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Dissertations / Theses on the topic 'Organometallic compounds – Synthesis'

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Published: 4 June 2021

Last updated: 30 January 2023

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1

Lawrence, Heather Bunting Elizabeth. "Organometallic compounds with non-linear optical properties." Thesis, University of Oxford, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.276835.

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2

Callahan, Ryan Patrick. "The synthesis of perfluorinated compounds by direct fluorination organometallic compounds and carboranes /." Access restricted to users with UT Austin EID Full text (PDF) from UMI/Dissertation Abstracts International, 2001. http://wwwlib.umi.com/cr/utexas/fullcit?p3036160.

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3

Frazier, Joy Faith. "Organo-iridium compounds : synthesis, characterization and reactivity /." Thesis, This resource online, 1991. http://scholar.lib.vt.edu/theses/available/etd-08222009-040309/.

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4

Wallner, Olov. "Palladium-Catalyzed Synthesis and Transformations of Organometallic Compounds." Doctoral thesis, Stockholm : Dept. of Organic Chemistry, Stockholm University, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-804.

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5

Cloete, Jezreel. "Synthesis and applications of functionalized pyridinyl imine complexes of palladium." Thesis, University of the Western Cape, 2005. http://etd.uwc.ac.za/index.php?module=etd&amp.

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The synthesis and characterization of pyridinyl &alpha<br>-diimine Pd(II) complexes having a functionalized hydrocarbon attached to the imino nitrogen was performed. The catalytic activity of these complexes were then evaluated in the polymerization of ethylene and in the Heck coupling reaction of methyl acrylate with iodobenzene.<br /> <br /> Unconjugated &beta<br>-diimine complexes of palladium were also synthesized and their activities towards ethylene polymerization and the Heck coupling of methyl acrylate and iodobenzene also evaluated and compared to that of the &alpha<br>-diimine comple

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6

Hart, Suzanne L. "Synthesis and applications of chiral-at-titanium organometallic compounds." Thesis, University of Warwick, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.245941.

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7

Kou, Xiaodi. "Synthesis, characterization and reactivity of organic bismuth compounds." Fort Worth, Tex. : Texas Christian University, 2007. http://etd.tcu.edu/etdfiles/available/etd-07312007-125631/unrestricted/kou.pdf.

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8

Choi, Ka Ho. "Synthesis, characterization and properties of luminescent rigid-rod organometallic acetylide materials." HKBU Institutional Repository, 2001. http://repository.hkbu.edu.hk/etd_ra/360.

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9

Peatt, Anna C. (Anna Clare-Doreen) 1976. "New reaction media for organometallic chemistry." Monash University, School of Chemistry, 2003. http://arrow.monash.edu.au/hdl/1959.1/5829.

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10

Mock, Michael T. "Synthesis and reactivity of thioether-supported organoiron and low-valent iron complexes and cyanide-bridged binuclear complexes." Access to citation, abstract and download form provided by ProQuest Information and Learning Company; downloadable PDF file, 282 p, 2008. http://proquest.umi.com/pqdweb?did=1481668291&sid=19&Fmt=2&clientId=8331&RQT=309&VName=PQD.

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11

Kui, Chi-fai, and 居智輝. "Non-covalent weak interactions in group IV, PT(II) and AU(I) organometallic complexes: synthesis,structures and properties." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2005. http://hub.hku.hk/bib/B32021331.

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12

Pearson, Mark. "Organometallic reagents for catalytic cross-coupling." Thesis, University of Oxford, 1992. http://ora.ox.ac.uk/objects/uuid:c5eea9a0-8f0c-46bf-a1ea-28a40b79546d.

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Phosphine complexes of nickel and palladium provide the best catalysts for the homogeneous catalysed carbon-carbon bond forming reaction between an organometallic nucleophile and an organic electrophile. Use of a homochiral ligand on the catalyst can lead to stereoselectivity in the cross-coupling reaction, with high ee's of coupled product being obtained. The processes of selectivity in the transmetalation step of the catalytic cycle have not been elucidated and the initial aim of the project was to study these processes. Initial experiments using organotin derivatives as the organometallic n

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13

Bunge, Scott Daniel. "The molecular design of metal amides." Diss., Georgia Institute of Technology, 2001. http://hdl.handle.net/1853/30990.

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14

Ortu, Fabrizio. "Synthesis of s-block complexes supported by sterically demanding N-based ligands." Thesis, University of Nottingham, 2013. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.713701.

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Despite the well-established tradition of organomagnesium reagents, lit-tIe attention was given to the heavier congeners, until very recently. Since the 1990s, researchers have intensified their efforts in the quest for sterically demanding ligand frameworks capable of preventing classic decomposition re› actions of Ae organometallics. Sterically demanding N -donors have become increasingly popular owing to their ability (i) to provide stable metal-donor interactions and (ii) to achieve kinetic stabilisation of the complex via steric crowding around the metal centre. This has led to reports wh

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15

Stolberg, Tonie Louis. "Synthesis and properties of bidentate coordination compounds of tin." Thesis, University of Oxford, 1991. http://ora.ox.ac.uk/objects/uuid:ff861007-1ff0-470e-8554-86749bc291a1.

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This Thesis describes the synthesis, structural characterization and properties of some tin(II) and tin(IV) compounds containing bidentate ligands. Chapter 1 describes the main spectroscopic techniques used in the identification of tin(II) compounds; infra-red, <sup>119</sup>Sn Mössbauer and n.m.r spectroscopy are outlined, and relevant examples given. A comprehensive listing is given of the main spectroscopic and structural properties of known tin(]3) compounds. Chapter 2 describes the general synthetic methods employed for the formation of tin(II)-oxygen heterocyclic compounds. A range of ca

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16

Joshi, Kiran. "Synthesis, characterisation and reactivity of phosphide and methylidene complexes of iridium." Thesis, University of British Columbia, 1990. http://hdl.handle.net/2429/30661.

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The iridium(III) methyl diarylphosphide complexes, Ir(CH₃PR₂-[N(SiMe₂CH₂PPh₂)₂] (2a: R = phenyl, 2b: R = meta-tolyl) had been prepared previous to this work. The iridium(III) dimethylphosphide complex, Ir(CH₃)PMe₂-[N(SiMe₂CH₂PPh₂)₂], 2c, is readily prepared in situ by transmetallation of the Ir(CH₃)I[N(SiMe₂CH₂PPh₂)₂] with KPMe₂ at -30°C. The synthesis of the phenylphosphide complex Ir(CH₃)PHPh[N(SiMe₂CH₂PPh₂)₂], 2d, involves deprotonation of the six-coordinate iridium(III) phenylphosphine complex, Ir(CH₃)I-(PH₂Ph)[N(SiMe₂CH₂PPh₂)₂], with KO¹Bu. Thermolysis of 2a and 2b yields the six-coordin

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17

Low, Kam-hung, and 魯錦鴻. "Synthesis, structural characterization and applications of homoleptic organosulfur and organoselenium metal polymers." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2009. http://hub.hku.hk/bib/B43703859.

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18

黃維揚 and Wai-yeung Wong. "The chemistry of triosmium alkylidyne carbonyl clusters." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1995. http://hub.hku.hk/bib/B31234537.

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19

Brassington, David Steven. "Synthesis and characterisation of organometallic compounds of B, Mn and Re." Thesis, Bangor University, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.273666.

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20

Nozari, Ali-Reza. "Synthesis and characterisation of organometallic and organic compounds towards novel applications." Thesis, University of Cambridge, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.615960.

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21

Pang, Ka Chuen. "Hydrothermal synthesis of chiral metal-organic frameworks and photo-chromic materials /." View abstract or full-text, 2009. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202009%20PANG.

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22

Saleh, Liban Mohamoud Ali. "Rare earth metal boryl and gallyl compounds : synthesis and reactivity." Thesis, University of Oxford, 2014. http://ora.ox.ac.uk/objects/uuid:b511fe23-8b79-47b5-9ac6-dcfd52c58239.

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This Thesis describes the syntheses, characterisation and reactivity of rare earth metal boryl and gallyl compounds. Experimental and computational studies were performed to investigate the structure and bonding in these compounds. <b>Chapter 1</b> introduces key metal-boryl and metal-gallyl compounds of the s, p, d and f-blocks via literature review. <b>Chapter 2</b> describes the syntheses, structures and bonding analyses of rare earth metal boryl compounds. A short introduction to rare earth metal cations is given. Chapter 3</b> describes the syntheses, structures and bonding analyses of ra

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23

Gitlits, Alexander 1975. "Synthesis and structural survey of novel rare earth aryloxide and pyrazolate complexes." Monash University, Dept. of Chemistry, 2001. http://arrow.monash.edu.au/hdl/1959.1/8996.

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24

Low, Kam-hung. "Synthesis, structural characterization and applications of homoleptic organosulfur and organoselenium metal polymers." Click to view the E-thesis via HKUTO, 2009. http://sunzi.lib.hku.hk/hkuto/record/B43703859.

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25

Phelps, Jennifer. "Synthesis of homoleptic PT(0) acceptor phosphine complexes." Laramie, Wyo. : University of Wyoming, 2008. http://proquest.umi.com/pqdweb?did=1594481221&sid=1&Fmt=2&clientId=18949&RQT=309&VName=PQD.

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26

Wong, Ka-Leung. "Synthesis, characterization, and photophysical studies of organic-lanthanide complexes." Click to view the E-thesis via HKUTO, 2006. http://sunzi.lib.hku.hk/hkuto/record/B36875351.

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27

Poon, Suk Yue. "Synthesis, characterization and photophysics of alkynyl-derived inorganic and organometallic materials comprising group 13,14 and 16 elements." HKBU Institutional Repository, 2005. http://repository.hkbu.edu.hk/etd_ra/662.

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28

李詠文 and Wing-man Lee. "Synthesis, photophysics and photochemistry of mono- and polynuclear complexes of Ruthenium (II) containing crown ether pendants, redoxactive moieties, and organometallic fragments." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1996. http://hub.hku.hk/bib/B31234975.

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29

Abdalhadi, Saifaldeen Muwafag. "Synthesis and study of new organic and organometallic compounds with photovoltaic applications." Thesis, University of Glasgow, 2017. http://theses.gla.ac.uk/8365/.

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This thesis describes the synthesis and characterisation of novel organic and organometallic materials with potential optoelectronic application. Chapter one provides a general introduction about the different types of solar cells and an overview of the working principle of two types of solar cells, DSSCs and BHJs, including examples of some molecular designs of the best performing dyes. Chapter two describes the successful synthesis and characterization of two organometallic molecules based on the porphyrin moiety (PorTh and PorFu). These dyes were employed to fabricate DSSCs devices, reporti

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30

Cordiner, Richard L. "Synthesis, structure and electrochemistry of organometallic compounds bearing C(_n)N ligands." Thesis, Durham University, 2005. http://etheses.dur.ac.uk/3007/.

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In this thesis, the synthesis of the organic cyanoacetylenes NCC≡CC(_6)H(_5) and NCC≡CC(_6)H(_4)-4-NMc(_2) and the metal cyanoacetylides Ru(C≡CC≡N)(PPh(_3))(_2)Cp, Ru(C≡CC≡N)(dppe)Cp* and Fe(C≡CC≡N)(dppe)Cp is presented and their coordination chemistry is explored. The structure and electrochemical behaviour of these novel cyano-carbon complexes is investigated and spectro-electrochemical methods are used to investigate the electronic structure of the cyanoacetylide compounds. In addition, in order to gain a greater understanding of the metal/ligand bonding interaction in these systems, the sy

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31

Kui, Chi-fai. "Non-covalent weak interactions in group IV, PT(II) and AU(I) organometallic complexes synthesis, structures and properties /." Click to view the E-thesis via HKUTO, 2005. http://sunzi.lib.hku.hk/hkuto/record/B32021331.

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32

Leech, Matthew Christopher. "Transition metal cyaphides : synthesis, reactivity, and electrochemistry." Thesis, University of Sussex, 2019. http://sro.sussex.ac.uk/id/eprint/82053/.

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33

McBurnett, Brian Gordon. "Synthesis, structure, and reactivity of some heavier main group compounds /." Digital version accessible at:, 1998. http://wwwlib.umi.com/cr/utexas/main.

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34

Lev, Daniel Abraham. "Group 8 and 9 half sandwich complexes of N-heterocyclic phosphines : synthesis, reactivity, and catalysis /." Diss., Connect to a 24 p. preview or request complete full text in PDF format. Access restricted to UC campuses, 2004. http://wwwlib.umi.com/cr/ucsd/fullcit?p3158465.

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35

Wong, Ka-Leung, and 黃嘉良. "Synthesis, characterization, and photophysical studies of organic-lanthanide complexes." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2006. http://hub.hku.hk/bib/B36875351.

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36

Mapolie, Selwyn Frank. "The synthesis and reactivity of binuclear μ-hydrocarbyl complexes of some transition metals". Doctoral thesis, University of Cape Town, 1988. http://hdl.handle.net/11427/22208.

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The new μ-(l,n)-alkanediyl compounds [(ƞ⁵-C₅R₄Me)Fe(CO)₂ ]₂{μ-(CH₂)n}, (R = H, n = 3 -10 and R =Me, n =3 - 6), [Mn(CO)₅]₂{μ-(CH₂)n} (M = Mn, n = 4-6 and M = Re, n= 3 and 4) have been prepared using essentially two synthetic routes. Thus the iron compounds were synthesized by the reaction of Na[(ƞ⁵-C₅R₄Me)Fe(CO)₂ ] with the appropriate dibromoalkane. The manganese and rhenium compounds on the other hand, were prepared by the decarbonylation of the corresponding diacyl compounds of the type, [M(CO)₅]₂{μ-CO(CH₂)nCO} (M = Mn or Re). These diacyl species in turn were synthesized by the reaction of

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37

林立基 and Lap-kay Wilson Lam. "Organometallic reactions involving long chain fatty acid esters." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1987. http://hub.hku.hk/bib/B31231196.

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38

Xiao, Jiajia. "Study of factors affecting the synthesis of carbon nanotubes by spray pyrolysis." To access this resource online via ProQuest Dissertations and Theses @ UTEP, 2007. http://0-proquest.umi.com.lib.utep.edu/login?COPT=REJTPTU0YmImSU5UPTAmVkVSPTI=&clientId=2515.

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39

Bradley, Mark. "The synthesis of alkaline earth complexes using sterically-demanding multidentate amido ligands." Thesis, University of Nottingham, 2014. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.718678.

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Despite the well-established use of organomagnesium reagents, research into the chemistry of the alkaline earth metals has received an increase in popularity over the last two decades, largely due to their applications as reagents and catalysts. Recently, sterically-demanding A-donor ligands have become more popular because of their ability to provide stable metal-donor interactions and achieve kinetic stabilisation of the complex by crowding the metal centre. Furthermore, the isolation of subvalent magnesium and calcium complexes which challenged established knowledge of the metals prompted f

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40

Schauer, Philip A. "Organometallic synthons for highly conjugated redox-active materials." University of Western Australia. School of Biomedical, Biomolecular and Chemical Sciences, 2009. http://theses.library.uwa.edu.au/adt-WU2009.0166.

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[Truncated abstract] This thesis describes various synthetic approaches toward the synthesis of highly conjugated complexes incorporating multiple transition metal centres. Particular attention is given to the synthesis of mononuclear complexes that allow for the facile assembly of discrete oligo- and poly-nuclear complexes in a controlled, stepwise fashion. Conjugated multi-metallic materials are of interest on account of their unique photophysical and electronic properties, with a particular emphasis on elucidating the nature of intramolecular communication between multiple metal centres. Ch

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41

Hallam, Malcolm Francis. "Synthetic and spectroscopic studies on heterometallic clusters of platinum." Thesis, University of Oxford, 1986. http://ora.ox.ac.uk/objects/uuid:a74b7c1b-4201-46cf-89aa-92d3f7160a9a.

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This Thesis describes the synthesis and structural characterisation of a range of heterometallic cluster compounds of platinum. Chapter 1 reviews the current knowledge in this area and gives examples of the kinds of cluster compounds which have been characterised, with some emphasis on their mode of synthesis and their structural and spectroscopic characterisation. The structures of the cluster compounds are rationalised in terms of the triangular Pt<sub>3</sub> unit which dominates the cluster chemistry of platinum. The bonding in the simplest triplatinum cluster compounds is analysed and is

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42

Moreno, Debra Ann. "Design, synthesis, and characterization of monomeric group 2 element Bis(alkoxide) compounds ; Part II, Synthesis and characterization of some group 2 element imidophosphonate compounds." Diss., Georgia Institute of Technology, 1997. http://hdl.handle.net/1853/30267.

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43

Lee, Wing-man. "Synthesis, photophysics and photochemistry of mono- and polynuclear complexes of Ruthenium (II) containing crown ether pendants, redox active moieties, and organometallic fragments /." Hong Kong : University of Hong Kong, 1996. http://sunzi.lib.hku.hk/hkuto/record.jsp?B18061734.

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44

Li, Jun. "Synthesis, characterization and application studies of ionic platinum(II) complexes." HKBU Institutional Repository, 2017. https://repository.hkbu.edu.hk/etd_oa/394.

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This thesis is dedicated to developing novel charged Pt(II) complexes and exploring their applications in electroluminescence, bio-imaging and the preparation of soft salts. At the beginning, a brief introduction about the development of ionic transition metal complexes and an overview of their applications in electroluminescence, bio-imaging and soft salts are presented. In chapter 2, a series of anionic Pt(II) complexes were successfully synthesized and fully characterized for their application in electroluminescence with relatively small current density. All the complexes show highly intens

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45

Samanamu, Christian. "Studies on the synthesis of main group and late transition element frameworks." [Fort Worth, Tex.] : Texas Christian University, 2009. http://etd.tcu.edu/etdfiles/available/etd-04232009-112540/unrestricted/Samanamu.pdf.

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46

Shaffer, Andrew Ronald. "Synthesis, reactivity, and catalysis of 3-iminophosphine palladium complexes /." Connect to full text in OhioLINK ETD Center, 2009. http://rave.ohiolink.edu/etdc/view?acc_num=toledo1248288981.

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Thesis (Ph. D.)--University of Toledo, 2009.<br>Typescript. "Submitted as partial fulfillment of the requirements for the Doctor of Philosophy in Chemistry." Includes bibliographical references (leaves 183-217).

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47

Curtis, H. "Synthesis, characterisation and reactivity of transition metal carbido-carbonyl cluster and other organometallic compounds." Thesis, University of Cambridge, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.377825.

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48

Guo, Jianping. "Synthesis, structure and characterization of long distance electrostatic force and hydrogen bond supramolecular polymers synthesis, structure and characterization of bis[2,4-di(pyridyl)-1,3,5-triazapenta-dienato] metal complexes." HKBU Institutional Repository, 2004. http://repository.hkbu.edu.hk/etd_ra/506.

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49

Meyer, Annalene. "The synthesis of α-alkoxy and α-aminostannanes as precursors to Novel Chromium Fischer Carbenes". Thesis, Rhodes University, 2012. http://hdl.handle.net/10962/d1005036.

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The present study involves the use of main group organometallics: organostannanes and organolithiums as precursors to chromium Fischer carbene complexes. Fischer carbenes are well stabilized by the π‐donor substituents such as alkoxy and amino groups and low oxidation state metals such as Group 6 (Chromium, Molybdenum or Tungsten). Carbenes are an important intermediate in the synthesis of a range of compounds through cyclopropanations, insertions, coupling and photochemical reactions. Synthesis and successful characterisation of three α‐alkoxystannanes was achieved via nucleophilic addition o

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50

Carson, Cantwell G. "Noble and transition metal aromatic frameworks synthesis, properties, and stability /." Diss., Atlanta, Ga. : Georgia Institute of Technology, 2009. http://hdl.handle.net/1853/29657.

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Thesis (Ph. D.)--Materials Science and Engineering, Georgia Institute of Technology, 2009.<br>Committee Chair: Rina Tannenbaum; Committee Co-Chair: Rosario A. Gerhardt; Committee Member: E. Kent Barefield; Committee Member: Karl I. Jacob; Committee Member: Preet Singh; Committee Member: R. Bruce King. Part of the SMARTech Electronic Thesis and Dissertation Collection.

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