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Relevant bibliographies by topics / Palladium catalysed synthesis

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Dissertations / Theses

Academic literature on the topic 'Palladium catalysed synthesis'

Author: Grafiati

Published: 4 June 2021

Last updated: 7 February 2022

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Dissertations / Theses on the topic "Palladium catalysed synthesis"

1

Ostovar, Peyman. "Palladium-catalysed neuroleptic synthesis." Thesis, Imperial College London, 1989. http://hdl.handle.net/10044/1/47601.

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2

Sadig, Jessie E. R. "Palladium-catalysed heterocycle synthesis." Thesis, University of Oxford, 2012. http://ora.ox.ac.uk/objects/uuid:c9608957-d215-4a15-87e3-5871c1391946.

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Chapter 1 is a literature review of selected palladium-catalysed aryl C-N and C-S bond forming reactions. The application of these reactions to the synthesis of heterocycles is also discussed. Chapter 2 highlights the importance of the benzimidazole motif and gives a brief discussion of the existing routes to this scaffold. The utility of N-(o-halophenyl)imidoyl chlorides and imidates as precursors to heterocycles is demonstrated in a palladium-catalysed reaction with N-nucleophiles to afford benzimidazole products. Chapter 3 provides a brief introduction to the synthesis of benzothiazoles and

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3

Li, Meiling. "Palladium catalysed allene carbocyclisation." Thesis, University of Oxford, 2010. http://ora.ox.ac.uk/objects/uuid:747420b6-c11f-451c-83c7-fa9fca5f7752.

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In this thesis, firstly, a Pd-catalysed diastereoselective carbocyclisation of allenes with aryl halides or vinyl iodides was designed and developed to form arylative or vinylative spirolactam compounds. High yields and diastereoselectivities were obtained in the presence of Pd<sub>2</sub>(dba)<sub>3</sub>/dppe and K<sub>2</sub>CO<sub>3</sub> in DMSO at 70 °C, particularly when spiropiperidin-2-ones were formed. The method is simple to perform and broad in scope. Having established the diastereoselective methodology for the arylative or vinylative allene carbocyclisation, a Pd-catalysed en

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4

Damian, Karen Serena. "Pd catalysed synthesis of phosphines for homogeneous catalysis." Thesis, St Andrews, 2009. http://hdl.handle.net/10023/907.

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5

Watson, Emma Louise. "Palladium-catalysed synthesis of 3-aminooxindoles." Thesis, University of Leeds, 2010. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.531596.

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6

Tadd, Andrew. "Palladium and copper catalysed heterocycle synthesis." Thesis, University of Oxford, 2009. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.504606.

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7

Ball, Catherine Jane. "Palladium- and copper-catalysed heterocycle synthesis." Thesis, University of Oxford, 2014. http://ora.ox.ac.uk/objects/uuid:589b70fb-0823-4ccf-8b35-1883908f917d.

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A number of privileged starting materials based on aryl halide frameworks have emerged that allow access to a variety of different heterocyclic scaffolds through judicious choice of reaction conditions. This work describes efforts to develop and extend the utility of two of these general heterocycle precursors - ortho-(haloalkenyl)aryl halides A and α-(ortho-haloaryl) ketones B - in conjunction with cascade reactions involving the construction of key carbon-heteroatom bonds via palladium or copper catalysis. Chapter 1 entails an overview of the development of palladium- and copper-catalysed ca

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8

Gatland, Alice Elizabeth. "Palladium-catalysed enolate arylation in the synthesis of isoquinolines." Thesis, University of Oxford, 2014. http://ora.ox.ac.uk/objects/uuid:f106760d-2375-4d56-81b2-faa6ee96cabc.

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<strong>Chapter 1. Introduction</strong> Scientific background on the development of homogeneous palladium-catalysed cross coupling reactions, focusing on the α-arylation reaction of enolates and its application to the synthesis of heteroaromatic compounds. The classical syntheses of isoquinolines are discussed, followed by an account of modern methods for their synthesis, including the recent α-arylation-based methodology developed by the Donohoe group. <strong>Chapter 2. Results and Discussion</strong> 2.1 Studies towards the development of a palladium-catalysed, C–H activation-b

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9

Phillips, David J. "Palladium-catalysed synthesis of highly functionalised compounds." Thesis, University of Glasgow, 2018. http://theses.gla.ac.uk/9011/.

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Palladium-catalysis is extremely important in fine chemical synthesis. This thesis looks at the development of new palladium-catalysed carbon–carbon bond formation reactions, with particular attention to forming new bonds to sp3 carbons. The opening chapter of this thesis gives an overview of current methods for palladium-catalysed heterocyclisation, and the methods for incorporating further functionalisation into this process, then focuses on the optimisation and expansion of a new palladium-catalysed carboallylation reaction. The reaction mechanism was demonstrated via a deuterium-labelling

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10

Yagoubi, Myriam. "Synthesis of heterocycles via palladium-catalysed direct arylation." Thesis, University of Oxford, 2011. http://ora.ox.ac.uk/objects/uuid:e1206b3a-b9e8-4371-a94c-da3bc04c116e.

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Chapter 1 is a brief review on some of the recents developments in palladium-catalysed C-H functionalisation chemistry. The synthesis and functionalisation of heterocycles using these methodologies was particularly emphasised. Chapter 2 presents our efforts to identify a new catalytic system to promote the intramolecular coupling of vinyl bromides with unfunctionalised aryl C-H bonds for the formation of benzofurans. Dihydrobenzofurans were obtained efficiently under mild conditions in the presence of Pd(OAc)₂, X-Phos and K₂CO₃ in DMA at 80 °C and a subsequent one-pot isomerisation under acidi

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