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Journal articles on the topic 'Phthalic Acid Esters'

Author: Grafiati

Published: 7 June 2025

Last updated: 2 August 2025

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1

Zhao, Xiao Li, Wei Zhu, De Fu Xu, et al. "Contents and Characteristics of Phthalic Acid Esters in Municipal Sewage Sludge in Jiangsu Province." Advanced Materials Research 864-867 (December 2013): 861–65. http://dx.doi.org/10.4028/www.scientific.net/amr.864-867.861.

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Concentrations of 6 kinds of phthalic acid esters (PAEs) in sewage sludge from 20 typical municipal wastewater treatment plants (WWTPs) in Jiangsu province were determined by gas chromatography-mass spectrometry (GC-MS) . The results shows that the sewage sludge samples contain phthalic acid ester compounds, which total content of phthalic acid esters ( PAEs) range from 15.126 to 71.107 ug/g (dry sludge). The content of diethylhexyl phthalate (DEHP) is the highest, which amounts more than 80% of total phthalic acid esters (PAE); the content of dimethyl phthalate (DMP) is low ,which is less tha

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2

Shariati, S., C. Ebenau-Jehle, A. A. Pourbabaee, et al. "Degradation of dibutyl phthalate by Paenarthrobacter sp. Shss isolated from Saravan landfill, Hyrcanian Forests, Iran." Biodegradation 33, no. 1 (2021): 59–70. http://dx.doi.org/10.1007/s10532-021-09966-7.

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AbstractPhthalic acid esters are predominantly used as plasticizers and are industrially produced on the million ton scale per year. They exhibit endocrine-disrupting, carcinogenic, teratogenic, and mutagenic effects on wildlife and humans. For this reason, biodegradation, the major process of phthalic acid ester elimination from the environment, is of global importance. Here, we studied bacterial phthalic acid ester degradation at Saravan landfill in Hyrcanian Forests, Iran, an active disposal site with 800 tons of solid waste input per day. A di-n-butyl phthalate degrading enrichment culture

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3

Jarošová, A. "Phthalic acid esters (PAEs) in the food chain." Czech Journal of Food Sciences 24, No. 5 (2011): 223–31. http://dx.doi.org/10.17221/3318-cjfs.

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Phthalic acid esters (PAEs) rank among the primary risk pollutants and their adverse effects may endanger the environmental balance and affect the ontogenetic development of live organisms and their body functions. Therefore, the aim of this study was to monitor the occurrence of PAEs in packaging materials and plastics (infusion sets), to evaluate the accumulation and distribution of the most common phthalates such as DEHP (di-2-ethylhexyl phthalate) and DBP (di-n-butyl phthalate) in body tissues and organs of pigs and broiler chicks having been administered the phthalates per os, to assess t

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4

Jandlová, Marcela, Alžbeta Jarošová, Jozef Kameník, Vojtech Kumbár, and Šárka Nedomová. "The concentrations of phthalic acid esters in a water bath at sous-vide heat treatment." Potravinarstvo Slovak Journal of Food Sciences 13, no. 1 (2019): 681–87. http://dx.doi.org/10.5219/1114.

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Esters of phthalic acid are common contaminants of the environment because of their large application in plastics. Phthalic acid esters are used as plasticizers in plastics, and they are also used in plastic intended for contact with food. In our research, we investigated the influence of heating on the migration of phthalic acid esters into the water used as a water bath. The water bath was used to heat the vacuum-wrapped meat, this heating is called the sous-vide method. The plastic thermostable bags containing phthalates were used on the meat packaging. Two esters of phthalic acid dibutyl p

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5

Jandlová, Marcela, Vojtěch Kumbár, Alžbeta Jarošová, et al. "The Impact of Storage on Phthalic Acid Esters Concentrations in Yogurts Packed in Plastic Cups." Acta Universitatis Agriculturae et Silviculturae Mendelianae Brunensis 67, no. 3 (2019): 689–93. http://dx.doi.org/10.11118/actaun201967030689.

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Phthalic acid esters are used as plastic softeners and also can be found in food packaging materials. European legislation defines specific migration limits of plastic additives for plastic materials that come into contact with food. This study monitors the phthalic acid ester concentrations in yogurts after manufacturing and then after a 3‑week storage. The studied yoghurts were natural yogurt with 1 % of chia flour, natural yogurt with 5 % of chia flour, natural yogurt with 1 % of bamboo fibre, natural yogurt with 5 % of bamboo fibre and natural yogurt. The analysed phthalic acid esters were

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6

Liao, De Zhong, Jie Yu He, Li Xin Mao, and Yi Xue Xu. "Green Ester Lubricants Based on Rapeseed Acid and their Lubricity." Advanced Materials Research 781-784 (September 2013): 988–92. http://dx.doi.org/10.4028/www.scientific.net/amr.781-784.988.

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Several complex esters were synthesized from phthalic anhydride, neopentyl glycol and rapeseed acid. Their rheological properties, biodegradability and tribological properties were measured. It was found that the complex esters have a wide viscosity range of 126~325mm2/s at 40°C with viscosity indices about 127~143, and solidifying points lower than-38°C. The maximum non seizure load of a complex ester with degree of polymerization 1.42 is as high as 735 N, with a wear scar diameter of 0.41mm, superior to mineral oil. The biodegradation rates are higher than 73%, and the thermal stability is g

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7

Zhang, Yong Tao, Guo Xing Zhao, Li Zhang, Xiao Ya Li, Jian Ye Gui, and Chen Ling Zhang. "Ultrasonic Wave Extraction and Simultaneous Analysis of Polycyclic Aromatic Hydrocarbons (PAHs) and Phthalic Esters in Soil." Advanced Materials Research 726-731 (August 2013): 1555–59. http://dx.doi.org/10.4028/www.scientific.net/amr.726-731.1555.

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A method was developed for the determination of polycyclic aromatic hydrocarbons (PAHs) and Phthalic Acid Esters (PAEs) in soil sample. Ultrasonic Wave Extraction under airtight circumstance was adopted to extract the analyte in soil sample with n-hexane acetone (V:V=1:1) to be extraction solvent. This method has advantages of high efficiency extraction, short time, convenience and simplicity, which can be popularized in polycyclic aromatic hydrocarbons (PAHs) and Phthalic Acid Esters (PAEs) detection in soil.

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8

Tomoto, Takashi, and Akihiro Moriyoshi. "Decalcification mechanism of concrete by organic matters in atmosphere." Canadian Journal of Civil Engineering 35, no. 7 (2008): 744–50. http://dx.doi.org/10.1139/l08-038.

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This study confirmed that concrete structures and historical structures made of limestone absorb environmental endocrine disrupters such as anion surfactant and phthalic acid esters contained in windshield washer fluid by using 1H nuclear magnetic resonance (NMR), high-performance liquid chromatography (HPLC), gas chromatograph mass spectrometer (GC–MS), and other analytical techniques. Furthermore, it was confirmed that environmental endocrine disrupting organic matter, including phthalic acid esters, penetrated into concrete and accelerated its deterioration and that calcium salt of phthalic

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9

Xue, Linke, Dongxia Zhang, Tiane Wang, Xue-Mei Wang, and Xinzhen Du. "Dispersive liquid–liquid microextraction followed by high performance liquid chromatography for determination of phthalic esters in environmental water samples." Anal. Methods 6, no. 4 (2014): 1121–27. http://dx.doi.org/10.1039/c3ay41996g.

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10

Harazim, Jirí, Alžbeta Jarošová, Lenka Krátká, Vlasta Stancova, and Pavel Suchý. "Contamination of feedstuffs with phthalic acid esters." Toxicology Letters 180 (October 2008): S67. http://dx.doi.org/10.1016/j.toxlet.2008.06.564.

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11

Jonsson, S., V. A. Vavilin, and B. H. Svensson. "Phthalate hydrolysis under landfill conditions." Water Science and Technology 53, no. 8 (2006): 119–27. http://dx.doi.org/10.2166/wst.2006.242.

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Experimental data from a study using a landfill simulation reactor were used to develop and calibrate a one-dimensional distributed model of co-digestion of municipal solid waste and three phthalic acid diesters with different water solubilities. The three diesters were diethyl phthalate, dibutyl phthalate, and di-2-ethylhexyl phthalate. Two types of municipal solid wastes were assumed, easily degradable and recalcitrant. The model considered inhibition of hydrolysis of the recalcitrant fraction and phthalic acid esters, and also methanogenesis at acidic pH. The results indicated that the prol

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12

Lim, Duck Soo, Bum Soo Shin, Sun Dong Yoo, et al. "Toxicokinetics of Phthalic Acid: The Common Final Metabolite of Phthalic Acid Esters in Rats." Journal of Toxicology and Environmental Health, Part A 70, no. 15-16 (2007): 1344–49. http://dx.doi.org/10.1080/15287390701432293.

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13

Yan, Yinghua, Yujie Lu, Baichun Wang, et al. "Facile preparation of a hydrophilic magnetic hybrid nanomaterial with solid-phase extraction capability for highly efficient enrichment of phthalates in environmental water." Analytical Methods 10, no. 24 (2018): 2924–30. http://dx.doi.org/10.1039/c8ay00883c.

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14

Xu, Shuling, Hefu Li, Meng Guo, Lei Wang, Xia Li, and Qingwang Xue. "Liquid–liquid interfacial self-assembled triangular Ag nanoplate-based high-density and ordered SERS-active arrays for the sensitive detection of dibutyl phthalate (DBP) in edible oils." Analyst 146, no. 15 (2021): 4858–64. http://dx.doi.org/10.1039/d1an00713k.

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15

Huang, Ling, Xunzhi Zhu, Shixing Zhou, et al. "Phthalic Acid Esters: Natural Sources and Biological Activities." Toxins 13, no. 7 (2021): 495. http://dx.doi.org/10.3390/toxins13070495.

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Phthalic acid esters (PAEs) are a class of lipophilic chemicals widely used as plasticizers and additives to improve various products’ mechanical extensibility and flexibility. At present, synthesized PAEs, which are considered to cause potential hazards to ecosystem functioning and public health, have been easily detected in the atmosphere, water, soil, and sediments; PAEs are also frequently discovered in plant and microorganism sources, suggesting the possibility that they might be biosynthesized in nature. In this review, we summarize that PAEs have not only been identified in the organic

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16

Bajkin, Ivana, Artur Bjelica, Tijana Icin, Vesna Dobric, Branka Kovacev-Zavisic, and Milica Medic-Stojanoska. "Effects of phthalic acid esters on fetal health." Medical review 67, no. 5-6 (2014): 172–75. http://dx.doi.org/10.2298/mpns1406172b.

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Introduction. Phthalates are synthetic industrial compounds capable of disrupting endocrine system. Effects of phthalates depend on dosage, duration of action and stage of development of the individual, thus making the fetus, newborn, and children at puberty the most vulnerable groups. Metabolism of Phthalates: Metabolism of these compounds consists of at least two steps: hydrolysis and conjugation. They are mainly excreted in urine, with a low percent being excreted through feces. Exposure to Phthalates. Exposure to the effects of phthalates begins at the intrauterine stage since the phthalat

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17

Shanker, Rishi, C. Ramakrishma, and Prahlad K. Seth. "Degradation of some phthalic acid esters in soil." Environmental Pollution Series A, Ecological and Biological 39, no. 1 (1985): 1–7. http://dx.doi.org/10.1016/0143-1471(85)90057-1.

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18

Sato, K., T. Sato, H. Nagase, H. Kito, and K. Chikazawa. "Modification of chemical mutagenesis by phthalic acid esters." Mutation Research/Environmental Mutagenesis and Related Subjects 253, no. 3 (1991): 273–74. http://dx.doi.org/10.1016/0165-1161(91)90210-y.

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19

Salwa Abd Al-Satar Jabbar. "Synthesis and Characterization of some New Amic acid and Imides and study the Biological Activity." Tikrit Journal of Pure Science 23, no. 9 (2023): 39–50. http://dx.doi.org/10.25130/tjps.v23i9.811.

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This study includs the synthesis of some new Amic acid and Imides,starting from the esters [S1] of Terephthalic acid which then converted toits hydrazide [S2] then to amic acid derivatives [S3-S7] and finally withimides [S8-S12]. Preparing of ester [S1] by usual esterification ofterephthalic acid with absolute ethanol in acidic medium, then hasconverted to its hydrazide [S2] by reacting it with hydrazine hydrate. Theamic acid derivatives [S3-S7] have been synthesized by the reaction ofhydrazide [S2] with anhydrides (2,3-dimethyl malic anhydride, 3-nitrophthalic anhydride, hexahydro phthalic an

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20

Meghna, Verma, Deshmukh Vikrant, and Yadav Roshni. "Phthalic Acid Esters Accumulation and Biodegradation in Mesozooplankton: A Comprehensive Review." Int. Res. Journal of Science & Engineering, 2024, 12, no. 5 (2024): 269–77. https://doi.org/10.5281/zenodo.14430321.

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Ocean is a place for various living organisms but the threat to marine life is increasing day by day due to various anthropogenic activities such as dredging, over exploration, dumping of waste, and land reclamation. Burning of fossil fuel causes an increase in CO₂ content that decreases the pH of the ocean. Zooplankton are organisms that drift along the currents, tide and waves of the ocean. They are distributed unevenly all over the ocean. Their diversity, abundance and distribution are influenced by various climatic and physico-chemical parameters. Their existence plays an important role an

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21

Caporossi, Lidia, and Maria Marino. "Phthalate Exposure: From Quantification to Risk Assessment." Toxics 10, no. 6 (2022): 330. http://dx.doi.org/10.3390/toxics10060330.

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22

Ema, Makoto, Emiko Miyawaki, Akira Harazono, and Kunio Kawashima. "Developmental toxicity evaluation of phthalic acid, one of the metabolites of phthalic acid esters, in rats." Toxicology Letters 93, no. 2-3 (1997): 109–15. http://dx.doi.org/10.1016/s0378-4274(97)00078-7.

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23

Savinova, O. S., A. V. Shabaev, O. A. Glazunova, S. A. Eremin, and T. V. Fedorova. "Biodestruction of Phthalic Acid Esters by White Rot Fungi." Applied Biochemistry and Microbiology 58, no. 5 (2022): 598–612. http://dx.doi.org/10.1134/s0003683822050143.

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24

UMEDA, Hiroshi, Kokichi HAMADA, and Tosihide OKUNO. "Biodegradation of phthalic acid esters in the Kako River." Japan journal of water pollution research 11, no. 7 (1988): 427–33. http://dx.doi.org/10.2965/jswe1978.11.427.

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25

Painter, S. E., and W. J. Jones. "Anaerobic bioconversion of phthalic acid esters by natural inocula." Environmental Technology 11, no. 11 (1990): 1015–26. http://dx.doi.org/10.1080/09593339009384956.

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26

Zheng, Zhong, Pin-Jing He, Li-Ming Shao, and Duu-Jong Lee. "Phthalic acid esters in dissolved fractions of landfill leachates." Water Research 41, no. 20 (2007): 4696–702. http://dx.doi.org/10.1016/j.watres.2007.06.040.

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27

Wang, Jianlong, Ping Liu, and Yi Qian. "Biodegradation of phthalic acid esters by acclimated activated sludge." Environment International 22, no. 6 (1996): 737–41. http://dx.doi.org/10.1016/s0160-4120(96)00065-7.

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28

KASHIHIRA, Nobuyuki. "Response of phthalic acid esters to electron capture detector." Bunseki kagaku 36, no. 10 (1987): T103—T107. http://dx.doi.org/10.2116/bunsekikagaku.36.10_t103.

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29

Lu, Q., H. Shen, X. Wang, Y. Zhao, and X. Cai. "Exposure to phthalic acid esters in early human pregnancy." Fertility and Sterility 94, no. 4 (2010): S230—S231. http://dx.doi.org/10.1016/j.fertnstert.2010.07.895.

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30

Liu, L., L. Shen, F. Yang, F. Han, P. Hu, and M. Song. "Determining Phthalic Acid Esters Using Terahertz Time Domain Spectroscopy." Journal of Applied Spectroscopy 83, no. 4 (2016): 603–9. http://dx.doi.org/10.1007/s10812-016-0335-9.

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31

Bahrololoomi Fard, Sayyed Massoud, Seyyed Hamid Ahmadi, Mannan Hajimahmodi, Reza Fazaeli, and Mohsen Amini. "Preparation of magnetic iron oxide nanoparticles modified with imidazolium-based ionic liquids as a sorbent for the extraction of eight phthalate acid esters in water samples followed by UPLC-MS/MS analysis: an experimental design methodology." Analytical Methods 12, no. 1 (2020): 73–84. http://dx.doi.org/10.1039/c9ay02073j.

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In the present study, different ionic liquid modified magnetic nanoparticles have been prepared and tested as nano-metric adsorbents for the analysis of eight phthalic acid esters (PAEs) from water samples using dispersive micro solid-phase extraction (D-micro-SPE).

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32

Boldrini, Amedeo, Nicola Gaggelli, Francesco Falcai, et al. "Emerging Contaminants from Bioplastic Pollution in Marine Waters." Water 16, no. 24 (2024): 3676. https://doi.org/10.3390/w16243676.

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The increasing presence of compostable bioplastics as substitutes for conventional fossil-based plastics necessitates a deeper understanding of their environmental impacts, particularly in marine ecosystems, where they often accumulate. This study examines the leaching potential of different phthalic acid esters (PAEs) from commercial biodegradable plastic bags into natural seawater over a three-month period. Degradation experiments were conducted to investigate the release of PAEs under direct solar radiation exposure and in shielded conditions. 1H-NMR analysis of the seawater confirmed the r

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33

Shafikova, T. N., U. V. Оmelichkina, S. V. Boyarkina, А. G. Еnikeev, L. А. Мaksimova, and А. А. Semenov. "Detection of endogenous phthalates in bacterial pathogens of plants and animals." Доклады Академии наук 484, no. 1 (2019): 121–24. http://dx.doi.org/10.31857/s0869-56524841121-124.

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The endogenous esters of ortho-phthalic acid, dibutil phthalate (DBP) and di-(2-ethylhexil)-o-phthalate (DEHP), have been first detected in bacterial pathogens of plants (Clavibacter michiganensis ssp. sepedonicus, Pectobacterium carotovorum ssp. carotovorum, Rhizobium rhizogenes, Rhizobium radiobacter) and animals (Escherichia coli).

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34

Wang, Chun Xiao, Xiao Ling Shao, and Xiang Yang Wu. "Sorption of Phthalate Esters on Surficial Sediment of the Yangtze River, China." Advanced Materials Research 1073-1076 (December 2014): 263–67. http://dx.doi.org/10.4028/www.scientific.net/amr.1073-1076.263.

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The sorption of three kinds of phthalic acid esters (PAEs) in the Yangtze River sediment was investigated in this paper. Langmuir and Freundlich model were used to fit their adsorption isotherms. Results showed that Langmuir model could better fit the adsorption isotherms of PAEs in the sediment.

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35

Zhang, Bo, Hongmei Qu, Zhongxuan Li, Yuanyuan Zhai, Xiaolu Zhou, and Liqiang Liu. "Zirconocene-mediated selective synthesis of 1,4-bis(alkynyl)benzenes." Journal of Chemical Research 44, no. 9-10 (2020): 571–75. http://dx.doi.org/10.1177/1747519820912675.

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A series of novel 1,4-bis(alkynyl)benzene derivatives were synthesized from trimethylsilyl-substituted alkynes by the mediation of zirconocene with excellent regioselectivity in high yields. The 3,6-bis(trimethylsilyl)-4,5-dialkylphthalic acid dimethyl esters were prepared by cycloaddition of 2,5-bis(trimethylsilyl)zirconacyclopentadienes to dimethyl acetylenedicarboxylate. After iodination with iodine monochloride, 3,6-diiodo-4,5-dialkylphthalic acid dimethyl esters reacted with terminal alkynes to prepare the corresponding 1,4-bis(alkynyl)benzene derivatives by Sonogashira coupling reactions

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36

O'Conno, Owen A., M. D. Rivera, and L. Y. Young. "TOXICITY AND BIODEGRADATION OF PHTHALIC ACID ESTERS UNDER METHANOGENIC CONDITIONS." Environmental Toxicology and Chemistry 8, no. 7 (1989): 569. http://dx.doi.org/10.1897/1552-8618(1989)8[569:tabopa]2.0.co;2.

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37

Cheng, Hao, Chao Qin, Bing Yang, et al. "Non-covalent binding interaction between phthalic acid esters and DNA." Environment International 161 (March 2022): 107095. http://dx.doi.org/10.1016/j.envint.2022.107095.

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38

Hinton, R. H., F. E. Mitchell, A. Mann, et al. "Effects of phthalic acid esters on the liver and thyroid." Environmental Health Perspectives 70 (December 1986): 195–210. http://dx.doi.org/10.1289/ehp.8670195.

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39

Agarwal, D. K., W. H. Lawrence, L. J. Nunez, and J. Autian. "Mutagenicity evaluation of phthalic acid esters and metabolitesin salmonella typhimuriumcultures." Journal of Toxicology and Environmental Health 16, no. 1 (1985): 61–69. http://dx.doi.org/10.1080/15287398509530719.

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40

Zorníková, Gabriela, A. Jarošová, and L. Hřivna. "Distribution of phthalic acid esters in agricultural plants and soil." Acta Universitatis Agriculturae et Silviculturae Mendelianae Brunensis 59, no. 3 (2011): 233–38. http://dx.doi.org/10.11118/actaun201159030233.

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The study observed the occurrence of di-n-butyl phthalate (DBP) and di-(2-ethylhexyl) phthalate (DEHP) in the soil and agricultural crops (Triticum aestivum, Brassica napus, Zea mays) and their distribution to the individual parts. For the experiment were selected 4 locations in central Moravia. At two locations (L1, L2) winter wheat (Triticum aestivum) was grown, at the third location (L3) winter oilseed rape (Brassica napus), and at the fourth location (L4) flint corn (Zea mays). The soil samples (n = 72) and whole plant samples (n = 78) were collected during the vegetation. The aboveground

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41

Srivastava, Abhinav, Vinod P. Sharma, Ranu Tripathi, Rakesh Kumar, Devendra K. Patel, and Pradeep Kumar Mathur. "Occurrence of phthalic acid esters in Gomti River Sediment, India." Environmental Monitoring and Assessment 169, no. 1-4 (2009): 397–406. http://dx.doi.org/10.1007/s10661-009-1182-4.

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42

Hizal, G., Q. Q. Zhu, Ch H. Fischer, T. Majima, and W. Schnabel. "Photoreactions of phthalic acid dialkyl esters: a flash photolysis study." Journal of Photochemistry and Photobiology A: Chemistry 69, no. 1 (1992): 33–39. http://dx.doi.org/10.1016/1010-6030(92)85257-u.

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43

Tavares, I. A., and N. D. Vine. "Phthalic acid esters inhibit arachidonate metabolism by rat peritoneal leucocytes." Journal of Pharmacy and Pharmacology 37, no. 1 (1985): 67–68. http://dx.doi.org/10.1111/j.2042-7158.1985.tb04936.x.

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44

Kao, Po-Hsu, Fang-Yin Lee, and Zeng-Yei Hseu. "Sorption and Biodegradation of Phthalic Acid Esters in Freshwater Sediments." Journal of Environmental Science and Health, Part A 40, no. 1 (2005): 103–15. http://dx.doi.org/10.1081/ese-200033605.

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45

Begum, A., H. Katsumata, S. Kaneco, T. Suzuki, and K. Ohta. "Biodegradation of Phthalic Acid Esters by Bakery Yeast Saccharomyces cerevisiae." Bulletin of Environmental Contamination and Toxicology 70, no. 2 (2003): 255–61. http://dx.doi.org/10.1007/s00128-002-0185-4.

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46

Ren, Lei, Zhong Lin, Hongming Liu, and Hanqiao Hu. "Bacteria-mediated phthalic acid esters degradation and related molecular mechanisms." Applied Microbiology and Biotechnology 102, no. 3 (2017): 1085–96. http://dx.doi.org/10.1007/s00253-017-8687-5.

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47

Trotta, Francesco. "Phthalic acid esters hydrolysis under inverse phase-transfer catalysis conditions." Journal of Molecular Catalysis 85, no. 3 (1993): L265—L267. http://dx.doi.org/10.1016/0304-5102(93)80052-v.

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48

LAMB, J. "Reproductive effects of four phthalic acid esters in the mouse." Toxicology and Applied Pharmacology 88, no. 2 (1987): 255–69. http://dx.doi.org/10.1016/0041-008x(87)90011-1.

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49

O'Connor, Owen A., M. D. Rivera, and L. Y. Young. "Toxicity and biodegradation of phthalic acid esters under methanogenic conditions." Environmental Toxicology and Chemistry 8, no. 7 (1989): 569–76. http://dx.doi.org/10.1002/etc.5620080704.

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50

Li, Zhipeng, Yue Zhao, Yong Wang, Wen-Hua Zhang, and Chuanjiang Hu. "Chirality Sensing of Amino Acid Esters by S-2-Methylbutanamido-Substituted m-Phthalic Diamide-Linked Zinc Bisporphyrinate." Molecules 29, no. 15 (2024): 3652. http://dx.doi.org/10.3390/molecules29153652.

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Abstract:

To understand the role of an additional coordination site in the linker in chirality sensing, we designed and synthesized an S-2-methylbutanamido-substituted m-phthalic diamide-linked zinc bisporphyrinate, [Zn2(S-MAABis)] and investigated its ability to sense the chirality of amino acid esters. The 1H NMR spectra and the crystal structure showed that the amido oxygen adjacent to the chiral carbon was coordinated with zinc. NMR and UV–vis titration showed that the binding of [Zn2(S-MAABis)] to amino acid esters occurred via two equilibria, forming 1:1 and 1:2 host–guest complexes. The CD spectr

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