Relevant bibliographies by topics / PANI-DBSA

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Academic literature on the topic 'PANI-DBSA'

Author: Grafiati
Published: 4 June 2021
Last updated: 19 February 2022

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Journal articles on the topic "PANI-DBSA"

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Wei, Pan, Yang Shenglin, Li Guang, and Jiang Jianming. "Hydrogen Bonding Effects on the Electrical Properties and Phase Morphology of Polyaniline Blends." Polymers and Polymer Composites 13, no. 4 (May 2005): 415–23. http://dx.doi.org/10.1177/096739110501300408.

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Blends of dodecylbenzene sulfonic acid-doped polyaniline (PANI-DBSA) with either polyacrylonitrile copolymer (PAN) or polystyrene (PS) were solution cast. The investigation focused on the interaction between the components, the morphology and the resulting electrical conductivity of blends. The results showed that with the same PANI-DBSA content the conductivity of PANI-DBSA/PAN was higher than that of PANI-DBSA/PS. PANI-DBSA was dispersed uniformly in the PAN matrix and its cluster size was rather smaller than in the PS matrix. This is attributed to hydrogen bonding between the carbonyl groups in PAN and the imine groups in PANI, which should lead to better compatibility between PANI-DBSA and PAN.
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Dywili, Nomxolisi R., Afroditi Ntziouni, Chinwe Ikpo, Miranda Ndipingwi, Ntuthuko W. Hlongwa, Anne Yonkeu, Milua Masikini, Konstantinos Kordatos, and Emmanuel I. Iwuoha. "Graphene Oxide Decorated Nanometal-Poly(Anilino-Dodecylbenzene Sulfonic Acid) for Application in High Performance Supercapacitors." Micromachines 10, no. 2 (February 11, 2019): 115. http://dx.doi.org/10.3390/mi10020115.

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Graphene oxide (GO) decorated with silver (Ag), copper (Cu) or platinum (Pt) nanoparticles that are anchored on dodecylbenzene sulfonic acid (DBSA)-doped polyaniline (PANI) were prepared by a simple one-step method and applied as novel materials for high performance supercapacitors. High-resolution transmission electron microscopy (HRTEM) and high-resolution scanning electron microscopy (HRSEM) analyses revealed that a metal-decorated polymer matrix is embedded within the GO sheet. This caused the M/DBSA–PANI (M = Ag, Cu or Pt) particles to adsorb on the surface of the GO sheets, appearing as aggregated dark regions in the HRSEM images. The Fourier transform infrared (FTIR) spectroscopy studies revealed that GO was successfully produced and decorated with Ag, Cu or Pt nanoparticles anchored on DBSA–PANI. This was confirmed by the appearance of the GO signature epoxy C–O vibration band at 1040 cm−1 (which decreased upon the introduction of metal nanoparticle) and the PANI characteristic N–H stretching vibration band at 3144 cm−1 present only in the GO/M/DBSA–PANI systems. The composites were tested for their suitability as supercapacitor materials; and specific capacitance values of 206.4, 192.8 and 227.2 F·g−1 were determined for GO/Ag/DBSA–PANI, GO/Cu/DBSA–PANI and GO/Pt/DBSA–PANI, respectively. The GO/Pt/DBSA–PANI electrode exhibited the best specific capacitance value of the three electrodes and also had twice the specific capacitance value reported for Graphene/MnO2//ACN (113.5 F·g−1). This makes GO/Pt/DBSA–PANI a very promising organic supercapacitor material.
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Yadav, Anju, Ajay Agarwal, Pankaj B. Agarwal, and Parveen Saini. "Ammonia Sensing by PANI-DBSA Based Gas Sensor Exploiting Kelvin Probe Technique." Journal of Nanoparticles 2015 (November 17, 2015): 1–6. http://dx.doi.org/10.1155/2015/842536.

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Dodecyl benzene sulfonic acid (DBSA) doped polyaniline (PANI-DBSA) has been synthesized by chemical oxidative polymerization of aniline monomer in the presence of DBSA. The UV-visible spectroscopy and X-ray diffraction measurements confirm the formation of PANI and its doping by DBSA. SEM images show the formation of submicron size rod shaped PANI particles. A vibrating capacitor based ammonia gas sensor was prepared by spin coating PANI-DBSA film over copper (Cu) substrate. The sensor exploited Kelvin probe technique to monitor contact potential difference between PANI and Cu as a function of time and ammonia concentration. Upon exposure to 30 ppm ammonia, the sensor displays response time of 329 s, recovery time of 3600 s, and sensitivity value of 1.54 along with good repeatability.
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Pan, Wei, Xiao Wei He, and Yan Chen. "Preparation and Characterization of Polyacrylonitrile-Polyaniline Blend Nanofibers." Applied Mechanics and Materials 44-47 (December 2010): 2195–98. http://dx.doi.org/10.4028/www.scientific.net/amm.44-47.2195.

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Composite nanofibers of polyaniline doped with dodecylbenzene sulfonic acid (PANI-DBSA) and polyacrylonitrile (PAN) were prepared via an electrospinning process. The surface morphology of PANI-DBSA/PAN nanofibers was characterized using scanning electron microscopy (SEM). Differential scanning calorimetry (DSC) and Fourier transform infrared spectroscopy (FTIR) were used to investigate the hydrogen bonding and miscibility behavior of the blend. It was found that the average fiber diameter of composites nanofiber was increased with the increase of PANI-DBSA content. The formation of the hydrogen bonding between PAN and PANI-DBSA was identified by the FTIR spectra
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Wang, Xiao Hua. "Properties of Polyaniline with the Doping of Different Acid." Advanced Materials Research 502 (April 2012): 31–35. http://dx.doi.org/10.4028/www.scientific.net/amr.502.31.

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Polyaniline(PANI) with the doping of hydrochloride(HC1), aminosulfonic acid (NH2SO3H) or dodecylbenzenesulfonic acid(DBSA) was prepared by in-situ polymerization. Effects of acid content, reaction time, oxidant ammonium persulfate (APS) dosage and reaction temperature on the conductivity of PANI were studied. The resistance and thermal stability of them were compared. Results show that the largest conductivity of HC1-PANI is 1.98 s.cm-1 among them in case the C(HC1)=0.5mol/L, reaction time is 6.0h, n(APS/aniline)=1.0; The conductivity of NH2SO3H-PANI is 0.2s.cm-1 in case the C(NH2SO3H)=1.0mol/L, reaction time is 6.0h, n(APS/aniline)=2.0; The conductivity of DBSA-PANI is 0.98s.cm-1 in case the C(DBSA)=1.0 mol/L, reaction time is 8.0h, n(APS/aniline) = 2.0. The the least resistance of HC1-PANI is 10Ω, and that of NH2SO3H- PANI is the largest of 120Ω. The order of their thermal stability is DBSA-PANI > NH2SO3H-PANI > HC1-PANI before 350°C, that of their thermal stability is inverse when it reaches 350°C.
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Zhang, Wang Xi. "Characterization of Polyvinyl Alcohol-Polyaniline Blend Films." Applied Mechanics and Materials 44-47 (December 2010): 2191–94. http://dx.doi.org/10.4028/www.scientific.net/amm.44-47.2191.

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In this study a solution-blend method is adopted to prepare conductive polyvinyl alcohol (PVA) and polyaniline doped with dodecyl benzene sulfonic acid (PVA/PANI-DBSA) blend films. Emeraldine base (EB)-type polyaniline (PANI) is dissolved in N-methyl-2-pyrrolidinone (NMP) and then blended with PVA/dodecyl benzene sulfonic acid (DBSA) solution by various amounts. The morphological structures and characterized of the films were observed via scanning electronic microscopy (SEM), thermogravimetric analysis (TGA) and X-ray powder diffraction (XRD). Electrical properties of the blends were characterized by means of electrical conductivity measurements. It is found that the electrical conductivity and the thermal degradation onset temperature of the PVA/PANI-DBSA blend film are increased as the amount of PANI-DBSA is increased.
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Xu, Jun, Sheng Ren, Yao Wu, Jian Gang Li, Mei Li, and Ying Guo. "Preparation and Characterisation of Polyaniline Grafted Multiwalled Carbon Nanotubes/Epoxy Composite." Advanced Materials Research 194-196 (February 2011): 1510–15. http://dx.doi.org/10.4028/www.scientific.net/amr.194-196.1510.

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Dodecyl benzene sulfonic acid (DBSA) doped polyaniline (PANI) grafted MWNTs (PANI-g-MWNTs)/Epoxy composite were prepared by aniline in situ polymerization in the presence of phenylamine groups contained MWNTs followed by solution blending and mould casting. Phenylamine groups grafted on the surface of MWNTs via amide bond join in the in situ polymerization and MWNTs are encapsulated by PANI coatings forming a core (MWNTs)-shell (PANI) nano-structure. DBSA doped PANI coatings swell in tetrahydrofuran (THF) and core-shell nano-structures are stabilized in epoxy solution, which is in favor of MWNTs dispersion in epoxy resin and formation of a homogenous MWNTs/Epoxy composite. After DBSA doped PANI-g-MWNTs are introduced in Epoxy, initial curing and exothermic peak temperatures as well as curing reaction enthalpy decrease, which indicates addition of DBSA doped PANI-g-MWNTs promotes curing reaction of Epoxy. Tensile strength, Young’s modulus, elongation at break, flexural strength and flexural modulus of the composite are improved by 71.7%, 42.3%, 99.8%, 55.01% and 39.86% compared with Epoxy, respectively.
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Chen, Zheng, Rui Qi Li, and Qing Guo. "Synthesis and Characterization of Polyaniline Conductive Composite Films." Applied Mechanics and Materials 217-219 (November 2012): 1166–69. http://dx.doi.org/10.4028/www.scientific.net/amm.217-219.1166.

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Conductive polyaniline(PANI) was synthesized by chemical oxidative copolymerization , using dodecylbenzene sulfonic acid (DBSA)as doping agent. PANI-DBSA/ABS conductive films were obtained by solution blending method, using chloroform as organic solvents. The products were characterized by means of digital four-point probe meter, FT-IR spectroscopy, thermal gravimetric analysis (TGA) and inverted metallurgical microscope. The results indicate that PANI-DBSA has good solubility because dodecylbenzene sulfonic acid (DBSA) plays a good doping role in polyaniline. Composite films’ electric conductivity improves with the increasing content of PANI and the percolation threshold is about 10wt% when conducting network formed. TGA curves demonstrate that product’s glass transition temperature is much higher than acrylonitrile-butadiene-styrene resin, furthermore, the thermal stability of composite films also improves compared with polyaniline or resin.
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Long, Yunze, Zhaojia Chen, Nanlin Wang, Junchao Li, and Meixiang Wan. "Electronic transport in PANI-CSA/PANI-DBSA polyblends." Physica B: Condensed Matter 344, no. 1-4 (February 2004): 82–87. http://dx.doi.org/10.1016/j.physb.2003.09.245.

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Kumar, V., T. Yokozeki, T. Goto, and T. Takahashi. "Synthesis and characterization of PANI-DBSA/DVB composite using roll-milled PANI-DBSA complex." Polymer 86 (March 2016): 129–37. http://dx.doi.org/10.1016/j.polymer.2016.01.054.

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Dissertations / Theses on the topic "PANI-DBSA"

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Shreepathi, Subrahmanya. "Dodecylbenzenesulfonic Acid: A Surfactant and Dopant for the Synthesis of Processable Polyaniline and its Copolymers." Doctoral thesis, Universitätsbibliothek Chemnitz, 2006. http://nbn-resolving.de/urn:nbn:de:swb:ch1-200602029.

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Das Ziel der vorliegenden Arbeit ist die bessere Verarbeitung von Polyanilin (PANI), da dies bisher ein großer Nachteil unter leitfähigen Polymeren war. Dazu wird ein sperriges Tensid und Dotand, Dodecylbenzensulfonsäure (DBSA) verwendet. Zur Synthese der PANI kommen zwei verschiedene Methoden zur Anwendung, die in dieser Dissertation in zwei Kapiteln beschrieben werden. Im ersten Teil wurden in einem kleinen Reaktionsvolumen (250 mL) PANI-DBSA-Suspensionen synthetisiert, wobei mit einem binären Gemisch aus 2-Propanol und Wasser als Lösungsmittel gearbeitet wird um die Löslichkeit zu unterstützen. Die micellenunterstützte Synthese produziert grüne Dispersionen, welche nach länger als einem Jahr noch keine sichtbare Ausscheidung zeigen. Eine detaillierte spectroelektrochemische Untersuchung der PANI-DBSA-Nanokolloide wurde durchgeführt und gibt eine bessere Erklärung der Charge-Transfer-Prozesse zwischen PANI-Kolloiden und Elektrodenoberfläche. In einem alkalischen Medium ist das UV-Vis-Spektrum von der Beweglichkeit der Anionen und von einem elektrokinetischen Phänomen abhängig. Um den „metal-to-insulator”-Übergang zwischen PANI-Kolloiden, welcher durch pH-Wert-Änderung des Mediums geschehen kann, zu zeigen, wurden UV-Vis- und pre-resonanz-Raman-Spektroskopie verwendet. Im zweiten Teil der Dissertation wird zur Polymerisation von Anilin sowie seinen Copolymeren mit o-Toluidin eine neue Technik der Polymerisation beschrieben, welche durch inverse Emulsion erfolgt. Diese benutzt Benzoylperoxid, ein ungewöhnlicheres organisches Oxidationsmittel. Die erhaltenen PANI sind in gebräuchlichen organischen Lösungsmitteln, wie in Chloroform, vollständig löslich. Mit einer klar-transparenten, grünen Lösung von PANI können metallische Oberflächen oder Glas leicht tropfenbeschichtet werden. Zyklische Voltammetrie und spektroelektrochemische Verfahren kamen zum Einsatz, um die Elektroaktivität, das UV-Vis-Verhalten und die „metal-to-insulator”-Übergänge der chemisch synthetisierten PANI als Funktion des verwendeten Elektrodenpotentials zu untersuchen. Die elektrische Leitfähigkeit der Materialien ist relativ hoch (R = 10 ). SEM-Untersuchungen zeigen, dass die Menge des zugesetzten DBSA die Morphologie des Polymers stark beeinflusst. Aus in situ UV-Vis-spektroskopischen Messungen lässt sich eine gute elektrochromische Reversibilität des Polymers erkennen. DBSA kann Poly(o-toluidin) (POT) effektiv dotieren, auch wenn von der Methylgruppe eine sterische Hinderung ausgeht. Die spektroskopischen Untersuchungen, wie UV-Vis, FT-IR, Raman-Spektroskopie und zyklische Voltammetrie, zeigen deutlich, dass wirkliche Copolymere gebildet werden und die Möglichkeit von Kompositen nicht in Betracht kommt. Das entstandene Poly(anilin-co-o-toluidin) (PAT) ist in schwach polaren Lösungsmitteln wie Chloroform löslich. Wie erwartet, sind die elektrischen Leitfähigkeiten der Copolymere viel kleiner als die Leitfähigkeit von PANI-DBSA.
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Dywili, Nomxolisi Ruth. "Development of Metal Nanoparticle-Doped Polyanilino-Graphene Oxide High Performance Supercapacitor Cells." University of the Western Cape, 2018. http://hdl.handle.net/11394/6251.

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Philosophiae Doctor - PhD (Chemistry)
Supercapacitors, also known as ultracapacitors or electrochemical capacitors, are considered one of the most important subjects concerning electricity or energy storage which has proven to be problematic for South Africa. In this work, graphene oxide (GO) was supported with platinum, silver and copper nanoparticles anchored with dodecylbenzenesulphonic acid (DBSA) doped polyaniline (PANI) to form nanocomposites. Their properties were investigated with different characterization techniques. The high resolution transmission electron microscopy (HRTEM) revealed GO's nanosheets to be light, flat, transparent and appeared to be larger than 1.5 ?m in thickness. This was also confirmed by high resolution scanning electron microscopy (HRSEM) with smooth surfaces and wrinkled edges observed with the energy dispersive X-ray analysis (EDX) confirming the presence of the functional groups such as carbon and oxygen. The HRTEM analysis of decorated GO with platinum, silver and copper nanoparticles (NPs) revealed small and uniformly dispersed NPs on the surface of GO with mean particle sizes of 2.3 ± 0.2 nm, 2.6 ± 0.3 nm and 3.5 ± 0.5 nm respectively and the surface of GO showed increasing roughness as observed in HRSEM micrographs. The X-ray fluorescence microscopy (XRF) and EDX confirmed the presence of the nanoparticles on the surface of GO as platinum, silver and copper which appeared in abundance in each spectra. Anchoring the GO with DBSA doped PANI revealed that single GO sheets were embedded into the polymer latex, which caused the DBSA-PANI particles to become adsorbed on their surfaces. This process then appeared as dark regions in the HRTEM images. Morphological studies by HRSEM also supported that single GO sheets were embedded into the polymer latex as composite formation appeared aggregated and as bounded particles with smooth and toothed edges.
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Shreepathi, Subrahmanya, Hung Van Hoang, and Rudolf Holze. "Corrosion Protection Performance and Spectroscopic Investigations of Soluble Conducting Polyaniline-Dodecylbenzenesulfonate Synthesized via Inverse Emulsion Procedure." Universitätsbibliothek Chemnitz, 2009. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-200900775.

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Corrosion protection performance of a completely soluble polyaniline-dodecylbenzenesulfonic acid salt (PANI-DBSA) on C45 steel has been studied with electrochemical impedance and potentiodynamic measurements. Chloroform is the most suitable solvent to process the pristine PANI-DBSA because of negligible interaction of the solvent with the polyaniline (PANI) backbone. An anodic shift in the corrosion potential (DeltaE=~70  mV), a decrease in the corrosion current and a significant increase in the charge transfer resistance indicate a significant anti-corrosion performance of the soluble PANI deposited on the protected steel surface. Corrosion protection follows the mechanism of formation of a passive oxide layer on the surface of C45 steel. In situ UV-Vis spectroscopy was used to investigate the differences in permeability of aqueous anions into PANI-DBSA. Preliminary results of electron diffraction studies show that PANI-DBSA possesses an orthorhombic type of crystal structure. An increase in the feed ratio of DBSA to aniline increases the tendency of aggregation of spherical particles of PANI obvious in transmission electron microscopy. PANI-DBSA slowly loses its electrochemical activity in acid free electrolyte without undergoing degradation.
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Chia-Hung, Hsieh, and 謝嘉鴻. "Study of preparation and physical properties of polyaniline-DBSA/polyacrylic acid (PANI-DBSA/PAA) blends." Thesis, 2006. http://ndltd.ncl.edu.tw/handle/17947297189589800643.

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碩士
輔仁大學
化學系
94
A high dielectric constant nano-composite of polyaniline, PANI-DBSA/PAA, has been synthesized by using the technique of in-situ polymerization of aniline in an aqueous dispersion of poly(acrylic acid)(PAA) in the presence of dodecylbenzenesulfate(DBSA). The water-soluble PAA serves as a suspension agent and its carboxylic acid group participated in forming micelle structure with DBSA-anilinium complex. SEM micrograph confirms that their composite consists of numerous nano-scale PANI grains(ca. 15~25nm) evenly distributed within the PAA matrix. The high dielectric attributed to the accumulation of this tiny capacitors. 　　In this study, a number of factors that can effect the outcomes of this synthesis work are investigated, which includes the molar ratio of aniline to DBSA, the molar ratio of aniline-DBSA to PAA, the formation of DBSA micelles, as well as the blending speed used in the in-situ polymerization process. The extra ordinary dielectric behaviors of this PANI-DBSA/PAA composite renders it an ideal prototype material to study the mechanism of metal-insulator transition in the conductive polymer composites.
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Huang, Chien Yi, and 黃建億. "The morphological and dielectric behaviors of PANI－DBSA/PAA nanocomposites." Thesis, 2007. http://ndltd.ncl.edu.tw/handle/34954407727699432747.

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碩士
輔仁大學
化學系
95
Abstract A high dielectric constant composite of polyaniline,PANI-DBSA/PAA has been synthesized by using the technique of in-situ polymerization of aniline in a aqueous dispersion of poly(acrylic acid) (PAA) in the presence of dodecylbenzene sulfonate (DBSA). The water-soluble PAA serves as a polymeric stabilizer which can protect the PANI particles from macroscopic aggregation . SEM micrograph reveals that the composite prepared consists of numerous nano-scale (~70nm) PANI particles evenly distributed within the PAA matrix . A high dielectric constant value of ca. 105(at 1 kHZ ) was obtained by the composite containing 20 wt% of PANI . The high dielectric constants of these composites are attributed to the accumulation of the tiny capacitors formed by PANI nano particles . The influences of PANI and water contents on various properties such as morphological ,thermal dielectric and electrical behaviors were investigated . On the other hand ,these composites exhibit high dielectric loss due the conductive nature of the PANI particles , especially when PANI content in the composite is high.
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Book chapters on the topic "PANI-DBSA"

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Khalid, Nor Aisah, Jeefferie Abd Razak, Hazman Hasib, and Mohd Muzafar Ismail. "A Review on Polyaniline-Graphene Nanoplatelets (PANI/GNPs-DBSA) Based Nanocomposites Enhancing the Electrical Conductivity." In Lecture Notes in Mechanical Engineering, 951–58. Singapore: Springer Singapore, 2021. http://dx.doi.org/10.1007/978-981-16-0866-7_83.

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Conference papers on the topic "PANI-DBSA"

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Polpaya, Indu Chanchal, C. Lakshmana Rao, and Susy Varughese. "Electromechanical Behavior and Microstructure of Highly Sensitive Polyaniline/Ethylene Vinyl Acetate Composite Piezo-Resistive Materials." In ASME 2016 Conference on Smart Materials, Adaptive Structures and Intelligent Systems. American Society of Mechanical Engineers, 2016. http://dx.doi.org/10.1115/smasis2016-9163.

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The unique micro/nano-structure of an intrinsically conducting polymer can be tuned to get higher gauge factors (GF) and reliability, which make them better materials for piezo-resistive applications than conducting carbon based composites and metallic composites. This work reports a highly sensitive conducting polyaniline (PANI)-based composite film that showed a GF ∼66. This high GF was achieved by forming a particular microstructure of conducting PANI particles in a free standing film of PANI-DBSA/EVA. The paper also attempts to explain the mechanism for the observed high sensitivity using the electronic percolation theory, shape and size of the conducting particles and the changes in the microstructure, due to strain. The high sensitivity, high stability during cyclic loading and low electrical hysteresis together with high mechanical strength make PANI-DBSA/EVA conducting composite film a promising material for piezo-resistive strain sensing applications.
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Yadav, Anju, Rahul Prajesh, Parveen Saini, and Ajay Agarwal. "Synthesis and Characterization of PANI-DBSA/MWCNT Nanocomposites for Ammonia Gas Sensing." In 2019 IEEE 16th India Council International Conference (INDICON). IEEE, 2019. http://dx.doi.org/10.1109/indicon47234.2019.9029050.

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Nano, Anju Yadav, Rahul Prajesh, Parveen Saini, and Ajay Agarwal. "Performance Analysis of Ammonia Sensors based on Nanostructured PANI-DBSA Synthesised by Template Free Direct Doping Route using Surfactant and Indirect Doping Route." In 2019 IEEE 16th India Council International Conference (INDICON). IEEE, 2019. http://dx.doi.org/10.1109/indicon47234.2019.9029041.

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