Academic literature on the topic 'Pre-derivatization'

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Journal articles on the topic "Pre-derivatization"

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SP., Karuppiah, and Anverbasha K. "Derivatization methodology in analytical separation." Journal of Indian Chemical Society Vol. 92, Apr 2015 (2015): 447–50. https://doi.org/10.5281/zenodo.5594449.

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Department of Chemistry, Sathyabama University, Chennai-600 117, India <em>E-mail </em>: Karu70123@rediffmail.com Derivatization is the transformation of one chemical compound into another with similar chemical structure. The chemical compounds specific functional group that involves in the derivatization reaction which transforms a educt to a derivate from boiling point, melting point, solubility, reactivity and chemical composition. This results in new chemical properties is used for separation and quantification. In HPLC there are two kinds of derivatization methods such as pre-column deriv
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Soma, Yuki, Yoshihiro Izumi, Takehiko Shimohira, et al. "In-Needle Pre-Column Derivatization for Amino Acid Quantification (iPDAQ) Using HPLC." Metabolites 12, no. 9 (2022): 807. http://dx.doi.org/10.3390/metabo12090807.

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Pre-column fluorescent derivatization has been used for the fast quantification of amino acids using high-performance liquid chromatography (HPLC) systems. However, it generally requires an offline in-vial derivatization process with multiple derivatization reagents. The offline derivatization requires the same number of reaction vials as the number of sample vials for use as a reaction chamber for the derivatization reaction in an autosampler. Therefore, the number of samples analyzed per batch using the pre-column derivatization method is halved. To benefit from the pre-column derivatization
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Sanzheev, A. P., A. A. Mikhina, D. A. Sevko, et al. "Existing problems and ways of their solution in the analysis of amino acid composition." Proceedings of the Voronezh State University of Engineering Technologies 80, no. 4 (2019): 185–89. http://dx.doi.org/10.20914/2310-1202-2018-4-185-189.

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For obtain accurate aminoacids analysis results for peptide samples it is need to pay attention for method of analysis and method of sample preparation. Now some samplpreparation methods are known: acid and basic hydrolysis. In this article the comparison of two methods of aminoacids analysis were observed: pre-column or post-column derivatization. Analysis of lysine in lysine sulphate was studied, results were compared with control samples. For pre-column derivatization o-phthalic anhydride was used, and for post-column derivatization ninhydrin reagent was used. In experimental part advantage
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Alimzhanova, M., and D. Makhayeva. "Identification of flavonoids in plant samples by gas chromatography-mass spectrometry with pre-derivatization." International Journal of Biology and Chemistry 9, no. 1 (2016): 46–51. http://dx.doi.org/10.26577/2218-7979-2016-9-1-46-51.

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Okayama, A., S. Fujii, and R. Miura. "Optimized fluorometric determination of urinary delta-aminolevulinic acid by using pre-column derivatization, and identification of the derivative." Clinical Chemistry 36, no. 8 (1990): 1494–97. http://dx.doi.org/10.1093/clinchem/36.8.1494.

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Abstract We previously reported the usefulness of a fluorometric method to determine urinary delta-aminolevulinic acid (ALA) concentrations by using post-column derivatization to monitor the effect of lead exposure. We have further improved the method by introducing pre-column derivatization by using reaction of ALA with acetylacetone and formaldehyde. Response of the hematopoietic system to lead exposure can now be easily detected at blood lead concentrations as low as 162 micrograms/L. The fluorescent ALA derivative, a new aromatic product, 2-methylideneamino-3,5-diacetyl-4,6-dimethylphenylp
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Xiao, Cenjun, Jing Xiao, Yuan Wu, et al. "Determination of Amino Acids of Novel Food in Food by HPLC Coupled with Pre-Column Derivatization." Foods 13, no. 24 (2024): 4012. https://doi.org/10.3390/foods13244012.

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A method for simultaneous determination of Theanine and γ-aminobutyric acid (GABA), as the novel food of amino acids, which was established using pre-column derivatization and high-performance liquid chromatography (HPLC). 4-Dimethylaminoazobe nzene-4′-sulfonyl chloride (DABS-Cl) is employed as the derivatization reagent with chromophore linked to Theanine and GABA, which lacks chromophore for DAD analysis in its pristine structure. After the detection wavelength was confirmed, the chromatographic and derivatization conditions were also optimized, including the chromatographic column, mobile p
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Kawasue, Shimba, Kyoko Kuniyoshi, Masashi Uema, and Naomasa Oshiro. "Tetrodotoxin Derivatization with a Newly Designed Boron Reagent Leads to Conventional Reversed-Phase Liquid Chromatography." Toxins 16, no. 6 (2024): 260. http://dx.doi.org/10.3390/toxins16060260.

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Tetrodotoxin (TTX) is a representative natural toxin causing pufferfish food poisoning, which is especially prominent in East and Southeast Asia, including Japan. TTX has been analyzed through post-column derivatization high-performance liquid chromatography (HPLC), ion-pair LC-MS(/MS), and hydrophilic interaction liquid chromatography (HILIC)-MS(/MS) as alternatives to the mouse bioassay method. However, post-column derivatization requires a system for online derivatization reactions, and with the ion-pair LC-MS approach, it is difficult to remove residual ion-pair reagents remaining in the e
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Itsusei, Fujita. "Determination of sugars in sports drinks." International Journal of Case Studies 1, no. 3 (2013): 1–6. https://doi.org/10.5281/zenodo.3520399.

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Mono- and disaccharides are routinely quantified with a differential refractometer. However, we developed a simpler analytical method involving pre-derivatization and high- performance liquid chromatography to achieve a high recovery rate.The purpose of our study was to understand the amount of sugar in sports drinks in order to determine marked consumption leads to tooth decay. Therefore, we quantified sugars in sports drinks.
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Bardelmeijer, Heleen A., Joop C. M. Waterval, Henk Lingeman, Ron van 't Hof, Auke Bult, and Willy J. M. Underberg. "Pre-, on- and post-column derivatization in capillary electrophoresis." Electrophoresis 18, no. 12-13 (1997): 2214–27. http://dx.doi.org/10.1002/elps.1150181212.

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Li, Yi, Jinhui Zhou, Xiaofeng Xue, et al. "Fluorometric determination of proline in honey by high-performance liquid chromatography after pre-column derivatization with 7-fluoro-4-nitrobenzo-2-oxa-1,3-diazole (NBD-F)." Analytical Methods 7, no. 18 (2015): 7625–30. http://dx.doi.org/10.1039/c4ay02886d.

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Dissertations / Theses on the topic "Pre-derivatization"

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Cavalheiro, Joana. "Développement de techniques de séparation et de détection pour l’analyse des polluants organiques et organométalliques dans des échantillons environnementaux." Thesis, Pau, 2014. http://www.theses.fr/2014PAUU3019/document.

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La Directive Cadre sur l'Eau (DCE) (2000/60) a mis en place une liste de 33 substances prioritaires, avec des normes qualité de l'environnement (NQE) pour chaque substance, et leur concentration dans les milieux aquatiques qui ne doivent pas dépasser c es NQE. De plus, elle exige des performances analytiques spécifiques pour ces méthodes: la limite de quantification doit être au moins aussi basse que 30% des NQE et l'incertitude de la méthode au niveau de la NQE doit être inférieure à 50%, pour k = 2. Par conséquent, le défi analytique actuel est de mesurer de faibles concentrations de ces pol
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Vítková, Kateřina. "Stanovení thiaminu v ječmeni, sladu a potravních doplňcích." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2008. http://www.nusl.cz/ntk/nusl-216421.

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The aim of this diploma thesis is focused on determination of B vitamin in food especially in malting barley and malt. This diploma thesis is consists of theoretical and experimental parts including the conclusion and supplements. Theoretical part describes thiamine characteristic, chemical structure, chemical and physical properties, function of thiamin in organism, impact it´s insufficiency to the human health, occurrence in common food and methods for it´s determination. Further are describing theoretical principles of high-efficiency liquid chromatography, chromatography on reverse phase,
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Books on the topic "Pre-derivatization"

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Lingeman, Hendrik. Selective pre-chromatographic derivatization methods for carboxylic acids: (high-performance liquid chromatography with fluorescence detection and gas-liquid chromatography with nitrogen-phosphorous detection). [s.n.], 1986.

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Noffsinger, James Bruce. Use of metal complexes for pre- and post-column derivatization with high performance liquid chromatography. 1986.

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Book chapters on the topic "Pre-derivatization"

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Cohen, Steven A. "Amino Acid Analysis Using Pre-Column Derivatization with 6-AminoquinolylN-Hydroxysuccinimidyl Carbamate." In Protein Sequencing Protocols. Humana Press, 2003. http://dx.doi.org/10.1385/1-59259-342-9:143.

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Li, Peng, and Guoyao Wu. "Analysis of Gizzerosine in Foodstuffs by HPLC Involving Pre-column Derivatization with o-Phthaldialdehyde." In Nutrition and Metabolism of Dogs and Cats. Springer Nature Switzerland, 2024. http://dx.doi.org/10.1007/978-3-031-54192-6_11.

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Cohen, Steven A., Thomas L. Tarvin, and Brian A. Bidlingmeyer. "Amino Acid Analysis Using Pre-Column Derivatization with Phenylisothiocyanate: Matrix Effects and Tryptophan Analysis." In Proteins. Springer US, 1987. http://dx.doi.org/10.1007/978-1-4613-1787-6_22.

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Hou, Yongqing, Xilong Li, Zhaolai Dai, Zhenlong Wu, Fuller W. Bazer, and Guoyao Wu. "Analysis of Glutathione in Biological Samples by HPLC Involving Pre-Column Derivatization with o-Phthalaldehyde." In Methods in Molecular Biology. Springer New York, 2017. http://dx.doi.org/10.1007/978-1-4939-7398-9_10.

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Deng, Shuang, David Scott, and Uttam Garg. "Quantification of Five Clinically Important Amino Acids by HPLC-Triple TOF™ 5600 Based on Pre-column Double Derivatization Method." In Clinical Applications of Mass Spectrometry in Biomolecular Analysis. Springer New York, 2016. http://dx.doi.org/10.1007/978-1-4939-3182-8_6.

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Taka-ichi, Ken-ichi. "Fluorometric Determination of MMAN as a Sensitizer in Water Gel Explosives by HPLC Using Pre-Column Derivatization with 7-Dimethylaminocoumarin-3-Carbonyl Fluoride." In Advances in Analysis and Detection of Explosives. Springer Netherlands, 1993. http://dx.doi.org/10.1007/978-94-017-0639-1_22.

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Czauderna, M., J. Kowalczyk, and E. Kwiatkowska. "HPLC methods with pre-column derivatization for measurement of 2, 6-diaminopimelic acid." In Book of Abstracts of the 48th Annual Meeting of the European Association for Animal Production. Brill | Wageningen Academic, 1998. https://doi.org/10.1163/9789004683976_194.

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Hase, Sumihiro. "Chapter 28 Pre- and post-column detection-oriented derivatization techniques in HPLC of carbohydrates." In Journal of Chromatography Library. Elsevier, 2002. http://dx.doi.org/10.1016/s0301-4770(02)80053-7.

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Hase, Sumihiro. "Chapter 15 Pre- and Post-Column Detection-Oriented Derivatization Techniques in HPLC of Carbohydrates." In Journal of Chromatography Library. Elsevier, 1995. http://dx.doi.org/10.1016/s0301-4770(08)60520-5.

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Brueckner, Hans, Matthias Langer, and Herbert Godel. "LC-Determination of D-and L-Amino Acids in Peptide Hydrolysates by Pre-column Derivatization with a Chiral Reagent." In Techniques in Protein Chemistry III. Elsevier, 1992. http://dx.doi.org/10.1016/b978-0-12-058756-8.50030-4.

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Conference papers on the topic "Pre-derivatization"

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Pisarev, D. I., and K. A. Alekseeva. "The use of RP HPLC with pre-column derivatization to determine glutathione in samples of natural origin." In Наука России: Цели и задачи. НИЦ «Л-Журнал», 2019. http://dx.doi.org/10.18411/sr-10-02-2019-63.

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