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Journal articles on the topic 'Organometallic synthesis'

Author: Grafiati

Published: 4 June 2021

Last updated: 8 June 2024

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1

Khalid, Maher, and Shireen Mohammedand Amin Kalo. "Recent Developments in Weinreb Synthesis and Their Applications." Oriental Journal of Chemistry 35, no. 6 (December 23, 2019): 1611–26. http://dx.doi.org/10.13005/ojc/350601.

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N-methoxy-N-methyl amides or Weinreb amides are worthy embranchment of amide group and their rich functional groups in organic synthesis become a strong else unfeasible conversion. Weinreb amides are produced as an intermediate product of the reaction of carboxylic acids, acid chloride or esters with organometallic reagents, which was first uncovered in 1981. The direct conversion of carboxylic acids or acid chlorides or esters to ketones or aldehydes using organometallic reagents do not lead in high yields, because the intermediate ketones are still highly reactive toward the organometallic reagent. However, after derivatization to the corresponding Weinreb Amide, reaction with organometallics does give the desired ketones, as the initial adduct is stabilized and doesn't undergo further reactions. A nucleophilic addition to the Weinreb amides results in a unique and stable five-membered cyclic tetrahedral intermediate which protects the over-addition, leading to a selective conversion.

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2

Laine, Richard M. "Transition Metal Catalysed Synthesis of Oligo- and Polysilazanes." Platinum Metals Review 32, no. 2 (April 1, 1988): 64–71. http://dx.doi.org/10.1595/003214088x3226471.

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Organometallic polymer research offers many potential academic and industrial rewards because of the number of elemental variations possible. Unfortunately, there are no general synthetic methods as found for carbon based polymers. Transition metal catalysed dehydrocoupling reactions may prove to be generally applicable to the synthesis of silicon based organometallic polymers. We report here our efforts to synthesise organometallic polymers with a silicon-nitrogen backbone, polysilazanes, using the dehydrocoupling reaction. We also describe the synthesis of polysilazanes for use as precursors to silicon nitride.

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3

Dong, Zhi-Bing, and Jin-Quan Chen. "Recent Progress in Utilization of Functionalized Organometallic Reagents in Cross Coupling Reactions and Nucleophilic Additions." Synthesis 52, no. 24 (November 4, 2020): 3714–34. http://dx.doi.org/10.1055/s-0040-1706550.

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AbstractOrganometallic compounds have become increasingly important in organic synthesis because of their high chemoselectivity and excellent reactivity. Recently, a variety of organometallic reagents were found to facilitate transition-metal-catalyzed cross-coupling reactions and nucleophilic addition reactions. Here, we have summarized the latest progress in cross-coupling reactions and in nucleophilic addition reactions with functionalized organometallic reagents present to illustrate their application value. Due to the tremendous contribution made by the Knochel group towards the development of novel organometallic reagents, this review draws extensively from their work in this area in recent years.Introduction1 Transition-Metal-Catalyzed Cross Couplings Involving Organozinc Reagents2 Transition-Metal-Catalyzed Cross Couplings Involving Organomagnesium Reagents3 Transition-Metal-Free Cross Couplings Involving Zn and Mg Organometallic Reagents4 Nucleophilic Additions Involving Zn and Mg Organometallic Reagents5 Cross-Coupling Reactions or Nucleophilic Additions Involving Mn, Al-, La-, Li-, Sm- and In-Organometallics6 Conclusion

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4

Asaad, Noora, Ahmed Z. M. AL-Bassam, and Sahar S. M. Alabdullah. "Uses of organometallic compounds in chemical processes." International Journal of Research in Engineering and Innovation 06, no. 02 (2022): 98–103. http://dx.doi.org/10.36037/ijrei.2022.6203.

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This review is proposed to address knowledge of organometallic compounds (OMC) in chemical applications and show these compounds' depth scope in different scientific studies. This review is based on outlining the gap between the traditional preparations and green chemistry synthesis of organometallic materials purposes in the experimental section of a researcher's papers. The most comparative research considers the drawbacks of organometallic compounds, including their applications in industrial, clinical, drug forms, and chemical reactions. However, many organometallic compounds are inherently poisonous. The most general challenge is producing alternative substances to creative green organometallic compounds, specifically in drug formulations systems. A wide range of chemical reactions have been investigated and formulated new organometallic properties this may be associated with an increased level of enhancement health systems. This study aims to determine the importance of organometallic compound in many path ways in various articles and confirmed how papers trying to characterize new organometallic substances in various chemical processes. Particular interest is given to knowledge synthesis OMC in medicine and industrially.

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5

AMIENS, C., and B. CHAUDRET. "ORGANOMETALLIC SYNTHESIS OF NANOPARTICLES." Modern Physics Letters B 21, no. 18 (August 10, 2007): 1133–41. http://dx.doi.org/10.1142/s0217984907013833.

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Nanoparticles can be synthesized from metal-organic or organometallic precursors, either by classical thermal decomposition, ultrasound activation, photolysis as well as hydrogenation or hydrolysis reactions. The size, size distribution and more importantly surface state of these nanoparticles are much better controlled than when they are produced by chemical or electrochemical reduction of metal salts. Hence, metal or oxide nanoparticles can be obtained that are suitable for fundamental physics at the nanoscale, especially for magnetic studies. This is currently of particular interest as many applications require systems of still smaller sizes, the properties of which are not yet fully understood.

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6

Smith, Amos B., Melean Visnick, John N. Haseltine, and Paul A. Sprengeler. "Organometallic reagents in synthesis." Tetrahedron 42, no. 11 (January 1986): 2957–69. http://dx.doi.org/10.1016/s0040-4020(01)90586-1.

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7

Hanson, J. R. "Organometallic reagents in synthesis." Journal of Organometallic Chemistry 493, no. 1-2 (May 1995): C29. http://dx.doi.org/10.1016/0022-328x(95)90879-j.

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8

Heinze, Katja. "Solid-Phase Organometallic Synthesis." Chemistry - A European Journal 7, no. 13 (July 2, 2001): 2922–32. http://dx.doi.org/10.1002/1521-3765(20010702)7:13<2922::aid-chem2922>3.0.co;2-m.

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9

Rightmire, Nicholas R., and Timothy P. Hanusa. "Advances in organometallic synthesis with mechanochemical methods." Dalton Transactions 45, no. 6 (2016): 2352–62. http://dx.doi.org/10.1039/c5dt03866a.

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Mechanochemical methods of synthesis (specifically grinding and milling) have not yet been widely used by organometallic chemists, but there is growing interest in their potential. This Perspective surveys recent developments in the field, describing the outcomes of organometallic reactions conducted in the absence of solvents.

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10

Burton, Donald J., and Zhen-Yu Yang. "Fluorinated organometallics: Perfluoroalkyl and functionalized perfluoroalkyl organometallic reagents in organic synthesis." Tetrahedron 48, no. 2 (1992): 189–275. http://dx.doi.org/10.1016/s0040-4020(01)88139-4.

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11

Hiyama, Tamejiro. "Activation of stable σ-bonds for organic synthesis." Pure and Applied Chemistry 86, no. 3 (March 20, 2014): 299–306. http://dx.doi.org/10.1515/pac-2014-5031.

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Abstract Since the conference on Organometallic Chemisrty Directed Towards Organic Synthesis (OMCOS) started in 1981, the author has been involved in the invention of novel synthetic reactions for C–C bond formation, taking advantage of organometallic reagents and catalysis. Herein is described a guideline story of how it is done.

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12

Chan, T. H., C. J. Li, M. C. Lee, and Z. Y. Wei. "1993 R.U. Lemieux Award Lecture Organometallic-type reactions in aqueous media—a new challenge in organic synthesis." Canadian Journal of Chemistry 72, no. 5 (May 1, 1994): 1181–92. http://dx.doi.org/10.1139/v94-151.

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The development of organometallic-type reactions in aqueous media is reviewed. Coupling reactions of allyl halides with carbonyl compounds mediated by zinc, or tin, or indium in aqueous media to give homoallylic alcohols are discussed. The stereochemical outcome is compared with similar reactions in organic solvents. A concise synthesis of (+)-muscarine is used to illustrate the usefulness of aqueous organometallic-type reactions in organic synthesis. The procedure to protect–deprotect hydroxy functional groups may not be necessary in these reactions. An application in the carbohydrate area is demonstrated with the synthesis of (+)-3-deoxy-D-glycero-D-galacto-nonulosonic acid (KDN). The mechanistic possibilities of organometallic-type reactions in aqueous media are outlined.

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13

Boyt, Stuart M., Niko A. Jenek, and Ulrich Hintermair. "Synthesis of organometallic pentalenide complexes." Dalton Transactions 48, no. 16 (2019): 5107–24. http://dx.doi.org/10.1039/c9dt00689c.

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14

Tang, Jian, and Liang Zhao. "Polynuclear organometallic clusters: synthesis, structure, and reactivity studies." Chemical Communications 56, no. 13 (2020): 1915–25. http://dx.doi.org/10.1039/c9cc09354k.

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15

TOKUDA, Masao. "Organometallic compounds in electroorganic synthesis." Journal of Synthetic Organic Chemistry, Japan 43, no. 6 (1985): 522–32. http://dx.doi.org/10.5059/yukigoseikyokaishi.43.522.

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16

Birch, Arthur J., Brian Chauncy, Lawrence F. Kelly, and David J. Thompson. "Organometallic compounds in organic synthesis." Journal of Organometallic Chemistry 286, no. 1 (April 1985): 37–46. http://dx.doi.org/10.1016/0022-328x(85)87233-8.

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17

Chakravorty, D. "Organometallic route to nanocomposite synthesis." Sadhana 13, no. 1-2 (July 1988): 13–18. http://dx.doi.org/10.1007/bf02811955.

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18

Tang, Jing, Franz Redl, Yimei Zhu, Theo Siegrist, Louis E. Brus, and Michael L. Steigerwald. "An Organometallic Synthesis of TiO2Nanoparticles." Nano Letters 5, no. 3 (March 2005): 543–48. http://dx.doi.org/10.1021/nl047992h.

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19

Rodríguez-Álvarez, María Jesús, Nicolás Ríos-Lombardía, Sergio E. García-Garrido, Carmen Concellón, Vicente del Amo, Vito Capriati, and Joaquín García-Álvarez. "Recent Advancements in the Utilization of s-Block Organometallic Reagents in Organic Synthesis with Sustainable Solvents." Molecules 29, no. 7 (March 22, 2024): 1422. http://dx.doi.org/10.3390/molecules29071422.

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This mini-review offers a comprehensive overview of the advancements made over the last three years in utilizing highly polar s-block organometallic reagents (specifically, RLi, RNa and RMgX compounds) in organic synthesis run under bench-type reaction conditions. These conditions involve exposure to air/moisture and are carried out at room temperature, with the use of sustainable solvents as reaction media. In the examples provided, the adoption of Deep Eutectic Solvents (DESs) or even water as non-conventional and protic reaction media has not only replicated the traditional chemistry of these organometallic reagents in conventional and toxic volatile organic compounds under Schlenk-type reaction conditions (typically involving low temperatures of −78 °C to 0 °C and a protective atmosphere of N2 or Ar), but has also resulted in higher conversions and selectivities within remarkably short reaction times (measured in s/min). Furthermore, the application of the aforementioned polar organometallics under bench-type reaction conditions (at room temperature/under air) has been extended to other environmentally responsible reaction media, such as more sustainable ethereal solvents (e.g., CPME or 2-MeTHF). Notably, this innovative approach contributes to enhancing the overall sustainability of s-block-metal-mediated organic processes, thereby aligning with several key principles of Green Chemistry.

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20

Law, Chung-kay Edwin, and István T. Horváth. "Synthesis and applications of fluorous phosphines." Organic Chemistry Frontiers 3, no. 8 (2016): 1048–62. http://dx.doi.org/10.1039/c6qo00115g.

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21

Cannadine, Jason, Andrew Hector, and Anthony F. Hill. "Organometallic macrocycle chemistry. 2. Synthesis of organometallic (trithiacyclononane)ruthenium(II) complexes." Organometallics 11, no. 7 (July 1992): 2323–24. http://dx.doi.org/10.1021/om00043a001.

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22

Cloke, F. Geoffrey N. "Organometallic pentalene complexes." Pure and Applied Chemistry 73, no. 2 (January 1, 2001): 233–38. http://dx.doi.org/10.1351/pac200173020233.

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There has been a recent renaissance in the organometallic chemistry of pentalene, following the discovery of the first complexes incorporating pentalene η8-ligated to a single metal center. This short review outlines recent work in the author's laboratory on the preparation of silylated pentalene ligands and the subsequent synthesis of novel, monometallic, and bimetallic pentalene sandwich and half-sandwich complexes of the f- and d-block elements.

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23

Mistryukov, �. A., and I. K. Korshevits. "Organometallic synthesis in aqueous media. Synthesis of vinylallylcarbinols." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 35, no. 11 (November 1986): 2396–97. http://dx.doi.org/10.1007/bf00953369.

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24

Zafar, Ayesha, China Takeda, Asif Manzoor, Daiki Tanaka, Masashi Kobayashi, Yoshitora Wadayama, Daisuke Nakane, Adnan Majeed, Muhammad Adnan Iqbal, and Takashiro Akitsu. "Towards Industrially Important Applications of Enhanced Organic Reactions by Microfluidic Systems." Molecules 29, no. 2 (January 13, 2024): 398. http://dx.doi.org/10.3390/molecules29020398.

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This review presents a comprehensive evaluation for the manufacture of organic molecules via efficient microfluidic synthesis. Microfluidic systems provide considerably higher control over the growth, nucleation, and reaction conditions compared with traditional large-scale synthetic methods. Microfluidic synthesis has become a crucial technique for the quick, affordable, and efficient manufacture of organic and organometallic compounds with complicated characteristics and functions. Therefore, a unique, straightforward flow synthetic methodology can be developed to conduct organic syntheses and improve their efficiency.

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25

Ma, Li-Li, Jia-Qin Han, Wei-Guo Jia, and Ying-Feng Han. "Coordination-driven self-assembly vs dynamic covalent chemistry: versatile methods for the synthesis of molecular metallarectangles." Beilstein Journal of Organic Chemistry 14 (August 3, 2018): 2027–34. http://dx.doi.org/10.3762/bjoc.14.178.

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Supramolecular coordination assemblies have a range of potential applications in chemical and biological sciences. Herein, simple modular methods for the synthesis of metallarectangles are described. The desired tetranuclear metallarectangles were synthesized by using coordination-driven self-assembly of half-sandwich rhodium-based organometallic clip units and organic ligands. The reaction of such an organometallic clip with 4-formylpyridine provided a dinuclear molecular tweezer with pendant aldehyde groups, and subsequent [4 + 4] condensation reactions with diamines provides another route to the target metallarectangles in good yields. The same assemblies can also be easily isolated in one-pot procedures by mixing the organometallic clip, diamines and 4-formylpyridine.

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26

Peters, David W., and Richard G. Blair. "Mechanochemical synthesis of an organometallic compound: a high volume manufacturing method." Faraday Discuss. 170 (2014): 83–91. http://dx.doi.org/10.1039/c3fd00157a.

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Chemical vapor deposition (CVD) precursor chemicals are held to some of the highest purity levels in industry. Many metal reagents form stable, unbreakable adducts with the coordinating solvents that are necessary for solvating highly polar reagents. These adducts are undesirable and must be removed prior to usage. Herein we describe a mechanochemical approach to the synthesis of bis(n-propyltetramethylcyclopentadienyl)strontium that eliminates the use of strongly coordinating solvents. This method overcomes the solubility problems of the two reagents without the formation of stable, unbreakable adducts. We utilize a unique reactor geometry that facilitates mechanochemical syntheses while simplifying handling and allowing for “one pot” production. The synthesis was scaled to five hundred gram lot sizes in a six liter reactor. This technique is applicable to many syntheses and is linearly scalable – limited only by reactor size.

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27

Cademartiri, Ludovico, and Geoffrey A. Ozin. "Emerging strategies for the synthesis of highly monodisperse colloidal nanostructures." Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences 368, no. 1927 (September 28, 2010): 4229–48. http://dx.doi.org/10.1098/rsta.2010.0126.

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This short perspective describes recent developments in the synthesis of nanoscale colloids from sparingly soluble precursors. These strategies, which we dubbed ‘heterogeneous nanocrystal syntheses’ owing to the presence of a precursor in a non-colloidal solid state, have demonstrated the ability to generate new colloidal shapes, a superior monodispersity and a remarkable ability to delay the onset of Ostwald ripening, when compared with more traditional and purely colloidal strategies. We review the key contributions to this emerging area of research and discuss in detail the remarkable number of differences between these syntheses and the widely used homogeneous organometallic syntheses for making nanoscale colloids.

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28

BURTON, D. J., and Z. Y. YANG. "ChemInform Abstract: Fluorinated Organometallics: Perfluoroalkyl and Functionalized Perfluoroalkyl Organometallic Reagents in Organic Synthesis." ChemInform 23, no. 17 (August 22, 2010): no. http://dx.doi.org/10.1002/chin.199217330.

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29

Ding, Aishun, Marta Meazza, Hao Guo, Jung Woon Yang, and Ramon Rios. "New development in the enantioselective synthesis of spiro compounds." Chemical Society Reviews 47, no. 15 (2018): 5946–96. http://dx.doi.org/10.1039/c6cs00825a.

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30

Graden, H., and N. Kann. "Solid Phase Synthesis Using Organometallic Reagents." Current Organic Chemistry 9, no. 8 (May 1, 2005): 733–63. http://dx.doi.org/10.2174/1385272053764962.

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31

Storozhenko, P. A., A. A. Grachev, A. O. Klochkov, and V. I. Shiryaev. "Continuous organomagnesium synthesis of organometallic compounds." Russian Journal of Applied Chemistry 86, no. 3 (March 2013): 387–93. http://dx.doi.org/10.1134/s1070427213030166.

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32

Gedye, R., F. Smith, and K. Westaway. "Microwaves in Organic and Organometallic Synthesis." Journal of Microwave Power and Electromagnetic Energy 26, no. 1 (January 1991): 3–17. http://dx.doi.org/10.1080/08327823.1991.11688134.

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33

Degennaro, Leonardo, Claudia Carlucci, Sonia De Angelis, and Renzo Luisi. "Flow technology for organometallic-mediated synthesis." Journal of Flow Chemistry 6, no. 3 (September 2016): 136–66. http://dx.doi.org/10.1556/1846.2016.00014.

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34

NAKAJIMA, Atsushi. "Laser Synthesis of Organometallic Sandwich Nanowires." Kobunshi 54, no. 2 (2005): 81. http://dx.doi.org/10.1295/kobunshi.54.81.

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35

Fallis, Alex G., Pat Forgione, Simon Woo, Stephanie Legoupy, Sandrine Py, Curtis Harwig, and Tanya Rietveld. "Organometallic reagents and protocols for synthesis." Polyhedron 19, no. 5 (March 2000): 533–35. http://dx.doi.org/10.1016/s0277-5387(99)00402-7.

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36

Krause, Norbert, and Anja Hoffmann-Röder. "Synthesis of allenes with organometallic reagents." Tetrahedron 60, no. 51 (December 2004): 11671–94. http://dx.doi.org/10.1016/j.tet.2004.09.094.

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37

Toste, F. Dean. "Asymmetric Synthesis Enabled by Organometallic Complexes." Organometallics 38, no. 20 (October 28, 2019): 3899–901. http://dx.doi.org/10.1021/acs.organomet.9b00627.

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38

Cai, Xiaolei, Ruoyu Zhan, Guangxue Feng, and Bin Liu. "Organometallic Conjugated Polyelectrolytes: Synthesis and Applications." Journal of Inorganic and Organometallic Polymers and Materials 25, no. 1 (October 5, 2014): 27–36. http://dx.doi.org/10.1007/s10904-014-0093-1.

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39

Nomura, Mitsushiro, Fumiaki Imamura, Nguyen Ba Tuyet Nga, Chikako Fujita-Takayama, Toru Sugiyama, and Masatsugu Kajitani. "Synthesis and Electrochemistry of Organometallic Cobaltadithiaazulenes." Inorganic Chemistry 51, no. 20 (October 2012): 10695–703. http://dx.doi.org/10.1021/ic300993a.

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40

de Frémont, Pierre, Nicolas Marion, and Steven P. Nolan. "Carbenes: Synthesis, properties, and organometallic chemistry." Coordination Chemistry Reviews 253, no. 7-8 (April 2009): 862–92. http://dx.doi.org/10.1016/j.ccr.2008.05.018.

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41

Schwartz, J., G. M. Arvanitis, J. A. Smegel, I. K. Meier, S. M. Clift, and D. Van Engen. "New organometallic reagents for olefin synthesis." Pure and Applied Chemistry 60, no. 1 (January 1, 1988): 65–70. http://dx.doi.org/10.1351/pac198860010065.

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42

Noyori, R., M. Uchiyama, H. Kato, S. Wakabayashi, and Y. Hayakawa. "Organometallic methodologies for nucleic acid synthesis." Pure and Applied Chemistry 62, no. 4 (January 1, 1990): 613–22. http://dx.doi.org/10.1351/pac199062040613.

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43

Beletskaya, I. P. "Organometallic compounds in synthesis and catalysis." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 39, no. 10 (October 1990): 2013–28. http://dx.doi.org/10.1007/bf01557731.

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44

Abbott, Julia K. C., Brenda A. Dougan, and Zi-Ling Xue. "ChemInform Abstract: Synthesis of Organometallic Compounds." ChemInform 42, no. 23 (May 12, 2011): no. http://dx.doi.org/10.1002/chin.201123214.

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45

MANCHAND, P. S. "ChemInform Abstract: Carotenoid Synthesis. Organometallic Reactions." ChemInform 28, no. 2 (August 4, 2010): no. http://dx.doi.org/10.1002/chin.199702261.

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46

Da Pian, M., O. De Lucchi, G. Strukul, F. Fabris, and A. Scarso. "Cation templated improved synthesis of pillar[6]arenes." RSC Advances 6, no. 54 (2016): 48272–75. http://dx.doi.org/10.1039/c6ra07164c.

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Improved high yield syntheses of the larger pillar[6]arenes (P[6]) bearing different alkoxy substituents through cation templated syntheses using a series of small organic and organometallic cations is reported.

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47

Farinola, Gianluca M., Francesco Babudri, Antonio Cardone, Omar Hassan Omar, Carmela Martinelli, Francesco Naso, Vita Pinto, and Roberta Ragni. "Synthesis of Fluorinated Organic and Organometallic Electroluminescent Materials: Tuning Emission in the Blue." Advances in Science and Technology 75 (October 2010): 108–17. http://dx.doi.org/10.4028/www.scientific.net/ast.75.108.

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Functionalization with fluorine atoms represents a versatile structural modification to finely tune both the emission colour and the electronic properties of organic and organometallic electroluminescent compounds. This paper reports an overview of our systematic investigation on the design and synthesis of the fluorinated version of two important classes of materials for organic light emitting diodes (OLEDs), namely poly(arylenevinylene)s and phosphorescent phenylpyridine Iridium complexes. Synthetic pathways based on organometallic methodologies affording selectively fluorinated molecular structures will be discussed together with a summary of the effect of fluorination on the optical properties of the resulting materials. In particular we will highlight the possibilities offered by the organometallic methodologies as straightforward and resourceful tools to provide a wide series of fluorinated molecular architectures with high regio- and stereoselectivity, mild experimental conditions and good yields.

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48

Liang, Guodong, Xiaodong Li, Suping Bao, Haiyang Gao, Fangming Zhu, and Qing Wu. "Large-scale synthesis of organometallic polymer flowers with ultrathin petals for hydrogen peroxide sensing." Polymer Chemistry 6, no. 24 (2015): 4447–54. http://dx.doi.org/10.1039/c5py00382b.

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49

Simi, N. J., Libin Kuriakose, R. Vinayakan, and V. V. Ison. "CuInS2–In2Se3 quantum dots – a novel material via a green synthesis approach." RSC Advances 8, no. 65 (2018): 37146–50. http://dx.doi.org/10.1039/c8ra07389a.

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50

Bunzen, Hana, Maciej Grzywa, Andreas Kalytta-Mewes, and Dirk Volkmer. "One-pot synthesis of ultrastable pentanuclear alkylzinc complexes." Dalton Transactions 46, no. 8 (2017): 2618–25. http://dx.doi.org/10.1039/c6dt04778e.

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