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Journal articles on the topic 'One-pot reactions'

Author: Grafiati

Published: 4 June 2021

Last updated: 26 July 2025

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1

Vaaland, Ingrid Caroline, and Magne Olav Sydnes. "Consecutive Palladium Catalyzed Reactions in One-Pot Reactions." Mini-Reviews in Organic Chemistry 17, no. 5 (2020): 559–69. http://dx.doi.org/10.2174/1570193x16666190716150048.

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Combining palladium catalyzed reactions in one-pot reactions represents an efficient and economical use of catalyst. The Suzuki-Miyaura cross-coupling has been proven to be a reaction which can be combined with other palladium catalyzed reactions in the same pot. This mini-review will highlight some of the latest examples where Suzuki-Miyaura cross-coupling reactions have been combined with other palladium catalyzed reactions in one-pot reaction. Predominantly, examples with homogeneous reaction conditions will be discussed in addition to a few examples from the authors where Pd/C have been us

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2

Wood, Jonathan. "One pot, many reactions." Nano Today 2, no. 6 (2007): 8. http://dx.doi.org/10.1016/s1748-0132(07)70163-9.

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3

Hayashi, Yujiro. "Pot economy and one-pot synthesis." Chemical Science 7, no. 2 (2016): 866–80. http://dx.doi.org/10.1039/c5sc02913a.

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4

Lombardo, Marco, and Claudio Trombini. "ChemInform Abstract: One-Pot Multicomponent Reactions." ChemInform 32, no. 52 (2010): no. http://dx.doi.org/10.1002/chin.200152263.

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5

Kim, Ye Eun, Hyunsung Cho, Yoo Jin Lim, Chorong Kim, and Sang Hyup Lee. "One-Pot Synthesis of Novel Multisubstituted 1-Alkoxyindoles." Molecules 26, no. 5 (2021): 1466. http://dx.doi.org/10.3390/molecules26051466.

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Studies on a one-pot synthesis of novel multisubstituted 1-alkoxyindoles 1 and their mechanistic investigations are presented. The synthesis of 1 was successfully achieved through consecutive four step reactions from substrates 2. The substrates 2, prepared through a two-step synthetic sequence, underwent three consecutive reactions of nitro reduction, intramolecular condensation, and nucleophilic 1,5-addition to provide the intermediates, 1-hydroxyindoles 8, which then were alkylated in situ with alkyl halide to afford the novel target products 1. We optimized the reaction conditions for 1 fo

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6

Ma, Xiaoming, Suzhi Meng, Xiaofeng Zhang, et al. "Synthesis of pyrrolidinedione-fused hexahydropyrrolo[2,1-a]isoquinolines via three-component [3 + 2] cycloaddition followed by one-pot N-allylation and intramolecular Heck reactions." Beilstein Journal of Organic Chemistry 16 (June 4, 2020): 1225–33. http://dx.doi.org/10.3762/bjoc.16.106.

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Two kinds of [3 + 2] cycloaddition intermediates generated from the three-component reactions of 2-bromobenzaldehydes and maleimides with amino esters or amino acids were used for a one-pot N-allylation and intramolecular Heck reactions to form pyrrolidinedione-fused hexahydropyrrolo[2,1-a]isoquinolines. The multicomponent reaction was combined with one-pot reactions to make a synthetic method with good pot, atom and step economy. MeCN was used as a preferable green solvent for the reactions.

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7

Griwatz, Jan H., and Hermann A. Wegner. "One-Pot Synthesis of Cycloparaphenylenes." Organic Materials 02, no. 04 (2020): 306–12. http://dx.doi.org/10.1055/s-0040-1721082.

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The preparation of cycloparaphenylenes ([n]CPPs) with their bent π-system poses a long-standing challenge in organic synthesis. In the current multi-step approaches to access CPPs, pre-angulated precursors were combined using transition metal-catalysed or mediated coupling reactions. Therefore, there is a long way to the realisation of the idea of an ‘ideal synthesis’. An easy and efficient synthesis of different [n]CPPs would represent a breakthrough, also pushing their incorporation into organic materials. By combining multiple steps in a one-pot approach, the overall time and workload can b

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8

Prashant, R. Latthe, R. Kamble Ravindra, and V. Badami Bharati. "Ring transformation reactions of 3-[3/4-acetylphenyl] sydnones; synthesis of oxime, hydrazone and dibromo derivatives of 3-[3/4-acetylphenyl] sydnones and 3-[3/4-acetylphenyl]-5-methyl-[1,3,4]oxadiazolin-2-ones." Journal of Indian Chemical Society Vol. 82, Jul 2005 (2005): 654–58. https://doi.org/10.5281/zenodo.5830564.

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Department of Chemistry, Karnatak University, Dharwad-580 003, India <em>E-mail</em>: bbadami@rediffmail.com Yuvaraja's College, University of Mysore, Mysore-570 005, India <em>Manuscript received 9 June 2004. revised 18 December 2004, accepted 22 March 2005</em> The oximes (3 and 4) and hydrazone (5a,b and 6a,b) derivatives of <em>m/p</em>-acetylphenylsydnones (1 and 2) have been subjected to one-pot ring conversion to the 3-[<em>m</em>/p-acetylphenyl]-5-methyl[1,3,4joxadiazolin-2-ones (7, 8, 9a,b and 10a,b). The ¤, ß unsaturated ketones (11a-h and 12a-h) obtained by the Clai

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9

Doyon, Tyler J., and Alison R. H. Narayan. "Synthetic Utility of One-Pot Chemoenzymatic Reaction Sequences." Synlett 31, no. 03 (2019): 230–36. http://dx.doi.org/10.1055/s-0037-1611848.

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In recent years, there has been a rapid and sustained increase in the development and use of one-pot chemoenzymatic reaction processes for the efficient synthesis of high-value molecules. This strategy can provide a number of advantages over traditional synthetic methods, including high levels of selectivity in reactions, mild and sustainable reaction conditions, and the ability to rapidly build molecular complexity in a single reaction vessel. Here, we present several examples of chemoenzymatic one-pot reaction sequences that demonstrate the diversity of transformations that can be incorporat

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10

Atkinson, M. B. J., S. Oyola-Reynoso, R. E. Luna, D. K. Bwambok, and M. M. Thuo. "Pot-in-pot reactions: a simple and green approach to efficient organic synthesis." RSC Advances 5, no. 1 (2015): 597–607. http://dx.doi.org/10.1039/c4ra13506g.

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11

Thiemann, Thies, Masataka Watanabe, Yasuko Tanaka, and Shuntaro Mataka. "One pot Suzuki coupling - Wittig olefination reactions." Journal of Chemical Research 2004, no. 11 (2004): 723–27. http://dx.doi.org/10.3184/0308234043431609.

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12

Sharghi, Hashem, Mona Hosseini-Sarvari, and Fatemeh Moeini. "Copper-catalyzed one-pot synthesis of benzimidazole derivatives." Canadian Journal of Chemistry 86, no. 11 (2008): 1044–51. http://dx.doi.org/10.1139/v08-153.

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A simple, efficient, and environmentally benign method has been developed for the synthesis of 2-substituted benzimidazoles through a one-pot reaction of phenylenediamines with aryl aldehydes in excellent isolated yields under mild conditions using Cu(II) complex as the selective, recyclable, and heterogeneous catalyst at ambient temperature. The Cu(II) complex as a heterogeneous catalyst can be reused in further catalytic reactions, and it was found that its activity remained largely unchanged for eight successive runs. No metal-complex leaching was observed after the consecutive catalytic re

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13

Hastings, Courtney J., Nicholas P. Adams, Jurgen Bushi, and Samuel J. Kolb. "One-pot chemoenzymatic reactions in water enabled by micellar encapsulation." Green Chemistry 22, no. 18 (2020): 6187–93. http://dx.doi.org/10.1039/d0gc01989e.

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14

Siva Prasad, Aviraboina, and Talupula Venkateswara Rao. "STREAMLINED SYNTHESIS: ENHANCING THE LEIMGRUBER-BATCHO INDOLE ROUTE FOR ONE-POT TANDEM PRODUCTION OF 2,3-UNSUBSTITUTED INDOLES." International Journal of Advanced Research 12, no. 02 (2024): 528–32. http://dx.doi.org/10.21474/ijar01/18325.

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Aim:This study aims to create a new one-pot synthesis method for substituted indoles, focusing on efficiency, by-product reduction, and comparative advantages over conventional Leimgruber-Batcho reactions. Methods:Researchers optimized a one-pot synthesis strategy for maximum yield, reduced by-products, and resource utilization, comparing it to traditional Leimgruber-Batcho reactions, ensuring a sustainable, environmentally friendly approach. Results:The one-pot synthesis method efficiently produced substituted indoles with reduced environmental impact, yielding more than conventional reaction

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15

Marinho, Elina. "One-Pot Reactions of Triethyl Orthoformate with Amines." Reactions 4, no. 4 (2023): 779–800. http://dx.doi.org/10.3390/reactions4040045.

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One-pot reactions offer advantages like easy automation, higher product yields, minimal waste generation, operational simplicity, and thus reduced cost, time and energy. This review presents a comprehensive overview of one-pot reactions including triethyl orthoformate and amines as valuable and efficient reagents for carrying out two-, three- or four-component organic reactions.

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16

Tabatabaeian, Khalil, Mohammad Ali Zanjanchi, Manouchehr Mamaghani, and Ali Dadashi. "Ultrasonic-assisted ruthenium-catalyzed one-pot synthesis of biscoumarins." JOURNAL OF ADVANCES IN CHEMISTRY 11, no. 2 (2016): 3532–39. http://dx.doi.org/10.24297/jac.v11i2.2219.

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The Ru-grafted zeolite beta was found to be an excellent heterogeneous catalyst for one-pot synthesis of biscoumarins. This reaction was carried out under reflux condition and ultrasonic irradiation. On the other hand, the catalyst could be recovered for the subsequent reactions and reused without appreciable loss of activity.

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17

Hong, Wan Pyo, Inji Shin, and Hee Nam Lim. "Recent Advances in One-Pot Modular Synthesis of 2-Quinolones." Molecules 25, no. 22 (2020): 5450. http://dx.doi.org/10.3390/molecules25225450.

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It is known that 2-quinolones are broadly applicable chemical structures in medicinal and agrochemical research as well as various functional materials. A number of current publications about their synthesis and their applications emphasize the importance of these small molecules. The early synthetic chemistry originated from the same principle of the classical Friedländer and Knorr procedures for the preparation of quinolines. The analogous processes were developed by applying new synthetic tools such as novel catalysts, the microwave irradiation method, etc., whereas recent innovations in ne

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18

Boddapati, S. N. Murthy, Ramana Tamminana, Ravi Kumar Gollapudi, et al. "Copper-Promoted One-Pot Approach: Synthesis of Benzimidazoles." Molecules 25, no. 8 (2020): 1788. http://dx.doi.org/10.3390/molecules25081788.

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A facile, one-pot, and proficient method was developed for the production of various 2-arylaminobenzimidazoles. This methodology is based for the first time on a copper catalyst promoted domino C–N cross-coupling reaction for the generation of 2-arylaminobenzimidazoles. Mechanistic investigations revealed that the synthetic pathway involves a copper-based desulphurization/nucleophilic substitution and a subsequent domino intra and intermolecular C–N cross-coupling reactions. Some of the issues typically encountered during the synthesis of 2-arylaminobezimidazoles, including the use of expensiv

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19

Sydnes, Magne. "One-Pot Reactions: A Step Towards Greener Chemistry." Current Green Chemistry 1, no. 3 (2014): 216–26. http://dx.doi.org/10.2174/2213346101666140221225404.

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20

Dinica, Rodica, Bianca Furdui, Geta Cârâc, and Constantin Stanciu. "Fluorescent N-Heterocycles via One-Pot Tandem Reactions." Chemistry Journal of Moldova 4, no. 2 (2009): 82–85. http://dx.doi.org/10.19261/cjm.2009.04(2).06.

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Substituted indolizines are very attractive heterocyclic units. On developing efficient methods toward differently substituted indolizines, we were particularly interested in elaborating efficient approaches toward three-component reaction of these compounds which are very interested from the point of view fluorescent properties. The microwave-mediated three component reaction of acyl bromide, bipyridine and dipolarophyl is catalyzed by basic alumina to give corresponding bis-indolizines in excellent yields in a one –pot reaction.

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21

Hall, N. "Chemists Clean Up Synthesis With One-Pot Reactions." Science 266, no. 5182 (1994): 32–34. http://dx.doi.org/10.1126/science.266.5182.32.

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22

Hoelderich, Wolfgang F. "‘One-pot’ reactions: a contribution to environmental protection." Applied Catalysis A: General 194-195 (March 2000): 487–96. http://dx.doi.org/10.1016/s0926-860x(99)00395-6.

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23

Brooks, David W., Dianne Epp, and Helen B. Brooks. "Small-Scale Potentiometry and Silver One-Pot Reactions." Journal of Chemical Education 72, no. 8 (1995): A162. http://dx.doi.org/10.1021/ed072pa162.

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24

Wang, Wengui, and Marvin Yu. "One-pot sequential Baylis–Hillman and Michael reactions." Tetrahedron Letters 45, no. 38 (2004): 7141–43. http://dx.doi.org/10.1016/j.tetlet.2004.07.122.

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25

Tsogoeva, Svetlana B. "Catalytic multi-step domino and one-pot reactions." Beilstein Journal of Organic Chemistry 20 (February 8, 2024): 254–56. http://dx.doi.org/10.3762/bjoc.20.25.

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26

Winz, Marie-Luise, Eva Christina Linder, Juliane Becker, and Andres Jäschke. "Site-specific one-pot triple click labeling for DNA and RNA." Chemical Communications 54, no. 83 (2018): 11781–84. http://dx.doi.org/10.1039/c8cc04520h.

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We report site-specific triple click labeling for DNA and RNA in a one-pot setup by performing inverse electron demand Diels–Alder reaction and strain-promoted and copper catalyzed click reactions sequentially.

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27

Jeyachandran, Rajkumar, Harish Kumar Potukuchi, and Lutz Ackermann. "Copper-catalyzed CuAAC/intramolecular C–H arylation sequence: Synthesis of annulated 1,2,3-triazoles." Beilstein Journal of Organic Chemistry 8 (October 16, 2012): 1771–77. http://dx.doi.org/10.3762/bjoc.8.202.

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Step-economical syntheses of annulated 1,2,3-triazoles were accomplished through copper-catalyzed intramolecular direct arylations in sustainable one-pot reactions. Thus, catalyzed cascade reactions involving [3 + 2]-azide–alkyne cycloadditions (CuAAC) and C–H bond functionalizations provided direct access to fully substituted 1,2,3-triazoles with excellent chemo- and regioselectivities. Likewise, the optimized catalytic system proved applicable to the direct preparation of 1,2-diarylated azoles through a one-pot C–H/N–H arylation reaction.

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28

Gupta, Pradeep Kumar, Kumaran Ganesan, Ambuja Pande, and Ramesh Chandra Malhotra. "A convenient one pot synthesis of fentanyl." Journal of Chemical Research 2005, no. 7 (2005): 452–53. http://dx.doi.org/10.3184/030823405774309078.

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29

Klein, Andreas Sebastian, Anna Christina Albrecht, and Jörg Pietruszka. "Chemoenzymatic One-Pot Process for the Synthesis of Tetrahydroisoquinolines." Catalysts 11, no. 11 (2021): 1389. http://dx.doi.org/10.3390/catal11111389.

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1,2,3,4-Tetrahydroisoquinolines form a valuable scaffold for a variety of bioactive secondary metabolites and commercial pharmaceuticals. Due to the harsh or complex conditions of the conventional chemical synthesis of this molecular motif, alternative mild reaction pathways are in demand. Here we present an easy-to-operate chemoenzymatic one-pot process for the synthesis of tetrahydroisoquinolines starting from benzylic alcohols and an amino alcohol. We initially demonstrate the oxidation of 12 benzylic alcohols by a laccase/TEMPO system to the corresponding aldehydes, which are subsequently

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30

Li, Li-Jun, Ying-Xia Song, Yan-Su Gao, Yan-Feng Li, and Jian-Feng Zhang. "Solvent-free Synthesis of Nitriles from Aldehydes Catalyzed by KF/Al2O3, Montmorillonite KSF and K10." E-Journal of Chemistry 3, no. 3 (2006): 164–68. http://dx.doi.org/10.1155/2006/709594.

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Multistep and one-pot conversion of aldehydes to nitriles were carried out conveniently with out solvent using KF/Al2O3, montmorillonite KSF and K10 as catalyst, under microwave irradiation. The reactions are completed within 6-8 min to give satisfactory yields. KF/Al2O3was more effective catalyst both in multistep procedure and one-pot reaction.

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31

Niu, Jiawei, Yuhui Wang, Shenghu Yan, et al. "One-pot Ugi-azide and Heck reactions for the synthesis of heterocyclic systems containing tetrazole and 1,2,3,4-tetrahydroisoquinoline." Beilstein Journal of Organic Chemistry 20 (April 23, 2024): 912–20. http://dx.doi.org/10.3762/bjoc.20.81.

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A new method for the synthesis of heterocyclic systems containing tetrazole and tetrahydroisoquinoline is developed via the performance of one-pot Ugi-azide and Heck cyclization reactions. The integration of the multicomponent and post-condensation reactions in one-pot maximizes the pot-, atom-, and step-economy (PASE).

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32

Sachinta, Mahato, and Majee Adinath. "Mild, efficient and diastereoselective one-pot synthesis of substituted oxazolidine under neat conditions." Journal of Indian Chemical Society Vol. 97, No. 12c, Dec 2020 (2020): 2867–73. https://doi.org/10.5281/zenodo.5654556.

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Department of Chemistry, Visva-Bharati (A Central University), Santiniketan-731 235, West Bengal, India <em>E-mail:</em> adinath.majee@visva-bharati.ac.in <em>Manuscript received online 05 December 2020, revised and accepted 26 December 2020</em> A diastereoselective synthesis of substituted oxazolidine systems by one-pot reaction of aromatic aldehydes with L-proline followed by catalyst-free, solvent-free, 1,3-dipolar cycloaddition reactions via non-stabilized azomethine intermediate. The reaction of aldehydes and amino acids produces the azomethine intermediate. NMR spectroscopy as well as s

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33

Zomordbakhsh, Shahab, Hossein Anaraki-Ardakani, Mohsen Zeeb, Mahdi Sadeghi, and Manouchehr Mazraeh-Seffid. "Microwave-Assisted, Solvent-Free, Three-Component Synthesis of 2,4,6-Triarylpyridines from Benign Components." Journal of Chemical Research 36, no. 3 (2012): 138–40. http://dx.doi.org/10.3184/174751912x13295721847185.

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2,4,6-Triarylpyridine derivatives were synthesised by the reaction of guanidine with an acetophenone and a chalcone. These reactions were carried out as economical one-pot reactions under green conditions: no catalyst and solvent free.

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34

Vuong, Hien, Samantha Duarte, and Douglas A. Klumpp. "One-Pot Reactions Involving the Fischer Indole Synthesis and Friedel–Crafts Reactions." Topics in Catalysis 61, no. 7-8 (2018): 685–88. http://dx.doi.org/10.1007/s11244-018-0908-3.

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35

C., A. M. A. Huq, and Sivakumar S. "One-pot synthesis of novel heterocyclic compounds via tandem reactions." Journal of Indian Chemical Society Vol. 91, Feb 2014 (2014): 313–17. https://doi.org/10.5281/zenodo.5749168.

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Post Graduate and Research Department of Chemistry, The New College, Affiliated to the University of Madras, Chennai-600 014, India <em>E-mail</em> : drmdabdulhuq@yahoo.com <em>Manuscript received 19 September 2012, revised 04 February 2013, accepted 07 May 2013</em> Novel heterocyclic compounds (2), (4) and (6) have been prepared by a tandem oxy-Cope rearrangement/S<sub>N</sub> displacement reaction, a tandem dianionic oxy-Cope rearrangement/nucleophilic substitution at carbonyl carbon and a tandem anionic oxy-Cope rearrangement/transannular reaction respectively. The oxy-Cope rearrangement i

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36

Jeong, Hye Jin, Suyeon Chae, Keunhong Jeong, and Sung Keon Namgoong. "Diverse One-Pot Electrophilic Trapping Reactions of 2-Quinolylzincates with Acyl Chlorides and Allyl Iodide." Synthesis 52, no. 03 (2019): 378–92. http://dx.doi.org/10.1055/s-0039-1690036.

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The tandem acylation reactions of 2-quinolylzincates under one-pot reaction conditions facilitated the formation of biologically active (Z)-3-alkylidenephthalides and multifunctionalized quinoline derivatives at specific positions. The reactions of these zincates with allyl iodide produced three different types of temperature- and alkyl-ligand-dependent C-2 homologated quinolines. The reaction mechanisms for the formation of the presented products from 2-quinolylzincates are also proposed in detail.

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37

Pirouz, Maryam, M. Saeed Abaee, Pernille Harris, and Mohammad M. Mojtahedi. "One-pot synthesis of benzofurans via heteroannulation of benzoquinones." Heterocyclic Communications 27, no. 1 (2021): 24–31. http://dx.doi.org/10.1515/hc-2020-0120.

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Abstract Three different reactions were explored leading to the synthesis of various benzofurans. All reactions took place under AcOH catalysis in a one-pot manner. As a result, benzoquinone derivatives underwent heteroannulation with either itself or cyclohexanones to produce furanylidene-benzofuran or benzofuran structures, respectively.

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38

Zulfiqar, Fazila, and Tomoya Kitazume. "One-pot aza-Diels–Alder reactions in ionic liquids." Green Chemistry 2, no. 4 (2000): 137–39. http://dx.doi.org/10.1039/b002671i.

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39

Snieckus, V., M. Alessi, A. Larkin, et al. "One-Pot Directed Metallation-Coupling Reactions of Pyridine Derivatives." Synfacts 2007, no. 5 (2007): 0525. http://dx.doi.org/10.1055/s-2007-968428.

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40

Handy, Scott. "One-Pot Halogenation-Heck Coupling Reactions in Ionic Liquids." Synlett 2006, no. 18 (2006): 3176–78. http://dx.doi.org/10.1055/s-2006-948192.

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41

Andrei, Radu Dorin, Marcel Ionel Popa, François Fajula, et al. "Ethylene to Propylene by One-Pot Catalytic Cascade Reactions." ACS Catalysis 5, no. 5 (2015): 2774–77. http://dx.doi.org/10.1021/acscatal.5b00383.

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42

Ghosh, Sunil K., Usha Singh, and Vasant R. Mamdapur. "One pot amide/ peptide synthesis via two redox reactions." Tetrahedron Letters 33, no. 6 (1992): 805–8. http://dx.doi.org/10.1016/s0040-4039(00)77720-3.

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43

Lai, Jiun-Ting, Pei-Shan Shieh, Wei-Hao Huang, and Ding-Yah Yang. "Syntheses of Oxazabicycle Library via One-Pot Tandem Reactions." Journal of Combinatorial Chemistry 10, no. 3 (2008): 381–86. http://dx.doi.org/10.1021/cc8000025.

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44

Fleischer, Ivana, and Samuel Quintero-Duque. "Tandem and One-Pot Hydroformylation/Michael Reactions of Acrylates." Synthesis 49, no. 04 (2017): 925–32. http://dx.doi.org/10.1055/s-0036-1588394.

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45

Chou, Ta Shue, Hsi Hwa Tso, and Lung Ching Lin. "One-pot sequential acylation/alkylation reactions of 3-sulfolenes." Journal of Organic Chemistry 51, no. 7 (1986): 1000–1002. http://dx.doi.org/10.1021/jo00357a009.

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46

Kamble, Vinod T., Bhaskar S. Davane, Sanjay A. Chavan, Dnyanoba B. Muley, and Sandeep T. Atkore. "Imino Diels–Alder reactions: One-pot synthesis of tetrahydroquinolines." Chinese Chemical Letters 21, no. 3 (2010): 265–68. http://dx.doi.org/10.1016/j.cclet.2009.11.016.

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47

Wang, Jun-Liang, Xiao-Yang Chen, Qi Wu, and Xian-Fu Lin. "One-Pot Synthesis of Spirooxazino DerivativesviaEnzyme- Initiated Multicomponent Reactions." Advanced Synthesis & Catalysis 356, no. 5 (2014): 999–1005. http://dx.doi.org/10.1002/adsc.201300965.

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48

Tang, Christina, and Bridget T. McInnes. "Cascade Processes with Micellar Reaction Media: Recent Advances and Future Directions." Molecules 27, no. 17 (2022): 5611. http://dx.doi.org/10.3390/molecules27175611.

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Reducing the use of solvents is an important aim of green chemistry. Using micelles self-assembled from amphiphilic molecules dispersed in water (considered a green solvent) has facilitated reactions of organic compounds. When performing reactions in micelles, the hydrophobic effect can considerably accelerate apparent reaction rates, as well as enhance selectivity. Here, we review micellar reaction media and their potential role in sustainable chemical production. The focus of this review is applications of engineered amphiphilic systems for reactions (surface-active ionic liquids, designer s

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49

Xiong, Jun, Qi-Xun Feng, Zhi-Ying Mu, et al. "Efficient Synthesis of 4H-3,1-Benzoxazine Derivatives via One-Pot Sequential Passerini-Azide/Palladium-Catalyzed Azide–Isocyanide Coupling/Cyclization Reaction." Synlett 31, no. 10 (2020): 1003–6. http://dx.doi.org/10.1055/s-0039-1690831.

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A new, one-pot method for the synthesis of 4H-3,1-benzoxazine derivatives has been developed. The Passerini-azide reactions of 2-azidobenzaldehydes, trimethylsilyl azide, and isocyanides produced azide intermediate without separation, which then reacted with isocyanides to give 4H-3,1-benzoxazine derivatives via a tandem one-pot palladium-catalyzed azide–isocyanide coupling/cyclization reaction in moderate to good yields.

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Akkarasamiyo, Sunisa, Somsak Ruchirawat, Poonsaksi Ploypradith та Joseph S. M. Samec. "Transition-Metal-Catalyzed Suzuki–Miyaura-Type Cross-Coupling Reactions of π-Activated Alcohols". Synthesis 52, № 05 (2020): 645–59. http://dx.doi.org/10.1055/s-0039-1690740.

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Abstract:

The Suzuki–Miyaura reaction is one of the most powerful tools for the formation of carbon–carbon bonds in organic synthesis. The utilization of alcohols in this powerful reaction is a challenging task. This short review covers progress in the transition-metal-catalyzed Suzuki–Miyaura-type cross-coupling reaction of π-activated alcohol, such as aryl, benzylic, allylic, propargylic and allenic alcohols, between 2000 and June 2019.1 Introduction2 Suzuki–Miyaura Cross-Coupling Reactions of Aryl Alcohols2.1 One-Pot Reactions with Pre-activation of the C–O Bond2.1.1 Palladium Catalysis2.1.2 Nickel

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