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Dissertations / Theses on the topic 'Organometallic synthesis'

Author: Grafiati

Published: 4 June 2021

Last updated: 25 July 2025

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1

Zini, Simone. "Synthesis of manganese organometallic complexes." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2021. http://amslaurea.unibo.it/22235/.

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Il presente lavoro di tesi si inserisce in un progetto di ricerca volto alla sintesi di nuovi complessi di metalli di transizione per lo sviluppo di catalizzatori da impiegare in reazioni di catalisi omogenea. In particolare il mio progetto si è concentrato sulla sintesi di complessi organometallici di manganese con leganti carbenici N-eterociclici (NHC). La scelta dei leganti è stata effettuata in modo tale da poter avere leganti chelanti NHC di tipo MIC (mesoionic carbene) sintetizzati tramite cicloaddizione tra un alchino ed un azide catalizzata da rame (CuAAC) e N-alchilazione. Lo studio d

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2

Lee, Peter D. "Organometallic synthesis in supercritical fluids." Thesis, University of Nottingham, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.336862.

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3

Berridge, Rory. "The synthesis of novel organometallic materials." Thesis, Sheffield Hallam University, 2001. http://shura.shu.ac.uk/19349/.

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Due to their highly interesting electroactive properties, complexes based on the sulphur heterocycle DMIT have been studied extensively for several decades. The literature is abundant with materials exhibiting semiconducting and metallic properties and up to early 2000 there are eight examples of DMIT based superconductors. In the case of the DMIT complexes, previous work has been constrained to the variation of the transition metal and/or the counter-anion. The work herein concerns the synthesis of a novel series of electroactive ligands, similar to the well-known DMIT species. In contrast to

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4

Abdelsalam, Mansour. "Synthesis of piperidines using organometallic chemistry." Thesis, University of Sheffield, 2013. http://etheses.whiterose.ac.uk/4069/.

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5

Ashcroft, R. C. "Organometallic precursors for pillared clay synthesis." Thesis, Aston University, 1993. http://publications.aston.ac.uk/9773/.

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The synthetic hectorite, laponite has been used within the paper industry to produce mildly conducting paper for use in electrographic printing. The aim of this research was to modify laponite in order to improve the electrical conductivity. In a continuation of a previous investigation involving organotin intercalation of laponite, the organotin precursor (p-CH3,OC6H4)4Sn was synthesised and characterised using Mass Spectroscopy, Infrared Spectroscopy and elemental analysis. Results of intercalation with this compound and a range of organobismuth and organoantimony compounds suggested that a

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6

Lee, Linda I.-Lin. "Synthesis and reactivity of organometallic enediynes /." Diss., Connect to a 24 p. preview or request complete full text in PDF format. Access restricted to UC campuses, 2001. http://wwwlib.umi.com/cr/ucsd/fullcit?p3025940.

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7

Atefi, Farzad. "Synthesis and reactions of organometallic porphyrins." Thesis, Queensland University of Technology, 2007. https://eprints.qut.edu.au/17563/1/Farzad_Atefi_Thesis.pdf.

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This thesis reports progress in three major aspects of σ-bonded organometallic porphyrins that are described in the published papers found in chapters 4, 5 and 6. meso-Iodoporphyrins, which were prepared in a rapid, selective and high yielding methodology from the respective 1-palladioporphyrins or bromoporphyrins, are important starting materials for further functionalisations of porphyrins. Their utility was confirmed in a palladium-catalysed coupling reaction and this novel synthetic strategy could potentially be applied for iodine/bromine exchange on other organic substrates.. A 1-pal

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8

Atefi, Farzad. "Synthesis and reactions of organometallic porphyrins." Queensland University of Technology, 2007. http://eprints.qut.edu.au/17563/.

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This thesis reports progress in three major aspects of σ-bonded organometallic porphyrins that are described in the published papers found in chapters 4, 5 and 6. meso-Iodoporphyrins, which were prepared in a rapid, selective and high yielding methodology from the respective 1-palladioporphyrins or bromoporphyrins, are important starting materials for further functionalisations of porphyrins. Their utility was confirmed in a palladium-catalysed coupling reaction and this novel synthetic strategy could potentially be applied for iodine/bromine exchange on other organic substrates.. A 1-pal

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9

Qin, J. "Studies in organometallic solid state chemistry." Thesis, University of Oxford, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.379942.

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10

Stewart, A. S. J. "Organometallic derivatives of amino acids and peptides." Thesis, Robert Gordon University, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.376684.

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11

Moss, James Edward. "The Synthesis and Organometallic Chemistry of NonamethyIfluorene." Thesis, University of Oxford, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.491509.

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The focus of this thesis is the synthesis and organometallic chemistry of the nonamethylfluorene ligand (Flu*). Chapter One summarises the properties and uses of the fluorene molecule and the incorporation of both the neutral and deprotonated forms of the ligand into organometallic complexes. The chapter concludes with a discussion of the properties that are bestowed upon organometallic compounds containing fully methylated ligands, detailing the need for nonamethylfluorene. Chapter Two describes a relatively high yielding total synthesis of the fully methylated fluorene, Flu*H, using techniqu

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12

Beck, Victoria Holly. "Synthesis and characterisation of bimetallic organometallic complexes." Thesis, University of Oxford, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.403935.

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13

Meng, Weidong. "Organometallic approaches to the synthesis of tridachiapyrones." Thesis, University of East Anglia, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.256766.

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14

Alshammari, Mohammed. "Use of organometallic intermediates in organic synthesis." Thesis, Cardiff University, 2012. http://orca.cf.ac.uk/45471/.

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Chapter One: Chapter one describes a historical overview and the practical consideration of lithiation reactions and highlight of some of the factors that could influence the site of lithiation. It also provides reviews of the directed and side-chain lithiation of substituted aromatics. Chapter Two: Chapter two deals with lithiation of N′-phenethyl-N,N-dimethylurea with three equivalents of t-BuLi in THF at –78 °C followed by reaction with various electrophiles to give side-chain substituted products due to lithiation and substitution at the CH2 next to the phenyl ring (α-lithiation). The 2-li

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15

Murphy, Vincent John. "Synthesis and characterisation of organometallic molecular materials." Thesis, University of Oxford, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.357440.

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16

Dickerson, Bryan Douglas. "Organometallic Synthesis Kinetics of CdSe Quantum Dots." Diss., Virginia Tech, 2005. http://hdl.handle.net/10919/27322.

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CdSe quantum dots produced by organometallic synthesis are useful as tunable emitters for photonic devices and as multi-colored protein markers for biomedical imaging, applications requiring bright and narrow emission. A diffusion-limited model helped monitor growth rates via photoluminescence and absorbance spectroscopy, in order to characterize synthesis kinetics in stearic acid, dodecylamine, and in trioctylphosphine oxide. The nucleation rate increased with Se concentration, while the growth rate followed the Cd concentration. Emission peak widths, emission redshift rates, nanocrystal gr

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17

Lovett, Victoria Jane. "Synthesis of amino acids using organometallic chemistry." Thesis, University of Sheffield, 2013. http://etheses.whiterose.ac.uk/5416/.

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18

Lawrence, Heather Bunting Elizabeth. "Organometallic compounds with non-linear optical properties." Thesis, University of Oxford, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.276835.

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19

Rumble, Sarah Louise Chemistry Faculty of Science UNSW. "The synthesis of amines and imines organometallic catalysts." Awarded by:University of New South Wales. School of Chemistry, 2005. http://handle.unsw.edu.au/1959.4/23422.

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This thesis describes investigations into the catalysed syntheses of amines and imines using organoiridium and organorhodium complexes with N-donor ligands as the catalysts. These catalysed syntheses were achieved via hydroamination, hydrosilylation, and hydrogenation reactions, as well as tandem hydroamination/imine reduction reactions. An in situ catalysis study found that the most active catalysts for the hydroamination of 4-pentyn-1-amine (1) to give 2-methyl-1-pyrroline (4) were formed from a combination of catalyst components that resulted in an electron deficient metal centre, indicatin

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20

Wallner, Olov. "Palladium-Catalyzed Synthesis and Transformations of Organometallic Compounds." Doctoral thesis, Stockholm : Dept. of Organic Chemistry, Stockholm University, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-804.

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21

Manville, Charles. "New organic and organometallic catalysts for asymmetric synthesis." Thesis, University of Warwick, 2010. http://wrap.warwick.ac.uk/35525/.

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Monodentate phosphorus ligands based on BINOL have been synthesised and applied to metal catalysed pressure hydrogenation and conjugate addition. Novel phosphorus containing enantioselective organocatalysts have been synthesised from DPEN and proline, and studied in the Michael addition of acetone to trans-β- nitrostyrenes, with up to 96 % e.e. The optimum reaction conditions for reaction rate and enantioselectivity have been investigated. Related proline-DPEN coupled organocatalysts have been synthesised and applied to the coupling reaction between DEAD and aldehydes. The proline-DPEN coupled

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22

Stunt, R. A. "Synthesis and luminescence studies of some organometallic complexes." Thesis, University of East Anglia, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.380965.

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23

King, Andrew John. "An organometallic approach to total synthesis of phyllanthocin." Thesis, University of Southampton, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.307326.

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24

Dutkiewicz, Michal Seweryn. "Organometallic neptunium complexes : synthesis, structure and reduction chemistry." Thesis, University of Edinburgh, 2017. http://hdl.handle.net/1842/25503.

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The aim of the work described in this thesis was to develop a more extensive knowledge of the chemistry of neptunium compounds by making rare, air- and moisture sensitive, low formal oxidation state neptunium compounds with full structural and synthetic characterization. The thesis contains three results chapters. Chapter one introduces neptunium chemistry as a background to the results presented. The first review on the molecular non-aqueous neptunium chemistry is provided and the literature reports to date discussed in the context of this. Chapter two describes exploratory synthetic and stru

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25

Shen, Chengshuo. "Heteroatomic and organometallic helicenes : synthesis and chiroptical properties." Thesis, Rennes 1, 2015. http://www.theses.fr/2015REN1S159.

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Mes travaux de thèse se sont portés sur la synthèse d'hélicènes organométalliques et hétéroatomiques, et se divisent suivant trois axes majeurs. Le premier sujet est l'étude des hélicènes avec un centre métallique redox. Nous avons introduit un motif chimique contenant un atome de fer sur l'hélicène connecté par une liaison C≡C. Dans ce sujet, nous avons étudié les propriétés chiroptiques avec le changement d'état redox du centre métallique. Pour cela, nous avons utilisé des techniques spectroscopiques chiroptiques comme le dichroïsme circulaire vibrationnel, le spectre d'activité optique Rama

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26

Pearson, Mark. "Organometallic reagents for catalytic cross-coupling." Thesis, University of Oxford, 1992. http://ora.ox.ac.uk/objects/uuid:c5eea9a0-8f0c-46bf-a1ea-28a40b79546d.

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Phosphine complexes of nickel and palladium provide the best catalysts for the homogeneous catalysed carbon-carbon bond forming reaction between an organometallic nucleophile and an organic electrophile. Use of a homochiral ligand on the catalyst can lead to stereoselectivity in the cross-coupling reaction, with high ee's of coupled product being obtained. The processes of selectivity in the transmetalation step of the catalytic cycle have not been elucidated and the initial aim of the project was to study these processes. Initial experiments using organotin derivatives as the organometallic n

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27

Hartnell, Regan David. "The synthesis and investigation of novel n¹-organometallic porphyrins." Thesis, Queensland University of Technology, 2003. https://eprints.qut.edu.au/37151/1/37151_Digitised%20Thesis.pdf.

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28

Frazier, Joy Faith. "Organo-iridium compounds : synthesis, characterization and reactivity /." Thesis, This resource online, 1991. http://scholar.lib.vt.edu/theses/available/etd-08222009-040309/.

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29

Choi, Ka Ho. "Synthesis, characterization and properties of luminescent rigid-rod organometallic acetylide materials." HKBU Institutional Repository, 2001. http://repository.hkbu.edu.hk/etd_ra/360.

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30

Clayton, C. W. "The synthesis and chemistry of some novel trimethylphosphine hydride complexes of iridium." Thesis, University of Oxford, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.379909.

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31

Clark, Robert Andrew. "Studies on novel molecular solids." Thesis, Bangor University, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.252653.

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32

Luker, Tim John. "Tandem reactions on a zirconocene template." Thesis, University of Southampton, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.295252.

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33

Melis, Diana. "Quinoline-triazole half-sandwich iridium(III) complexes: Synthesis, antiplasmodial activity and preliminary transfer hydrogenation studies." Master's thesis, Faculty of Science, 2020. http://hdl.handle.net/11427/32414.

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Malaria is a devastating and pervasive infectious disease and continues to be a major global health issue, with over half the world's population being at risk of transmission. In the absence of a suitable vaccine, efforts to eradicate the disease rely heavily on clinically available drugs. Plasmodium falciparum, the deadliest species of malaria, has however become resistant to most conventional antimalarial treatments, resulting in the worldwide search for new, effective drugs. Amongst other requirements, these drugs should target resistant parasitic strains in an attempt to curb the escalatio

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34

Guest, Ruth Winifred. "Synthesis and Reactions of Iron and Ruthenium Dinitrogen Complexes." University of Sydney, 2008. http://hdl.handle.net/2123/3533.

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Doctor of Philosophy (PhD)<br>This thesis is primarily concerned with the synthesis and reactions of iron and ruthenium dinitrogen complexes of tripodal phosphine ligands. Of particular interest is the cationic dinitrogen bridged iron complex [(FeH(PP3))2(μ-N2)]2+ 23, containing the tetradentate ligand P(CH2CH2PMe2)3, PP3 1, and its potential for facilitating the reduction of the bound dinitrogen upon treatment with acid. The synthesis of a selection of novel and known tripodal phosphine and amino phosphine ligands is described. New ligands N(CH2CH2CH2PMe2)3 N3P3 7 and P(CH2CH2CH2PiPr2)3 P3Pi3

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35

Humphries, Kristina. "Synthesis and reactivity of chiral ferrocene complexes." Thesis, Keele University, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.265643.

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36

Peatt, Anna C. (Anna Clare-Doreen) 1976. "New reaction media for organometallic chemistry." Monash University, School of Chemistry, 2003. http://arrow.monash.edu.au/hdl/1959.1/5829.

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37

Zhang, Fan. "Synthesis of organometallic foldamers and cyclopropene alpha-amino acids." Access to citation, abstract and download form provided by ProQuest Information and Learning Company; downloadable PDF file, 211 p, 2006. http://proquest.umi.com/pqdweb?did=1172109511&sid=6&Fmt=2&clientId=8331&RQT=309&VName=PQD.

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38

Saberi, Stephen Philip. "The synthesis, characterisation and photochemistry of novel organometallic complexes." Thesis, University of Central Lancashire, 1990. http://clok.uclan.ac.uk/20983/.

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Complexation of an organic ligand by a transition metal can radically alter the ligand photochemistry. In order to investigate these effects, we synthesised a series of organometallic complexes with several different modes of ligand-metal bonding. The synthesis of various cyclopentadienyl, arene, diene and enone complexes was attempted. Novel ferrocenyl fulgides, including several methoxy-substituted analogues were synthesised, and have been shown to display E/Z-photoisomerism. In contrast with the report by McVey et al,81 we showed that methoxyferrocene would not Friedel-Crafts acetylate in t

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39

Tudor, Jonathan Simon. "Synthesis and catalytic activity of organometallic-inorganic composite materials." Thesis, University of Oxford, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.339188.

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40

Aguirre, Etcheverry Paulina Loreto. "The synthesis and characterisation of new homobimetallic organometallic complexes." Thesis, University of Oxford, 2008. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.496818.

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41

Hart, Suzanne L. "Synthesis and applications of chiral-at-titanium organometallic compounds." Thesis, University of Warwick, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.245941.

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42

Zeng, Renqiang. "The synthesis, characterization and properties of new organometallic polymers." Master's thesis, University of Cape Town, 1996. http://hdl.handle.net/11427/26231.

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We have reviewed recent work on highly branched polymers called dendrimers. Two novel block copolymers consisting of organoruthenium dendritic wedges and linear polyethylene glycol blocks have been prepared. These new block copolymers have been characterized by IR, ¹H and ¹³C NMR, microanalysis, as well as size exclusion chromatography. The SEC results of some very large organoruthenium dendrimers are also discussed. The thermal properties of these block copolymers have been studied by differential scanning calorimetry and thermogravimetric analysis. The morphology of these block copolymers ha

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43

Skilbeck, Melanie C. "Synthesis of substituted nitriles and indoxyls using organometallic reagents." Thesis, University of Sheffield, 2013. http://etheses.whiterose.ac.uk/4652/.

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44

Webb, Samantha Jane. "The synthesis of functionalized polysilanes for microlithographic applications." Thesis, University of Kent, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.240671.

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45

Dolby, P. A. "Synthesis and reactivity of unsaturated triosmium carbonyl clusters." Thesis, University of Liverpool, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.233836.

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46

Kamarudin, R. A. "The synthesis and study of some haxanuclear clusters." Thesis, University of Cambridge, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.233257.

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47

Cloete, Jezreel. "Synthesis and applications of functionalized pyridinyl imine complexes of palladium." Thesis, University of the Western Cape, 2005. http://etd.uwc.ac.za/index.php?module=etd&amp.

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The synthesis and characterization of pyridinyl &alpha<br>-diimine Pd(II) complexes having a functionalized hydrocarbon attached to the imino nitrogen was performed. The catalytic activity of these complexes were then evaluated in the polymerization of ethylene and in the Heck coupling reaction of methyl acrylate with iodobenzene.<br /> <br /> Unconjugated &beta<br>-diimine complexes of palladium were also synthesized and their activities towards ethylene polymerization and the Heck coupling of methyl acrylate and iodobenzene also evaluated and compared to that of the &alpha<br>-diimine comple

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48

Buffet, Jean-Charles. "Homochiral metal complexes for biodegradable polymer synthesis." Thesis, University of Edinburgh, 2010. http://hdl.handle.net/1842/4618.

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Chapter One introduces the principle of alkoxide and phosphine oxide as ligands for lanthanides and electropositive metals, ligand self-recognition, stereoselective polymerisation of lactide, fixation of CO2 and finally copolymerisation of CO2 and epoxide. Chapter Two shows the synthesis of the proligands rac-HLR (a racemic phosphine oxide-alkoxide, A, where R = tBu, Ph or C6H3-Me-3,5) and explores the resolution into diastereomeric RRR- and SSS-M(LR)3 to afford C3–symmetric M(LR)3 complexes, B (where M = Sc, Lu, Y, In, Bi or La). It also demonstrates that the process is under thermodynamic co

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49

Callahan, Ryan Patrick. "The synthesis of perfluorinated compounds by direct fluorination organometallic compounds and carboranes /." Access restricted to users with UT Austin EID Full text (PDF) from UMI/Dissertation Abstracts International, 2001. http://wwwlib.umi.com/cr/utexas/fullcit?p3036160.

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50

Sharp, William Brett. "Synthesis and ligand reactivity of group 6 organometallic nitrosyl complexes." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2001. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp04/NQ61173.pdf.

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