusão congruente nos compósitos Al2O3/NbC e Al2O3/TaC, foram também observadas evidências de formação de líquido no compósito com adição de TaC. Com base nesses resultados foram estudadas duas técnicas de produção das ferramentas de corte: prensagem uniaxial seguida de sinterização sem pressão e sinterização por prensagem a quente. Todas as amostras foram caracterizadas microestruturalmente e quanto às propriedades mecânicas, tendo-se determinado que as amostras produzidas por prensagem a quente possuem microestrutura mais controlada e propriedades mecânicas superiores às produzidas por sinterização sem pressão. Pelos processos estudados foi observado que os carbetos influenciam diferentemente a sinterização da alumina. De maneira geral a presença destas fases nos contornos de grãos promove alterações na microestrutura modificando o tamanho de grãos da alumina. Foi proposta a hipótese de que esse comportamento é afetado pela formação de uma camada superficial resultante da oxidação dos reforços, com isto, de acordo com os diagramas de fase é possível a formação de soluções sólidas entre alumina e Ta2O5 e Nb2O5 além da formação de fase líquida, estes mecanismos alterariam a mobilidade dos contornos de grão da alumina. Para o processamento das ferramentas de corte foi utilizada prensagem a quente, escolhido pelo critério da microestrutura e propriedades mecânicas. Os testes de usinagem foram realizados com ferramentas de corte de geometria quadrada, em peças de ferro fundido cinzento e vermicular. O tempo de vida útil da ferramenta produzida com o compósito Al2O3/ NbC foi 13% superior quando comparado à uma ferramenta cerâmica comercial no teste de usinagem de ferro fundido cinzento.
In the present work alumina based composites with addition of transition metal carbides, NbC, TaC and TiC as reinforcement phase were developed. The carbides, in particulate form, were added in 1.5vol.% on the alumina matrix during attritor milling. The processing was conducted by attritor milling, drying in a rotoevaporator and deagglomeration in sieve. The oxidation dynamics of carbides and composities were studied in order to define the sintering and processing parameter of composites. The sintering kinetics was studied by dilatometry at 10° C/min. up to 1600 ° C in synthetic air atmosphere and up to 1800°C in argon, with this step it was possible to verify that the NbC and TiC hindered the sintering of alumina and the TaC helped in the retraction process. In the sintered by dilatometer in air phases resultant from congruent melting on Al2O3/NbC and Al2O3/TaC composites were detected in the composite with TaC addition was also observed evidence of liquid phase. In the samples sintered in dilatometer in air were detected solid solutions on composites CN and CTa and evidence of liquid formation in the composite with TaC addition. Based on these results two techniques were studied in order to produce cutting tools: uniaxial pressing, followed by pressureless sintering and hot pressing. All samples were characterized by microstructure and mechanical properties, and it was shown that samples produced by hot pressing have more controlled microstructure and mechanical properties superior to those produced by pressureless sintering. With the studied processes it was observed that the carbides influence differently alumina sintering. Generally the presence of these phases at the grain boundary causes changes in the microstructure modifying alumina grain size alumina. The proposed hypothesis is that this behavior would be affected by the formation of a surface layer resulting from oxidation of reinforcements with that, according to the phase diagrams, it is possible to find solid solutions between alumina and Ta2O5 and Nb2O5 and possible formation of liquid phase, which alter the mobility of the grain boundary of alumina. Hot pressing was used for the processing of cutting tools, chosen due to the microstructure and mechanical properties. The machining tests were performed with square geometry cutting tools, in samples of gray cast iron and compacted graphite iron. The tool life of cutting tool produced with Al2O3 / NbC composite was 13% higher when compared to a commercial ceramic cutting tool on machining of gray cast iron.

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Qi, Chuan. "NCF/Wax nano composites inspired by plant cuticles." Thesis, KTH, Skolan för kemivetenskap (CHE), 2012. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-146034.

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Plant cuticles are extracellular membranes covering aerial organs of plants, whose main functions rely on the protection against water loss, mechanical injury from the environment, attack of microorganism, and also regulation of gas exchange. Among the several constituents of plant cuticles, waxes are those that play an important role in their barrier properties. In order to enhance the mechanical properties of wax, NFC was applied in. In the project, mainly two kinds of methods were used to prepare wax-NFC composites. One way was wax and NFC were dissolved in toluene and casted to be a film, another way was to prepare NFC aerogel firstly, and then, impregnated the aerogel into wax liquid. After pressing it the structure was more compact. In order to characterize the properties of samples, SEM, XRD, TGA, DSC, Contact angle testing, tensile test and oxygen permeability methods were applied in.

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Silva, Paulo Henrique Lubas. "Dimensionamento de pilares mistos de aço e concreto." Universidade de São Paulo, 2012. http://www.teses.usp.br/teses/disponiveis/3/3144/tde-17062013-150832/.

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Os pilares mistos de aço e concreto consistem em um ou mais perfis de aço ligados entre si, trabalhando em conjunto com o concreto, simples ou armado, solicitados à compressão ou à flexocompressão. Os pilares mistos são, basicamente, de dois tipos: revestidos ou preenchidos. O sistema misto apresenta grandes vantagens estruturais, uma vez que herda a capacidade resistente dos pilares de aço e, dos pilares de concreto, sua robustez. Este trabalho estuda o emprego dessa solução de acordo com as principais normas internacionais de dimensionamento à temperatura ambiente, comparando-as entre si e às normas brasileiras. A ABNT NBR 8800:2008, apresenta dois modelos de cálculo simplificados para o dimensionamento de pilares mistos com seções transversais simétricas, com base em duas normas internacionais. O primeiro, o Modelo I, com base no ANSI/AISC 360 (2005) e o segundo, o Modelo II, no Eurocode 4 Part 1-1 (2004). Fica a critério do engenheiro estruturista a escolha do método a ser utilizado. Apresenta-se uma comparação gráfica e tabular da capacidade resistente à temperatura ambiente entre os dois modelos de cálculo da norma brasileira e as normas internacionais. No caso de seções transversais não simétricas, são propostos dois roteiros de dimensionamento inéditos em aplicações de pilares mistos: um com base no Fiber Elemento Method e nas recomendações do Eurocode 4 Part 1-1 (2004), e outro adaptando o primeiro às normas brasileiras. Ambos são avaliados graficamente e por meio de tabelas. Para o auxílio de todos esses estudos, foi utilizado o código CalcPM v1.0, desenvolvido especialmente para esse estudo.
The composite columns have the concrete and the steel profile working together to support loads. The composite columns are basically of two types: encased and filled. The composite system has the advantage to unite the inherent robustness of the concrete columns and high resistance of the steel columns. This work studies the use of this solution according to the main international standards, comparing them with each other and with the Brazilian norms. The Brazilian standard ABNT NBR 8800:2008, presents two simplified models of the composite columns design with symmetrical cross sections, based on two international standards. Model I, based on American standard ANSI/AISC 360 (2005) and Model II, with reference to the European standard Eurocode 4 Part 1-1 (2004). Is up to the engineer to choose the method to be used. It presents a tabular and graphical comparison of the strength between the two calculation models of the Brazilian and international standards. In the case of non-symmetrical cross sections there are two proposed routes unprecedented scale applications of composite columns: one based on \"Fiber Element Method\" and the recommendations of Eurocode 4 Part 1-1 (2004) and another one to adapt the first one to the Brazilian standards. Both are evaluated graphically and by the use of tables. To support all these studies the software CalcPM v1.0 was used and specially developed for this study.

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Yousefiandivkolaei, Seyedeh Hajar. "Nanocrystalline cellulose (NCC) filled thermoplastics : production and characterization of composites and foams." Doctoral thesis, Université Laval, 2016. http://hdl.handle.net/20.500.11794/26611.

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Cette thèse est consacrée à la compréhension des propriétés morphologiques et mécaniques de la nanocellulose cristalline (NCC) dans des résines thermoplastiques mises en forme à l’état fondu (extrusion et moulage par injection). Dans la première partie, des composites à base de Nylon 6 et de NCC (0-7% en poids) sont préparés et les propriétés morphologiques/mécaniques (tension, flexion, impact) sont présentées. Les résultats montrent que la NCC est efficace pour améliorer les propriétés mécaniques (principalement le module de flexion) avec une faible augmentation de la masse volumique totale. Dans la deuxième partie, un système hybride est évalué en utilisant la NCC (1%) et de la farine de bois d'érable (20%) dans le polypropylène (PP), avec et sans PP maléaté (MAPP) comme agent de couplage. L'analyse mécanique révèle que ces deux fibres produisent un renforcement efficace, en particulier pour améliorer les modules élastiques des échantillons contenant du MAPP. La troisième partie examine la caractérisation morphologique, physique et mécanique de nano-composites moussés à base de NCC et de Nylon 6. Différentes concentrations de NCC (0-5%) et d'agent moussant chimique (azodicarbonamide) (0-2%), ainsi que la température du moule (30 et 80⁰C) sont utilisés pour produire les échantillons. Les résultats montrent que la NCC est très efficace pour améliorer la structure de la mousse (réduction de la taille des cellules, augmentation de la densité cellulaire) et les propriétés mécaniques, en particulier les modules élastiques. Aussi, la concentration de l'agent moussant et la température du moule ont un effet direct sur les propriétés mécaniques car ils contrôlent l'épaisseur de la couche de peau. Enfin, des composites et des mousses sont produits à base de PP. Similairement au Nylon 6, la NCC est très efficace pour réduire la taille des cellules et augmenter la densité cellulaire. Par ailleurs, la NCC permet d'améliorer les propriétés mécaniques du PP, en particulier les modules élastiques spécifiques.
This thesis is devoted to the understanding of the morphological and mechanical properties of nanocrystalline cellulose (NCC) filled thermoplastics produced by melt compounding (extrusion and injection molding). In the first part, composites based on Nylon 6 and NCC (0-7% wt.) are prepared and morphological/mechanical properties (tension, flexion, impact) are presented. The results show that NCC is effective to improve the mechanical properties (mainly flexural modulus) with limited overall density increase. In the second part, a hybrid system is evaluated based on NCC (1%) and maple wood flour (20%) filled polypropylene (PP), with and without maleated PP (MAPP) as a coupling agent. The mechanical analysis reveal that these two fibers have effective reinforcing role, especially to improve the elastic moduli of samples containing MAPP. The third part examines the morphological, physical and mechanical characterization of NCC/Nylon 6 nano-composite foams. Different content of NCC (0-5%) and chemical foaming agent (azodicarbonamide) (0-2%), as well as mold temperature (30 and 80⁰C) are used to produce the samples. The results show that NCC is very effective to improve the foam structure (reduced cell size, increased cell density) and mechanical properties, especially elastic moduli. Also, foaming agent content and mold temperature have a direct effect on the mechanical properties because they control the skin layer thickness. Finally, composites and foams are produced based on PP. Similarly to Nylon 6, NCC is very effective to reduce cell size and increase cell density. Moreover, NCC is able to improve the mechanical properties of PP, especially the specific elastic moduli.

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Vincent, Cécile. "Le composite cuivre / nanofibres de carbone." Phd thesis, Université Sciences et Technologies - Bordeaux I, 2008. http://tel.archives-ouvertes.fr/tel-00377607.

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Le matériau composite Cu/NFC (Nano Fibre de Carbone) peut être utilisé en tant que drain thermique par les industriels de l'électronique de puissance. En remplacement du cuivre, il doit combiner une conductivité thermique élevée et un coefficient de dilatation thermique adapté à celui de la céramique du circuit imprimé (alumine ou nitrure d'aluminium). Après avoir étudié les propriétés de la matrice cuivre et des NFC, plusieurs méthodes de synthèse du composite Cu/NFC ont été développées. Le composite a tout d'abord été élaboré par métallurgie des poudres. Puis, dans le but d'améliorer l'homogénéité, il a été envisagé de revêtir individuellement chaque NFC par du cuivre déposé par voie chimique electroless ainsi que par une méthode originale de décomposition d'un sel métallique. Des mesures de densité et de propriétés thermiques (conductivité et dilatation) ainsi que les caractérisations microstructurales de ces matériaux montrent la complexité de l'élaboration d'un tel composite. En effet, la dispersion des nanofibres, la nature des interfaces fibres/matrice et surtout les phénomènes thermiques à l'échelle nanométrique sont autant de paramètres à contrôler afin d'obtenir les propriétés recherchées. La simulation numérique et analytique, qui a été mise en oeuvre en parallèle a été corrélée aux résultats expérimentaux, afin de prédire les propriétés finales de nos matériaux.

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Zhang, Jie. "Multifunctional composite interphase." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2012. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-88763.

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In this work, carbon nanotubes were deposited onto the insulative glass fibre surface to form a semiconductive network. Utilizing the unique properties of CNTs network, a multifunctional composite interphase could be achieved. The interfacial adhesion strength was improved by CNTs distributed in the interphase. The semiconductive interphase have been used as a chemical/phaysical sensor, strain sensor and microswitch.

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Beaudoin, Jean-François. "Etude et réalisation de composites filamentaires supraconducteurs à base de Nb3(Al0. 8Ge0. 2)." Grenoble INPG, 1988. http://www.theses.fr/1988INPG0121.

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Production des filaments supraconducteurs nb::(3)(al,ge) susceptibles d'etre utilises dans un champ magnetique superieur a 20t. Mise au point d'une technique de fusion par induction et levitation electromagnetique en creuset froid. Obtention de la phase a125 pure en controlant la stoechiometrie des 3 elements et les recuits. Les poudres sont etirees et trefilees dans une matrice de cuivre. La pulverisation est effectuee par hydruration et deshydruration du materiau massif. Les mesures de susceptibilite, alternative ont montre que les grains de poudres sont couples entre eux par effet josephson. Determination des caracteristiques en courant critique

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22

Nestler, Daisy Julia. "Beitrag zum Thema VERBUNDWERKSTOFFE - WERKSTOFFVERBUNDE." Doctoral thesis, Universitätsbibliothek Chemnitz, 2014. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-134459.

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Vielschichtige Eigenschaftsprofile benötigen zunehmend moderne Verbundwerkstoffe und Werkstoffverbunde einschließlich der raschen Entfaltung neuer Fertigungstechnologien, da der monolithische Werkstoff bzw. ein einziger Werkstoff den heutigen komplexen Anforderungen nicht mehr genügen kann. Zukünftige Werkstoffsysteme haben wirtschaftlich eine Schlüsselposition und sind auf den Wachstumsmärkten von grundlegender Bedeutung. Gefragt sind maßgeschneiderte Leichtbauwerkstoffe (tailor-made composites) mit einem adaptierten Design. Dazu müssen Konzepte entwickelt werden, um die Kombination der Komponenten optimal zu gestalten. Das erfordert werkstoffspezifisches Wissen und Korrelationsvermögen sowie die Gestaltung komplexer Technologien, auch unter dem Aspekt der kontinuierlichen Massen- und Großserienfertigung (in-line, in-situ) und damit der Kostenreduzierung bislang teurer Verbundwerkstoffe und Werkstoffverbunde. In der vorliegenden Arbeit wird in vergleichbarer und vergleichender Art und Weise sowie abstrahierter Form ein Bogen über das Gesamtgebiet der Verbundwerkstoffe und Werkstoffverbunde gespannt. Eine zusammenfassende Publikation über dieses noch sehr junge, aber bereits breit aufgestellte Wissenschaftsgebiet fehlt bislang. Das ist der Separierung der einzelnen, fest aufgeteilten Gruppierungen der Verbundwerkstoffe geschuldet. Querverbindungen werden selten hergestellt. Dieses Defizit in einem gewissen Maße auszugleichen, ist Ziel der Arbeit. Besondere Berücksichtigung finden Begriffsbestimmungen und Klassifikationen, Herstellungsverfahren und Eigenschaften der Werkstoffe. Es werden klare Strukturierungen und Übersichten herausgearbeitet. Zuordnungen von etablierten und neuen Technologien sollen zur Begriffsstabilität der Terminologien „Mischbauweise“ und „Hybrider Verbund“ beitragen. Zudem wird die Problematik „Recycling und Recyclingtechnologien“ diskutiert. Zusammenfassend werden Handlungsfelder zukünftiger Forschungs- und Entwicklungsprojekte spezifiziert. Aus dem Blickwinkel der verschiedenen Herstellungsrouten insbesondere für Halbzeuge und Bauteile und der dabei gewonnenen Erkenntnisse werden verallgemeinerte Konzepte für tailor-made Verbundwerkstoffe und Werkstoffverbunde vorgeschlagen („Stellschraubenschema“). Diese allgemeinen Werkstoffkonzepte werden auf eigene aktuelle Forschungsprojekte der Schwerpunktthemen Metallmatrix- und Polymermatrix-Verbundwerkstoffe sowie der hybriden Werkstoffverbunde appliziert. Forschungsfelder für zukünftige Projekte werden abgeleitet. Besonderes Augenmerk gilt den hybriden Verbunden als tragende Säule zukünftiger Entwicklungen im Leichtbau. Hier spielen in-line- und in-situ-Prozesse eine entscheidende Rolle für eine großseriennahe, kosteneffiziente und ressourcenschonende Produktion
Complex property profiles require increasingly advanced composite materials and material compounds, including the rapid deployment of new production technologies, because the monolithic material or a single material can no longer satisfy today's complex requirements. Future material systems are fundamentally important to growth markets, in which they have an economically key position. Tailor-made lightweight materials (tailor-made composites) with an adapted design are needed. These concepts have to be developed to design the optimum combination of components. This requires material-specific knowledge and the ability to make correlations, as well as the design of complex technologies. Continuous large-scale and mass production (in-line, in-situ), thus reducing the costs of previously expensive composite materials and material compounds, is also necessary. The present work spans the entire field of composite materials and material compounds in a comparable and comparative manner and abstract form. A summarizing publication on this still very new, but already broad-based scientific field is not yet available. The separation of the individual, firmly divided groups of the composite materials is the reason for this. Cross-connections are rarely made. The objective of this work is to compensate to some extent for this deficiency. Special consideration is given to definitions and classifications, manufacturing processes and the properties of the materials. Clear structures and overviews are presented. Mapping established and new technologies will contribute to the stability of the terms "mixed material compounds" and "hybrid material compounds". In addition, the problem of recycling and recycling technologies is discussed. In summary, areas for future research and development projects will be specified. Generalized concepts for tailor-made composite materials and material compounds are proposed ("adjusting screw scheme") with an eye toward various production routes, especially for semi-finished products and components, and the associated findings. These general material concepts are applied to own current research projects pertaining to metal-matrix and polymer-matrix composites and hybrid material compounds. Research fields for future projects are extrapolated. Particular attention is paid to hybrid material compounds as the mainstay of future developments in lightweight construction. In-line and in-situ processes play a key role for large-scale, cost- and resource-efficient production

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Fernandes, Maria Roseane de Pontes. "Comp?sitos de matriz met?lica ? base n?quel com adi??o de TaC e NbC produzidos via metalurgia do p?" Universidade Federal do Rio Grande do Norte, 2014. http://repositorio.ufrn.br:8080/jspui/handle/123456789/12857.

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Made available in DSpace on 2014-12-17T14:07:20Z (GMT). No. of bitstreams: 1 MariaRPF_TESE.pdf: 4797522 bytes, checksum: 8d9626466b01e2425f6ea6036398adcf (MD5) Previous issue date: 2014-01-24
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Carbide reinforced metallic alloys potentially improve some important mechanical properties required for the overall use of important engineering materials such as steel and nickel. Nevertheless, improved performance is achieved not only by composition enhancement but also by adequate processing techniques, such as novel sintering methods in the case of powder metallurgy. The method minimizes energy losses in addition to providing uniform heating during sintering. Thus, the general objective of this study was to evaluate the density, hardness, flexural strength, dilatometric behavior and to analyze the microstructure of metal matrix composites based nickel with addition of carbides of tantalum and / or niobium when sintered in a conventional furnace and Plasma assisted debinding and sintering (PADS). Initially, were defineds best parameters of granulation, screening and mixing procedure. After, mixtures of carbonyl Ni and 5%, 10% and 15 wt.% NbC and TaC were prepared in a Y-type mixer under wet conditions during 60 minutes. The mixtures were then dried and granulated using 1.5 wt. % paraffin diluted in hexane. Granulates were cold pressed under 600 MPa. Paraffin was then removed from the pressed pellets during a pre-sintering process carried out in a tubular furnace at 500 ?C during 30 min. The heating rate was 3 ?C/min. The pellets were then sintered using either a plasma assisted reactor or a conventional resistive tubular furnace. For both methods, the heating rate was set to 8 ?C/min up to 1150 ?C. The holding time was 60 minutes. The microstructure of the sintered samples was evaluated by SEM. Brinell hardness tests were also carried out. The results revealed that higher density and higher hardness values were observed in the plasma-assisted sintered samples. Hardness increased with the concentration of carbides in the Ni-matrix. The flexural strength also increased by adding the carbides. The decline was larger for the sample with addition of 5% 5% TaC and NbC. In general, compositions containing added carbide 10% showed less porous and more uniform distribution of carbides in the nickel matrix microstructural appearance. Thus, both added carbide and plasma sintering improved density, hardness, flexural strength and microstructural appearance of the composites
Ligas met?licas refor?adas por carbetos melhoram potencialmente algumas propriedades mec?nicas necess?rias para a utiliza??o de importantes materiais de engenharia, tais como o a?o e o n?quel. No entanto, o desempenho ? conseguido n?o apenas pela melhoria de composi??o, mas tamb?m por t?cnicas de processamento adequadas, tais como, novos m?todos de sinteriza??o, no caso da metalurgia do p?. Desta forma, o objetivo do presente trabalho foi avaliar a dureza, resist?ncia ? flex?o, comportamento dilatom?trico e analisar a microestrutura de comp?sitos de matriz met?lica base n?quel com adi??o de carbetos de t?ntalo e/ou ni?bio quando sinterizados em forno tubular convencional e Plasma assisted debinding sintering (PADS). Os carbetos (5%, 10% e 15% em massa) foram misturados ao p? de n?quel carbonila via ?mido com aux?lio do misturador Y adaptado durante 1h. Ap?s secagem, as misturas foram submetidas ao processo denominado de granula??o em tambor. Utilizou-se 1,5% de parafina (% massa) dilu?da em hexano. Os p?s granulados foram compactados a frio utilizando press?o de 600 MPa. Antes da sinteriza??o a uma taxa de 8 ?C/min com patamar 1h na temperatura de 1150?C tanto em forno tubular quanto em reator PADS, as amostras foram pr?-sinterizadas em forno tubular para extra??o da parafina a uma taxa de 3 ?C/min com patamar 30 min em 500 ?C. A dureza avaliada foi a Brinell e a an?lise microestrutural por MEV. Os resultados mostraram que as amostras sinterizadas assistidas por plasma apresentaram dureza superior ?quelas sinterizadas em forno convencional. As imagens por MEV comprovaram esses maiores valores de durezas, uma vez que a matriz apresentou-se mais densificada. Com rela??o ? adi??o dos carbetos, a dureza aumentou com o aumento da concentra??o dos mesmos. A resist?ncia ? flex?o tamb?m aumentou ao adicionar os carbetos. A retra??o foi maior para a amostra com adi??o de 5% de TaC e 5% NbC. De maneira geral, as composi??es com adi??o de 10% de carbetos apresentaram um aspecto microestrutural menos poroso e com uma distribui??o mais uniforme dos mesmos na matriz de n?quel. Assim, tanto a adi??o de carbetos quanto a sinteriza??o com aux?lio do plasma melhoraram a dureza e o aspecto microestrutural dos comp?sitos

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Blank, Christa, Veneta Hein, Michael Thieme, Hartmut Worch, Susanne Höhne, and Frank Simon. "Ultrahydrophobe chitosanstabilisierte Composite-Schichten auf Aluminiumwerkstoffen." Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2013. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-108237.

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Selbstreinigende, ultrahydrophobe Oberflächen lassen sich in der Technik vielfältig einsetzen. Das ultrahydrophobe Verhalten beruht einerseits auf einer Rauigkeit im μm-Bereich und andererseits auf der chemischen Zusammensetzung der Oberfläche. Durch den gegebenen Oberflächenaufbau sind derartige Materialien jedoch empfindlich gegen Verschleiß. In diesem Beitrag wird ein Schichtverbund bestehend aus Aluminiumoxid und zwei polymeren Komponenten vorgestellt. Die Aluminiumoxidschicht wird auf dem Wege der anodischen Oxidation erzeugt. Dieses seit langem bekannte Verfahren ermöglicht nicht nur die Oxidation der Aluminiumoberfläche, sondern gestattet es, auch, definierte Oberflächenprofile einzustellen. Durch den gezielten Einbau des hochmolekularen Polymers Chitosan in die mikroprofilierte Aluminiumoxidschicht wurde eine mechanische Stabilisierung der Schicht im Sinne eines anorganisch-organischen Composites erreicht. Außerdem dienten die Amino-Seitengruppen des Chitosans als reaktives Interface für die notwendige chemische Hydrophobierung und als Reaktionszentrum für Vernetzungen, wodurch eine weitere mechanische Stabilisierung bewirkt wird. Der Schichtaufbau hat wesentlichen

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Gao, Shang-Lin, Jian-Wen Liu, Rong-Chuang Zhuang, Rosemarie Plonka, and Edith Mäder. "Healing Microcracks and Early Warning Composite Fractures." Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2011. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-77852.

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A functional nanometer-scale hybrid coating layer with multi-walled carbon nanotubes (MWCNTs) and/or nanoclays, as mechanical enhancement to ‘heal’ surface microcracks and environmental barrier layer is applied to alkaliresistant glass (ARG) fibres. The nanostructured and functionalised traditional glass fibres show both significantly improved mechanical properties and environmental corrosion resistance. Early warning material damage can be achieved by carbon nanotubes concentrated interphases in the composites
Eine funktionale nanometerskalige Hybridbeschichtung mit multi-walled carbon nanotubes (MWCNTs) und/oder Nanoclay wurde als mechanische Verbesserung des „Ausheilens“ von Oberflächen-Mikrorissen und Barriereschicht gegenüber Umwelteinflüssen auf alkaliresistente Glasfasern (ARG) appliziert. Die nanostrukturierten und funktionalisierten traditionellen Glasfasern zeigen signifikant verbesserte mechanische Eigenschaften und Korrosionsbeständigkeit. Die Frühwarnung des Materialversagens kann durch Carbon Nanotubes, konzentriert in der Grenzschicht der Composites, erreicht werden

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Deng, Yinhu. "Bio-inspired Multifunctional Coatings and Composite Interphases." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-212223.

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Graphene nanoplatelets have been introduced into the interphase between electrically insulating glass fibre and polymer matrix to functionalize the traditional composite. Owing to the distribution of network structure of GNPs, the interphase can transfer the signals about various internal change of material. Consequently, due to the novel bio-inspired overlapping structure, our GNPs-glass fibre shows a unique opportunity as a micro-scale multifunctional sensor. The following conclusions can be drawn from present research: • We prepared GNPs solution via a scalable and highly effective liquid-phase exfoliation method. This method produces high-quality, unoxidized graphene flakes from flake graphite. We control the thickness and size of GNPs by varying the centrifugation rate. • A simple fibre oriented capillary flow which can suppress ‘coffee ring’ effect to deposit GNPs onto the curved glass fibre surface. The GNPs form continuous fish scales like overlapping structure. • The electrical conductivity of our GNPs-glass fibre shows semiconductive property. The electrical resistance value scattering and the advancing contact angle value scattering indicate a uniform deposit structure. The uniform overlapping structure is a key factor for higher electrical conductivity compared with our previous work with CNTs. • The contact angles of our GNPs-glass fibre with water indicate that the GNPs are almost unoxidized, so the inert GNPs coating decreases the interfacial shears strength. • A micro scale GNPs-glass fibre sensor for gas sensing is achieved by deposit GNPs onto glass fibre surface. This sensor can be used to detect solvents vapours, such as water, ethanol and acetone. All these vapours work as electron acceptor when reacting with GNPs. The acetone shows the highest sensitivity (45000%) compared with water and ethanol. • The doping-dedoping of GNPs-glass fibres during adsorption-desorption cycles of acetone result in the efficient “break-junction” (GNPs lost electron carrier concentration) mechanism, which provides the possibility to fabricate the electrochemical “switch” in a simple and unique way. • The resistance of our GNPs-glass fibre shows exponential relationship with RH. This is attributed to two points. Firstly, the water vapours show similar exponential adsorption on carbon surface; secondly, the bandgap of GNPs increases with the increase of adsorbed water vapour concentration. • Due to the weak van der Waals interaction when water molecules are adsorbed on GNPs surface, our GNPs-glass fibre shows extreme fast response and recovery time with RH. It is potential for our GNPs-glass fibre being used to monitor the breath frequency. • Utilizing the negative temperature coefficient of GNPs, our GNPs-glass fibre can be used as temperature sensor with a sensing region of -150 to 30 °C. • Through the observed abnormal resistance change at a temperature of about – 18 °C, we discovered a phase change of the trance confined water in graphene layers. Based on the resistance change, we can study the interaction of water and carbon nanoparticles. • The bio-inspired novel overlapped multilayer structure of GNPs coating shows structural colours. Even more, our GNPs-glass fibre can be used to monitor the loading force in the interphase when it is embedded into epoxy resin. • Our GNPs-glass fibre shows an excellent piezoresistive property, the single GNPs-glass fibre shows a larger gauge factor than the commercial strains sensor. • The semiconductive interphase was formed when the GNPs-glass fibre was embedded in polymer matrix. This semiconductive interphase is very sensitive to the deformation of material, therefore, an in-situ strain sensor was manufactured to real-time monitor the microcracks in a composite instead of external sensors. The area of resistance ‘jump’ increase can be seen as the feature area for damage’s early warning. • Monitoring the resistance variation of the single fibre composite was conducted under cyclic loading with progressively increasing the strain peaks in order to further investigate the response of in-situ sensor to the interphase damage process. The deviation of resistance/strain when the stress is larger than 2 % highlights the accumulation of damage, which gives insight into the mechanism of resistance change.

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Shagolsem, Lenin S., and Jens-Uwe Sommer. "Diblock copolymer–selective nanoparticle mixtures in the lamellar phase confined between two parallel walls: a mean field model." Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2014. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-139324.

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We present a mean field model for a mixture of AB diblock-copolymers and A-block selective nanoparticles confined between two identical non-selective walls. A horizontally symmetric lamellar structure of the nanocomposite is considered where nanoparticles are allowed to segregate between the polymer–wall interfaces. For a fixed value of wall separation, we study changes in the free energy as a function of the number of lamellar layers and the amount of nanoparticle uptake in the A-phase denoted by y = ϕx with 0 ≤ x ≤ 1 for a given value of ϕ, where ϕ is the overall nanoparticle volume fraction. The absorption isotherm for nanoparticle uptake in the A-phase as a function of ϕ shows saturation beyond a threshold value ϕs, and the optimal value of uptake y increases with increasing strength of monomer–nanoparticle attractive interaction. Increasing ϕ above ϕs produces a decrease in the optimal number of lamellar layers which is related to a jump-like transition of the chain extension. The effect of varying film thickness is also studied. By considering A-block selective walls we also investigated a wetting transition of the copolymer film and found the transition to be discontinuous. A corresponding phase diagram is constructed
Dieser Beitrag ist mit Zustimmung des Rechteinhabers aufgrund einer (DFG-geförderten) Allianz- bzw. Nationallizenz frei zugänglich

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Schleinitz, Armin, Sven Eichhorn, and Christine Schubert. "Hängefördersystem mit Trag- und Gleitelement aus Wood Plastic Composite (WPC)." Universitätsbibliothek Chemnitz, 2017. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-230689.

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Erneuerbare Werkstoffe (z.B. WPC) können metallische substituieren, indem eine Kombination aus technischen, wirtschaftlichen und ökologischen Vorteilen in Bauweise und Bauteilen in der Intralogistik Anwendung finden. Vorgestellt werden die wichtigsten Schritte zur Entwicklung eines Hängefördersystems mit einem Trag- und Gleitprofil aus WPC. Schwerpunkte sind die Verbindungsstellen, die Kurvensegmente und die Weiche. Es erfolgt eine Beurteilung der Gebrauchstauglichkeit des Gesamtsystems.

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Lu, Yan. "Polypyrrole-containing Composite Particles: Preparation, Characterization and Application." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2005. http://nbn-resolving.de/urn:nbn:de:swb:14-1109235925474-80822.

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This research is focused on preparation of polypyrrole (PPy) composite particles by using socalled template oxidative polymerization method. As a template, water-soluble polymers, polymeric microgels, latex particles or bulk gels can be used. The morphology and properties of the composite particles can be controlled effectively by the proper use of the template. By choosing the dopant anion or oxidation agent it is possible to vary the conductivity of the polymer. In the case when uncrosslinked PVME was used as stabilizer, core-type polypyrrole spherical particles in the range of 50-100 nm were formed in both aqueous ethanol and water. Results of the elementary analysis, IR spectroscopy confirmed that the anionic salts can be incorporated in the PPy particles and play as the dopants. The presence of dopants in polypyrrole enhances the conductivity, especially in the case of sodium benzoate the conductivity of the final product has been improved by 3 orders. Polymeric microgels were also applied as the templates for polypyrrole deposition. When crosslinked PVME microgels were used in the oxidation polymerization of pyrrole, large PPy fibrils (appr. 400nm) were formed. Needle-like particles were formed due to the porous structure of microgels, which play a template role in the pyrrole polymerization process. When poly(VCL/AAEM) microgels were used as a template for oxidative polymerization of pyrrole, "raspberry-like" composite particles will be formed with PPy domains located in swollen hydropholic particle shell. Obtained stable composite microgels show similar thermal sensitivity as poly(VCL/AAEM) particles with fully reversible collapse-swelling properties. Increase of PPy content in composite particles increases conductivity of the composite material. The conductivity of composite particles prepared in water was much higher than that of prepared in water : ethanol mixtures. Furthermore, monodisperse PS-PEGMA particles, which were prepared in water medium by polymerization with sodium peroxydisulfate have been used as a template for deposition of polypyrrole (PPy). Obtained composite particles possess core-shell morphology where shell is composed out of small PPy nano-domains. The shell thickness can be varied by changing PPy load, controlling the overall template surface area in the system, and by influencing the pyrrole polymerization kinetics in presence of different oxidants. The last possibility provides also incorporation of different anions into polypyrrole shell. The stability of composite particles decreases gradually if the deposited PPy amount increases. It has been established that obtained particles are intrinsically coloured and the colour can be changed by the PS-PEGMA core size. Conductivity measurement shows that PS/PEGMA/PPy composite particles prepared by using phosphomolybdate as the oxidant are much more conductive than the particles prepared by the other two oxidants. The conductivity increases with the increase of PPy load in the system. Overall, the proper design of the template should give a possibility to control effectively the morphology, particle size and provide sufficient stability to the composite particles. Different morphologies, such as spherical, core-shell, raspberry and needle-like, with different particle size are expected to be available in different cases. By choosing the dopant anion or oxidation agent it is possible to vary the conductivity of the polymer. The stable water-based dispersions are expected to be used as additives for paint formulations, in electrorheology, microelectronic, ion-separation or disease diagnostics.

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Werniewicz, Katarzyna. "Fe-based composite materials with advanced mechanical properties." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2010. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-38543.

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In this study a series of novel Fe-based materials derived from a bulk metallic glass-forming composition was investigated to improve the ductility of this high-strength glassy alloy. The interplay between the factors chemistry, structure and resulting mechanical properties was analyzed in detail. It has been recognized that subtle modifications of the chemical composition (carbon addition) lead to appreciable changes in the phase formation, which occurs upon solidification (from a single-phase structure to composite materials). As a consequence, significant differences in the mechanical response of the particular samples have been observed. The materials developed here were fabricated by centrifugal casting. To explore the structure features of the as-cast cylinders, manifold experimental techniques (X-ray diffraction, optical, as well as electron microscopy) were employed. The occurrence of the numerous reflections on the X-ray diffraction patterns has confirmed the crystalline nature of the studied Fe-based alloy systems. The subsequent extensive research on their deformation behavior (Vickers hardness and room temperature compression tests) has revealed that, although the glass-forming ability of the investigated compositions is not high enough to obtain a glassy phase as a product of casting, excellent mechanical characteristics (high strength - comparable to that of the reference bulk metallic glass (BMG) - associated with good ductility) were achieved for the “composite-like” alloys. In contrast, the single phase cylinders, subjected to compressive loading, manifested an amazing capacity for plastic deformation – no failure occurred. The fracture motives developed during deformation of the “composite-structured” samples were studied by scanning electron microscopy. The main emphasis has been put on understanding the mechanisms of crack propagation. Owing to the structural complexity of the deformed samples, it was crucial to elucidate the properties of the individual compounds. Based on the obtained results it was concluded that the coexistence of a soft f.c.c. γ-Fe phase in combination with a hard complex matrix is responsible for the outstanding mechanical response of the tested composites. While the soft particles of an austenite contribute to the ductility (they hinder the crack propagation and hence, cause unequivocal strain-hardening), the hard constituents of the matrix phase yield the strength.

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Guilleaume, Christina, Alexander Brosius, and Ali Mousavi. "Investigation of Alternative Polymer Composite Materials for Forming Applications." Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2018. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-235022.

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In diesem Paper werden Untersuchungen eines Tiefziehwerkzeugs aus Mineralguss vorgestellt. Der Grund für die Verwendung von Mineralguss als alternativen Werkstoff für schnelle Werkzeuge liegt in den relativ geringen Initialkosten zur Herstellung und seiner Eignung für Kleinserien und Prototypenversuche. Ähnliche Konzepte mit Werkzeugen aus Mineralguss haben gezeigt, dass eine entscheidende Grenze in der Tribologie und dem bei diesem Werkstoff großen Oberflächenverschleiß liegt. Daher fokussiert das vorliegende Paper auf die Ergebnisse der Analyse verschiedener Mineralgussmischungen unter Anwendung von Streifenzugbiegeversuchen. Die Reibzahl wurde hierbei berechnet und vergleichend einem Stahlwerkzeug gegenübergestellt
This paper presents the investigation of polymer concrete drawing tools for deep drawing operations. The goal of using polymer concrete as an alternative material is a rapid tooling process at relatively low initial tools costs that is suitable for small batch production. Similar concepts based on hydraulic concrete and polymer composites have shown that the surface tri-bology and consequently wear is the main limiting factor. Therefore, this paper focusses on the results of strip draw-bending tests with different polymer concrete mixtures. The friction coefficient is calculated and compared to a steel tool

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Eichhorn, Sven, and Brit Clauß. "Charakterisierende Untersuchungen zum Reibungs- und Verschleißverhalten von WPC (Wood Polymer Composite)." Universitätsbibliothek Chemnitz, 2009. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-200901840.

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Die vorliegende Forschungsarbeit resultierte aus dem Ansatz, die theoretisch ableitbaren Vorteile der Werkstoffgruppe WPC (Wood Polymer Composite) zur Herstellung von Gleitelementen für fördertechnische Anwendungen (z.B. Gleitschienen in Stückgutförderern) zu nutzen. Diesem Ansatz lag der Gedanke zu Grunde, dass der anfängliche abrasive Verschleiß der polymeren Komponente als Schmiermittel den Abrieb und den Reibwert der stärker tragenden Holzkomponente verringert. Im WPC würde damit eine Funktionstrennung zwischen „tragendem“ Holz und „schmierendem“ Kunststoff vorherrschen. Darauf aufbauend erschien die These zulässig, dass sich im tribologisch aktiven Maschinenteil (Gleitschienen) die typischen Verschleißursachen hochbelasteter polymerer Gleitelemente wie einer starke Abrasion der Reibpartner, mechanische Überlast und damit Deformation in den Kontaktstellen und thermisch bedingter Verschleiß durch Temperaturstau in der Reibzone durch gezielten Holzzusatz in eine Kunststoffmatrix minimieren bzw. zu höheren Grenzen hin verschieben lassen. Diese These wurde in verschiedenen tribologischen Untersuchungen an spritzgegossenen und extrudierten Versuchskörpern grundlegend bestätigt. Die dargestellten Ausführungen zu den Untersuchungen gliedern sich inhaltlich in drei Schwerpunkte. Im ersten Punkt werden die Ergebnisse aus einfachen Tests zum grundlegenden Reibungsverhalten von WPC unter Nutzung des Stift–Scheibe–Versuches und einer nach praxisnahen fördertechnischen Anforderungen konzipierten Versuchseinrichtung vorgestellt sowie in den Stand der Technik eingeordnet. Die Praxisnähe der Versuche wird dabei durch die Probeauswahl weiter erhöht, indem Versuchskörper aus extrudierten Halbzeugen (Terrassendecks aus kommerziellen WPC) und Segmenten aus Förderketten ausgewählt werden. Die daraus resultierenden Aussagen ermöglichen erste Erkenntnisse hinsichtlich des dynamischen Reibwertes des WPC im relevanten tribologischen Belastungsspektrum für Gleitschienen. Im zweiten Punkt wird, aufbauend auf den gewonnenen Erkenntnissen, eine Betrachtungsweise vorgestellt, die neben dem Reibwert Aussagen zum Verschleißverhalten beinhaltet und eine vereinfachte Möglichkeit bietet, mittels des „Tribologiewertes“ die gewonnenen Erkenntnisse in einer praxisnahen Sichtweise darzustellen. Zudem wird die Versuchsmatrix hinsichtlich der verwendeten Parameter (Reibpartner, Reibgeschwindigkeit, theoretischer Flächenpressung) konkretisiert und erweitert. Die vorgestellte Betrachtungsweise und das verwendete Parameterfeld werden an spritzgegossenen Proben aus tribologisch „bekannten“ Materialien (Stand der Technik) und den Bestandteilen des untersuchten WPC (PP, PE, Fichte) überprüft. Weiterhin wird an vergleichbaren Proben aus WPC (50% PP / 50% Weichholz Fichte/Tanne) das tribologische Verhalten des Holzkunststoff - Verbundes klassifiziert. Dieses Verhalten wird hinsichtlich der tribologisch „bekannten“ Materialien in den Stand der Technik eingeordnet und eine These zum Wirkmechanismus bezüglich des Reibungs- und Verschleißverhaltens von WPC vorgestellt. Der dritten Punkt beinhaltet vertiefende Untersuchungen an spritzgegossenen Proben aus WPC mit 50% Weichholz und 50% PP - Matrix hinsichtlich des Einflussesder Spritzrichtung bzw. Holzpartikelorientierung, einer Wasserlagerung, der Konzentration des Haftvermittlers, einer Oberflächenbearbeitung. Weiterhin werden Aussagen zum Reibungs- und Verschleißverhalten von WPC mit PE-Matrix an spritzgegossenen Proben erarbeitet und eine erste Gegenüberstellung der Herstellungsverfahren Spritzguss und Extrusion vorgenommen. Die Untersuchungen ermöglichten in Summe das Gleitreibungs- und Verschleißverhalten des WPC grundlegend aber nicht vollständig zu charakterisieren. Die tribologischen Betrachtungen zur Werkstoffgruppe WPC stehen noch am Anfang ihrer Entwicklung. Die dargestellten Ergebnisse sind somit zudem als Startpunkt eines wissenschaftlichen Diskurses zu sehen.

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Schubert, Christine, Sven Friedrich, Brit Clauß, Klaus Nendel, and Michael Gehde. "Grundlagenuntersuchung zum Heizelementschweißen von Wood Plastic Composite (WPC) Prozessparameter - Eigenschaftsbeziehung." Universitätsbibliothek Chemnitz, 2013. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-129724.

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Das Schweißen von WPC stellt zunächst aufgrund der thermoplastischen Matrix eine effektive Fügetechnologie dar. Der Beitrag behandelt das Heizelementschweißen von WPC und liefert Aussagen zur Wirkung der Prozessparameter auf die mechanischen und geometrischen Nahteigenschaften, dem Rezeptureinfluss und der thermischen Instabilität der Holzfaser. An den WPC-Rezepturen auf Basis von Polypropylen mit 40 Gew.-% und 50 Gew.-% Holzfasern sowie des Einsatzes von PET-Fasern im Compound, werden die Zusammenhänge untersucht und die Versagensmechanismen aufgezeigt.

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Sadeghi, Amir. "Microstructure evolution and strengthening mechanism in Ni-based composite coatings." Doctoral thesis, Universitätsbibliothek Chemnitz, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-211837.

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Ni electrodeposition is a suitable process for producing thick deposits and thick metallic microstructures, especially for producing relatively deep micromoulds in Microsystems industry. Ni-P deposits, due to their better properties compared to Ni deposits – particularly high mechanical properties (hardness, wear resistivity), corrosion resistance, magnetic properties, a higher fatigue limit and lower macroscopic deformation – can be a very good alternative for producing Microsystems, especially for MEMS or Microengines. According to few limited literature and our primary investigations, dispersion coating and adding particle into the electrolyte can be considered as an approach in order to decrease the stress and ease the deposition of Ni-P galvanically. Although in the last decades the influence of particles embedment in the matrix by electroplating techniques have attracted the scientific interest, there are still contradictions among the research community concerning the influence of codeposited particles on the microstructure and strengthening properties of Ni-based composites coatings. In many cases, it is believed that the enhanced mechanical performance of the coatings is mainly caused by a change in the microstructure of the metal matrix and not so much by the presence of the particles themselves. In other words, the role of particle characteristics - like their nature, size and concentration - on the layer features and strengthening mechanism of electrodeposited Ni-based composite coating with different matrix is not cleared well. Furthermore, the incorporation of particles into the deposit is mainly considered as a key factor for determining the composite coatings properties. Despite of existing models of ECD, the mechanism of particle incorporation into the film under influence of different particle characteristics has not been well understood yet. Therefore, the main aim of this study is to shed light on the effect of particle characteristics (size, concentration, type) on the codeposition process, microstructure and strengthening mechanisms in Ni and Ni-P electrodeposited composite coatings.

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Eichhorn, Sven, Ronny Eckardt, Christoph Alt, and Klaus Nendel. "Verwendung von Holzwerkstoffen in Fördertechnik der Automobilfertigung." Universitätsbibliothek Chemnitz, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-203240.

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Aufbauend auf einer an der TU Chemnitz, Professur Fördertechnik, Forschungsgruppe Anwendungstechnik Erneuerbarer Werkstoffe entwickelten Holzbauweise für den Maschinenbau, wird die tragende Anwendung von Holzwerkstoffen innerhalb der Fördertechnik der Automobilfertigung aufgezeigt. Am Beispiel von Skidfördertechnik aus WVC (Wood Veneer Composite) bei der Volkswagen AG in Wolfsburg, wird der Transfer von Forschungsergebnissen thematisiert. Dabei wird die Entwicklung und Umsetzung verschiedener Skidförderer in Holzbauweise bis zur Serienanwendung dargestellt. Die Schwerpunkte der Darstellung sind ausgewählte, konstruktiv relevante Aspekteund ein Vergleich zu den tradierten metallischen Bauweisen.

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Schlecht, Sylvia. "Auswirkungen einer prophylaktischen Verabreichung der Präparate Carduus compositum, Coenzyme compositum, Lachesis compositum und Traumeel QP auf die Eutergesundheit von Milchkühen." Diss., lmu, 2004. http://nbn-resolving.de/urn:nbn:de:bvb:19-28190.

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Chiang, Yu-Chih. "Polymerization Shrinkage with Light-Initiated Dental Composites." Diss., lmu, 2009. http://nbn-resolving.de/urn:nbn:de:bvb:19-107085.

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38

Fabbrici, Simone. "Studio delle proprietà meccaniche e smorzanti dei compositi in fibra di carbonio nano-rinforzati." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2020.

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Nella tesi in esame ci si pone come obiettivo principale quello di indagare il comportamento meccanico e dinamico di un materiale composito nano-rinforzato. Il composito posto in esame risulta essere un materiale innovativo in quanto unisce un prepreg in fibra di carbonio con fibre unidirezionali e membrane di nano-fibre in gomma. Negli ultimi anni si è notata una crescente esigenza nel settore industriale volta a diminuire le vibrazione in sistemi meccanici sottoposti a sollecitazioni periodiche, come ad esempio, mandrini per macchine automatiche o rulli per il settore tissue o covering, tutto questo giustifica la ricerca portata avanti in questa tesi che consiste nello sviluppare un materiale composito innovativo in grado di attenuare le vibrazioni senza d’altra parte aumentarne il peso. Sono da tempo riconosciute le alte capacita smorzanti della gomma, ma spesso l’integrazione nei materiali compositi avviene attraverso l’inserimento di una strato spesso di gomma tra due layer rigidi (struttura a sandwich), questo porta ad un aumento considerevole del peso e dello spessore, caratteristiche che possono rendere un materiale composito meno attraente in alcuni campi di applicazione. Lo smorzamento o damping risulta essere un fenomeno impegnativo da studiare nei materiali metallici perché esso è influenzato da innumerevoli fattori. Per quanto riguarda i materiali compositi la sfida diventa ancora più impegnativa data la loro natura intrinsecamente eterogenea. Concludendo, dalle prove sperimentali, è emerso un incremento notevole delle prestazioni smorzanti dei provini nano-modificati, lasciando inalterate le prestazioni meccaniche.

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Glowania, Micheal, Oliver Weichold, Markus Hojczyk, Gunnar Seide, and Thomas Gries. "Neue Beschichtungsverfahren für PVA-Zement-Composite in textilbewehrtem Beton." Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2009. http://nbn-resolving.de/urn:nbn:de:bsz:14-ds-1244043027880-94266.

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Im Rahmen des Transferprojektes T01 „Textilbeschichtung mit hochviskosen Massen“ des Sonderforschungsbereiches 532 (SFB 532) wird die Realisierung und Bewertung eines integrierten Beschichtungskonzeptes zur nachhaltigen Verbesserung der Tragfähigkeit von textilbewehrten Betonbauteilen an der RWTH Aachen University untersucht. Dazu wird eine neue Auftragstechnik für hochviskose Beschichtungsmassen entwickelt, die eine vollständige Penetration von Multifilamentgarnen mit großen Garntitern und einer hohen Anzahl an Filamenten in textilen Gelegen erzielt. Des Weiteren werden aktive Beschichtungsmassen auf der Basis von Polyvinylalkohol-Zement-Compositen, die eine homogene Anbindung aller Einzelfilamente an die Zementmatrix ermöglichen, erforscht.

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Eichhorn, Sven, Brit Clauß, and Ann-Kathrin Harsch. "Rad aus WPC (Wood Polymer Composite) zum Einsatz in der Fördertechnik." Universitätsbibliothek Chemnitz, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-188694.

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Es wird die Bauteilentwicklung für ein Rad aus WPC (Wood Polymer Composite) vorgestellt. Das Rad ist der Demonstrator für eine WPC-Radbauweise zur Anwendung in der Intralogistik. Das Rad hat eine Lastgrenze von 150kg. Es werden statisch-mechanische Untersuchungen zu verschiedenen Materialrezepturen und Radkonstruktionen vorgestellt. Ergänzend werden tribologische Versuche von ausgewählten Rädern dargestellt, um die Praxistauglichkeit des Demonstrators und der Bauweise abzuschätzen
A component- and material development for a wheel made from WPC (Wood Polymer Composite) is presented. The wheel is the demonstrator for a WPC-wheel design for the use in the intralogistics. The wheel has a load limit of 150kg. Staticmechanical investigations of different material compositions and wheel designs are presented. Tribological investigations of selected wheels are shown, to give an estimation of the prototype’s usability and the effectiveness of the general wheel design

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Kim, Young Eun. "Modified Phenol-Formaldehyde Resins for C-Fiber Reinforced Composites: Chemical Characteristics of Resins, Microstructure and Mechanical Properties of their Composites." Doctoral thesis, Universitätsbibliothek Chemnitz, 2011. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-64064.

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This work correlates the chemistry of phenol-formaldehyde (PF) resins, its functionalities with their microstructural and mechanical properties in composite materials. The main focus is put on the development of the pores in dependence on the chemical composition of the resins and their influence on the structure of the material. Chemical characteristics of the synthesized resins are analyzed and physical/mechanical properties of the matrices based on PF resins are determined. Differences in the chemical properties are detected e.g. by FT-IR and NMR spectroscopy. They indicate the existence of similar molecular basic structure units, but different network conditions of the resins. DSC investigations point on different reaction mechanisms and temperatures; they reveal also their changed thermal behavior. The bulk matrix behavior differs from that of the composite based on the same resin due to the three dimensional stress and strain fields in the composites. The structure of the CFRP composites is strongly depended on the fiber/matrix interaction. The fiber matrix bonding (FMB) strength controls the load transfer via shear forces and therefore the segmentation of the fiber bundles.

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Matik, Marek, Miroslava Václavíková, and Vladimír Šepelák. "Preparation and study of maghemite-zeolite composites." Universitätsbibliothek Leipzig, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-188162.

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Figiel, Lukasz. "Sensitivity Analysis of Interface Fatigue Crack Propagation in Elastic Composite Laminates." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2004. http://nbn-resolving.de/urn:nbn:de:swb:14-1102358246078-89903.

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Composite laminates are an important subject of modern technology and engineering. The most common mode of failure in these materials is probably interlaminar fracture (delamination). Delamination growth under applied fatigue loads usually leads to structural integrity loss of the composite laminate, and hence its catastrophic failure. It is known that several parameters can affect the fatigue fracture performance of laminates. These include the constituent material properties, composite geometry, fatigue load variables or environmental factors. The knowledge about effects of these parameters on fatigue delamination growth can lead to a better understanding of composite fatigue fracture behaviour. Effects of some of these parameters can be elucidated by undertaking appropriate sensitivity analysis combined with the finite element method (FEM) and related software. The purpose of this work was three-fold. The first goal was the elaboration and computational implementation of FEM-based numerical strategies for the sensitivity analysis of interface fatigue crack propagation in elastic composite laminates. The second goal of this work was the numerical determination and investigation of displacement and stress fields near the crack tip, contact pressures along crack surfaces, mixed mode angle, energy release rate and the number of cumulative fatigue cycles. The third aim of the present study was to use the developed strategies to evaluate numerically the sensitivity gradients of the total energy release rate and fatigue life with respect to design variables of the curved boron/epoxy-aluminium (B/Ep-Al) composite laminate in two different material configurations under cyclic shear of constant amplitude. This study provided novel strategies for undertaking sensitivity analysis of the delamination growth under fatigue loads for elastic composite laminates using the package ANSYS. The numerical results of the work shed more light on mechanisms of interfacial crack propagation under cyclic shear in the case of a curved B/Ep-Al composite laminate. Moreover, the outcome of the sensitivity gradients demonstrated some advantages for using the sensitivity analysis to pinpoint directions for the optimisation of fatigue fracture performance of elastic laminates. The strategies proposed in this work can be used to study the sensitivity of the interface fatigue crack propagation in other elastic laminates, if the crack propagates at the interface between the elastic and isotropic components. However, the strategies can be potentially extended to composites with interfacial cracks propagating between two non-isotropic constituents under a constant amplitude fatigue load. Finally, the strategies can also be used to undertake the sensitivity analysis of composite fatigue life with respect to variables of fatigue load.

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Okulov, Ilya. "Microstructure and mechanical properties of new composite structured Ti-based alloys." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-160897.

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The demanding structural applications (e.g. aerospace, biomedical, etc.) require new materials with improved mechanical performance. The novel Ti-based dendrite + nano-/ultrafine-structured (Ti-based DNUS) composites exhibit an advantageous combination of high compressive strength (2000 – 2500 MPa) and large compressive ductility (10 – 30 %) already in the as-cast state [1,2] and, therefore, can be referred as high-performance materials. However, these Ti-based composites frequently exhibit very low or even lack of tensile ductility [3]. Therefore, the aim of this research work is to develop high strength Ti-based DNUS composites with pronounced tensile plasticity and to correlate the mechanical properties with their microstructure. In order to reach the goal, the high-strength Ti66Nb13Cu8Ni6.8Al6.2 (at.%) alloy exhibiting large compressive ductility [4] was selected for the modification. The microstructure of Ti66Nb13Cu8Ni6.8Al6.2 is composed of two metallographic constituents including β-Ti dendrites and an interdendritic component. The β-Ti dendrites are enriched in Nb and, therefore, Nb is referred as “dendritic element” whereas the interdendritic component is enriched in Ni and Cu and, therefore, these are referred as “interdendritic elements”. To perform a systematic study of the “interdendritic elements” (Ni, Cu and Co) effect on microstructure, a number of alloys with different concentration and types of alloying elements (Ti-Nb-Cu-Ni-Al, Ti-Nb-Co-Ni-Al, Ti-Nb-Cu-Co-Al and Ti-Nb-Ni(Co)-Al) were developed. It was shown that a higher concentration of the “interdendritic elements” in a composition within one alloy system corresponds to a higher volume fraction of the interdendritic component. Additionally, the crystal structure of the interdendritic phases is affected by type of the “interdendritic elements”. Since the most advanced applications (e.g. aerospace) require materials with high specific strengths, the new ductile Ti-Nb-Cu-Ni-Al alloys were modified to reduce their density, i.e. the Nb was substituted by lighter V. As a result, a new family of Ti-V-Cu-Ni-Al alloys with improved specific strength compared to the Ti-Nb-Cu-Ni-Al alloys was developed. Additionally, moduli of resilience of the Ti-V-Ni-Cu-Al alloys are superior when compared with those of the commercial Ti-based spring materials. The effect of microstructure on deformation of the newly developed alloys was studied through the in-situ microstructural analysis of samples at different strained states by means of scanning electron microscopy. To reveal the effect of the metallographic constituents on strength, the microhardness mapping of the new alloys was performed. Using the obtained empirical principles of microstructure adjustment, a new Ti68.8Nb13.6Co6Cu5.1Al6.5 (at.%) alloy with a large static toughness (superior to those of the recently developed Ti-based metallic glass composites) was developed. This large static toughness is due to both high strength and significant tensile plasticity. To study the effect of microstructure on tensile plasticity of Ti68.8Nb13.6Co6Cu5.1Al6.5 the in-situ microstructural analysis of samples at different strained states in the scanning electron microscope as well as the transmission electron microscopy studies were performed
Der erhöhte Anspruch an strukturelle Anwendungen (z.B. Luftfahrt, Biomedizin, etc.) verlangt neue Werkstoffe mit verbesserten mechanischen Leistungsfähigkeiten. Neuartige Ti-basierte dendritische nano-/ultrafeine Komposite (Ti-basierte DNUS Komposite) besitzen eine vorteilhafte Kombination von hoher Druckfestigkeit mit großer plastischer Verformbarkeit unter Druckbelastung bereits im Gusszustand [1,2] wodurch sie als hochleistungsfähige Werkstoffe angesehen werden. Jedoch besitzen diese Ti-basierte DNUS Komposite heufig eine stark verringerte oder gar keine Duktilität unter Zugbelastung [3]. Deswegen ist es das Ziel dieser Forschungsarbeit neue hochfeste Ti-basierte DNUS Komposite mit ausgeprägter Duktilität unter Zugbelastung zu entwickeln und die mechanischen Eingeschaften mit ihrer Mikrostruktur zu korrelieren. Um dieses Ziel zu erreichen wurde die hochfeste Legierung Ti66Nb13Cu8Ni6.8Al6.2 (at.%) [4], die eine große plastische Verformbarkeit unter Druckbelastung aufweist, ausgewählt. Die Mikrostruktur von Ti66Nb13Cu8Ni6.8Al6.2 setzt sich aus zwei metallographischen Konstituenten, einschließlich β-Ti Dendriten und einer interdendritischen Komponente, zusammen. Die β-Ti Dendriten sind mit Nb angereichert, weswegen Nb als “dendritisches Element” bezeichnet wird, wohingegen die interdendritische Komponente mit Ni und Cu angereichert ist und deswegen diese als “interdendritische Elemente” bezeichnet werden. Um den Einfluss der “interdendritischen Elemente” (Ni, Cu and Co) auf die Mikrostruktur zu untersuchen wurden Legierungen mit verschiedenen Konzentrationen unterschiedlicher Legierungselemente (Ti-Nb-Cu-Ni-Al, Ti-Nb-Co-Ni-Al, Ti-Nb-Cu-Co-Al and Ti-Nb-Ni(Co)-Al) entwickelt. Es wurde gezeigt, dass eine höhere Konzentration “interdendritischer Elemente” in einer bestimmten Zusammensetzung einem höheren Volumanteil der interdendritischen Komponente entspricht. Zusätzlich wird die Kristallstruktur der interdendritischen Phase sehr stark durch die “interdendritischen Elemente” beeinflusst. Da die meisten hoch entwickelten Anwendungen (z.B. Luftfahrt) gesteigerte spezifische Festigkeiten erforden, wurden die neuen duktilen Ti-Nb-Cu-Ni-Al Legierungen modifiziert um ihre Dichte zu reduzieren, indem Nb durch das leichtere V ersetzt wurde. Als Ergebniss wurde eine neue Familie von Ti-V-Cu-Ni-Al Legierungen, mit im Vergleich zu Ti-Nb-Cu-Ni-Al Legierungen verbesserten spezifischen Festigkeiten, entwickelt. Zusäzlich ist die elastische Formänderungsenergiedichte der neu entwickelten Legierungen höher verglichen mit kommerziellen Ti-basierten Federmaterialien. Der Effekt der Mikrostruktur auf das Verformungsverhalten der Legierungen wurde mittels in-situ mikrostruktureller Analysen verschiedener Verformungszustände im Rasterelektronenmikroskop untersucht. Um ein Einfluss der metallographischen Konstituenten auf die Festigkeit zu bestimmen wurden Mikrohärtekarten erstellt. Unter Verwendung der erhalten empirischen Prinzipen zur Einstellung der Mikrostruktur wurde eine neue Legierung Ti68.8Nb13.6Co6Cu5.1Al6.5 (at.%) mit hoher statischer Zähigkeit (besser als die der kürzlich entwickelten Ti-basierten gläsernen metallischen Kompositlegierungen) entwickelt. Diese hohe statische Zähigkeit wird sowohl durch die hohe Festigkeit als auch durch die ausgeprägte Plastizität unter Zugbelastung verursacht. Um den Einfluss der Mikrostruktur auf die Plastizität unter Zug zu untersuchen wurde Transmissionelektronmikroskopie sowie in-situ mikrostrukturelle Analysen verschiedener Verformungszustände im Rasterelektronmikroskop durchgefühlt

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Gao, Deyu. "Superabsorbent polymer composite (SAPC) materials and their industrial and high-tech applications." Doctoral thesis, Technische Universitaet Bergakademie Freiberg Universitaetsbibliothek "Georgius Agricola&quot, 2009. http://nbn-resolving.de/urn:nbn:de:swb:105-1484776.

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Quellfähige Verbundwerkstoffe aus Ton und Polyakrylamid können große Quantitäten von Wasser absorbieren, behalten aber dabei eine hohe mechanische Festigkeit und gute Dämpfungseigenschaften und stellen daher eine neue Klasse von Hydrogelen mit potentiell interessanten technologischen Eigenschaften dar. Solche superabsorbierende Verbundwerkstoffe (SAPC) werden durch Polymerisation mit einem Elektronenstrahl oder Bestrahlung mit UV-Licht hergestellt. Die Untersuchung der Eigenschaften von SAPC mit Hilfe von XRD, SEM, DSC, TGA, FTIR und NMR (27Al, 29Si und C) zeigen, dass in der SAPC-Struktur das Akrylamid (AM) mit Montmorillonit in dreierlei unterschiedlichen Weisen verbunden ist: a. AM interkaliert in den Zwischenschichtraum von Montmorillonit in bimolekularen Schichten, die durch van-der-Waals-Kräfte und Wasserstoffbindungen verknüpft sind; b. AM gebunden an der Oberfläche von Montmorillonit durch Wasserstoffbindungen; c. AM als freies Polymernetzwerk. Die Ergebnisse der rheologischen, mechanischen und thermischen Untersuchungen von SAPC zeigen eine völlig vernetzte Struktur mit vergleichsweise hoher mechanischer Festigkeit und thermischer Stabilität. Die Verwendung von SAPC bei der Ölgewinnung (Erhöhung der Ausbeute), im Umweltschutz (Reduzierung sauerer Berge), der Agri- und Silvikultur (Pflanzen, Samenbau), der petrochemischen Industrie (Entwässern), im Bauingenieurwesen (Zementbeimischung) und als Sensorsubstanz demonstriert, dass SAPC ein hohes Potential für umweltfreundliche und wirtschaftliche alternative Zwecke hat.

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Eichhorn, Sven, Brit Clauß, and Klaus Nendel. "Untersuchungen zum tribologischen Verhalten von hochgefüllten WPC (Wood Polymer Composite) als Maschinenbaukomponente." Universitätsbibliothek Chemnitz, 2012. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-89811.

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Ziel der Untersuchungen war es, Grundlagen für den Einsatz von hochgefüllten WPC in tribologisch funktionalen Maschinenelementen, wie z. B. Gleitschienen in Stückgutförderern zu schaffen. Aufbauend auf einem Kurzzeitversuch verschiedener hoch gefüllter WPC mit Polypropylenmatrix (PP- Matrix), wurde untersucht, wie sich ein steigender Holzanteil, eine Wasserlagerung sowie die Matrix selbst durch Ersatz der PP durch eine Polyethylenmatrix (PE-Matrix) auf das tribologische Langzeitverhalten des Werkstoffes auswirken
The aim of the research was to create basic knowledge for the use of highly filled WPC in tribological functional machine elements, e. g. sliding rails in conveyors. Based on a short-term test of several highly filled WPCs with polypropylene matrix (PP matrix), the impact of several parameters on the long-term performance of WPC was investigated. These parameters were: a rising proportion of wood, an immersion in water over 700 hours and the matrix itself. In that case the PP matrix was replaced by a polyethylene matrix (PE matrix)

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Seidlitz, Holger, Lars Ulke-Winter, Colin Gerstenberger, and Lothar Kroll. "Dimensioning of Punctiform Metal-Composite Joints: A Section-Force Related Failure Criterion." Universitätsbibliothek Chemnitz, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-152889.

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Reliable line production processes and simulation tools play a central role for the structural integration of thermoplastic composites in advanced lightweight constructions. Provided that material- adapted joining technologies are available, they can be applied in heavy-duty multi-material designs (MMD). A load-adapted approach was implemented into the new fully automatic and faulttolerant thermo mechanical flow drill joining (FDJ) concept. With this method it is possible to manufacture reproducible high strength FRP/metal-joints within short cycle times and without use of extra joining elements for the first time. The analysis of FDJ joints requires a simplified model of the joint to enable efficient numerical simulations. The present work introduces a strategy in modeling a finite-element based analogous-approach for FDJ-joints with glass fiber reinforced polypropylene and high-strength steel. Combined with a newly developed section-force related failure criterion, it is possible to predict the fundamental failure behavior in multi-axial stress states. The functionality of the holistic approach is illustrated by a demonstrator that represents a part of a car body-in-white structure. The comparison of simulated and experimentally determined failure loads proves the applicability for several combined load cases.

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Heuer, Dennis, Norbert Schwarzer, and Thomas Chudoba. "Contact Mechanics in Dentistry: A systematic investigation of modern composite materials used for fillings." Universitätsbibliothek Chemnitz, 2006. http://nbn-resolving.de/urn:nbn:de:swb:ch1-200600133.

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Nowadays, high demands are made on filling materials in modern dentistry: Durability, Reliability &Aesthetic Requirements Thus, a group of physicists and an independent practicing dentist investigated 11 different teeth fillings (composite materials) as used in modern dental practices according to their stability and ability to withstand contact loadings.

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Zikánová, Arlette, Pavel Hrabánek, Milan Kočiřík, Libor Brabec, Klára Juristová, Pavel Čapek, Bohumil Bernauer, Vladimír Hejtmánek, Olga Šolcová, and Petr Uchytil. "Mass transport in the hierarchical porous structure of zeolite-based composite membranes." Universitätsbibliothek Leipzig, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-196794.

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Höhe, Bettina. "Vergleichende Untersuchung - Composite Graft versus Doppelgabellappen - bei bilateralen Lippen-Kiefer-Gaumen-Spalten." [S.l. : s.n.], 2008. http://nbn-resolving.de/urn:nbn:de:bsz:289-vts-63966.

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Dissertations / Theses on the topic 'NbC composite'

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