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Dissertations / Theses on the topic 'Palladium-catalyzed cross couplings in organic synthesis'

Author: Grafiati

Published: 3 June 2025

Last updated: 31 July 2025

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1

Marelli, Enrico. "Nickel- and palladium-catalysed deprotonative cross-couplings." Thesis, University of St Andrews, 2017. http://hdl.handle.net/10023/15603.

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Transition metal-catalysed cross coupling chemistry is a valuable tool for synthetic organic chemistry, enabling the preparation of compounds of great interest. The catalytic metal of choice is usually palladium, which generally offer better performances in term of catalytic activity and easy handling. On the other hand, the use of nickel in this class of reactions is gaining attention, as it would provide more economically and environmentally sustainable processes. Deprotonative cross couplings are a subgroup of these reactions, in which the nucleophile is generated in situ by direct deproton

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2

Lightowler, Stephen. "Palladium-catalysed cross-coupling reactions in the synthesis of novel organic polymers and monodisperse oligomers." Thesis, University of Hull, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.342874.

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3

Onuska, Nicholas Paul Ralph. "Studies Towards the Synthesis of 2,5-Disubstituted-3-Fluorothiophenes Using a Directed Ortho-Metalation/Nickel-Catalyzed Cross-Coupling Approach." Kent State University Honors College / OhioLINK, 2016. http://rave.ohiolink.edu/etdc/view?acc_num=ksuhonors1460652408.

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4

Yin, Lunxiang. "Synthesis of new calcineurin inhibitors via Pd-catalyzed cross coupling reactions." Doctoral thesis, [S.l. : s.n.], 2005. http://deposit.ddb.de/cgi-bin/dokserv?idn=975817868.

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5

Liang, Yong. "Novel Approaches for the Synthesis of C-5 Modified Pyrimidine Nucleosides." FIU Digital Commons, 2014. http://digitalcommons.fiu.edu/etd/1591.

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The antiviral or anticancer activities of C-5 modified pyrimidine nucleoside analogues validate the need for the development of their syntheses. In the first half of this dissertation, I explore the Pd-catalyzed cross-coupling reaction of allylphenylgermanes with aryl halides in the presence of SbF5/TBAF to give various biaryls by transferring multiple phenyl groups, which has also been applied to the 5-halo pyrimidine nucleosides for the synthesis of 5-aryl derivatives. To avoid the use of organometallic reagents, I developed Pd-catalyzed direct arylation of 5-halo pyrimidine nucleosides. It

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6

Black, Daniel. "Imines in copper-catalyzed cross-coupling reactions." Thesis, McGill University, 2006. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=102960.

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The purpose of this study was to develop new catalytic methods to mediate carbon-carbon bond forming reactions with imines under mild conditions and in a general manner. We found that copper catalysts were compatible in cross-coupling of a range of mild organometallic reagents, providing simple, efficient routes to alpha-substituted amides and amines.<br>Chapter 2 of this thesis describes a new copper-catalyzed multicomponent synthesis of alpha-substituted amides. This reaction was developed based upon previous work in this laboratory, which showed that palladium catalysts were competent in St

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7

Norinder, Jakob. "Asymmetric Synthesis and Mechanistic Studies on Copper(I)-Catalyzed Substitution of Allylic Substrates." Doctoral thesis, Stockholm : Department of Organic Chemistry, Stockholm University, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-1031.

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8

Zhang, Ye. "Development of amide-derived P,O-ligands for Suzuki cross-coupling of aryl chlorides and the asymmetric version /." View abstract or full-text, 2005. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202005%20ZHANG.

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9

Jawade, K. "Synthesis of naturally occurring polyhydroxylated δ--lactones, aryne mediated synthesis of phenyl indolines and pd-sba-tat catalyzed c-c cross coupling reactions". Thesis(Ph.D.), CSIR-National Chemical Laboratory, Pune, 2018. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/5868.

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10

Emmett, Edward J. "Development of catalytic methods to exploit sulfur dioxide in organic synthesis." Thesis, University of Oxford, 2014. http://ora.ox.ac.uk/objects/uuid:be60729b-5467-4758-8d88-9dff3a2d5810.

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In the following thesis, new methodologies towards the synthesis of a range of sulfonyl (-SO<sub>2</sub>-) containing functional groups are documented. These methods utilise easy-to-handle sulfur dioxide surrogates, such as DABSO (vide infra), and exploit palladium catalysis as a new mechanistic protocol for the incorporation of the -SO2- unit. <b>Chapter 1</b> is a literature review surveying sulfur dioxide in organic synthesis, the established uses of SO<sub>2</sub> surrogates and the importance of the sulfonyl moiety in chemistry. Palladium-catalysed (carbonylative) cross-couplings are also

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11

Kawamura, Shintaro. "Development of Iron-Catalyzed Cross-Coupling Reactions with Organoaluminum,-magnesium, and -zinc Reagents Directed toward Controlled Organic Synthesis." 京都大学 (Kyoto University), 2013. http://hdl.handle.net/2433/174951.

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12

Wu, Xiayan. "Promoting nickel catalysts by visible-light illuminated gold and palladium nanoparticles." Thesis, Queensland University of Technology, 2021. https://eprints.qut.edu.au/227208/1/Xiayan_Wu_Thesis.pdf.

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This research focuses on promoting nickel-based catalysts by visible-light illuminated gold and palladium nanoparticles in fine organic synthesis. Using lignin model compound cleavage as the model reaction, the performance of three distinct systems, in-situ formed Ni(OH)2 on ZrO2 supported Au NPs, non-plasmonic NiPd alloy NPs supported on ZrO2 and the mechanical mixture of ZrO2 supported Au NPs and Ni NPs are investigated. Ultra-low palladium loading on sodium titanate sheets for Heck cross-coupling reaction under visible light is also studied. This research has provided innovative findings in

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13

Peiris, Gallage Sunari. "Pd and Pd based alloy nanoparticles as visible light photocatalysts for coupling reactions under ambient conditions." Thesis, Queensland University of Technology, 2017. https://eprints.qut.edu.au/113715/1/Gallage%20Sunari_Peiris_Thesis.pdf.

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This PhD thesis presents an investigation on the development of novel metal nanoparticle (NP) photocatalysts including non-plasmonic NPs and their alloy NPs for several important organic synthesis reactions. This study has provided solid information and advances in new materials design, synthesis and application for photocatalysis. The findings of this study demonstrate the use of visible light or sunlight to drive chemical reactions, which is an important aspect in the view of a sustainable and green chemistry.

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14

Milton, Edward J. "Pd catalysed C-C & C-O bond formation using bis-(dialkyl/diarylphosphino)ferrocene ligands." Thesis, University of St Andrews, 2010. http://hdl.handle.net/10023/1022.

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A brief introduction explaining phosphine ligand properties, Pd catalysed cross-coupling reactions; the importance of the steps involved in the catalytic cycle (oxidative addition, transmetalation & reductive elimination), mechanistic studies and a comparison of various reactions will give an overview of important cross-coupling reactions and their limitations. The development of a “super-concentrated” (5M) Pd catalysed Kumada type coupling reaction has been developed for coupling a range of aryl bromide and chloride substrates with the Grignard reagents ((p-CF₃-C₆H₄)MgBr)) and PhMgBr in methy

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15

Chalker, Justin M. "Reaction engineering for protein modification : tools for chemistry and biology." Thesis, University of Oxford, 2011. http://ora.ox.ac.uk/objects/uuid:52d92917-5c7f-4223-b554-2e1b4fc0b2ea.

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Chemical modification of proteins is critical for many areas of biochemistry and medicine. Several methods for site-selective protein modification are reported in this Thesis that are useful in accessing both natural and artificial protein architectures. Multiple, complementary methods for the conversion of cysteine to dehydroalanine are described. Dehydroalanine is used as a general precursor to several post-translational modifications and glycosylation, polyprenylation, phosphorylation, and lysine methylation and acetylation are all accessible. These modifications and their mimics were explo

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16

Regens, Christopher. "Palladium-catalyzed cross-coupling reactions of organosilanolates : methods development and application in the total synthesis of (+)-papulacandin D /." 2009. http://gateway.proquest.com/openurl?url_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:dissertation&res_dat=xri:pqdiss&rft_dat=xri:pqdiss:3363072.

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Thesis (Ph.D.)--University of Illinois at Urbana-Champaign, 2009.<br>Source: Dissertation Abstracts International, Volume: 70-06, Section: B, page: 3515. Adviser: Scott E. Denmark. Includes bibliographical references (leaves 342-373) Available on microfilm from Pro Quest Information and Learning.

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17

Lesenyeho, Lehlogonolo Godfrey. "Palladium-catalyzed heteroannulation of 2-ARYL- 3-IODO-4-(Phenylamino)quinolines and 4-(N,N-allylphenylamino)-2-ARYL-3-iodoquinolines." Diss., 2010. http://hdl.handle.net/10500/3970.

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The previously described 2-aryl-4-chloro-3-iodoquinolines were prepared following literature procedure and in turn converted to the corresponding hitherto unknown 2-aryl-3-iodo-4-(phenylamino)quinoline derivatives using aniline in refluxing ethanol. These 2-aryl-3-iodo-4-(phenylamino)quinolines were reacted with allybromide in ethanol at room temperature to afford 4-(N,N-allylphenylamino)-2-aryl-3-iodoquinoline derivatives. The 2-aryl-3-iodo-4-(phenylamino)quinoline and 4-(N,N-allylphenylamino)-2-aryl-3-iodoquinoline derivatives were subjected to metal-catalysed carbon-carbon bond formations.

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18

Bryan, Christopher. "Synthesis of Aromatic Heterocycles and Carbocycles Through Tandem Palladium-catalyzed Cross-couplings of gem-dihaloolefins." Thesis, 2010. http://hdl.handle.net/1807/26133.

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Our group has developed a strategy for the synthesis of benzofused carbocycles and heterocycles through tandem palladium-catalyzed reactions of gem-dibromoolefins. In these syntheses, one bromide undergoes a Pd-catalyzed cyclization reaction, and the other participates in an orthogonal inter- or intramolecular Pd-catalyzed reaction to functionalize or annulate that ring, respectively. Chapter 1 describes the pairing of an intramolecular C–N bond forming reaction (the Buchwald-Hartwig coupling) with an intramolecular direct arylation for the synthesis of fused indole derivatives. A range of pre

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19

Sithebe, Siphamandla. "Synthetic, photophysical studies of 2-alkenyl/arylbenzo-1,3,2- diazaborole compounds and their palladium-catalysed cross-coupling reactions." Thesis, 2013. http://hdl.handle.net/10413/10563.

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This study was aimed at investigating the suitability of 2-alkyl/alkenylbenzo-1,3,2-diazaborolane compounds as potential nucleophilic coupling partners in the Suzuki-Miyaura cross-coupling reaction. A range of aryl bromides and iodides bearing electron-donating as well as electron-withdrawing substituents were reacted with 2-alkyl/alkenylbenzo-1,3,2-diazaborolane compounds under the influence of Pd(OAc)2/PCy3 combination. The cross coupling reaction afforded the desired products in yields ranging from 35% to 89% in less than 20 minutes. The catalytic system was found to be versatile and genera

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20

Jones, Matthew Thomas. "The chemoenzymatic synthesis of the lycorine framework and the synthesis of C-3-mono-alkylated oxindoles via the palladium-catalysed Ullmann cross-coupling reaction." Phd thesis, 2013. http://hdl.handle.net/1885/150048.

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Chapter One of this Thesis briefly describes the history and production of cis-1,2-dihydrocatechol chiral starting materials and summarises their synthetic attributes as well as providing several examples of their use in natural product synthesis. Chapter Two begins with a succinct review of the structural characteristics and biological properties of the Amaryllidaceae alkaloid ({uF02D})-lycorine and describes several established synthetic approaches to compounds of this type. Thereafter, experimentally-based research leading to the development of a rapid and enantioselective synthesis of the

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