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Journal articles on the topic 'Perlin aldehyde'

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Published: 5 June 2025

Last updated: 1 August 2025

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1

Suvendu, Halder, Bai Addanki Rupa, and K. Kancharla Pavan. "Three-step synthesis of protected L-altrose from D-galactose derived Perlin aldehyde." Journal of Indian Chemical Society Vol. 97, Feb 2020 (2020): 243–50. https://doi.org/10.5281/zenodo.5651737.

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Department of Chemistry, Indian Institute of Technology Guwahati, Guwahati-781 039, Assam, India E-mail: pavankancharla@iitg.ac.in Manuscript received online 01 October 2019, revised and accepted 07 December 2019 A new short three-step strategy has been designed for the synthesis of L-hexoses that are rare antipodes of the common hexoses from the commercially available glycals. S<sub>N<sup>2</sup></sub><sup> </sup>inversion of the triflate derived from the easily accessible Perlin aldehydes, followed by the dihydroxylation, leads to L-hexoses in good yields. The strategy has been successfully

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2

Vankar, Yashwant, Parasuraman Rajasekaran, and Yakkala Mallikharjunarao. "Synthesis of 1C-Aryl/Alkyl 2C-Branched Sugar-Fused Isochroman Derivatives by Sequential Prins and Friedel–Crafts Cyclizations on a Perlin Aldehyde Derived Substrate." Synlett 28, no. 11 (2017): 1346–52. http://dx.doi.org/10.1055/s-0036-1588156.

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The synthesis of C-aryl/alkyl 2C-branched sugar-fused isochromans by using a carbohydrate-derived starting material is described. Our approach makes use of sequential Prins and Friedel–Crafts cyclizations in which a Perlin aldehyde derived homoallylic alcohol is converted into the target molecule. This strategy works well with many aldehydes and gives good yields with excellent selectivity.

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3

DIL, BAHAR SINGH MITTAL. "CONDENSATION OF o-, m-, AND p- NITROBENZALDE- HYDES WITH MALONIC ACID IN THE PRESENCE OF ORGANIC BASES." Journal of Indian Chemical Society Vol. 19, Jan-Dec 1942 (2022): 47–48. https://doi.org/10.5281/zenodo.6601955.

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Aldehydes have been condensed with malonic acid using a mixture of pyridine (I mol.) and piperidine (traces) by Haworth, Perkin. and Rankin (J. Chem. Soc.. 1924, 125, 1693) and by Dutt (J. Indian Chem. Soc<em>., </em>1925, 1, 297) and a few other bases each in molecular proportions (Dalal and Dutt, ibid.<em>, </em>1932. 9, 309). The pyridine-piperidine method, originally given by Haworth, Perkin and Rankin (loc. cit.)<em> </em>and modified by Robinson and Shinoda (J. Chem. Soc., 1924, 1693) has been applied by Chakravarti, Haworth and Perkin, who using <em>m- </em>methoxybenzaldellyde and

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4

Reddy, L. Vijaya Raghava, Vikas Kumar, Ram Sagar та Arun K. Shaw. "Glycal-Derived δ-Hydroxy α,β-Unsaturated Aldehydes (Perlin Aldehydes): Versatile Building Blocks in Organic Synthesis". Chemical Reviews 113, № 5 (2013): 3605–31. http://dx.doi.org/10.1021/cr200016m.

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5

Reddy, L. Vijaya Raghava, Vikas Kumar, Ram Sagar та Arun K. Shaw. "ChemInform Abstract: Glycal-Derived δ-Hydroxy α,β-Unsaturated Aldehydes (Perlin Aldehydes): Versatile Building Blocks in Organic Synthesis". ChemInform 44, № 27 (2013): no. http://dx.doi.org/10.1002/chin.201327216.

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6

Zhang, Min, Guoling Huang, Xuefang Zhang, et al. "Inexpensive Weight-Reducing Aid (L-Carnitine) as An Efficient Catalyst for Synthesis of Benzimidazoles." Combinatorial Chemistry & High Throughput Screening 21, no. 8 (2018): 567–70. http://dx.doi.org/10.2174/1386207321666181018163940.

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Aim and Objective: The benzimidazole derivatives have been obtained via weightreducing aid (L-Carnitine) as a cheap catalyst. A wide range of aromatic aldehydes easily undergo condensations with substituted o-phenylendiamine under mild condition to afford the target molecular in excellent yields. Materials and Methods: Melting points were measured on an Electrothemal X6 microscopy digital melting point apparatus. 1H NMR and 13C NMR spectra were recorded in DMSO-d6 on a Bruker AVANCE 400 (400 MHz) instrument with the TMS at d 0.00 ppm as an internal standard. C, H and N analysis were performed

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7

Adebayo Ibikunle Farounbi and Oghenekaro Nelson Odume. "Physicochemical and FT-IR analyses of some freshwater and inflow wastewater-treated effluents in the Eastern Cape Province of South Africa." GSC Advanced Research and Reviews 19, no. 1 (2024): 178–99. http://dx.doi.org/10.30574/gscarr.2024.19.1.0138.

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Monitoring changes occurring in water bodies is a tool to make a sound decision on water quality management. This work investigates water quality parameters and metabolites in the Bloukrans, Buffalo, Swartkops and Tyhume Rivers in the Eastern Cape Province of South Africa. The water physicochemical parameters assessed include the dissolved oxygen, oxidation-reduction potentials, temperature, Hydrogen ion concentration, salinity, conductivity, turbidity and total dissolved solids measured with a pre-calibrated Hanna Multiparameter instrument on-site. Chemical oxygen demand, phosphate, chloride,

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8

Adebayo, Ibikunle Farounbi, and Nelson Odume Oghenekaro. "Physicochemical and FT-IR analyses of some freshwater and inflow wastewater-treated effluents in the Eastern Cape Province of South Africa." GSC Advanced Research and Reviews 19, no. 1 (2024): 178–99. https://doi.org/10.5281/zenodo.13486928.

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Monitoring changes occurring in water bodies is a tool to make a sound decision on water quality management. This work investigates water quality parameters and metabolites in the Bloukrans, Buffalo, Swartkops and Tyhume Rivers in the Eastern Cape Province of South Africa. The water physicochemical parameters assessed include the dissolved oxygen, oxidation-reduction potentials, temperature, Hydrogen ion concentration, salinity, conductivity, turbidity and total dissolved solids measured with a pre-calibrated Hanna Multiparameter instrument on-site. Chemical oxygen demand, phosphate, chloride,

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9

Adebayo, Ibikunle Farounbi, and Nelson Odume Oghenekaro. "Physicochemical and FT-IR analyses of some freshwater and inflow wastewater-treated effluents in the Eastern Cape Province of South Africa." GSC Advanced Research and Reviews 19, no. 1 (2024): 178–99. https://doi.org/10.5281/zenodo.13486928.

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Monitoring changes occurring in water bodies is a tool to make a sound decision on water quality management. This work investigates water quality parameters and metabolites in the Bloukrans, Buffalo, Swartkops and Tyhume Rivers in the Eastern Cape Province of South Africa. The water physicochemical parameters assessed include the dissolved oxygen, oxidation-reduction potentials, temperature, Hydrogen ion concentration, salinity, conductivity, turbidity and total dissolved solids measured with a pre-calibrated Hanna Multiparameter instrument on-site. Chemical oxygen demand, phosphate, chloride,

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10

Adebayo, Ibikunle Farounbi, and Nelson Odume Oghenekaro. "Physicochemical and FT-IR analyses of some freshwater and inflow wastewater-treated effluents in the Eastern Cape Province of South Africa." GSC Advanced Research and Reviews 19, no. 1 (2024): 178–99. https://doi.org/10.5281/zenodo.13486928.

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Monitoring changes occurring in water bodies is a tool to make a sound decision on water quality management. This work investigates water quality parameters and metabolites in the Bloukrans, Buffalo, Swartkops and Tyhume Rivers in the Eastern Cape Province of South Africa. The water physicochemical parameters assessed include the dissolved oxygen, oxidation-reduction potentials, temperature, Hydrogen ion concentration, salinity, conductivity, turbidity and total dissolved solids measured with a pre-calibrated Hanna Multiparameter instrument on-site. Chemical oxygen demand, phosphate, chloride,

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11

Adebayo, Ibikunle Farounbi, and Nelson Odume Oghenekaro. "Physicochemical and FT-IR analyses of some freshwater and inflow wastewater-treated effluents in the Eastern Cape Province of South Africa." GSC Advanced Research and Reviews 19, no. 1 (2024): 178–99. https://doi.org/10.5281/zenodo.13486928.

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Monitoring changes occurring in water bodies is a tool to make a sound decision on water quality management. This work investigates water quality parameters and metabolites in the Bloukrans, Buffalo, Swartkops and Tyhume Rivers in the Eastern Cape Province of South Africa. The water physicochemical parameters assessed include the dissolved oxygen, oxidation-reduction potentials, temperature, Hydrogen ion concentration, salinity, conductivity, turbidity and total dissolved solids measured with a pre-calibrated Hanna Multiparameter instrument on-site. Chemical oxygen demand, phosphate, chloride,

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12

Parveen, Mehtab, Afroz Aslam, Shahab A. A. Nami, and Musheer Ahmad. "Z-Acrylonitrile Derivatives: Improved Synthesis, X-ray Structure, and Interaction with Human Serum Albumin." Current Organic Synthesis 16, no. 8 (2020): 1149–60. http://dx.doi.org/10.2174/1570179416666191008085806.

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Aim and Objective: In the synthesis of heterocyclic compounds, acrylonitrile derivatives are the most important and appropriate precursors. These compounds are the most important intermediates and subunits for the enhancement of molecules having pharmaceutical or biological interests. Nitrogen-containing compounds have received extensive consideration in the literature over the years. Materials and Methods: A facile, economic and efficient method has been developed for the synthesis of acrylonitrile derivatives using p-nitrophenylacetonitrile and aromatic/heterocyclic aldehydes in the presence

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13

Rani, V. E., and L. K. Ravindranath. "Synthesis, Characterization and Antimicrobial Evaluation of Novel Mannich Bases Containing Pyrazole-5-One Phosphonates." Open Pharmaceutical Sciences Journal 3, no. 1 (2016): 49–55. http://dx.doi.org/10.2174/1874844901603010049.

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Background: Newly synthesised compounds of phosphonates were prepared by condensation of diethylphosphate with imine which undergoes a reaction of mannich bases with pyrazole containing schiffs base. The base was prepared by condensation of aldehyde with primary amine. These newly synthesised derivatives were characterised by spectral analysis. Objective: Mannich bases are very important to synthesize wide variety of natural products and pharmaceuticals. Method: Thin Layer Chromatography was performed on aluminum sheet of silica gel 60F254, E-Merk, Germany using iodine as visualizing agent. IR

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14

Nagaraj, Paramathevar, Muthupandian Ganesan, and Namakkal G. Ramesh. "InCl3–CH3CN–H2O: an efficient catalyst-solvent combination for the synthesis of Perlin aldehydes and related compounds. Application in the synthesis of unnatural l-azasugars." Tetrahedron 67, no. 4 (2011): 769–76. http://dx.doi.org/10.1016/j.tet.2010.11.050.

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15

Shi, Li-Lan, Zhang-Lin Zhou, and Yao-Zeng Huang. "Perkin communication. Formation of secondary alcohols from the reaction of trimethyl- and methyldiphenyl-telluronium salts with aldehydes by use of organolithium reagents." Journal of the Chemical Society, Perkin Transactions 1, no. 10 (1990): 2847. http://dx.doi.org/10.1039/p19900002847.

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16

Bogdanov, Milen G., Yavor Mitrev, and Ioannis Tiritiris. "New Highly Diastereoselective Perkin/Michael Addition Domino Reaction between Homophthalic Anhydride and Aromatic Aldehydes: A Facile Approach to Blue-Fluorescent Dibenzo[c,h]chromenones." European Journal of Organic Chemistry 2011, no. 2 (2010): 377–84. http://dx.doi.org/10.1002/ejoc.201000879.

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17

Malysheva, Alla G., O. V. Shelepova, and S. M. Yudin. "TRANSFORMATION OF THE COMPONENT STRUCTURE OF ESSENTIAL OIL AND VOLATILE ALLOCATION OF PLANTS UNDER THE IMPACT OF ARTIFICIAL LIGHTING." Hygiene and sanitation 98, no. 11 (2019): 1228–34. http://dx.doi.org/10.18821/0016-9900-2019-98-11-1228-1234.

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Introduction. Much attention is paid to the production of green products of aromatic plants from local raw materials, as one of the priorities implemented under the program “The Concept of the State Policy in the Field of Healthy Nutrition of the Population of the Russian Federation for the Period until 2020”. For the year-round consumption of green mass of plants, there are used different technologies of cultivation. Specific growing conditions (short light day and low light) in the autumn-winter period of highly productive plants in our country are possible only with the use of additional so

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18

Yadav, Yogesh, Amul Tiwari, Kavita Singh, and Ram Sagar. "Solvent-dependent Synthesis of Perlin’s Aldehyde from D-Glucal using Ceric Ammonium Nitrate and TMSCl." Synlett, July 3, 2025. https://doi.org/10.1055/a-2648-9142.

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In this study, a solvent-dependent ceric ammonium nitrate (CAN) and TMSCl-mediated synthesis of enantiopure 2,3-dideoxy-α,β-unsaturated carbohydrate enals (Perlin aldehydes), in CH3CN and 1,4-dioxane has been reported. This efficient protocol works well for the various D-glucals (O-acetyl, O-propyl, O-butyl, O-TIPS), and afforded Perlin aldehyde in acceptable to good yields. Thus, in this article we present a quick, efficient, and highly selective method for synthesizing Perlin aldehyde using CAN in 1.5 hours at 70 °C in good yield.

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19

Yadav, Yogesh, Rajdeep Tyagi та Ram Sagar. "Carbohydrate Derived α,β-Unsaturated Enals (Perlin’s Aldehyde) as Chiral Synthon for the Synthesis of Privileged Scaffolds". Current Organic Chemistry 28 (30 липня 2024). http://dx.doi.org/10.2174/0113852728320618240711104927.

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Perlin’s aldehyde is an α,β-unsaturated carbonyl compound with two well-defined chiral centres and a free hydroxy group. Since its discovery and synthesis by A. S. Perlin in 1975, it has been used as a flexible chiral synthon for synthesising natural products, its scaffolds and biologically significant compounds. Perlin’s aldehydes serve as useful starting materials in diversity-oriented synthesis (DOS) and chiral building blocks in organic synthesis. Currently, synthesising frameworks based on carbohydrates is at the forefront of organic synthesis. Inspired by the reactivity of Perlin’s aldeh

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20

Singh, Kavita, Sourav Sagar Behera, Rajdeep Tyagi, Ghanshyam Tiwari та Ram Sagar. "Metal free synthesis of 2,3-dideoxy-α, β-unsaturated carbohydrate enals (Perlin aldehydes)". Carbohydrate Research, червень 2023, 108890. http://dx.doi.org/10.1016/j.carres.2023.108890.

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21

Halder, Suvendu, Sangay Moktan, V. Sreeram, and Pavan K. Kancharla. "Synthesis of chiral functional polyhydroxylated arenes via Mukaiyama aldol reaction from Perlin aldehydes." Carbohydrate Research, December 2023, 109004. http://dx.doi.org/10.1016/j.carres.2023.109004.

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22

venkatapathy, K., and C. J. Magesh. "Synthesis, Spectral Characterization, Molecular Docking Studies, and Biological Evaluation of Pyranoquinolinyl Acrylic Acid (PQAA) Diastereomers as Antibacterial Agents Promoted by Indium (III) Triflate in 1-Butyl-3-Methylimidazolium Tetrafluoroborate Ionic Liquid." Letters in Organic Chemistry 21 (July 26, 2024). http://dx.doi.org/10.2174/0115701786333234240725110033.

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In the present investigation, we report the multistep synthesis of pyranoquinolinyl acrylic acid (PQAA)/furoquinolinyl acrylic acid (FQAA) diastereomers via perkin condensation and reduction, followed by one-pot inverse electron demand Diels-Alder reaction among 2,3 dihydropyran, amine, and aromatic aldehyde mediated by indium (III) triflate in 1-butyl-3-methylimidazolium tetrafluoroborate (In(OTf)3/ [bmim]BF4) at 25.0-27.0oC. The pyranoquinolinyl acrylic acid/furoquinolinyl acrylic acid diastereomers were evaluated for their in vitro antibacterial activity. Molecular docking studies were carr

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23

Krishna, M. P., and M. Mohan. "Evalution of Phytoconstituents of Syzygium arnottianum Leaves." International Journal of Pharmacognosy and Phytochemical Research 9, no. 10 (2017). http://dx.doi.org/10.25258/phyto.v9i10.10464.

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Aim: The present study is carried out to explore the major phytoconstituents and functional groups present in the methanolic extract of the leaves of Syzygium arnottianum using FTIR and GC-MS. Methods: For the identification of the phytochemical constituents, Perkin – Elmer GC Clarus 500 system (Auto system XL) Gas Chromatograph equipped and coupled to a mass detector Turbo mass gold – Perkin Elmer Turbomass 5.2 spectrometer with an Elite – 5MS (5% Diphenyl / 95% Dimethyl poly siloxane), 30m x 0.25 μm DF of capillary column is used. The molecular weight and structure of the compounds were dete

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24

Singh, Brajendra K., Sumit Kumar, Aditi Arora, Sandeep Kumar, Priti Kumari, and Sunil K. Singh. "Diastereoselective Synthesis of Carbohydrate Conjugates: Pyrano[3,2-c]quinolones." Synthesis, October 17, 2023. http://dx.doi.org/10.1055/s-0042-1751505.

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AbstractA facile and efficient protocol for the diastereoselective synthesis of pyrano[3,2-c]quinolone carbohydrate derivatives from Perlin aldehydes and 4-hydroxyquinolones has been developed using a one-pot condensation at room temperature. In this investigation, glucose and galactose were employed as inexpensive starting materials to synthesize two sets of pyrano[3,2-c]quinolone-based carbohydrate conjugates. A total of sixteen novel compounds were successfully synthesized using this methodology in good to excellent yields. The reaction exhibited remarkable diastereoselectivity, resulting i

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25

Mostoufi, Azar, Mohammad Reza Shushizadeh, Aedeh Sayahi, Seyed Mohammad Bagher Nabavi, and Bahar Mohandespour. "Marine solids/NaNO3: As Natural and Efficient Catalysts for Aldol condensation." International Journal of Ayurvedic Medicine 9, no. 1 (2018). http://dx.doi.org/10.47552/ijam.v9i1.1056.

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A new and efficient method have been developed for the synthesis of Î±,Î²-unsaturated carbonyl compounds from various aldehydes and ketones, using marine calcinated coral/NaNO3 and cuttlebone/NaNO3, as natural and efficient catalysts for cross aldol condensation. The aim of present study was to study the marine solids/NaNO3: as natural and efficient catalyst for Aldol condensation. The materials were purchased from Merck and Aldrich Companies. The IR spectra were recorded on a Perkin-Elmer RXI infrared spectrometer. H NMR spectra were recorded on a 400 MHz Brucker FT-NMR spectrometer. The SEM

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26

S, Sahaya Sathish, Janakiraman N, and Johnson M. "PHYTOCHEMICAL ANALYSIS OF VITEX ALTISSIMA L. USING UV-VIS, FTIR AND GC-MS." International Journal of Pharmaceutical Sciences and Drug Research, January 1, 2012, 56–62. https://doi.org/10.25004/ijpsdr.2012.040110.

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The present study was carried out to characterize the bioactive constituents present in different leaf extracts of Vitex altissima L. using UV-VIS, FTIR and GC-MS. The crude extracts were scanned in the wavelength ranging from 200-1100 nm by using Perkin Elmer Spectrophotometer and the characteristic peaks were detected. For GC-MS analysis, 10 g sample is extracted with 30 ml ethanol, filtered in ash less filter paper with 2 g sodium sulphate and the extract is concentrated to 1 ml by bubbling nitrogen into the solution. The compound detection employed the NIST Ver. 2.0 - Year 2005 library. Th

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27

Johnson, Marimuthu Antonysamy, and Joy Jeba Malar Tharmaraj Renisheya. "Spectroscopic profile as pharmacognostic criteria to distinguish the medicinally important Plumbago Species." Biohelikon 3, no. 1 (2015). https://doi.org/10.5281/zenodo.1069722.

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The root of the Plumbago species were examined phytochemically and their potentials are well studied. The spectrometric and chromatographic screening methods could provide the needed preliminary observations to select crude plant extracts with potentially useful properties for further chemical and pharmacological investigations. Objective: The present study was aimed to reveal the inter-specific similarity and variation among the selected Plumbago species viz., Plumbago zeylanica Linn, Plumbago auriculata Lam, Plumbago rosea Linn. using UV-VIS and FTIR profiles. Methods: To know the various ph

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28

Aslam, Afroz, Mehtab Parveen, and Kushvendra Singh. "Green synthesis of fused chromeno-pyrazolo-phthalazine derivatives with silica-supported bismuth nitrate under solvent-free condition." Current Organic Synthesis 17 (December 8, 2020). http://dx.doi.org/10.2174/1570179417666201208112520.

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Aim: To synthesize chromeno-pyrazolo[1,2-b]phthalazine-6,9,14(7H)-trione analogs with the help of silica-supported bismuth nitrate catalyst. Background: Nitrogen-containing heterocyclic compounds are widespread, and their applications to pharmaceuticals, agrochemicals, and functional materials are becoming more and more important. Pyrazoles are an important class of compounds for new drug development, as they are the core structure of numerous biologically active compounds, including blockbuster drugs such as celecoxib, viagra, pyrazofurine, and many others. Similarly, heterocycles containing

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29

Munde, Ganesh, Sunil S. Menghani, Nilesh Rarokar, Deweshri Kerzare, Mohammed Asif Ibal C., and P. B. Khedekar. "In-silico studies, Synthesis and Evaluation of Anti-inflammatory Activity of Novel Pyrimidine Scaffold." Letters in Drug Design & Discovery 19 (May 23, 2022). http://dx.doi.org/10.2174/1570180819666220523090351.

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Background: The heterocyclic nucleus pyrimidine is present in several natural and synthetic chemical analogues and has proved its broad medicinal applications. Further, pyrimidine in the form of parent structure or basic skeleton of RNA and DNA is involved in controlling the immune functioning, and in turn, inflammatory reactions. Method: Molecular docking studies of Indomethacin and selected analogues were carried out with COX-2 enzyme (PDB: 4ZOL). The synthesis of derivatives of 4-Phenyl-6-(phenylamino)pyrimidin-2-ol derivatives were begun by following Perkin condensation between substituted

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30

sprotocols. "Endodcytic labelling of visceral endoderm of mouse perigastrulation embryos." January 8, 2015. https://doi.org/10.5281/zenodo.13840.

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Authors: Yoh Wada, Minako Aoyama, Ge-Hong Sun-Wada, Nobuyuki Kawamura & Hiroyuki Tabata ### Abstract In this protocol we describe methods for observation endocytic activity in the mouse embryos. The methods are optimised for mouse embryos at E5.5~E7.2 pregastrulation/gastrulation stages. We optimise three different experimental schemes for tracing the embryonic endocytosis. In utero labelling scheme, an endocytic tracer is introduced into circulation of a pregnant mother to follow bulk uptake of fluid phase endocytosis. Rodent embryos are known to internalise maternal immunoglobulins, thus

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