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Dissertations / Theses on the topic 'Nucleophilic'

Author: Grafiati

Published: 4 June 2021

Last updated: 25 July 2025

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1

Antonsson, Rositha. "Nucleophilic aromatic substitutions using ethyl 3-mercaptopropionate as nucleophile : Scope and limitations." Thesis, Södertörn University College, School of Life Sciences, 2008. http://urn.kb.se/resolve?urn=urn:nbn:se:sh:diva-1517.

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<p>The scope and limitations of nucleophilic substitutions of aryl halides have been studied using ethyl 3-mercaptopropionate as nucleophile and microwave heating. A diversity of aromatic compounds have been investigated according to different types of leaving groups, regio isomers and substituents. Experimental design has been used as a tool to optimize the reaction. An electron-withdrawing group in ortho or para position of the leaving group proved to be necessary for a positive outcome of the reaction. Fluorine was, without competition, the best leaving group. Some examples of how the synth

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2

Thompson, Claire. "Aromatic nucleophilic nitration." Thesis, University of Exeter, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.390199.

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3

Harris, David T. "New Nucleophilic Organocatalysts." Thesis, The University of Arizona, 2011. http://hdl.handle.net/10150/144597.

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Acyl-transfer reactions have become commonplace in organic synthesis and organocatalysis of these reactions is becoming increasingly popular. 4-Dimethylaminopyridine has proven to be very useful in acylations; over the recent years chiral and more reactive analogs have received much attention. Interestingly, catalysis of acyl-transfers by diamines has also been shown to be effective. We present the synthesis of several DMAP analogs containing heteroatoms near the nucleophilic nitrogen. These analogs of DMAP vary from basic amidines, oxazolines, and amines, to alcohols, and fluoro-derivatives a

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4

Lees, Inez Nancy Lloyd. "Nucleophilic polymers for scavenging." Thesis, University of Cambridge, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.613095.

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5

Wei, Yin. "Theoretical Studies in Nucleophilic Organocatalysis." Diss., lmu, 2009. http://nbn-resolving.de/urn:nbn:de:bvb:19-95248.

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6

Maryasin, Boris. "Theoretical investigations in nucleophilic organocatalysis." Diss., lmu, 2011. http://nbn-resolving.de/urn:nbn:de:bvb:19-138820.

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7

Cresswell, Alex. "New methods for nucleophilic fluorination." Thesis, University of Oxford, 2011. http://ora.ox.ac.uk/objects/uuid:612ea592-2f52-407b-b761-36b02b746e9d.

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This thesis describes investigations into the utility of boron fluorides and tetrafluoroborates as sources of nucleophilic fluorine. Chapter 1 discusses the history and importance of the field of organofluorine chemistry and outlines some of the principle motivations for the site-selective fluorination of organic molecules. Some of the most commonly useed methods of nucleophilic fluorination are briefly surveyed, with an emphasis on the formation of fluorinated stereogenic centres. Literature precedent for the use of tetrafluoroborates and boron trifluoride as nucleophilic fluorinating agents

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8

Murray, Christopher B. "New methodology for nucleophilic fluorination." Thesis, Durham University, 2003. http://etheses.dur.ac.uk/3687/.

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This work describes the development of three methods for the fluorination of electrophilic substrates:1.) The reaction of caesium fluoride with perfluoro(2-methylpent-2-ene) leads to the formation of perfluoro(2-methylpentan-2-yl)caesium. This perfluoroalkyl carbanion has been shown to undergo significant fluoride ion exchange at temperatures above 60 C. Thus, reaction of a solution of the carbanion with a suitable electrophile resulted in the selective formation of a carbon-fluorine bond or perfluoroalkylation of the electrophile.2.) Caesium fluoride has been developed as a moderately effecti

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9

Kennedy, R. J. "Copper-promoted nucleophilic aromatic substitution." Thesis, University of Kent, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.355148.

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10

Haleem, Asad Bilal. "Crosslinking nucleophilic dyes on cotton." Thesis, University of Leeds, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.250890.

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11

Salim, A. M. "Nucleophilic cleavage of organic disulphides." Thesis, University of Essex, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.381243.

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12

De, Pascale Maria Egizia. "Asymmetric nucleophilic addition to vinylphosphonates." Thesis, King's College London (University of London), 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.407452.

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13

Maji, Biplab. "Reactivity parameters for understanding nucleophilic organocatalysis." Diss., lmu, 2012. http://nbn-resolving.de/urn:nbn:de:bvb:19-148415.

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14

Husein, Maen. "Nucleophilic sulfonation in microemulsions and emulsions." Thesis, McGill University, 2000. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=36814.

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The nucleophilic sulfonation of decyl halides and benzyl halides was carried out at 298.2 K in batches in o/w microemulsions and emulsions formed with the two-tailed cationic surfactants dioctyldimethylammomum chloride, R2(Me)2N +Cl-, or bromide, R2(Me) 2N+Br-. The effects of mixing, surfactant concentration and counterion, and reactant concentrations on the conversion of the halide were investigated. At the concentrations employed, phase separation occurred in most of the samples. Mixing did not affect the sulfonation of decyl halides, while it governed the sulfonation rate of benzyl halides.

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15

Fraser, Georgina. "Ionic liquid effects on nucleophilic substitutions." Thesis, Imperial College London, 2013. http://hdl.handle.net/10044/1/17827.

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In this thesis we demonstrate a fundamental difference between nucleophilic substitution reaction mechanisms in ionic liquids versus conventional solvents. Reported herein are the effects of ionic liquid solvents on substitution reactions between a cationic electrophile and the chloride anion of various organic and inorganic salts. We have combined novel quantitative studies of the nucleophilic source [Cat]Cl with our studies of [C4C1im]Cl and compared their reactivities, k2. For the first time, Eyring activation parameters have been calculated for substitution reactions between charged specie

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16

Annandale, Michael Thomas. "NMR spectroscopic studies of nucleophilic attack on dinitroaniline herbicides, reactions of selected nucleophiles with trifluralin and benefin." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1997. http://www.collectionscanada.ca/obj/s4/f2/dsk2/ftp04/mq22268.pdf.

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17

Tandon, Raman. "Tailor-Made highly nucleophilic pyridines for organocatalysis." Diss., Ludwig-Maximilians-Universität München, 2013. http://nbn-resolving.de/urn:nbn:de:bvb:19-157028.

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18

Nguyen, Huy Van. "Metallocene-Pyrrolidinopyridine Nucleophilic Catalysts for 1.V." Thesis, Queen Mary, University of London, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.498184.

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19

Martin, Peter Arnold. "Nucleophilic substitution reactions of some polyhalogenated compounds." Thesis, Durham University, 1987. http://etheses.dur.ac.uk/6876/.

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Rate measurements for the reactions of a series of polyfluoro - and polychloro - pyridines with aniline and ammonia in 60/40 dioxan/water at 25ºC has shown that chlorine, when ortho and para to the position of attack, is activating with respect to fluorine, but at the position meta to the point of attack, chlorine and fluorine are virtually equivalent in their effect on reaction rate. The trifluoromethyl and nitrile groups were found to be activating relative to fluorine when ortho and para to the position of substitution and the nitrile group was thus found to be ortho/para directing. The ort

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20

Hinch, Melissa Marie. "Catalytic asymmetric nucleophilic epoxidation of aliphatic enones." Thesis, University of Sheffield, 2005. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.425622.

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21

Lau, J. C. Y. "The mechanism of nucleophilic substitution at silicon." Thesis, Open University, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.374491.

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22

Aspinall, Garreth Martyn. "An investigation of nucleophilic cleavage of siloxanes." Thesis, University of Bristol, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.396724.

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23

Lester, Roy P. "Catalytic activation of nitriles towards nucleophilic addition." Thesis, University of Nottingham, 2015. http://eprints.nottingham.ac.uk/28449/.

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The work presented in this thesis is focused on the development of a multifaceted approach to the catalytic activation of nitriles. To develop a versatile method for catalytic nitrile activation two probes were utilised; i) the development of a direct synthesis of allylic amides from the corresponding allylic alcohol and nitrile using a commercial platinum salt, together with a detailed mechanistic investigation into the process, ii) the direct synthesis of 2-bezoxazole from the corresponding 2-aminophenol and nitrile with the aid of a commercial platinum salt as well as the use of alcoholic s

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24

Drees, Paul Frederick. "Secondary Isotope Effects of Nucleophilic Vinylic Substitution." W&M ScholarWorks, 1986. https://scholarworks.wm.edu/etd/1539625350.

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25

Whitmore, James Michael John. "Kinetic studies of nucleophilic displacement at heteroaromatic centres." Thesis, University of Kent, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.386135.

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26

Jones, Craig Warren. "Nucleophilic aromatic substitution using supported copper(I) reagents." Thesis, University of York, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.236184.

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27

Beaumont, Andrew J. "A study of some selective nucleophilic fluorination reactions." Thesis, University of York, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.306248.

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28

Butler, C. "New routes to polyurathene ionomers by nucleophilic substitution." Thesis, Imperial College London, 1987. http://hdl.handle.net/10044/1/38251.

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29

Hepburn, Hamish Bruce. "Enantioselective rhodium-catalysed nucleophilic allylation of cyclic imines." Thesis, University of Edinburgh, 2015. http://hdl.handle.net/1842/17614.

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A highly enantioselective and diastereoselective rhodium-catalysed addition of potassium allyltrifluoroborates to cyclic imines is described within. By utilising rhodium-chiral diene complexes, a wide range of cyclic imines were successfully allylated in high yields and enantioselectivities. Using a variety of more highly substituted allyl reagents, additional stereocentres and further molecular complexity was achieved with good yields, enantioselectivities and diastereoselectivities. Investigations involving isomeric allyl species and deuterated allyl species provided results that gave mechan

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30

Belknap, Ethan M. "Computational Model of the Nucleophilic Acyl Substitution Pathway." Wittenberg University Honors Theses / OhioLINK, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=wuhonors1623251026132848.

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31

Iagrossi, Anna. "Stereochemical studies of reactions of phosphate and thiophosphate esters." Thesis, University of Leicester, 1988. http://hdl.handle.net/2381/33748.

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Nucleophilic substitution reactions involving phosphate monoesters have been investigated. Two general syntheses of O-alkyl or O-aryl [16O,18O] thiophosphate monoesters are reported. An independent and general method for the determination of the enantiomeric excess of isotopically chiral thiophosphate monoesters has been developed and the absolute configurations of the diastereoisomers of (2R)-O-(O-ethyl thiophosphoryl)-3, 4S-dimethyl-5S-phenyl-l,3,2-oxazaphos- pholidin-2-one have been assigned. The solvolysis of p-nitrophenyl [R-16O,18O] thiophosphate in ethanol gives rise to ethyl [16O, 18O]

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32

Duff, Jack Lawrence. "Single electron transfer in nucleophilic reactions of substituted norbornanes." Thesis, Georgia Institute of Technology, 1989. http://hdl.handle.net/1853/27444.

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33

Nguyen, René-Viet 1981. "Catalytic tandem nucleophilic addition for the synthesis of heterocycles." Thesis, McGill University, 2008. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=115708.

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Classical methodologies for carbon-carbon bond formation often require stoichiometric amount of reagent to prefunctionalize a C-H bond. Such methods generate a lot of waste and are therefore not atom-efficient. On the other hand, the use of catalysts for the direct use of C-H bond without prior functionalization is a more desirable approach for carbon-carbon formation. For example, an overall addition reaction is 100% atom economical. This thesis focuses on the catalytic addition of the three types of C-H bonds (Csp-H, Csp2-H and Csp3-H) to unsaturated molecules such as conjugated dienes, imin

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34

McCullagh, John Francis. "Chromatographic studies of nucleophilic substitution in cyano cobalt complexes." Thesis, Queen's University Belfast, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.356946.

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35

Cozens, A. J. "Studies in heterocyclic-mediated nucleophilic displacements in aryl systems." Thesis, University of East Anglia, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.370378.

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36

Drew, S. M. "Photochemical nucleophilic substitution reactions of quinones and related systems." Thesis, University of Leeds, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.374182.

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37

Zhu, Fujiang. "Asymmetric acylation of alcohols by nucleophilic catalysis-synthetic studies." Thesis, University of Sheffield, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.412248.

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38

Garzon, Sanz Miguel. "Developing nucleophilic nitrenoids for the synthesis of complex heterocycles." Thesis, University of Birmingham, 2016. http://etheses.bham.ac.uk//id/eprint/7060/.

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The combination of nucleophilic nitrenoids and gold-catalysis has rapidly emerged as a powerful tool in the assembling of different nitrogen-containing motifs. The research presented in this thesis describes the advances in the field and the exploration of pyrimidium \(N\)-heteroaryl aminides as building blocks in the formation of several fused imidazoheterocycles. From the initial discovery of this reaction and its application in the synthesis of imidazo[1,2-a]pyrimidines, the scope of this convergent gold-catalysed strategy has been adapted to allow the access to fourteen classes of biologic

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39

Davies, Christopher Alan. "A-aryl quaternary centres via asymmetric vicarious nucleophilic substitution." Thesis, Cardiff University, 2005. http://orca.cf.ac.uk/54560/.

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This dissertation first describes a new method for the formation of a-aryl lactams based on the Vicarious Nucleophilic Substitution reaction. The route involves the three-component coupling of a nitroarene, an a-phenylsulfanyl lactam and an electrophile. The process incorporates various electrophiles and various-substituted cyclic amides and has been developed for the most part using nitrobenzene. The process was also applied to a-phenylsulfenyl pyrazolidinones. The process also includes examples of amides possessing a removable nitrogen protecting group to give access to functionalised amides

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40

Maza, Quiroga Ricardo José. "Nucleophilic boryl motifs and alpha-borylcarbanions: reactivity and trends." Doctoral thesis, Universitat Rovira i Virgili, 2021. http://hdl.handle.net/10803/673184.

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En el Capítol 2, coure(I) catalitza la ciclació borilativa de gamma-alquenil aldehids mitjançant una adició quimio- i regioselectiva de Cu-B sobre C=C, seguida d'una reacció intramolecular d'adició de Cu-C sobre C=O. Els productes s'han format amb diastereoselectivitat i un anàlisi computacional ha identificat els punts claus que determinen la quimio- i diastereoselectivitat observada. En el capítol 3, s'estudia la reactivitat dels compostos diborats amb diens 1,3 en un context lliure de metalls de transició. Unicament, l'addició de Na2CO3 sobre bis(pinacolat)diboro, en MeOH, permet la 1,4-hi

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41

Van, der Westhuizen Carl Johan. "Nucleophilic substitution reactions of α-haloketones : a computational study". Diss., University of Pretoria, 2017. http://hdl.handle.net/2263/63346.

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This dissertation describes the computational modelling of reactions between α-haloketones and various nucleophiles. Nucleophilic substitution reactions of α-haloketones (also known as α- halocarbonyls in literature) are utilised in synthetic laboratories to obtain 1,2-disconnections; which are typically difficult to obtain otherwise. To gain insight into these reactions, DFT modelling was carried out in this project, with further understanding into these reactions being obtained using Quantum Fragment Along Reaction Pathway (QFARP) which is an extension of Interacting Quantum Atoms (IQA

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42

Clough, Robert Steven. "The synthesis of aromatic polyethers by aromatic nucleophilic substitution." Case Western Reserve University School of Graduate Studies / OhioLINK, 1993. http://rave.ohiolink.edu/etdc/view?acc_num=case1057072167.

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43

Zhang, Lianhao. "Synthesis of perfluoro[2.2]paracyclophane and its nucleophilic substitutions." [Gainesville, Fla.] : University of Florida, 2009. http://purl.fcla.edu/fcla/etd/UFE0041102.

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44

Sohal, Gian Singh. "Reversible nucleophilic addition : a new approach to asymmetric catalysis." Thesis, University of Bath, 2001. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.341684.

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45

Sawadjoon, Supaporn. "Palladium-Catalyzed Nucleophilic Substitution of Alcohols : Mechanistic Studies and Synthetic Applications." Doctoral thesis, Uppsala universitet, Syntetisk organisk kemi, 2013. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-209541.

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This thesis deals with the palladium-catalyzed nucleophilic substitution of π-activated alcohols in which the C–O bond of a non-manipulated hydroxyl group is cleaved. The thesis is divided in two chapters describing two different catalytic systems. Chapter 2 describes a heterogeneous palladium-catalyzed transfer hydrogenolysis of primary, secondary, and tertiary benzylic alcohols to generate the corresponding aromatic hydrocarbons using formic acid as the hydrogen donor. A detailed mechanistic investigation of this reaction has been conducted that establish the kinetic order of each reaction c

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46

Cid, Torta Jessica. "Nucleophilic versus electrophilic boryl moieties: activation and application in catalysis." Doctoral thesis, Universitat Rovira i Virgili, 2013. http://hdl.handle.net/10803/129289.

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Els compostos de bortrivalent s’han considerat tradicionalment com a àcids de Lewis, preferint acceptar electrons més que donar-los en el curs de les reaccions, peròdarrerament han sorgit exemples a la bibliografia on el compost trivalent de bor presenta una reactivitat insòlita vers posicions electrofíliques. Aquest fet ens suggereix un nou context nucleofílic per als sintonsboril, que pot ser augmentat depenent dels substituents als quals estigui unit el bor. En aquesta tesi, volem mostrar una visió de les reactivitat soposades mitjançantl’estudi teòric de diferents compostos de bortri coord

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47

Balan, Gayatri. "Studies on the nucleophilic substitution reactions of a dimeric cyclopentadienone." Diss., Columbia, Mo. : University of Missouri-Columbia, 2007. http://hdl.handle.net/10355/6265.

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Thesis (M.S.)--University of Missouri-Columbia, 2007.<br>The entire dissertation/thesis text is included in the research.pdf file; the official abstract appears in the short.pdf file (which also appears in the research.pdf); a non-technical general description, or public abstract, appears in the public.pdf file. Title from title screen of research.pdf file (viewed on January 11, 2008) Includes bibliographical references.

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48

Duin, Marcel Adrianus. "Nucleophilic and electrophilic platinum compounds for C-H bond activation." [S.l. : Amsterdam : s.n.] ; Universiteit van Amsterdam [Host], 2004. http://dare.uva.nl/document/75218.

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49

James, Rachel Anne. "Nucleophilic substitution reactions of (alkoxymethylene) dimethylammonium chloride and cyclopropane methodology." Thesis, Imperial College London, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.342180.

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50

Patterson, Richard. "Novel organofluorine chemistry : nucleophilic fluorinating agents and potential anticancer compounds." Thesis, Cardiff University, 2006. http://orca.cf.ac.uk/55525/.

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This thesis covers work investigating the effects of fluorine incorporation on the structure, biological activity, and NMR properties of anticancer chalcones as well as novel methods for the inclusion of fluorinated moieties into organic compounds. The first chapter looks at the use of silanes as carriers of small fluorinated nucleophiles which can be activated by fluoride anion catalysis to deliver such nucleophiles to organic electrophiles such as aldehydes. The synthesis of a group of such silanes and an assessment of their reactivity towards aromatic aldehydes is described. The second and

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