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Journal articles on the topic 'Non-aqueous synthesis'

Author: Grafiati

Published: 9 March 2023

Last updated: 10 March 2023

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1

Zhang, Wu Ying, and Bao Hua Zhang. "Synthesis of Aqueous Non-Isocyanate Polyurethane." Applied Mechanics and Materials 618 (August 2014): 184–88. http://dx.doi.org/10.4028/www.scientific.net/amm.618.184.

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Cyclic carbonate emulsion was prepared by means of polymerization technology using DOMA (which was synthesized by glycidyl methacrylate and carbon dioxide) and acrylic monomers. Effect of temperature, amount of emulsifier, initiator, DOMA and acrylic acid on properties of the emulsion and the film were studied. It was found that with 4% emulsifier, of which the ratio of OP-10 and SDS was 2:1, and 0.4% initiator, 3.5% acrylic acid, 13.3% DOMA, the temperature was 78°C. Under this condition the performance was the best, and then the aqueous non-isocyanate polyurethane was synthesized by cyclic carbonate emulsion and diethylenetriamine as curing agent. The structure of emulsion and aqueous non-isocyanate polyurethane was characterized by FTIR.

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2

van Erp, W. A., H. W. Kouwenhoven, and J. M. Nanne. "Zeolite synthesis in non-aqueous solvents." Zeolites 7, no. 4 (1987): 286–88. http://dx.doi.org/10.1016/0144-2449(87)90027-3.

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3

Scott, Robert W. J., Neil Coombs, and Geoffrey A. Ozin. "Non-aqueous synthesis of mesostructured tin dioxide." Journal of Materials Chemistry 13, no. 4 (2003): 969–74. http://dx.doi.org/10.1039/b206002g.

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4

Petkar, Manish, Arvind Lali, Paolo Caimi, and Moreno Daminati. "Immobilization of lipases for non-aqueous synthesis." Journal of Molecular Catalysis B: Enzymatic 39, no. 1-4 (2006): 83–90. http://dx.doi.org/10.1016/j.molcatb.2006.01.034.

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5

Armes, S. P., and M. Aldissi. "Non-aqueous polypyrrole colloids: Synthesis and characterization." Synthetic Metals 37, no. 1-3 (1990): 137–44. http://dx.doi.org/10.1016/0379-6779(90)90140-g.

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6

Bonham, J. A., M. A. Faers, and J. S. van Duijneveldt. "Non-aqueous microgel particles: synthesis, properties and applications." Soft Matter 10, no. 47 (2014): 9384–98. http://dx.doi.org/10.1039/c4sm01834f.

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7

Niwayama, Satomi. "Non-Enzymatic Desymmetrization Reactions in Aqueous Media." Symmetry 13, no. 4 (2021): 720. http://dx.doi.org/10.3390/sym13040720.

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Symmetric organic compounds are generally obtained inexpensively, and therefore they can be attractive building blocks for the total synthesis of various pharmaceuticals and natural products. The drawback is that discriminating the identical functional groups in the symmetric compounds is difficult. Water is the most environmentally benign and inexpensive solvent. However, successful organic reactions in water are rather limited due to the hydrophobicity of organic compounds in general. Therefore, desymmetrization reactions in aqueous media are expected to offer versatile strategies for the synthesis of a variety of significant organic compounds. This review focuses on the recent progress of desymmetrization reactions of symmetric organic compounds in aqueous media without utilizing enzymes.

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8

Varghese, Mini, R. Aiswarya, and K. P. Surendran. "Non Aqueous Synthesis of Titania Ink for Printed Electronics." Materials Science Forum 830-831 (September 2015): 573–76. http://dx.doi.org/10.4028/www.scientific.net/msf.830-831.573.

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A non-aqueous synthesis technique of room temperature curable titania ink, screen printed on flexible BoPET film for printed electronics applications is reported. The phase evolution of rutile titania powder, formulation of a fast curing titania ink, as well as the microstructure and dielectric properties of printed pattern are discussed. In terms of ease of synthesis, cost effectiveness and faster curing time, the developed ink is found to be advantageous over water based dielectric inks.

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9

Bibby, D. M., and M. P. Dale. "Synthesis of silica-sodalite from non-aqueous systems." Nature 317, no. 6033 (1985): 157–58. http://dx.doi.org/10.1038/317157a0.

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10

Gao, Qiuming, Shougui Li, and Ruren Xu. "Synthesis of AlPO4-17 from non-aqueous systems." Journal of the Chemical Society, Chemical Communications, no. 12 (1994): 1465. http://dx.doi.org/10.1039/c39940001465.

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11

Venkatathri, N., S. G. Hegde, P. R. Rajamohanan, and S. Sivasanker. "Synthesis of SAPO-35 in non-aqueous gels." Journal of the Chemical Society, Faraday Transactions 93, no. 18 (1997): 3411–15. http://dx.doi.org/10.1039/a702450i.

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12

Yadav, Ganapati D., Sachin S. Joshi, and Piyush S. Lathi. "Enzymatic synthesis of isoniazid in non-aqueous medium." Enzyme and Microbial Technology 36, no. 2-3 (2005): 217–22. http://dx.doi.org/10.1016/j.enzmictec.2004.06.008.

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13

Clapes, Pere, Gloria Caminal, Josep A. Feliu, and Josep Lopez-Santin. "ChemInform Abstract: Peptide Synthesis in Non-Aqueous Media." ChemInform 32, no. 1 (2001): no. http://dx.doi.org/10.1002/chin.200101260.

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14

Mertens, Machteld M., Céline Schott-Darie, Philippe Reinert, and J. L. Guth. "Synthesis of microporous gallium phosphates from quasi non-aqueous synthesis mixtures." Microporous Materials 5, no. 1-2 (1995): 91–96. http://dx.doi.org/10.1016/0927-6513(95)00046-c.

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15

Asylbekova, D. D., M. Zh Duisembiyev, N. N. Issabayev, et al. "ELECTROCHEMICAL SYNTHESIS OF ZINC CHELATES IN NON-AQUEOUS MEDIA." Rasayan Journal of Chemistry 15, no. 01 (2022): 612–18. http://dx.doi.org/10.31788/rjc.2022.1516637.

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Electrochemical synthesis of zinc chelates in non-aqueous media has been studied by polarization, capacitance measurements, infrared spectrometry and electron microscopy. The dependences of the substance content and current yield on current density, ligand concentration, temperature and time were determined. Optimal conditions for the process were determined. The aim of the study is to perform electrochemical synthesis of polycarboxylic acidbased chelates in non-aqueous media and to determine the possibility of electrosynthesis in non-aqueous media. In order to study adsorption and material release, the electrochemical behavior of chelate complexes was studied by measuring the volt-ampere E-gi, i-τ, E-τ and capacitance curves. The measurements were performed using graphite and platinum electrodes in acidic alcohol solutions. Based on preliminary experiments it was found that the influence of the process temperature on the yield of the target product, copper chelate, was very small; increasing the temperature leads to some decrease in the yield of the target product, mainly due to resin formation. end products.

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16

Jaroszek, Hanna, and Piotr Dydo. "Ion-exchange membranes in chemical synthesis – a review." Open Chemistry 14, no. 1 (2016): 1–19. http://dx.doi.org/10.1515/chem-2016-0002.

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AbstractThe applicability of ion-exchange membranes (IEMs) in chemical synthesis was discussed based on the existing literature. At first, a brief description of properties and structures of commercially available ion-exchange membranes was provided. Then, the IEM-based synthesis methods reported in the literature were summarized, and areas of their application were discussed. The methods in question, namely: membrane electrolysis, electro-electrodialysis, electrodialysis metathesis, ion-substitution electrodialysis and electrodialysis with bipolar membrane, were found to be applicable for a number of organic and inorganic syntheses and acid/base production or recovery processes, which can be conducted in aqueous and non-aqueous solvents. The number and the quality of the scientific reports found indicate a great potential for IEMs in chemical synthesis.

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17

Pandey, Prem C., and Richa Singh. "Controlled Synthesis of Functional Silver Nanoparticles Dispersible in Aqueous and Non-Aqueous Medium." Journal of Nanoscience and Nanotechnology 15, no. 8 (2015): 5749–59. http://dx.doi.org/10.1166/jnn.2015.10045.

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18

Collins, Andrew M., Christine Spickermann, and Stephen Mann. "Synthesis of titania hollow microspheres using non-aqueous emulsions." Journal of Materials Chemistry 13, no. 5 (2003): 1112–14. http://dx.doi.org/10.1039/b301183f.

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19

Jansen, Nathan, John Yuzon, Erin McCardle-Blunk, James Barnes, Andrea Goforth, and Jun Jiao. "Non-Aqueous Synthesis of Graphene Supported Spinel Ferrite Nanoparticles." Microscopy and Microanalysis 25, S2 (2019): 2252–53. http://dx.doi.org/10.1017/s1431927619011991.

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20

Rossi, Laura I., and Rita H. de Rossi. "Synthesis of FeBr3-cyclodextrin complexes in non-aqueous solution." Journal of Supramolecular Chemistry 2, no. 6 (2002): 509–14. http://dx.doi.org/10.1016/s1472-7862(02)00076-x.

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21

Jardine, Roger S., and Paul Bartlett. "Synthesis of non-aqueous fluorescent hard-sphere polymer colloids." Colloids and Surfaces A: Physicochemical and Engineering Aspects 211, no. 2-3 (2002): 127–32. http://dx.doi.org/10.1016/s0927-7757(02)00258-3.

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22

Morris, Russell E., and Scott J. Weigel. "The synthesis of molecular sieves from non-aqueous solvents." Chemical Society Reviews 26, no. 4 (1997): 309. http://dx.doi.org/10.1039/cs9972600309.

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23

Müller, Kevin, Markus Klapper, and Klaus Müllen. "Synthesis of Conjugated Polymer Nanoparticles in Non-Aqueous Emulsions." Macromolecular Rapid Communications 27, no. 8 (2006): 586–93. http://dx.doi.org/10.1002/marc.200600027.

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24

Dushatinski, T., C. Huff, and T. M. Abdel-Fattah. "Synthesis and Characterizations of Cobalt Films Electrochemically Deposited from Aqueous and Non-Aqueous Media." ECS Transactions 64, no. 4 (2014): 487–91. http://dx.doi.org/10.1149/06404.0487ecst.

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25

Sinha Ray, Suprakas. "Synthesis and evaluation of conducting polypyrrole/Al2O3 nanocomposites in aqueous and non-aqueous medium." Materials Research Bulletin 37, no. 5 (2002): 813–24. http://dx.doi.org/10.1016/s0025-5408(02)00724-9.

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26

Khushalani, Deepa, Geoffrey A. Ozin, and Alex Kuperman. "Glycometallate surfactants. Part 1: non-aqueous synthesis of mesoporous silica." Journal of Materials Chemistry 9, no. 7 (1999): 1483–89. http://dx.doi.org/10.1039/a902289i.

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27

Athar, Taimur, Abdul Hakeem, and Waqar Ahmed. "Synthesis of MgO Nanopowder via Non Aqueous Sol–Gel Method." Advanced Science Letters 7, no. 1 (2012): 27–29. http://dx.doi.org/10.1166/asl.2012.2190.

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28

Styskalik, Ales, David Skoda, Zdenek Moravec, Pavla Roupcova, Craig E. Barnes, and Jiri Pinkas. "Non-aqueous template-assisted synthesis of mesoporous nanocrystalline silicon orthophosphate." RSC Advances 5, no. 90 (2015): 73670–76. http://dx.doi.org/10.1039/c5ra10982e.

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Mesoporous nanocrystalline silicon orthophosphate Si<sub>5</sub>P<sub>6</sub>O<sub>25</sub> was synthesized by the non-hydrolytic sol–gel reaction in the presence of Pluronic P123 template and displays superior catalytic activity and selectivity in methylstyrene dimerization.

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29

He, Wensen, Chengsheng Jia, Yuan Ma, et al. "Lipase-catalyzed synthesis of phytostanyl esters in non-aqueous media." Journal of Molecular Catalysis B: Enzymatic 67, no. 1-2 (2010): 60–65. http://dx.doi.org/10.1016/j.molcatb.2010.07.006.

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30

Wei, Dong-Zhi, Ping Zou, Mao-Bing Tu, and Hong Zheng. "Enzymatic synthesis of ethyl glucoside lactate in non-aqueous system." Journal of Molecular Catalysis B: Enzymatic 18, no. 4-6 (2002): 273–78. http://dx.doi.org/10.1016/s1381-1177(02)00106-6.

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31

Zheng, Hao, Changdong Xu, and Youqing Shen. "Facile synthesis of hydrogel microsphere by non-aqueous emulsion copolymerization." Nanomedicine: Nanotechnology, Biology and Medicine 14, no. 5 (2018): 1879. http://dx.doi.org/10.1016/j.nano.2017.11.367.

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32

Ahmad, Muhammad Z., Jin Chang, Muhammad S. Ahmad, Eric R. Waclawik, and Wojtek Wlodarski. "Non-aqueous synthesis of hexagonal ZnO nanopyramids: Gas sensing properties." Sensors and Actuators B: Chemical 177 (February 2013): 286–94. http://dx.doi.org/10.1016/j.snb.2012.11.013.

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33

GAO, Q., S. LI, and R. XU. "ChemInform Abstract: Synthesis of AlPO4-17 from Non-Aqueous Systems." ChemInform 25, no. 43 (2010): no. http://dx.doi.org/10.1002/chin.199443284.

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34

Rüdiger, Stephan, Udo Groß, and Erhard Kemnitz. "Non-aqueous sol–gel synthesis of nano-structured metal fluorides." Journal of Fluorine Chemistry 128, no. 4 (2007): 353–68. http://dx.doi.org/10.1016/j.jfluchem.2006.11.006.

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35

Herrmann, Christine, Daniel Crespy, and Katharina Landfester. "Synthesis of hydrophilic polyurethane particles in non-aqueous inverse miniemulsions." Colloid and Polymer Science 289, no. 10 (2011): 1111–17. http://dx.doi.org/10.1007/s00396-011-2430-z.

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36

Hudry, Damien, Christos Apostolidis, Olaf Walter, et al. "Non-aqueous Synthesis of Isotropic and Anisotropic Actinide Oxide Nanocrystals." Chemistry - A European Journal 18, no. 27 (2012): 8283–87. http://dx.doi.org/10.1002/chem.201200513.

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37

VENKATATHRI, N., S. G. HEGDE, P. R. RAJAMOHANAN, and S. SIVASANKER. "ChemInform Abstract: Synthesis of SAPO-35 in Non-Aqueous Gels." ChemInform 28, no. 48 (2010): no. http://dx.doi.org/10.1002/chin.199748285.

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38

Jin, Jia Rui, Yuan Zhi Chen, Hui Zhang Guo, Zhen Wei Wang, and Dong Liang Peng. "A Facile Non-Aqueous Approach for the Synthesis of Cu Nanowires." Advanced Materials Research 750-752 (August 2013): 245–48. http://dx.doi.org/10.4028/www.scientific.net/amr.750-752.245.

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A non-aqueous synthetic route has been developed for the preparation of uniform Cu nanowires with length up to tens of micrometers. Unlike commonly used one-pot synthesis approach that usually involve a fast reduction of metal precursors in the presence of reducing agents, a continuous-injection approach has been to utilized to control the speed of reaction and the concentration of Cu nuclei. In this approach, copper (II) chloride dihydrate and nickel (II) acetylacetone which are dissolved in oleylamine solutions have been injected into octadecene by a syringe-pump. The as-prepared samples have been characterized by transmission electron microscopy, scanning electron microscopy and energy-dispersive X-ray spectroscopy. The results show that the products are pure Cu nanowires which have preferred <110> growth directions. The formation mechanism and major influencing factors on the synthesis of Cu nanowires have been discussed.

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39

Zhang, Sainan, and Xiankai Jiang. "Synthesis and characterization of non-ionic and anionic two-component aromatic waterborne polyurethane." Pigment & Resin Technology 47, no. 4 (2018): 290–99. http://dx.doi.org/10.1108/prt-07-2017-0067.

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Purpose The purpose of this paper is to synthesize and characterize a series of two-component aromatic waterborne polyurethane (2K-WPU) which is composed of non-ionic and anionic polyisocyanate aqueous dispersion and polyurethane polyol aqueous dispersion. Design/methodology/approach The polyisocyanate aqueous dispersion was synthesized through non-ionic and anionic hydrophilic modification procedures. The values of the hydrogen bonding index (HBI) and molecule structures of WPU were obtained by Fourier transform infrared (FTIR). The thermal, mechanical and water resistance properties of 2K-WPU films were investigated. Findings The appearance of non-ionic polyisocyanate aqueous dispersion and anionic polyisocyanate aqueous dispersion was colorless translucent pan blue and yellow opaque emulsions, respectively. FTIR not only showed that 2K-WPU was obtained from the polymerization of polyisocyanate component and polyhydroxy component by polymerization but also showed that the content of hydrogen bondings of anionic 2K-WPU (WPU 2) was higher than non-ionic 2K-WPU (WPU 1). The glass-transition temperature (Tg), storage modulus and water resistance of WPU 2 were higher than WPU1, whereas the thermal stability of WPU1 was better than WPU 2. Practical implications The investigation established a method to prepare a series of 2K-WPU which was composed of non-ionic or anionic polyisocyanate aqueous dispersion and polyurethane polyol aqueous dispersion. The prepared 2K-WPU film could be applied as substrate resin material in the field of waterborne coating. Originality/value The paper established a method to synthesize a series of 2K-WPU. The effect of HBI value and the molecule structure of soft segment on the thermal stability, mechanical and water resistance properties of 2K-WPU films were studied.

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40

Kulkarni, S. K., A. S. Ethiraj, S. Kharrazi, D. N. Deobagkar, and D. D. Deobagkar. "Synthesis and spectral properties of DNA capped CdS nanoparticles in aqueous and non-aqueous media." Biosensors and Bioelectronics 21, no. 1 (2005): 95–102. http://dx.doi.org/10.1016/j.bios.2004.09.004.

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41

Kjeldgaard, Solveig, Iulian Dugulan, Aref Mamakhel, Marnix Wagemaker, Bo Brummerstedt Iversen, and Anders Bentien. "Strategies for synthesis of Prussian blue analogues." Royal Society Open Science 8, no. 1 (2021): 201779. http://dx.doi.org/10.1098/rsos.201779.

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We report a comparison of different common synthetic strategies for preparation of Prussian blue analogues (PBA). PBA are promising as cathode material for a number of different battery types, including K-ion and Na-ion batteries with both aqueous and non-aqueous electrolytes. PBA exhibit a significant degree of structural variation. The structure of the PBA determines the electrochemical performance, and it is, therefore, important to understand how synthesis parameters affect the structure of the obtained product. PBA are often synthesized by co-precipitation of a metal salt and a hexacyanoferrate complex, and parameters such as concentration and oxidation state of the precursors, flow rate, temperature and additional salts can all potentially affect the structure of the product. Here, we report 12 different syntheses and compare the structure of the obtained PBA materials.

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42

Geng, Weiguang, Ziheng Zhang, Zelong Yang, Huaiyuan Tang, and Guang He. "Non-aqueous synthesis of high-quality Prussian blue analogues for Na-ion batteries." Chemical Communications 58, no. 28 (2022): 4472–75. http://dx.doi.org/10.1039/d2cc00699e.

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43

Manthiram, Karthish. "(Invited) High-Rate Ammonia Synthesis at Non-Aqueous Gas Diffusion Electrodes." ECS Meeting Abstracts MA2021-02, no. 53 (2021): 1555. http://dx.doi.org/10.1149/ma2021-02531555mtgabs.

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44

Manthiram, Karthish. "(Invited) High-Rate Ammonia Synthesis at Non-Aqueous Gas Diffusion Electrodes." ECS Meeting Abstracts MA2021-01, no. 40 (2021): 1291. http://dx.doi.org/10.1149/ma2021-01401291mtgabs.

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45

Kemnitz, Erhard, and Johannes Noack. "The non-aqueous fluorolytic sol–gel synthesis of nanoscaled metal fluorides." Dalton Transactions 44, no. 45 (2015): 19411–31. http://dx.doi.org/10.1039/c5dt00914f.

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46

Kuperman, Alex, Susan Nadimi, Scott Oliver, Geoffrey A. Ozin, Juan M. Garcés, and Michael M. Olken. "Non-aqueous synthesis of giant crystals of zeolites and molecular sieves." Nature 365, no. 6443 (1993): 239–42. http://dx.doi.org/10.1038/365239a0.

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47

Kim, HunUk, Yang-Kook Sun, Kyung Hee Shin, and Chang Soo Jin. "Synthesis of Li4Mn5O12and its application to the non-aqueous hybrid capacitor." Physica Scripta T139 (May 2010): 014053. http://dx.doi.org/10.1088/0031-8949/2010/t139/014053.

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48

Yadav, Ganapati D., and Shrikant B. Dhoot. "Immobilized lipase-catalysed synthesis of cinnamyl laurate in non-aqueous media." Journal of Molecular Catalysis B: Enzymatic 57, no. 1-4 (2009): 34–39. http://dx.doi.org/10.1016/j.molcatb.2008.06.013.

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49

Fan, Shan, Xijun Liu, Yufeng Li, et al. "Non-aqueous synthesis of crystalline Co3O4 nanoparticles for lithium-ion batteries." Materials Letters 91 (January 2013): 291–93. http://dx.doi.org/10.1016/j.matlet.2012.10.008.

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50

Jha, Rupali, and Bharat Modhera. "Synthesis and Characterization of Nano-Crystalline Silicoaluminophosphate’s from Non-aqueous Media." Materials Today: Proceedings 4, no. 2 (2017): 4104–7. http://dx.doi.org/10.1016/j.matpr.2017.02.314.

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