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Journal articles on the topic 'Osmium compounds. Ruthenium compounds. Transition metal complexes'

Author: Grafiati

Published: 4 June 2021

Last updated: 8 February 2022

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1

Cerón-Camacho, Ricardo, Manuel A. Roque-Ramires, Alexander D. Ryabov, and Ronan Le Lagadec. "Cyclometalated Osmium Compounds and beyond: Synthesis, Properties, Applications." Molecules 26, no. 6 (2021): 1563. http://dx.doi.org/10.3390/molecules26061563.

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The synthesis of cyclometalated osmium complexes is usually more complicated than of other transition metals such as Ni, Pd, Pt, Rh, where cyclometalation reactions readily occur via direct activation of C–H bonds. It differs also from their ruthenium analogs. Cyclometalation for osmium usually occurs under more severe conditions, in polar solvents, using specific precursors, stronger acids, or bases. Such requirements expand reaction mechanisms to electrophilic activation, transmetalation, and oxidative addition, often involving C–H bond activations. Osmacycles exhibit specific applications i

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2

Zykova, A. "Synthesis and Structure of Aryl Phosphorus Compounds." Bulletin of the South Ural State University series "Chemistry" 12, no. 4 (2020): 5–50. http://dx.doi.org/10.14529/chem200401.

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Based on an analysis of the literature published from the late 20th century to the beginning of the 21st century, methods for the synthesis of some complex tetraorganylphosphonium salts are systematized and described, along with the features of the chemical transformations of pentaphenylphosphorus, which was first obtained in 1953. The tetraorganylphosphonium salts were known much earlier, however, the features of the synthesis of transition metal complexes, which are usually obtained from tetraorganylphosphorus halides and metal halides, have not been sufficiently studied. The present review

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3

Aleksanyan, Diana V., Svetlana G. Churusova, Ekaterina Yu Rybalkina, and Vladimir A. Kozlov. "Rhenium(I) Complexes with Pincer Ligands as a New Class of Potential Antitumor Agents." Proceedings 22, no. 1 (2019): 43. http://dx.doi.org/10.3390/proceedings2019022043.

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Transition metal complexes attract continuous research interest as potential antitumor agents. The most popular compounds are ruthenium, gold, titanium, osmium, iridium, zinc, and palladium complexes, which have already displayed cytotoxic features that are not typical for classical platinum-containing chemotherapeutic agents. Substantially lower attention is drawn to organometallic compounds of rhenium. However, the known examples of cytotoxic organometallic rhenium derivatives with bidentate heterocyclic, organophosphorus, labile alkoxide, and hydroxide ligands render further studies in this

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4

Gianino, Jacqueline, та Seth N. Brown. "Highly covalent metal–ligand π bonding in chelated bis- and tris(iminoxolene) complexes of osmium and ruthenium". Dalton Transactions 49, № 21 (2020): 7015–27. http://dx.doi.org/10.1039/d0dt01287d.

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5

D’Aléo, A., S. Welter, E. Cecchetto, and L. De Cola. "Electronic energy transfer in dinuclear metal complexes containing meta-substituted phenylene units." Pure and Applied Chemistry 77, no. 6 (2005): 1035–50. http://dx.doi.org/10.1351/pac200577061035.

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The synthesis and photophysical properties of heterometallic dinuclear complexes based on ruthenium and osmium trisbipyridine units, Ru-mPh3-Os and Ru-mPh5-Os, in which the metal complexes are linked via an oligophenylene bridge centrally connected in the meta position, are described. Electronic energy transfer from the excited ruthenium-based component (donor) to the osmium moiety (acceptor) has been investigated using steady-state and time-resolved spectroscopy. The results obtained for the meta-substituted compounds are compared with the analogous systems in which the phenylene spacers are

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6

Gaiddon, Christian, Isabelle Gross, Xiangjun Meng, et al. "Bypassing the Resistance Mechanisms of the Tumor Ecosystem by Targeting the Endoplasmic Reticulum Stress Pathway Using Ruthenium- and Osmium-Based Organometallic Compounds: An Exciting Long-Term Collaboration with Dr. Michel Pfeffer." Molecules 26, no. 17 (2021): 5386. http://dx.doi.org/10.3390/molecules26175386.

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Metal complexes have been used to treat cancer since the discovery of cisplatin and its interaction with DNA in the 1960’s. Facing the resistance mechanisms against platinum salts and their side effects, safer therapeutic approaches have been sought through other metals, including ruthenium. In the early 2000s, Michel Pfeffer and his collaborators started to investigate the biological activity of organo-ruthenium/osmium complexes, demonstrating their ability to interfere with the activity of purified redox enzymes. Then, they discovered that these organo-ruthenium/osmium complexes could act in

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7

Gałczyńska, Katarzyna, Zuzanna Drulis-Kawa, and Michał Arabski. "Antitumor Activity of Pt(II), Ru(III) and Cu(II) Complexes." Molecules 25, no. 15 (2020): 3492. http://dx.doi.org/10.3390/molecules25153492.

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Metal complexes are currently potential therapeutic compounds. The acquisition of resistance by cancer cells or the effective elimination of cancer-affected cells necessitates a constant search for chemical compounds with specific biological activities. One alternative option is the transition metal complexes having potential as antitumor agents. Here, we present the current knowledge about the application of transition metal complexes bearing nickel(II), cobalt(II), copper(II), ruthenium(III), and ruthenium(IV). The cytotoxic properties of the above complexes causing apoptosis, autophagy, DNA

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8

Varela, Jesús A., Carlos González-Rodríguez, Silvia G. Rubín, Luis Castedo, and Carlos Saá. "New cyclizations via catalytic ruthenium vinylidenes." Pure and Applied Chemistry 80, no. 5 (2008): 1167–77. http://dx.doi.org/10.1351/pac200880051167.

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New carbocyclizations that proceed via catalytic metal-vinylidenes are presented. Metal-vinylidene catalytic species, which are easily accessible from terminal alkynes and catalytic amounts of transition-metal complexes, can be involved either in pericyclic reactions or in tandem processes triggered by nucleophilic attack at the electrophilic position of the vinylidene. In both cases, a wide variety of valuable cyclic compounds are easily accessible. Some recent carbocyclizations will be described.

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9

Remita, Hynd, Renée Derai, and Marie-Odile Delcourt. "A new process using radiation for synthesising molecular metal clusters and complexes: First results concerning iron, ruthenium and osmium compounds." International Journal of Radiation Applications and Instrumentation. Part C. Radiation Physics and Chemistry 37, no. 2 (1991): 221–25. http://dx.doi.org/10.1016/1359-0197(91)90132-l.

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10

Sun, Qi, Yingsi Li, Hongdong Shi, Yi Wang, Jitian Zhang, and Qianling Zhang. "Ruthenium Complexes as Promising Candidates against Lung Cancer." Molecules 26, no. 15 (2021): 4389. http://dx.doi.org/10.3390/molecules26154389.

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Lung cancer is one of the most common malignancies with the highest mortality rate and the second-highest incidence rate after breast cancer, posing a serious threat to human health. The accidental discovery of the antitumor properties of cisplatin in the early 1960s aroused a growing interest in metal-based compounds for cancer treatment. However, the clinical application of cisplatin is limited by serious side effects and drug resistance. Therefore, other transition metal complexes have been developed for the treatment of different malignant cancers. Among them, Ru(II/III)-based complexes ha

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11

Akatsuka, Komi, Ryosuke Abe, Tsugiko Takase, and Dai Oyama. "Coordination Chemistry of Ru(II) Complexes of an Asymmetric Bipyridine Analogue: Synergistic Effects of Supporting Ligand and Coordination Geometry on Reactivities." Molecules 25, no. 1 (2019): 27. http://dx.doi.org/10.3390/molecules25010027.

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The reactivities of transition metal coordination compounds are often controlled by the environment around the coordination sphere. For ruthenium(II) complexes, differences in polypyridyl supporting ligands affect some types of reactivity despite identical coordination geometries. To evaluate the synergistic effects of (i) the supporting ligands, and (ii) the coordination geometry, a series of dicarbonyl–ruthenium(II) complexes that contain both asymmetric and symmetric bidentate polypyridyl ligands were synthesized. Molecular structures of the complexes were determined by X-ray crystallograph

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12

Siebert, Ronald, Florian Schlütter, Andreas Winter, et al. "Ruthenium(II)-bis(4′-(4-ethynylphenyl)-2,2′:6′, 2″-terpyridine) — A versatile synthon in supramolecular chemistry. Synthesis and characterization." Open Chemistry 9, no. 6 (2011): 990–99. http://dx.doi.org/10.2478/s11532-011-0087-6.

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AbstractA homoleptic ethynyl-substituted ruthenium(II)-bisterpyridine complex representing a versatile synthon in supramolecular chemistry was synthesized and analyzed by NMR spectroscopy, mass spectrometry and X-ray diffractometry. Furthermore, its photophysical properties were detailed by UV/Vis absorption, emission and resonance Raman spectroscopy. In order to place the results obtained in the context of the vast family of ruthenium coordination compounds, two structurally related complexes were investigated accordingly. These reference compounds bear either no or an increased chromophore i

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13

Werner, Helmut, Rudolf Weinand, Wolfgang Knaup, Karl Peters, and Hans George Von Schnering. "Vinylidene transition-metal complexes. 18. (Arene)osmium complexes containing alkynyl, vinyl, vinylidene, and thio- and selenoketene units as ligands: a series of organometallic compounds built up from 1-alkynes." Organometallics 10, no. 12 (1991): 3967–77. http://dx.doi.org/10.1021/om00058a010.

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14

Bilel, Hallouma, Rawdha Medyouni, A. S. Al-Ayed, Naceur Hamdi, Cédric Fischmeister, and Christian Bruneau. "Synthesis of Bioactives Coumarin Derivatives, Phthalocyanines and Terminal Conjugated Dienes via a Ruthenium Catalyzed Cross-Metathesis: Application to Renewable Resources." Materials Science Forum 842 (February 2016): 1–45. http://dx.doi.org/10.4028/www.scientific.net/msf.842.1.

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This study aimed for the synthesis of 4-Aryl-2-amino-6-(4-hydroxy coumarin-3-yl) pyridine-3-carbonitriles derivatives 4, suitable for use as antibacterial, anti-oxidant and anti-inflammatory activities via a versatile, readily accessible 3-((2E)-3(aryl)prop-2-enoyl)-2H-chromen-2-one, 3, which was prepared by refluxing 3-acetyl-4-hydroxycoumarin with aromatic aldehydes in chloroform in the presence of a catalytic amount of piperidine. Then the direct reaction of the obtained chalcones 3 with malonitrile in the presence of ammonium acetate in one step gave products 4. Most of the new compound 4

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15

Ryabov, Alexander D. "The Exchange of Cyclometalated Ligands." Molecules 26, no. 1 (2021): 210. http://dx.doi.org/10.3390/molecules26010210.

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Reactions of cyclometalated compounds are numerous. This account is focused on one of such reactions, the exchange of cyclometalated ligands, a reaction between a cyclometalated compound and an incoming ligand that replaces a previously cyclometalated ligand to form a new metalacycle: + H-C*~Z ⇄ + H-C~Y. Originally discovered for PdII complexes with Y/Z = N, P, S, the exchange appeared to be a mechanistically challenging, simple, and convenient routine for the synthesis of cyclopalladated complexes. Over four decades it was expanded to cyclometalated derivatives of platinum, ruthenium, mangane

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16

Masternak, Joanna, Agnieszka Gilewska, Barbara Barszcz, et al. "Ruthenium(II) and Iridium(III) Complexes as Tested Materials for New Anticancer Agents." Materials 13, no. 16 (2020): 3491. http://dx.doi.org/10.3390/ma13163491.

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The oncological use of cisplatin is hindered by its severe side effects and a very important resistance problem. To overcome these problems, scientists have attempted to design new generation transition-metal anticancer complexes. In this study, we present new complexes, ruthenium(II) [(η6-p-cymene)RuCl(py2CO)]PF6 (1), iridium(III) [(η5-Cp)IrCl(py2CO)]PF6 (2), and NH4[IrCl4(py2CO)]·H2O (3), based on di-2-pyridylketone (py2CO). The prepared complexes were characterized by FTIR, 1H, 13C, 15N NMR, UV-Vis, PL and elemental analysis techniques. The single-crystal X-ray structure analysis and compar

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17

Khalimon, Andrey, Kristina Gudun, and Davit Hayrapetyan. "Base Metal Catalysts for Deoxygenative Reduction of Amides to Amines." Catalysts 9, no. 6 (2019): 490. http://dx.doi.org/10.3390/catal9060490.

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The development of efficient methodologies for production of amines attracts significant attention from synthetic chemists, because amines serve as essential building blocks in the synthesis of many pharmaceuticals, natural products, and agrochemicals. In this regard, deoxygenative reduction of amides to amines by means of transition-metal-catalyzed hydrogenation, hydrosilylation, and hydroboration reactions represents an attractive alternative to conventional wasteful techniques based on stoichiometric reductions of the corresponding amides and imines, and reductive amination of aldehydes wit

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18

Braun, T., P. Steinert, and H. Werner. "Vinylidene transition metal complexes XXXIV the preparation and structure of neutral vinylidene and allenylidene ruthenium(II) compounds of the half-sandwich type containing iPr2PCH2CO2Me as supporting ligand." Journal of Organometallic Chemistry 488, no. 1-2 (1995): 169–76. http://dx.doi.org/10.1016/0022-328x(94)00015-5.

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19

Summers, Kelly L. "A Structural Chemistry Perspective on the Antimalarial Properties of Thiosemicarbazone Metal Complexes." Mini-Reviews in Medicinal Chemistry 19, no. 7 (2019): 569–90. http://dx.doi.org/10.2174/1389557518666181015152657.

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Malaria is a potentially life-threatening disease, affecting approx. 214 million people worldwide. Malaria is caused by a protozoan, Plasmodium falciparum, which is transmitted through the Anopheles mosquito. Malaria treatment is becoming more challenging due to rising resistance against the antimalarial drug, chloroquine. Novel compounds that target aspects of parasite development are being explored in attempts to overcome this wide-spread problem. Anti-malarial drugs target specific aspects of parasite growth and development within the human host. One of the most effective targets is the inh

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20

Bayrakdarian, Malken, Martin J. Davis, Christian Reber, and Davit Zargarian. "Absorption spectroscopy of (Ind)Ni(PPh3)X (Ind = indenyl, 1-Me-indenyl; X = Cl, Br, Me) and M(Ind)2 (M = Ni, Ru; Ind = indenyl)." Canadian Journal of Chemistry 74, no. 11 (1996): 2194–200. http://dx.doi.org/10.1139/v96-246.

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The electronic structures of two types of transition metal indenyl complexes have been studied. The first type, a series of (Ind)Ni(PPh3)X compounds (Ind = indenyl, 1-Me-indenyl; X = Cl, Br, Me) was investigated by absorption spectroscopy and Extended Hückel Molecular Orbital calculations. The energy differences between calculated levels are in good agreement with experimental band positions. For example, the lowest energy singlet–singlet band maximum for (Ind)Ni(PPh3)Cl is at 19 500 cm−1 and the calculated HOMO–LUMO difference is 19 817 cm−1. For X = Me, the calculated energy difference incre

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21

Kaim, Wolfgang, Natasa Doslik, Stephanie Frantz, et al. "Azo compounds as electron acceptor or radical ligands in transition metal species: spectroelectrochemistry and high-field EPR studies of ruthenium, rhodium and copper complexes of 2,2′-azobis(5-chloropyrimidine)." Journal of Molecular Structure 656, no. 1-3 (2003): 183–94. http://dx.doi.org/10.1016/s0022-2860(03)00339-9.

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22

Sellmann, Dieter, and Michael Waeber. "Übergangsmetallkomplexe mit Schwefelliganden, XVIII. Synthese und Reaktionen von [Ru(L)(PPh3)dttd]-Komplexen mit kleinen Stickstoffverbindungen L = NH3, N2H4, N2H3CH3, N2H3C6H5 sowie NO+ (dttd2- = 2,3;8,9-Dibenzo-1,4,7,10-tetrathiadecan (–2))/ Transition Metal Complexes with Sulfur Ligands, XVIII. Synthesis and Reactions of [Ru(L)(PPh3)dttd] Complexes with Small Nitrogen Compounds L = NH3, N2H4, N2H3CH3, N2H3C6H5 and NO+ (dttd2- = 2,3;8,9-Dibenzo-1,4,7,10-tetrathiadecane (–2))." Zeitschrift für Naturforschung B 41, no. 7 (1986): 877–84. http://dx.doi.org/10.1515/znb-1986-0714.

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Abstract Reaktionen von [Ru(L)(PPh3)dttd]-Komplexen mit kleinen Stickstoffverbindungen L = NH3, N2H4, N2H3CH3, N2H3C6H5 sowie NO+ (dttd2-= 2,3;8,9-Dibenzo-l,4,7,10-tetrathiadecan (—2)) Transition Metal Complexes with Sulfur Ligands, XVIII* Synthesis and Reactions of [R u(L)(PPh3)dttd] Complexes with Small Nitrogen Com pounds L = N H 3, N2H 4, N2H 3C H 3, N2H 3C6H 5 and N O + (dttd2-= 2,3;8,9-D ibenzo-l,4,7,10-tetrathiadecane (—2)) D ieter Sellmann+ Ruthenium Sulfur C om plexes, N itrogen Ligands The com plex fragment [Ru(PPh3)dttd], (dttd2-= 2,3;8,9-dibenzo-l,4,7,10-tetrath iad ecane (— 2)), c

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23

Durran, Sean E., Martin B. Smith, Alexandra MZ Slawin, Thomas Gelbrich, Michael B. Hursthouse, and Mark E. Light. "Synthesis and coordination studies of new aminoalcohol functionalized tertiary phosphines." Canadian Journal of Chemistry 79, no. 5-6 (2001): 780–91. http://dx.doi.org/10.1139/v01-037.

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The synthesis of two new aminoalcohol functionalized tertiary phosphines o-Ph2PCH2N(H)C6H4(OH) (I) and o-Ph2PCH2N(H)C6H4(CH2OH) (II) are reported. Oxidation with aqueous H2O2 gave the corresponding phosphine oxides o-Ph2P(O)CH2N(H)C6H4(OH) (III) and o-Ph2P(O)CH2N(H)C6H4(CH2OH) (IV) (31P NMR evidence only). The ligating ability of I, II and, in several cases, the known ligand 2,3-Ph2PCH2N(H)C5H3N(OH) (V), was investigated with a range of late transition-metal precursors. Accordingly, reaction of 2 equiv of I (or II) with [MCl2(cod)] (M = Pd or Pt, cod = cycloocta-1,5-diene) gave the correspondi

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24

Sellmann, Dieter, Olaf Käppler, Falk Knoch та Matthias Moll. "Übergangsmetallkomplexe mit Schwefelliganden, XLIX Außergewöhnliche Säure-Basenreaktionen an niedervalenten Ru-Nitrosyl-Komplexen mit dem Thiolat-amin-Liganden ′S2Ν2Ηχ'2- (χ = 1, 2) und Mo-Komplexe mit den Liganden′S2N2H2′2- und ′buS2N2H2′ 2-, Synthese, Struktur und Reaktionen / Transition Metal Complexes with Sulfur Ligands, XLIX Unusual Acid Base Reactions of Low Valence Ruthenium Nitrosyl Complexes with the Thiolate-amine Ligands ′S2Ν2ΗΧ'2- (χ = 1, 2) and Molybdenum Complexes with the Ligands ′S2N2H2′ 2- and ′buS2N2H2′ 2-, Syntheses, Structure and Reactions". Zeitschrift für Naturforschung B 45, № 6 (1990): 803–16. http://dx.doi.org/10.1515/znb-1990-0612.

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In order to find complexes suited as model compounds for oxidoreductases catalyzing reactions of the biological nitrogen cycle, Ru- and Mo-nitrosyl complexes with the ′S2N2H2'2- and ′buS2N2H2′ 2--** ligand were synthesized. The reaction of [Ru(NO)(PPh3)2Cl3] with Li2-'S2N2H2' yields the binuclear [Ru(NO)(′S2N2H′)]2 (1) and the mononuclear [Ru(NO)(PPh3)(′S2N2H2′ )]Cl (2). Formation of 1 is explained by HCl and subsequent PPh3 elimination from 2; the coordinatively unsaturated [Ru(NO)(′S2N2H′)] dimerize to give 1. 1 is also obtained a) when [Ru(NO)2(PPh3)2] is reacted with Li2-'S2N2H2′ , b) when

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25

Traub, Lukas, and Oliver Reiser. "Homogeneous visible light mediated transition metal catalysis other than Ruthenium and Iridium." Physical Sciences Reviews 4, no. 7 (2019). http://dx.doi.org/10.1515/psr-2017-0172.

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Abstract The field of photoredox chemistry is dominated by ruthenium- or iridium based metal complexes or organic dyes that are employed as catalysts. Other metal based coordination compounds provide a cost efficient alternative, however, the much shorter excited lifetimes generally observed for such complexes make their application more challenging. Nevertheless, a growing number of successful examples with metal complexes based on chromium, iron, nickel, zirconium, cerium, rhenium, platinum, uranium, and especially on copper exist, which is being reviewed in this chapter.

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26

SCHAAL, M., W. WEIGAND, U. NAGEL та W. BECK. "ChemInform Abstract: PSEUDOHALO METAL COMPOUNDS. LXIV. REACTIONS OF CYANO COMPLEXES OF IRON(II), RUTHENIUM(II), OSMIUM(II), AND PLATINUM(II) WITH α,β-UNSATURATED CARBONYL COMPOUNDS OR KETONES IN THE PRESENCE OF ACIDS: Γ-OXOISOCYANIDE COMPLEXES. X-RAY STRU". Chemischer Informationsdienst 16, № 40 (1985). http://dx.doi.org/10.1002/chin.198540316.

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27

Ricciardi, Loredana, and Massimo La Deda. "Recent advances in cancer photo-theranostics: the synergistic combination of transition metal complexes and gold nanostructures." SN Applied Sciences 3, no. 3 (2021). http://dx.doi.org/10.1007/s42452-021-04329-6.

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AbstractIn this mini review, we highlight advances in the last five years in light-activated cancer theranostics by using hybrid systems consisting of transition metal complexes (TMCs) and plasmonic gold nanostructures (AuNPs). TMCs are molecules with attractive properties and high potential in biomedical application. Due to their antiproliferative abilities, platinum-based compounds are currently first-choice drugs for the treatment of several solid tumors. Moreover, ruthenium, iridium and platinum complexes are well-known for their ability to photogenerate singlet oxygen, a highly cytotoxic

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