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Journal articles on the topic 'Organometallic synthesis'

Author: Grafiati

Published: 4 June 2021

Last updated: 25 July 2025

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1

Khalid, Maher, and Shireen Mohammedand Amin Kalo. "Recent Developments in Weinreb Synthesis and Their Applications." Oriental Journal of Chemistry 35, no. 6 (2019): 1611–26. http://dx.doi.org/10.13005/ojc/350601.

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N-methoxy-N-methyl amides or Weinreb amides are worthy embranchment of amide group and their rich functional groups in organic synthesis become a strong else unfeasible conversion. Weinreb amides are produced as an intermediate product of the reaction of carboxylic acids, acid chloride or esters with organometallic reagents, which was first uncovered in 1981. The direct conversion of carboxylic acids or acid chlorides or esters to ketones or aldehydes using organometallic reagents do not lead in high yields, because the intermediate ketones are still highly reactive toward the organometallic r

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2

Laine, Richard M. "Transition Metal Catalysed Synthesis of Oligo- and Polysilazanes." Platinum Metals Review 32, no. 2 (1988): 64–71. http://dx.doi.org/10.1595/003214088x3226471.

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Organometallic polymer research offers many potential academic and industrial rewards because of the number of elemental variations possible. Unfortunately, there are no general synthetic methods as found for carbon based polymers. Transition metal catalysed dehydrocoupling reactions may prove to be generally applicable to the synthesis of silicon based organometallic polymers. We report here our efforts to synthesise organometallic polymers with a silicon-nitrogen backbone, polysilazanes, using the dehydrocoupling reaction. We also describe the synthesis of polysilazanes for use as precursors

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3

Dong, Zhi-Bing, and Jin-Quan Chen. "Recent Progress in Utilization of Functionalized Organometallic Reagents in Cross Coupling Reactions and Nucleophilic Additions." Synthesis 52, no. 24 (2020): 3714–34. http://dx.doi.org/10.1055/s-0040-1706550.

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AbstractOrganometallic compounds have become increasingly important in organic synthesis because of their high chemoselectivity and excellent reactivity. Recently, a variety of organometallic reagents were found to facilitate transition-metal-catalyzed cross-coupling reactions and nucleophilic addition reactions. Here, we have summarized the latest progress in cross-coupling reactions and in nucleophilic addition reactions with functionalized organometallic reagents present to illustrate their application value. Due to the tremendous contribution made by the Knochel group towards the developme

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4

Lewis, David E. "The beginnings of synthetic organic chemistry: Zinc alkyls and the Kazan' school." Bulletin for the History of Chemistry 27, no. 1 (2002): 37–42. https://doi.org/10.70359/bhc2002v027p037.

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The rise of organometallic compds. as tools in org. synthesis is probably best traced to the development of the Grignard addn. reaction in 1900 but the real origins of organometallic synthesis date from some 30 yr earlier in the city of Kazan' at European Russia's eastern frontier. Modern org. synthesis would be inconceivable without the formation of carbon-carbon bonds by the reaction between an organometallic reagent and a carbonyl compd. Thus, modern org. synthesis owes a great debt, to the chemists at Kazan' University and their pioneering chem. with zinc alkyls.

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5

Asaad, Noora, Ahmed Z. M. AL-Bassam, and Sahar S. M. Alabdullah. "Uses of organometallic compounds in chemical processes." International Journal of Research in Engineering and Innovation 06, no. 02 (2022): 98–103. http://dx.doi.org/10.36037/ijrei.2022.6203.

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This review is proposed to address knowledge of organometallic compounds (OMC) in chemical applications and show these compounds' depth scope in different scientific studies. This review is based on outlining the gap between the traditional preparations and green chemistry synthesis of organometallic materials purposes in the experimental section of a researcher's papers. The most comparative research considers the drawbacks of organometallic compounds, including their applications in industrial, clinical, drug forms, and chemical reactions. However, many organometallic compounds are inherentl

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6

AMIENS, C., and B. CHAUDRET. "ORGANOMETALLIC SYNTHESIS OF NANOPARTICLES." Modern Physics Letters B 21, no. 18 (2007): 1133–41. http://dx.doi.org/10.1142/s0217984907013833.

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Nanoparticles can be synthesized from metal-organic or organometallic precursors, either by classical thermal decomposition, ultrasound activation, photolysis as well as hydrogenation or hydrolysis reactions. The size, size distribution and more importantly surface state of these nanoparticles are much better controlled than when they are produced by chemical or electrochemical reduction of metal salts. Hence, metal or oxide nanoparticles can be obtained that are suitable for fundamental physics at the nanoscale, especially for magnetic studies. This is currently of particular interest as many

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7

Smith, Amos B., Melean Visnick, John N. Haseltine, and Paul A. Sprengeler. "Organometallic reagents in synthesis." Tetrahedron 42, no. 11 (1986): 2957–69. http://dx.doi.org/10.1016/s0040-4020(01)90586-1.

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8

Hanson, J. R. "Organometallic reagents in synthesis." Journal of Organometallic Chemistry 493, no. 1-2 (1995): C29. http://dx.doi.org/10.1016/0022-328x(95)90879-j.

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9

Heinze, Katja. "Solid-Phase Organometallic Synthesis." Chemistry - A European Journal 7, no. 13 (2001): 2922–32. http://dx.doi.org/10.1002/1521-3765(20010702)7:13<2922::aid-chem2922>3.0.co;2-m.

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10

Rightmire, Nicholas R., and Timothy P. Hanusa. "Advances in organometallic synthesis with mechanochemical methods." Dalton Transactions 45, no. 6 (2016): 2352–62. http://dx.doi.org/10.1039/c5dt03866a.

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Mechanochemical methods of synthesis (specifically grinding and milling) have not yet been widely used by organometallic chemists, but there is growing interest in their potential. This Perspective surveys recent developments in the field, describing the outcomes of organometallic reactions conducted in the absence of solvents.

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11

Burton, Donald J., and Zhen-Yu Yang. "Fluorinated organometallics: Perfluoroalkyl and functionalized perfluoroalkyl organometallic reagents in organic synthesis." Tetrahedron 48, no. 2 (1992): 189–275. http://dx.doi.org/10.1016/s0040-4020(01)88139-4.

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12

Chan, T. H., C. J. Li, M. C. Lee, and Z. Y. Wei. "1993 R.U. Lemieux Award Lecture Organometallic-type reactions in aqueous media—a new challenge in organic synthesis." Canadian Journal of Chemistry 72, no. 5 (1994): 1181–92. http://dx.doi.org/10.1139/v94-151.

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The development of organometallic-type reactions in aqueous media is reviewed. Coupling reactions of allyl halides with carbonyl compounds mediated by zinc, or tin, or indium in aqueous media to give homoallylic alcohols are discussed. The stereochemical outcome is compared with similar reactions in organic solvents. A concise synthesis of (+)-muscarine is used to illustrate the usefulness of aqueous organometallic-type reactions in organic synthesis. The procedure to protect–deprotect hydroxy functional groups may not be necessary in these reactions. An application in the carbohydrate area is

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13

Hiyama, Tamejiro. "Activation of stable σ-bonds for organic synthesis". Pure and Applied Chemistry 86, № 3 (2014): 299–306. http://dx.doi.org/10.1515/pac-2014-5031.

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Abstract Since the conference on Organometallic Chemisrty Directed Towards Organic Synthesis (OMCOS) started in 1981, the author has been involved in the invention of novel synthetic reactions for C–C bond formation, taking advantage of organometallic reagents and catalysis. Herein is described a guideline story of how it is done.

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14

Boyt, Stuart M., Niko A. Jenek, and Ulrich Hintermair. "Synthesis of organometallic pentalenide complexes." Dalton Transactions 48, no. 16 (2019): 5107–24. http://dx.doi.org/10.1039/c9dt00689c.

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15

TOKUDA, Masao. "Organometallic compounds in electroorganic synthesis." Journal of Synthetic Organic Chemistry, Japan 43, no. 6 (1985): 522–32. http://dx.doi.org/10.5059/yukigoseikyokaishi.43.522.

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16

Birch, Arthur J., Brian Chauncy, Lawrence F. Kelly, and David J. Thompson. "Organometallic compounds in organic synthesis." Journal of Organometallic Chemistry 286, no. 1 (1985): 37–46. http://dx.doi.org/10.1016/0022-328x(85)87233-8.

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17

Chakravorty, D. "Organometallic route to nanocomposite synthesis." Sadhana 13, no. 1-2 (1988): 13–18. http://dx.doi.org/10.1007/bf02811955.

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18

Tang, Jing, Franz Redl, Yimei Zhu, Theo Siegrist, Louis E. Brus, and Michael L. Steigerwald. "An Organometallic Synthesis of TiO2Nanoparticles." Nano Letters 5, no. 3 (2005): 543–48. http://dx.doi.org/10.1021/nl047992h.

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19

Tang, Jian, and Liang Zhao. "Polynuclear organometallic clusters: synthesis, structure, and reactivity studies." Chemical Communications 56, no. 13 (2020): 1915–25. http://dx.doi.org/10.1039/c9cc09354k.

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20

Dieter, Enders, and Thiebes Christoph. "Enantioselective synthesis of both enantiomers of bgugaine employing the SAMP-hydrazone method." Journal of Indian Chemical Society Vol. 76, Nov-Dec 1999 (1999): 561–64. https://doi.org/10.5281/zenodo.5862094.

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Institut fur Organische Chemie, RWTH Aachen, Professor-Pirlet-Strasse 1 ,D-52074 Aachen, Germany <em>Manuscript received 20 August 1999</em> The synthesis of both enantiomers of bgugaine by 1,2-addition of organometallic reagents to aldehyde-SAMP-hydrazones, followed by N-N-bond cleavage and cyclization is described. The new method provides an entry into the preparation of enantiomerically pure 2-substituted pyrrolidines.

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21

Rodríguez-Álvarez, María Jesús, Nicolás Ríos-Lombardía, Sergio E. García-Garrido, et al. "Recent Advancements in the Utilization of s-Block Organometallic Reagents in Organic Synthesis with Sustainable Solvents." Molecules 29, no. 7 (2024): 1422. http://dx.doi.org/10.3390/molecules29071422.

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This mini-review offers a comprehensive overview of the advancements made over the last three years in utilizing highly polar s-block organometallic reagents (specifically, RLi, RNa and RMgX compounds) in organic synthesis run under bench-type reaction conditions. These conditions involve exposure to air/moisture and are carried out at room temperature, with the use of sustainable solvents as reaction media. In the examples provided, the adoption of Deep Eutectic Solvents (DESs) or even water as non-conventional and protic reaction media has not only replicated the traditional chemistry of the

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22

Law, Chung-kay Edwin, and István T. Horváth. "Synthesis and applications of fluorous phosphines." Organic Chemistry Frontiers 3, no. 8 (2016): 1048–62. http://dx.doi.org/10.1039/c6qo00115g.

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23

Cloke, F. Geoffrey N. "Organometallic pentalene complexes." Pure and Applied Chemistry 73, no. 2 (2001): 233–38. http://dx.doi.org/10.1351/pac200173020233.

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There has been a recent renaissance in the organometallic chemistry of pentalene, following the discovery of the first complexes incorporating pentalene η8-ligated to a single metal center. This short review outlines recent work in the author's laboratory on the preparation of silylated pentalene ligands and the subsequent synthesis of novel, monometallic, and bimetallic pentalene sandwich and half-sandwich complexes of the f- and d-block elements.

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24

Zafar, Ayesha, China Takeda, Asif Manzoor, et al. "Towards Industrially Important Applications of Enhanced Organic Reactions by Microfluidic Systems." Molecules 29, no. 2 (2024): 398. http://dx.doi.org/10.3390/molecules29020398.

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This review presents a comprehensive evaluation for the manufacture of organic molecules via efficient microfluidic synthesis. Microfluidic systems provide considerably higher control over the growth, nucleation, and reaction conditions compared with traditional large-scale synthetic methods. Microfluidic synthesis has become a crucial technique for the quick, affordable, and efficient manufacture of organic and organometallic compounds with complicated characteristics and functions. Therefore, a unique, straightforward flow synthetic methodology can be developed to conduct organic syntheses a

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25

Cannadine, Jason, Andrew Hector, and Anthony F. Hill. "Organometallic macrocycle chemistry. 2. Synthesis of organometallic (trithiacyclononane)ruthenium(II) complexes." Organometallics 11, no. 7 (1992): 2323–24. http://dx.doi.org/10.1021/om00043a001.

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26

Mistryukov, �. A., and I. K. Korshevits. "Organometallic synthesis in aqueous media. Synthesis of vinylallylcarbinols." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 35, no. 11 (1986): 2396–97. http://dx.doi.org/10.1007/bf00953369.

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27

Ma, Li-Li, Jia-Qin Han, Wei-Guo Jia, and Ying-Feng Han. "Coordination-driven self-assembly vs dynamic covalent chemistry: versatile methods for the synthesis of molecular metallarectangles." Beilstein Journal of Organic Chemistry 14 (August 3, 2018): 2027–34. http://dx.doi.org/10.3762/bjoc.14.178.

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Supramolecular coordination assemblies have a range of potential applications in chemical and biological sciences. Herein, simple modular methods for the synthesis of metallarectangles are described. The desired tetranuclear metallarectangles were synthesized by using coordination-driven self-assembly of half-sandwich rhodium-based organometallic clip units and organic ligands. The reaction of such an organometallic clip with 4-formylpyridine provided a dinuclear molecular tweezer with pendant aldehyde groups, and subsequent [4 + 4] condensation reactions with diamines provides another route t

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28

BURTON, D. J., and Z. Y. YANG. "ChemInform Abstract: Fluorinated Organometallics: Perfluoroalkyl and Functionalized Perfluoroalkyl Organometallic Reagents in Organic Synthesis." ChemInform 23, no. 17 (2010): no. http://dx.doi.org/10.1002/chin.199217330.

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29

Ding, Aishun, Marta Meazza, Hao Guo, Jung Woon Yang, and Ramon Rios. "New development in the enantioselective synthesis of spiro compounds." Chemical Society Reviews 47, no. 15 (2018): 5946–96. http://dx.doi.org/10.1039/c6cs00825a.

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30

Cademartiri, Ludovico, and Geoffrey A. Ozin. "Emerging strategies for the synthesis of highly monodisperse colloidal nanostructures." Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences 368, no. 1927 (2010): 4229–48. http://dx.doi.org/10.1098/rsta.2010.0126.

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This short perspective describes recent developments in the synthesis of nanoscale colloids from sparingly soluble precursors. These strategies, which we dubbed ‘heterogeneous nanocrystal syntheses’ owing to the presence of a precursor in a non-colloidal solid state, have demonstrated the ability to generate new colloidal shapes, a superior monodispersity and a remarkable ability to delay the onset of Ostwald ripening, when compared with more traditional and purely colloidal strategies. We review the key contributions to this emerging area of research and discuss in detail the remarkable numbe

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31

Peters, David W., and Richard G. Blair. "Mechanochemical synthesis of an organometallic compound: a high volume manufacturing method." Faraday Discuss. 170 (2014): 83–91. http://dx.doi.org/10.1039/c3fd00157a.

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Chemical vapor deposition (CVD) precursor chemicals are held to some of the highest purity levels in industry. Many metal reagents form stable, unbreakable adducts with the coordinating solvents that are necessary for solvating highly polar reagents. These adducts are undesirable and must be removed prior to usage. Herein we describe a mechanochemical approach to the synthesis of bis(n-propyltetramethylcyclopentadienyl)strontium that eliminates the use of strongly coordinating solvents. This method overcomes the solubility problems of the two reagents without the formation of stable, unbreakab

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32

Graden, H., and N. Kann. "Solid Phase Synthesis Using Organometallic Reagents." Current Organic Chemistry 9, no. 8 (2005): 733–63. http://dx.doi.org/10.2174/1385272053764962.

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33

Storozhenko, P. A., A. A. Grachev, A. O. Klochkov, and V. I. Shiryaev. "Continuous organomagnesium synthesis of organometallic compounds." Russian Journal of Applied Chemistry 86, no. 3 (2013): 387–93. http://dx.doi.org/10.1134/s1070427213030166.

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34

Gedye, R., F. Smith, and K. Westaway. "Microwaves in Organic and Organometallic Synthesis." Journal of Microwave Power and Electromagnetic Energy 26, no. 1 (1991): 3–17. http://dx.doi.org/10.1080/08327823.1991.11688134.

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35

Degennaro, Leonardo, Claudia Carlucci, Sonia De Angelis, and Renzo Luisi. "Flow technology for organometallic-mediated synthesis." Journal of Flow Chemistry 6, no. 3 (2016): 136–66. http://dx.doi.org/10.1556/1846.2016.00014.

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36

NAKAJIMA, Atsushi. "Laser Synthesis of Organometallic Sandwich Nanowires." Kobunshi 54, no. 2 (2005): 81. http://dx.doi.org/10.1295/kobunshi.54.81.

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37

Fallis, Alex G., Pat Forgione, Simon Woo, et al. "Organometallic reagents and protocols for synthesis." Polyhedron 19, no. 5 (2000): 533–35. http://dx.doi.org/10.1016/s0277-5387(99)00402-7.

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38

Krause, Norbert, and Anja Hoffmann-Röder. "Synthesis of allenes with organometallic reagents." Tetrahedron 60, no. 51 (2004): 11671–94. http://dx.doi.org/10.1016/j.tet.2004.09.094.

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39

Toste, F. Dean. "Asymmetric Synthesis Enabled by Organometallic Complexes." Organometallics 38, no. 20 (2019): 3899–901. http://dx.doi.org/10.1021/acs.organomet.9b00627.

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40

Cai, Xiaolei, Ruoyu Zhan, Guangxue Feng, and Bin Liu. "Organometallic Conjugated Polyelectrolytes: Synthesis and Applications." Journal of Inorganic and Organometallic Polymers and Materials 25, no. 1 (2014): 27–36. http://dx.doi.org/10.1007/s10904-014-0093-1.

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41

Nomura, Mitsushiro, Fumiaki Imamura, Nguyen Ba Tuyet Nga, Chikako Fujita-Takayama, Toru Sugiyama, and Masatsugu Kajitani. "Synthesis and Electrochemistry of Organometallic Cobaltadithiaazulenes." Inorganic Chemistry 51, no. 20 (2012): 10695–703. http://dx.doi.org/10.1021/ic300993a.

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42

de Frémont, Pierre, Nicolas Marion, and Steven P. Nolan. "Carbenes: Synthesis, properties, and organometallic chemistry." Coordination Chemistry Reviews 253, no. 7-8 (2009): 862–92. http://dx.doi.org/10.1016/j.ccr.2008.05.018.

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43

Schwartz, J., G. M. Arvanitis, J. A. Smegel, I. K. Meier, S. M. Clift, and D. Van Engen. "New organometallic reagents for olefin synthesis." Pure and Applied Chemistry 60, no. 1 (1988): 65–70. http://dx.doi.org/10.1351/pac198860010065.

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44

Noyori, R., M. Uchiyama, H. Kato, S. Wakabayashi, and Y. Hayakawa. "Organometallic methodologies for nucleic acid synthesis." Pure and Applied Chemistry 62, no. 4 (1990): 613–22. http://dx.doi.org/10.1351/pac199062040613.

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45

Beletskaya, I. P. "Organometallic compounds in synthesis and catalysis." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 39, no. 10 (1990): 2013–28. http://dx.doi.org/10.1007/bf01557731.

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46

Abbott, Julia K. C., Brenda A. Dougan, and Zi-Ling Xue. "ChemInform Abstract: Synthesis of Organometallic Compounds." ChemInform 42, no. 23 (2011): no. http://dx.doi.org/10.1002/chin.201123214.

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47

MANCHAND, P. S. "ChemInform Abstract: Carotenoid Synthesis. Organometallic Reactions." ChemInform 28, no. 2 (2010): no. http://dx.doi.org/10.1002/chin.199702261.

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48

Da Pian, M., O. De Lucchi, G. Strukul, F. Fabris, and A. Scarso. "Cation templated improved synthesis of pillar[6]arenes." RSC Advances 6, no. 54 (2016): 48272–75. http://dx.doi.org/10.1039/c6ra07164c.

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Improved high yield syntheses of the larger pillar[6]arenes (P[6]) bearing different alkoxy substituents through cation templated syntheses using a series of small organic and organometallic cations is reported.

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49

Farinola, Gianluca M., Francesco Babudri, Antonio Cardone, et al. "Synthesis of Fluorinated Organic and Organometallic Electroluminescent Materials: Tuning Emission in the Blue." Advances in Science and Technology 75 (October 2010): 108–17. http://dx.doi.org/10.4028/www.scientific.net/ast.75.108.

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Functionalization with fluorine atoms represents a versatile structural modification to finely tune both the emission colour and the electronic properties of organic and organometallic electroluminescent compounds. This paper reports an overview of our systematic investigation on the design and synthesis of the fluorinated version of two important classes of materials for organic light emitting diodes (OLEDs), namely poly(arylenevinylene)s and phosphorescent phenylpyridine Iridium complexes. Synthetic pathways based on organometallic methodologies affording selectively fluorinated molecular st

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50

Liang, Guodong, Xiaodong Li, Suping Bao, Haiyang Gao, Fangming Zhu, and Qing Wu. "Large-scale synthesis of organometallic polymer flowers with ultrathin petals for hydrogen peroxide sensing." Polymer Chemistry 6, no. 24 (2015): 4447–54. http://dx.doi.org/10.1039/c5py00382b.

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