Relevant bibliographies by topics / Organometallic synthesis

Contents

  1. Journal articles
  2. Dissertations / Theses
  3. Books
  4. Book chapters
  5. Conference papers
  6. Reports

Academic literature on the topic 'Organometallic synthesis'

Author: Grafiati
Published: 4 June 2021
Last updated: 8 June 2024

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Journal articles on the topic "Organometallic synthesis"

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Khalid, Maher, and Shireen Mohammedand Amin Kalo. "Recent Developments in Weinreb Synthesis and Their Applications." Oriental Journal of Chemistry 35, no. 6 (December 23, 2019): 1611–26. http://dx.doi.org/10.13005/ojc/350601.

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N-methoxy-N-methyl amides or Weinreb amides are worthy embranchment of amide group and their rich functional groups in organic synthesis become a strong else unfeasible conversion. Weinreb amides are produced as an intermediate product of the reaction of carboxylic acids, acid chloride or esters with organometallic reagents, which was first uncovered in 1981. The direct conversion of carboxylic acids or acid chlorides or esters to ketones or aldehydes using organometallic reagents do not lead in high yields, because the intermediate ketones are still highly reactive toward the organometallic reagent. However, after derivatization to the corresponding Weinreb Amide, reaction with organometallics does give the desired ketones, as the initial adduct is stabilized and doesn't undergo further reactions. A nucleophilic addition to the Weinreb amides results in a unique and stable five-membered cyclic tetrahedral intermediate which protects the over-addition, leading to a selective conversion.
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Laine, Richard M. "Transition Metal Catalysed Synthesis of Oligo- and Polysilazanes." Platinum Metals Review 32, no. 2 (April 1, 1988): 64–71. http://dx.doi.org/10.1595/003214088x3226471.

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Organometallic polymer research offers many potential academic and industrial rewards because of the number of elemental variations possible. Unfortunately, there are no general synthetic methods as found for carbon based polymers. Transition metal catalysed dehydrocoupling reactions may prove to be generally applicable to the synthesis of silicon based organometallic polymers. We report here our efforts to synthesise organometallic polymers with a silicon-nitrogen backbone, polysilazanes, using the dehydrocoupling reaction. We also describe the synthesis of polysilazanes for use as precursors to silicon nitride.
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Dong, Zhi-Bing, and Jin-Quan Chen. "Recent Progress in Utilization of Functionalized Organometallic Reagents in Cross Coupling Reactions and Nucleophilic Additions." Synthesis 52, no. 24 (November 4, 2020): 3714–34. http://dx.doi.org/10.1055/s-0040-1706550.

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AbstractOrganometallic compounds have become increasingly important in organic synthesis because of their high chemoselectivity and excellent reactivity. Recently, a variety of organometallic reagents were found to facilitate transition-metal-catalyzed cross-coupling reactions and nucleophilic addition reactions. Here, we have summarized the latest progress in cross-coupling reactions and in nucleophilic addition reactions with functionalized organometallic reagents present to illustrate their application value. Due to the tremendous contribution made by the Knochel group towards the development of novel organometallic reagents, this review draws extensively from their work in this area in recent years.Introduction1 Transition-Metal-Catalyzed Cross Couplings Involving Organo­zinc Reagents2 Transition-Metal-Catalyzed Cross Couplings Involving Organomagnesium Reagents3 Transition-Metal-Free Cross Couplings Involving Zn and Mg ­Organometallic Reagents4 Nucleophilic Additions Involving Zn and Mg Organometallic Reagents5 Cross-Coupling Reactions or Nucleophilic Additions Involving Mn, Al-, La-, Li-, Sm- and In-Organometallics6 Conclusion
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Asaad, Noora, Ahmed Z. M. AL-Bassam, and Sahar S. M. Alabdullah. "Uses of organometallic compounds in chemical processes." International Journal of Research in Engineering and Innovation 06, no. 02 (2022): 98–103. http://dx.doi.org/10.36037/ijrei.2022.6203.

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This review is proposed to address knowledge of organometallic compounds (OMC) in chemical applications and show these compounds' depth scope in different scientific studies. This review is based on outlining the gap between the traditional preparations and green chemistry synthesis of organometallic materials purposes in the experimental section of a researcher's papers. The most comparative research considers the drawbacks of organometallic compounds, including their applications in industrial, clinical, drug forms, and chemical reactions. However, many organometallic compounds are inherently poisonous. The most general challenge is producing alternative substances to creative green organometallic compounds, specifically in drug formulations systems. A wide range of chemical reactions have been investigated and formulated new organometallic properties this may be associated with an increased level of enhancement health systems. This study aims to determine the importance of organometallic compound in many path ways in various articles and confirmed how papers trying to characterize new organometallic substances in various chemical processes. Particular interest is given to knowledge synthesis OMC in medicine and industrially.
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AMIENS, C., and B. CHAUDRET. "ORGANOMETALLIC SYNTHESIS OF NANOPARTICLES." Modern Physics Letters B 21, no. 18 (August 10, 2007): 1133–41. http://dx.doi.org/10.1142/s0217984907013833.

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Nanoparticles can be synthesized from metal-organic or organometallic precursors, either by classical thermal decomposition, ultrasound activation, photolysis as well as hydrogenation or hydrolysis reactions. The size, size distribution and more importantly surface state of these nanoparticles are much better controlled than when they are produced by chemical or electrochemical reduction of metal salts. Hence, metal or oxide nanoparticles can be obtained that are suitable for fundamental physics at the nanoscale, especially for magnetic studies. This is currently of particular interest as many applications require systems of still smaller sizes, the properties of which are not yet fully understood.
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Smith, Amos B., Melean Visnick, John N. Haseltine, and Paul A. Sprengeler. "Organometallic reagents in synthesis." Tetrahedron 42, no. 11 (January 1986): 2957–69. http://dx.doi.org/10.1016/s0040-4020(01)90586-1.

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Hanson, J. R. "Organometallic reagents in synthesis." Journal of Organometallic Chemistry 493, no. 1-2 (May 1995): C29. http://dx.doi.org/10.1016/0022-328x(95)90879-j.

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Heinze, Katja. "Solid-Phase Organometallic Synthesis." Chemistry - A European Journal 7, no. 13 (July 2, 2001): 2922–32. http://dx.doi.org/10.1002/1521-3765(20010702)7:13<2922::aid-chem2922>3.0.co;2-m.

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Rightmire, Nicholas R., and Timothy P. Hanusa. "Advances in organometallic synthesis with mechanochemical methods." Dalton Transactions 45, no. 6 (2016): 2352–62. http://dx.doi.org/10.1039/c5dt03866a.

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Mechanochemical methods of synthesis (specifically grinding and milling) have not yet been widely used by organometallic chemists, but there is growing interest in their potential. This Perspective surveys recent developments in the field, describing the outcomes of organometallic reactions conducted in the absence of solvents.
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Burton, Donald J., and Zhen-Yu Yang. "Fluorinated organometallics: Perfluoroalkyl and functionalized perfluoroalkyl organometallic reagents in organic synthesis." Tetrahedron 48, no. 2 (1992): 189–275. http://dx.doi.org/10.1016/s0040-4020(01)88139-4.

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Dissertations / Theses on the topic "Organometallic synthesis"

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Zini, Simone. "Synthesis of manganese organometallic complexes." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2021. http://amslaurea.unibo.it/22235/.

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Il presente lavoro di tesi si inserisce in un progetto di ricerca volto alla sintesi di nuovi complessi di metalli di transizione per lo sviluppo di catalizzatori da impiegare in reazioni di catalisi omogenea. In particolare il mio progetto si è concentrato sulla sintesi di complessi organometallici di manganese con leganti carbenici N-eterociclici (NHC). La scelta dei leganti è stata effettuata in modo tale da poter avere leganti chelanti NHC di tipo MIC (mesoionic carbene) sintetizzati tramite cicloaddizione tra un alchino ed un azide catalizzata da rame (CuAAC) e N-alchilazione. Lo studio di questi complessi a base di manganese è ancora tutt’oggi agli albori, leganti NHC vengono molto utilizzati grazie alla possibilità di variarne le proprietà steriche ed elettroniche e alla possibilità di formare legami forti con quasi tutti i metalli. Il manganese è stato scelto poiché un elemento abbondante, poco tossico e poco costoso. The present thesis work is part of a research project aimed at the synthesis of new transition metal complexes to be used in homogeneous catalysis reactions. In particular my project focused on the synthesis of manganese organometallic complexes with N-heterocyclic carbene ligands (NHC). The choice of ligands was carried out to have NHC chelating ligands of the class of MIC (mesoionic carbene). These ligands are synthesized by cycloaddition between alkyl and azide with a copper-catalyzed reaction (CuAAC) and N-alkylation in order to obtain MIC after deprotonation. The study of these manganese-based complexes is still in its infancy today, NHC ligands are widely used thanks to the possibility of varying their steric and electronic properties and the possibility of forming strong bonds with almost all metals. The choice of manganese was made because is an abundant, low-toxic and inexpensive element.
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Lee, Peter D. "Organometallic synthesis in supercritical fluids." Thesis, University of Nottingham, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.336862.

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Berridge, Rory. "The synthesis of novel organometallic materials." Thesis, Sheffield Hallam University, 2001. http://shura.shu.ac.uk/19349/.

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Due to their highly interesting electroactive properties, complexes based on the sulphur heterocycle DMIT have been studied extensively for several decades. The literature is abundant with materials exhibiting semiconducting and metallic properties and up to early 2000 there are eight examples of DMIT based superconductors. In the case of the DMIT complexes, previous work has been constrained to the variation of the transition metal and/or the counter-anion. The work herein concerns the synthesis of a novel series of electroactive ligands, similar to the well-known DMIT species. In contrast to the DMIT ligand, our target derivatives incorporate two thioether and two dithiolate environments as the overall chelating entity. The thioether functionalities are linked via suitable spacer groups and this feature should present a major advantage over traditional DMIT complexes, by adding solubility and synthetic versatility to the overall nature of the complex. In addition to the metal complexes based on DMIT ligands, charge transfer (CT) halogen adducts of these DMIT ligands and their synthetic intermediates are described, providing highly interesting and novel solid state structures and atom-to-atom inter- and intra-molecular interactions.
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Abdelsalam, Mansour. "Synthesis of piperidines using organometallic chemistry." Thesis, University of Sheffield, 2013. http://etheses.whiterose.ac.uk/4069/.

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Ashcroft, R. C. "Organometallic precursors for pillared clay synthesis." Thesis, Aston University, 1993. http://publications.aston.ac.uk/9773/.

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The synthetic hectorite, laponite has been used within the paper industry to produce mildly conducting paper for use in electrographic printing. The aim of this research was to modify laponite in order to improve the electrical conductivity. In a continuation of a previous investigation involving organotin intercalation of laponite, the organotin precursor (p-CH3,OC6H4)4Sn was synthesised and characterised using Mass Spectroscopy, Infrared Spectroscopy and elemental analysis. Results of intercalation with this compound and a range of organobismuth and organoantimony compounds suggested that a halide content within the precursor was necessary for improvement in conductivity to be observed. Organometallic intercalation of a range of organotellurium compounds with laponite provided evidence that a hydrolysis reaction on the clay surface followed by the release of hydrochloric acid was an important first step if a reaction was to occur with the clay. Atomic Absorption Spectroscopy studies have shown that the acid protons underwent exchange with the interlayer sodium ions in the clay to varying degrees. Gas-liquid Chromatography and Infrared Spectroscopy revealed that the carbon-tellurium bond remained intact. Powder X-ray diffraction revealed that there had been no increase in the basal spacing. The a.c. conductivity of the modified clays in the form of pressed discs was studied over a frequency range of 12Hz - 100kHz using two electrode systems, silver paste and stainless steel. The a.c. conductivity consists of two components, ionic and reactive. The conductivity of laponite was increased by intercalation with organometallic compounds. The most impressive increase was gained using the organotellurium precursor (p-CH3OC6H4)2TeCl2. Conductivity investigations using the stainless steel electrode where measurements are made under pressure showed that in the case of laponite, where poor particle-particle contact exists at ambient pressure, there is a two order of magnitude increase in the measured a.c. conductivity. This significant increase was not seen in modified laponites where the particle-particle contact had already been improved upon. Investigations of the clay surface using Scanning Electron Microscopy suggested that the improvement in particle-particle contact is the largest factor in the determination of the conductivity. The other important factor is the nature and the concentration of the interlayer cations. A range of clays were synthesised in order to increase the concentration of sodium interlayer cations. A sol-gel method was employed to carry out these syntheses. A conductivity evaluation showed that increasing the concentration of the sodium cations within the clay led to an increase in the conductivity.
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Lee, Linda I.-Lin. "Synthesis and reactivity of organometallic enediynes /." Diss., Connect to a 24 p. preview or request complete full text in PDF format. Access restricted to UC campuses, 2001. http://wwwlib.umi.com/cr/ucsd/fullcit?p3025940.

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Atefi, Farzad. "Synthesis and reactions of organometallic porphyrins." Thesis, Queensland University of Technology, 2007. https://eprints.qut.edu.au/17563/1/Farzad_Atefi_Thesis.pdf.

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This thesis reports progress in three major aspects of σ-bonded organometallic porphyrins that are described in the published papers found in chapters 4, 5 and 6. meso-Iodoporphyrins, which were prepared in a rapid, selective and high yielding methodology from the respective 1-palladioporphyrins or bromoporphyrins, are important starting materials for further functionalisations of porphyrins. Their utility was confirmed in a palladium-catalysed coupling reaction and this novel synthetic strategy could potentially be applied for iodine/bromine exchange on other organic substrates.. A 1-palladioporphyrin was also utilised to optimise the reaction conditions leading to the formation of porphyrinylphosphine oxides. This synthetic strategy simplified the challenging optimisation of the palladium-catalysed reaction and has great potential to be applied in other catalytic processes. Subsequently a suite of porphyrinylphosphine oxides was prepared under the optimised catalytic conditions. These macrocycles, which represent a new class of porphyrins, were isolated cleanly in very high yields. Detailed spectroscopic investigations as well as X-ray single crystal analysis demonstrated their structures unambiguously and established their potential as ligands for supramolecular chemistry. The coordinating properties of phosphine oxides in general and porphyrinylphosphine oxides in particular, towards Mg(II) centred porphyrins were examined in further experiments. Triphenylphosphine oxide showed a strong affinity towards Mg(II) porphyrins and the calculated displacement constant of 5.3 × 105 M-1 was two orders of magnitude larger than any other Mg(II) porphyrin-ligand binding constant reported thus far. Di- and triporphyrin arrays consisting of Mg(II) porphyrin coordinated to free base and Ni(II) porphyrinyl mono- and bis-phosphine oxides were also prepared in high yields. Spectroscopic studies indicated that these porphyrin oligomers exhibit strong inter-porphyrin electronic interaction. A Mg(II) porphyrinylphosphine oxide dimer was also isolated in a satisfactory yield. The large self-association constant of 5.5 × 108 M-1 confirmed the strong affinity of porphyrinylphosphine oxides towards Mg(II) porphyrins and established these complexes as the first strongly bound synthetic Mg(II) porphyrin analogues of the "special pair" of the photosynthetic reaction centre.
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Atefi, Farzad. "Synthesis and reactions of organometallic porphyrins." Queensland University of Technology, 2007. http://eprints.qut.edu.au/17563/.

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This thesis reports progress in three major aspects of σ-bonded organometallic porphyrins that are described in the published papers found in chapters 4, 5 and 6. meso-Iodoporphyrins, which were prepared in a rapid, selective and high yielding methodology from the respective 1-palladioporphyrins or bromoporphyrins, are important starting materials for further functionalisations of porphyrins. Their utility was confirmed in a palladium-catalysed coupling reaction and this novel synthetic strategy could potentially be applied for iodine/bromine exchange on other organic substrates.. A 1-palladioporphyrin was also utilised to optimise the reaction conditions leading to the formation of porphyrinylphosphine oxides. This synthetic strategy simplified the challenging optimisation of the palladium-catalysed reaction and has great potential to be applied in other catalytic processes. Subsequently a suite of porphyrinylphosphine oxides was prepared under the optimised catalytic conditions. These macrocycles, which represent a new class of porphyrins, were isolated cleanly in very high yields. Detailed spectroscopic investigations as well as X-ray single crystal analysis demonstrated their structures unambiguously and established their potential as ligands for supramolecular chemistry. The coordinating properties of phosphine oxides in general and porphyrinylphosphine oxides in particular, towards Mg(II) centred porphyrins were examined in further experiments. Triphenylphosphine oxide showed a strong affinity towards Mg(II) porphyrins and the calculated displacement constant of 5.3 × 105 M-1 was two orders of magnitude larger than any other Mg(II) porphyrin-ligand binding constant reported thus far. Di- and triporphyrin arrays consisting of Mg(II) porphyrin coordinated to free base and Ni(II) porphyrinyl mono- and bis-phosphine oxides were also prepared in high yields. Spectroscopic studies indicated that these porphyrin oligomers exhibit strong inter-porphyrin electronic interaction. A Mg(II) porphyrinylphosphine oxide dimer was also isolated in a satisfactory yield. The large self-association constant of 5.5 × 108 M-1 confirmed the strong affinity of porphyrinylphosphine oxides towards Mg(II) porphyrins and established these complexes as the first strongly bound synthetic Mg(II) porphyrin analogues of the "special pair" of the photosynthetic reaction centre.
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Qin, J. "Studies in organometallic solid state chemistry." Thesis, University of Oxford, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.379942.

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Stewart, A. S. J. "Organometallic derivatives of amino acids and peptides." Thesis, Robert Gordon University, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.376684.

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Books on the topic "Organometallic synthesis"

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Organometallic reagents in synthesis. Oxford: Oxford University Press, 1992.

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1938-, King R. B., and Eisch John J. 1930-, eds. Organometallic syntheses. Amsterdam: Elsevier Science, 1986.

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Bruce, King R., and Eisch John J, eds. Organometallic syntheses: Volume 3. Amsterdam: Elsevier, 1986.

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Sanshiro, Komiya, ed. Synthesis of organometallic compounds: A practical guide. Chichester: Wiley, 1997.

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1937-, Murahashi Shunʾichi, ed. Ruthenium in organic synthesis. Weinheim: Wiley-VCH, 2004.

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Paul, Knochel, ed. Handbook of functionalized organometallics: Application in synthesis. Weinheim: Wiley-VCH, 2005.

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1954-, Wayda Andrea L., Darensbourg Marcetta Y. 1942-, American Chemical Society. Division of Inorganic Chemistry., and American Chemical Society Meeting, eds. Experimental organometallic chemistry: A practicum in synthesis and characterization. Washington, D.C: American Chemical Society, 1987.

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Pomogaĭlo, A. D. Synthesis and polymerization of metal-containing monomers. Boca Raton: CRC Press, 1994.

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D, Larsen R., and Abdel-Magid Ahmed F. 1947-, eds. Organometallics in process chemistry. Berlin: Springer, 2004.

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Meng, Weidong. Organometallic approaches to the synthesis of tridachiapyrones. Norwich: University of East Anglia, 1990.

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Book chapters on the topic "Organometallic synthesis"

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Schmalz, Hans-Günther, Battsengel Gotov, and Andreas Böttcher. "Natural Products Synthesis." In Topics in Organometallic Chemistry, 157–79. Berlin, Heidelberg: Springer Berlin Heidelberg, 2004. http://dx.doi.org/10.1007/b94494.

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Starowieyski, K. B. "Organometallic compounds: synthesis and properties." In Chemistry of Aluminium, Gallium, Indium and Thallium, 322–71. Dordrecht: Springer Netherlands, 1993. http://dx.doi.org/10.1007/978-94-011-2170-5_6.

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Bunz, Uwe, Viola Francke, Markus Klapper, Frank Uckert, and Klaus Müllen. "Polymer Synthesis with Organometallic Intermediates." In Organic Synthesis via Organometallics OSM 5, 21–49. Berlin, Heidelberg: Springer Berlin Heidelberg, 1997. http://dx.doi.org/10.1007/978-3-642-49348-5_2.

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Ripin, David H. Brown. "Synthesis of “Nucleophilic” Organometallic Reagents." In Practical Synthetic Organic Chemistry, 575–607. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2011. http://dx.doi.org/10.1002/9781118093559.ch12.

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Norman, Richard, and James M. Coxon. "Formation of carbon—carbon bonds: organometallic reagents." In Principles of Organic Synthesis, 184–205. Dordrecht: Springer Netherlands, 1993. http://dx.doi.org/10.1007/978-94-011-2166-8_6.

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Woodward, Simon. "The Primary Organometallic in Copper-Catalyzed Reactions." In Copper-Catalyzed Asymmetric Synthesis, 3–32. Weinheim, Germany: Wiley-VCH Verlag GmbH & Co. KGaA, 2014. http://dx.doi.org/10.1002/9783527664573.ch1.

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Lubineau, A., J. Augé, and Y. Queneau. "Carbonyl additions and organometallic chemistry in water." In Organic Synthesis in Water, 102–40. Dordrecht: Springer Netherlands, 1998. http://dx.doi.org/10.1007/978-94-011-4950-1_4.

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Khan, I. A., H. S. Ahuja, K. W. Bagnall, and Lee Sinf. "43. Uranium(IV) Chloride for Organometallic Synthesis." In Inorganic Syntheses, 187–90. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132524.ch43.

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Hughes, Alan N. "Bis(diphenylphosphino)methane in Organometallic Synthesis." In ACS Symposium Series, 173–85. Washington, DC: American Chemical Society, 1992. http://dx.doi.org/10.1021/bk-1992-0486.ch014.

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Jones, William D., Valerie L. Chandler, Robert P. Duttweiler, Frank J. Feher, Edward T. Hessell, Grace C. Hsu, and Walter P. Kosar. "Organometallic Transformations via C-H Bond Activation." In Organometallics in Organic Synthesis 2, 185–201. Berlin, Heidelberg: Springer Berlin Heidelberg, 1989. http://dx.doi.org/10.1007/978-3-642-74269-9_11.

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Conference papers on the topic "Organometallic synthesis"

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Santos, Fernanda M., and João H. C. Batista. "Functionalization of aromatic nitriles using hindered organometallic bases." In 15th BMOS - Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-15th_bmos_2.

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Garcia, M. Helena, Paulo J. Mendes, Pedro Florindo, and Tiago Silva. "Design and synthesis of NLO efficient organometallic molecules." In PROCEEDINGS OF THE INTERNATIONAL CONFERENCE OF COMPUTATIONAL METHODS IN SCIENCES AND ENGINEERING 2010 (ICCMSE-2010). AIP Publishing LLC, 2015. http://dx.doi.org/10.1063/1.4906731.

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Fernández-Figueiras, Adolfo, Fátima Lucio, Paula Munín, Francisco Reigosa, Jose Vila, Maria Pereira, and Paula Polo. "SYNTHESIS OF IMINOPHOSPHORANES AS LIGANDS FOR ORGANOMETALLIC COMPOUNDS." In The 20th International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 2016. http://dx.doi.org/10.3390/ecsoc-20-a016.

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Pina, Evelyn Mirella Lopes, Natália de Araujo Pereira, Rafael Augusto Soldi, and Giuliano Cesar Clososki. "Preparation and preliminiar evaluation of new organometallic bases from cis-2,6-dimethylpiperidine." In 15th Brazilian Meeting on Organic Synthesis. São Paulo: Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_2013915232924.

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Tagmatarchis, Nikos, and Kosmas Prassides. "Synthesis and characterization of organometallic compounds of fullerene derivatives." In ELECTRONIC PROPERTIES OF NOVEL MATERIALS--SCIENCE AND TECHNOLOGY OF MOLECULAR NANOSTRUCTURES. ASCE, 1999. http://dx.doi.org/10.1063/1.59779.

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Morales, M. P., A. G. Roca, and C. J. Serna. "Synthesis of Monodispersed Magnetite Particles from Different Organometallic Precursors." In INTERMAG 2006 - IEEE International Magnetics Conference. IEEE, 2006. http://dx.doi.org/10.1109/intmag.2006.376279.

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Bouachrine, M., J. P. Lère-Porte, J. Moreau, F. Serein-Spirau, and T. Lakhlifi. "An Organometallic Selective Synthesis of Conjugated Polymers with Improved Physical Properties." In The 8th International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 2004. http://dx.doi.org/10.3390/ecsoc-8-01994.

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Yang, Hongwei, Weiling Luan, and Shan-Tung Tu. "Large-Scale Synthesis of Monodisperse Nanocrystals via Microreaction." In 2007 First International Conference on Integration and Commercialization of Micro and Nanosystems. ASMEDC, 2007. http://dx.doi.org/10.1115/mnc2007-21605.

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A microfluidic reactor was set up to synthesize quantum dots (QDs) in large scale. The increased reaction channels in an individual reactor lead to improved throughput while maintaining sufficient residence time for the nucleation and growth of QDs. Uniform reaction conditions in the four capillaries realized by our set-up result in superior stability of the whole system. Organometallic synthesis of CdSe was chosen as a model system to evaluate the reactor, the absorption spectra of samples collected from different streams at various time intervals are indistinguishable from each other. By systematically varying the reaction parameters, fairly monodisperse CdSe NCs was produced with three times throughput higher than the conventional single-channel counterpart, and the FWHM of the PL. peaks can be controlled in the range from 37nm to 44nm. The large-scale synthesis route is characterized as excellent reproducibility, low-cost, fast reaction, and mass-production, by which 12ml CdSe NCs solution can be produced within 1h with the reaction time of 21s.
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Saliba, Sarmenio, Fabienne Gauffre, Myrtil L. Kahn, Lecante Pierre, Julie Massaad, Gerald Casterou, Pierre-Antoine Eliat, et al. "Synthesis of metal oxide nanoparticles by organometallic approach: From molecule to devices." In 2016 IEEE Nanotechnology Materials and Devices Conference (NMDC). IEEE, 2016. http://dx.doi.org/10.1109/nmdc.2016.7777146.

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Murray, Philip R. D., Duncan L. Browne, Julio C. Pastre, and Steven V. Ley. "Continuous Flow-Processing of Organometallic Reagents Using an Advanced Peristaltic Pumping System and the Telescoped Flow Synthesis of (E/Z)-Tamoxifen." In 15th Brazilian Meeting on Organic Synthesis. São Paulo: Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_2013914162643.

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Reports on the topic "Organometallic synthesis"

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Wright, Michael E., and Edward G. Toplikar. Organometallic Nonlinear Optical (NLO) Polymers. 2. Synthesis of Main-Chain Organometallic Polymers and a Structural Study of Ferrocene NLO-Phores. Fort Belvoir, VA: Defense Technical Information Center, May 1992. http://dx.doi.org/10.21236/ada250655.

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Tour, James M. Organometallics for Conducting Polymer Synthesis and Starburst Polymer Synthesis. Fort Belvoir, VA: Defense Technical Information Center, May 1991. http://dx.doi.org/10.21236/ada235933.

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Nolan, Steven. Synthetic and Thermodynamic Investigations of Ancillary Ligand Influence on Catalytic Organometallic Systems. Final Report. Office of Scientific and Technical Information (OSTI), March 2003. http://dx.doi.org/10.2172/821151.

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Synthesis and properties of novel organometallic polymers. Office of Scientific and Technical Information (OSTI), May 1990. http://dx.doi.org/10.2172/6243167.

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