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Journal articles on the topic 'Preformulation studies'

Author: Grafiati

Published: 8 September 2021

Last updated: 25 July 2025

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1

Komal, Bhusare1* Prathamesh Regade2 Nikita Patil3 Sardar Shelake4 Nilesh Chougule5. "Preformulation Studies An Overview." International Journal in Pharmaceutical Sciences 2, no. 7 (2024): 984–96. https://doi.org/10.5281/zenodo.12739436.

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Preformulation studies are a crucial step in the pharmaceutical and drug development process. These studies provide a comprehensive understanding of the physicochemical properties of a drug candidate, guiding subsequent formulation and optimization efforts. This overview highlights the significance of preformulation studies in drug development, their key components, and their role in ensuring the success of pharmaceutical products. Preformulation studies encompass a range of investigations, including drug characterization, stability assessment, and formulation compatibility evaluation. Charact

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2

Kuehl, P. J., W. L. Hoye, and P. B. Myrdal. "Preformulation Studies on Imexon." Drug Development and Industrial Pharmacy 32, no. 6 (2006): 687–97. http://dx.doi.org/10.1080/03639040600599830.

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3

Rajput, Pallavi, and Anju Gauniya. "Preformulation Studies of Rosuvastatin." Journal of Drug Delivery and Therapeutics 9, no. 3-s (2019): 729–35. http://dx.doi.org/10.22270/jddt.v9i3-s.2968.

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Reliable experimental determination of the solubility of active pharmaceutical ingredients (APIs) in solvents and the correlation for solubility analysis is crucial for the accelerated design and optimization of procedures in the drug industry for isolation, purification and formulation. In this study, the antihypercholesterolemic drug rosuvastatin was evaluated for solubility, effect of pH, compatibity with various exepients. In this research, the rosuvastatin, an antihypercholesterolemic drug was analysed for solubility, pH effect, and compatibility with different excipients. Drug dispersion

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4

Middaugh, C. Russell. "Expediting Early Preformulation Studies." Genetic Engineering & Biotechnology News 32, no. 15 (2012): 42–43. http://dx.doi.org/10.1089/gen.32.15.16.

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5

Ledeţi, Ionuţ, Mihaela Budiul, Petru Matusz, et al. "Preformulation studies for nortriptyline." Journal of Thermal Analysis and Calorimetry 131, no. 1 (2017): 191–99. http://dx.doi.org/10.1007/s10973-017-6269-5.

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6

Aodah, Alhassan, Aaron Pavlik, Kelly Karlage, and Paul B. Myrdal. "Preformulation Studies on Piperlongumine." PLOS ONE 11, no. 3 (2016): e0151707. http://dx.doi.org/10.1371/journal.pone.0151707.

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7

Cristea, Mihaela, Bianca Baul, Ionuţ Ledeţi, et al. "Preformulation studies for atorvastatin calcium." Journal of Thermal Analysis and Calorimetry 138, no. 4 (2019): 2799–806. http://dx.doi.org/10.1007/s10973-019-08798-1.

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8

Uhljar, Luca É., Péter Gieszinger, Piroska Szabó-Révész, and Rita Ambrus. "Preformulation Studies of Polymeric Nanocapsules." Acta Pharmaceutica Hungarica 91, no. 3-4 (2021): 322–23. http://dx.doi.org/10.33892/aph.2021.91.322-323.

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9

El-Shattawy, Hamed, Alaa Kassem, and Mahmoud El-Razzaz. "Controlled-Release Frusemide Microcapsules: Preformulation Studies." Drug Development and Industrial Pharmacy 17, no. 18 (1991): 2529–37. http://dx.doi.org/10.3109/03639049109048092.

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10

Allen, John D., David Bentley, Rowan A. Stringer та Nicholas Lowther. "Hybrid (BDBB) interferon-α: preformulation studies". International Journal of Pharmaceutics 187, № 2 (1999): 259–72. http://dx.doi.org/10.1016/s0378-5173(99)00124-6.

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11

Odri, S., M. Stupar, I. Erös, et al. "Transdermal delivery of phénobarbital Preformulation studies." Journal of Drug Delivery Science and Technology 18, no. 6 (2008): 417–23. http://dx.doi.org/10.1016/s1773-2247(08)50081-5.

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12

Burger, Artur, and Anita Lettenbichler. "Polymorphism and preformulation studies of lifibrol." European Journal of Pharmaceutics and Biopharmaceutics 49, no. 1 (2000): 65–72. http://dx.doi.org/10.1016/s0939-6411(99)00053-3.

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13

Singh, Abhinam, and Jitender K. Malik. "Preformulation Studies of Famciclovir: Vital Part of Formulation Design." EAS Journal of Pharmacy and Pharmacology 7, no. 02 (2025): 40–46. https://doi.org/10.36349/easjpp.2025.v07i02.001.

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The preformulation investigation commences upon the introduction of a new molecule. It encompasses the examination of physical, chemical, analytical, and medicinal aspects associated with molecules and offers insights into appropriate modifications to enhance molecular performance. The study of preformulation parameters is associated with the development of effective, safe, stable, and dependable pharmaceutical formulations. Famciclovir is a diacetyl-6-deoxy derivative of penciclovir. All of this is absorbed upon oral administration and is rapidly converted to penciclovir through deacetylation

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14

Sharma, Shyam Bihari, Suman Jain, and K. Ganesan. "Preformulation Studies of Pralidoxime Chloride for Formulation Development of Microspheres." Journal of Drug Delivery and Therapeutics 9, no. 4-s (2019): 338–42. http://dx.doi.org/10.22270/jddt.v9i4-s.3336.

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Microspheres are one of the novel drug delivery system which possess several applications and are made up of assorted polymers. Microspheres can be defined as solid, approximately spherical particles ranging in size from 1 to 1000 μm range in diameter having a core of drug and entirely outer layers of polymers as coating material. They are made up of polymeric, waxy or other protective materials i.e. biodegradable synthetic polymer and modified natural products such as starches, gums, proteins, fats and waxes. Preformulation is a group of studies that focus on the physicochemical properties of

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15

Sharma, Neha, and Priyanka Ahirwar. "Oxcarbazepine: Preformulation Studies of Authoritative Part of Formulation Design." Middle East Research Journal of Pharmaceutical Sciences 3, no. 03 (2023): 46–50. http://dx.doi.org/10.36348/merjps.2023.v03i03.001.

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Preformulation research is a stage that is started before the novel molecule is seeded. In a larger sense, it connects with studies of a molecule's physical, chemical, analytical, and medicinal properties and offers ideas about appropriate modifications that could be made to improve performance. The analysis of preformulation characteristics can contribute to the development of pharmaceutical formulations that are efficient, safe, dependable, and stable. Oxcarbazepine is an antiepileptic drug. It controls seizures or fits by declining the abnormal and excessive activity of the nerve cells in t

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16

Tushar, B. Aher Prof. Poonam P. Khade Dr. Megha T. Salve. "Pharmaceutical Formulation and Development: A Comprehensive Review." International Journal in Pharmaceutical Sciences 1, no. 1 (2023): 346–55. https://doi.org/10.5281/zenodo.10144551.

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The abstract discusses the significance of preformulation studies, which analyze the physicochemical characteristics of potential new drug candidates and their impact on drug performance and dosage form development. These studies provide essential information for designing formulations and may indicate the need for molecular modifications. Before creating pharmaceutical formulations, it's crucial to consider the inherent chemical and physical properties of each drug, which serve as the foundation for combining them with other ingredients in dosage form production. The primary objective of pref

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17

Chaudhary, Amit, Shivalika, and Bhupendra Tomar. "Preformulation Studies of Livofloxacin as Nanoemulsion for Ocular Drug Delivery." Asian Pacific Journal of Health Sciences 9, no. 2 (2022): 8–13. http://dx.doi.org/10.21276/apjhs.2022.9.2.03.

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Objective: Levofloxacin is the L-isomer of the racemate ofloxacin, a quinolone antimicrobial agent. The objective of this article is to exhibit the quantitative methods used to determine consistency in developmental research. Author represented methods of preformulation for Levofloxacin as ocular nanoemulsion capable of delivering the drug in a sustained manner, thus avoiding frequent instillation of the drops which may induce toxic side effects and cellular damage at the ocular surface. Preformulation studies are essential to make sure the development of established as well as therapeutically

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18

Golhar, A. R., V. K. Ghume, A. N. Merekar, and M. D. Dokhe. "Preformulation Testing Studies of Solid Dosage Forms." American Journal of PharmTech Research 10, no. 2 (2020): 19–32. http://dx.doi.org/10.46624/ajptr.2020.v10.i2.003.

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19

Aboutaleb, A., A. Abdel Rahman, and M. Ahmed. "PREFORMULATION STUDIES ON DIRECTLY COMPRESSED TEMAZEPAM TABLETS." Bulletin of Pharmaceutical Sciences. Assiut 9, no. 2 (1986): 172–86. http://dx.doi.org/10.21608/bfsa.1986.74588.

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20

Chaudhary, Piyush. "PREFORMULATION STUDIES FOR AYURVEDA DRUGS: A REVIEW." International Research Journal Of Pharmacy 10, no. 3 (2019): 16–19. http://dx.doi.org/10.7897/2230-8407.100372.

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21

Williams, Robert O., and Vorapann Mahaguna. "Preformulation Studies on Freund's Incomplete Adjuvant Emulsion." Drug Development and Industrial Pharmacy 24, no. 2 (1998): 157–62. http://dx.doi.org/10.3109/03639049809085600.

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22

Ledeţi, Adriana, Gabriela Vlase, Titus Vlase, et al. "Solid-state preformulation studies of amiodarone hydrochloride." Journal of Thermal Analysis and Calorimetry 126, no. 1 (2016): 181–87. http://dx.doi.org/10.1007/s10973-016-5256-6.

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23

Kumar, Mukesh, Mohit Saini, and Lalit Parihar. "Preformulation Studies of Pantoprazole: Fundamental Part of Formulation Design." Saudi Journal of Medical and Pharmaceutical Sciences 8, no. 8 (2022): 370–80. http://dx.doi.org/10.36348/sjmps.2022.v08i08.001.

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Once the novel molecule is planted, preformulation study is one of the fractions that is started. In a larger sense, it covers with research on a molecule's physical, chemical, analytical, and medicinal properties and offers suggestions for effective modifications that could be made to improve performance. The study of preformulation factors can contribute to the development of pharmaceutical formulations that are dependable, safe, stable, and efficacious. Pantoprazole is an irreversible proton pump inhibitor (PPI) that reduces gastric acid secretion. PPIs, pantoprazole binds to the proton pum

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24

Sharma, Urvashi, and Sanjay Jain. "Preformulation Studies of Bergenin: A Primary Step in Future Designing of Novel Drug Delivery System." International Journal of Drug Delivery Technology 15, no. 02 (2025): 01–05. https://doi.org/10.25258/ijddt.15.2.9.

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Preformulation studies are an essential stage in drug development, focused on elucidating the physicochemical and pharmacokinetic characteristics of a drug candidate to inform formulation design. Bergenin, a naturally occurring Cglucoside derivative of gallic acid, demonstrates a diverse array of pharmacological properties, encompassing antiinflammatory, hepatoprotective, antiviral, and antidiabetic effects. Nonetheless, the effective incorporation of bergenin into an appropriate drug delivery system requires an extensive preformulation analysis. This research work was done with an objective t

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25

Arya, Usha, and Jitender K. Malik. "Preformulation Studies of Aceclofenac: Major Part of Formulation Strategy." EAS Journal of Pharmacy and Pharmacology 4, no. 6 (2022): 91–95. http://dx.doi.org/10.36349/easjpp.2022.v04i06.001.

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Preformulation studies are fractions that are initiated once new molecules are seeded. In a broader sense, it deals with the study of physical, chemical, analytical, and pharmacological properties associated with molecules, providing ideas for appropriate modifications of molecules for better performance. The study of pre-formulation parameters can lead to the production of effective, safer, stable and reliable drug formulations. Aceclofenac is an analgesic. It relieves pain, stiffness and swelling caused by various conditions of bones and joints. It is also used to relieve headaches, toothach

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26

Thumma, Sridhar, Soumyajit Majumdar, Mahmoud A. ElSohly, Waseem Gul та Michael A. Repka. "Preformulation Studies of a Prodrug of Δ9-Tetrahydrocannabinol". AAPS PharmSciTech 9, № 3 (2008): 982–90. http://dx.doi.org/10.1208/s12249-008-9136-7.

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27

Şahbaz, Sevinç. "Preformulation Studies of Transdermal Therapeutic Systems Containing Betahistine." MARMARA PHARMACEUTCAL JOURNAL 2, no. 19 (2015): 168. http://dx.doi.org/10.12991/mpj.20151910464.

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28

Suryanarayanan, Raj. "Applications of XRD in Preformulation and Formulation Studies." Acta Crystallographica Section A Foundations and Advances 70, a1 (2014): C1562. http://dx.doi.org/10.1107/s205327331408437x.

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Conventionally, XRD has found widespread use for the identification of crystalline solid phases. Recent advances in instrumentation and software extend the utility of the technique to the study of multicomponent systems. Thus the active pharmaceutical ingredient in a complex dosage form, and more importantly, phase transitions induced during processing and storage can be characterized and quantified. The use of an X-ray microdiffractometer with an area detector enabled us to monitor phase transformations in tablets. The spatial information, gained by monitoring the tablet from the surface to t

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29

Longhi, Marcela R., Maria M. De Bertorello, and Gladys E. Granero. "Isoxazoles. 8. Preformulation Studies of an Isoxazolylnaphthoquinone Derivative." Journal of Pharmaceutical Sciences 83, no. 3 (1994): 336–38. http://dx.doi.org/10.1002/jps.2600830314.

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30

Chandan, Ahirwar. "PREFORMULATION AND PRELIMINARY STUDY ON THE USE OF NATURAL POLYMERS FOR THE DEVELOPMENT OF ORODISPERSIBLE TABLET USING CUT AND WEIGH METHODS." IAJPS 03, no. 10 (2016): 1086–91. https://doi.org/10.5281/zenodo.162624.

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The complexity in the physicochemical characteristics of drugs and there In Vivo fate needs the quality of polymers to be that which could suppress the enzymatic action over drugs. The emergence of technology in an extraction procedure of herbal products has led to the development of various natural polymers which ensures the development of such dosage form that could easily deceive various factors affecting the degradation of drug within the body. The use of synthetic polymers in the formulation of orodispersible tablet was very common but high dispersion time, low hardness and failure in fri

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31

Chandan, Ahirwar* Ashwani Kumar Mishra Anupan Kumar Pathak. "PREFORMULATION AND PRELIMINARY STUDY ON THE USE OF NATURAL POLYMERS FOR THE DEVELOPMENT OF ORODISPERSIBLE TABLET USING CUT AND WEIGH METHODS." indo american journal of pharmaceutical sciences 03, no. 10 (2016): 1086–91. https://doi.org/10.5281/zenodo.163848.

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The complexity in the physicochemical characteristics of drugs and there In Vivo fate needs the quality of polymers to be that which could suppress the enzymatic action over drugs. The emergence of technology in an extraction procedure of herbal products has led to the development of various natural polymers which ensures the development of such dosage form that could easily deceive various factors affecting the degradation of drug within the body. The use of synthetic polymers in the formulation of orodispersible tablet was very common but high dispersion time, low hardness and failure in fri

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32

Venkatesh, S., B. N. Babu, K. Latha, R. Alvala, M. B. Reddy, and R. Mullangi. "EVALUATION OF TRAPA BISPINOSA STARCH AS AN ALTERNATIVE TABLET EXCIPIENT TO MAIZE STARCH: ASSESSMENT BY PREFORMULATION AND FORMULATION STUDIES." INDIAN DRUGS 49, no. 08 (2012): 27–32. http://dx.doi.org/10.53879/id.49.08.p0027.

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Starch isolated from Trapa bispinosa (Trapaceae) fruit was studied as an alternative pharmaceutical excipient to maize starch. T. bispinosa starch has been evaluated by series of tests as mentioned in Indian Pharmacopoeia before being used for evaluation. It was tested along with maize starch as an alternative excipient by performing battery of preformulation and formulation tests. Preformulation studies like sieve analysis, micrometry, flow properties, moisture content, swelling index and compatibility studies were done as per recommended procedures. The tablets were prepared by wet and dry g

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33

Vishwakarma, Girjesh, Subhendu Sekhar Mishra, and Hemant Kumar Nagar. "PREFORMULATION STUDIES OF STAVUDINE FOR TARGETED DRUG DELIVERY SYSTEM." International Research Journal of Pharmacy 6, no. 9 (2015): 640–43. http://dx.doi.org/10.7897/2230-8407.069125.

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34

Vlad, Robert-Alexandru, Paula Antonoaea, Nicoleta Todoran, et al. "Pharmacotechnical and analytical preformulation studies for cannabidiol orodispersible tablets." Saudi Pharmaceutical Journal 29, no. 9 (2021): 1029–42. http://dx.doi.org/10.1016/j.jsps.2021.07.012.

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35

Nyqvist, HÅRkan. "Preformulation Studies of Drug Substances for Solid Dosage Forms." Drug Development and Industrial Pharmacy 12, no. 7 (1986): 953–68. http://dx.doi.org/10.3109/03639048609048051.

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36

Chiang, Chin-Chih, Praveen Tyle, and Amanda Johnston. "Preformulation Studies on ag-392, a Novel Antitumor Compound." Drug Development and Industrial Pharmacy 20, no. 17 (1994): 2721–28. http://dx.doi.org/10.3109/03639049409042675.

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37

Chauhan, Suruchi, and Abhishek Dwivedi. "Preformulation Studies, UV Spectral and FTIR Analysis of Allicin." INTERNATIONAL JOURNAL OF PHARMACEUTICAL QUALITY ASSURANCE 15, no. 03 (2024): 1168–70. http://dx.doi.org/10.25258/ijpqa.15.3.11.

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Allicin is chemically known as 3-prop-2-enylsulfinylsulfanylprop-1-ene. It is a volatile compound and poorly soluble in water. With a molecular weight is 162.3 g/mol, it is also known as diallyldisulfi-S-oxide, S-allyl-prop-2-ene-1-sulfinothionate and diallyl thiosulfinate. In the present study pre-formulation studies, UV spectral and fourier-transform infrared (FTIR) analysis of allicin was reported.

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38

Khunteta, Alok, Manish Kumar Gupta, and Surendra Kumar Swarnkar. "Preformulation Studies of Rapid Dissolving Films Containing Granisetron Hydrochloride." Journal of Drug Delivery and Therapeutics 9, no. 4-A (2019): 511–15. http://dx.doi.org/10.22270/jddt.v9i4-a.3524.

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Rapid-dissolving solid drug dosage forms for application onto the oral cavity for the pediatric population seem to be very appropriate, especially in preterm and term infants. The delivery of drugs via the oral mucosa offers easy application, prevents drug degradation by gastrointestinal fluids, avoids first-pass metabolism and potentially improves bioavailability. Granisetron hydrochloride (GSH) drug is used as antiemetic agent. Proposed work comprise of preformulation studies of Granisetron hydrochloride. For that, physicochemical parameters were determined; like melting point of GSH was det

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39

Hageman, Michael J., Juliane M. Bauer, Peggy L. Possert, and Richard T. Darrington. "Preformulation studies oriented toward sustained delivery of recombinant somatotropins." Journal of Agricultural and Food Chemistry 40, no. 2 (1992): 348–55. http://dx.doi.org/10.1021/jf00014a036.

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40

Rabel, S. R., J. A. Jona, and M. B. Maurin. "Applications of modulated differential scanning calorimetry in preformulation studies." Journal of Pharmaceutical and Biomedical Analysis 21, no. 2 (1999): 339–45. http://dx.doi.org/10.1016/s0731-7085(99)00142-9.

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41

Migoha, C. O., M. Ratansi, E. Kaale, and G. Kagashe. "Preformulation Studies for Generic Omeprazole Magnesium Enteric Coated Tablets." BioMed Research International 2015 (2015): 1–9. http://dx.doi.org/10.1155/2015/307032.

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Preformulation is an important step in the rational formulation of an active pharmaceutical ingredient (API). Micromeritics properties: bulk density (BD) and tapped density (TD), compressibility index (Carr’s index), Hauser’s ratio (H), and sieve analysis were performed in order to determine the best excipients to be used in the formulation development of omeprazole magnesium enteric coated tablets. Results show that omeprazole magnesium has fair flow and compressibility properties (BD 0.4 g/mL, TD 0.485 g/mL, Carr’s index 17.5%, Hauser’s ratio 1.2, and sieve analysis time 5 minutes). There we

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42

Perioli, Luana, and Cinzia Pagano. "Preformulation studies of mucoadhesive tablets for carbamazepine sublingual administration." Colloids and Surfaces B: Biointerfaces 102 (February 2013): 915–22. http://dx.doi.org/10.1016/j.colsurfb.2012.10.001.

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43

Salnikova, Maya S., Sangeeta B. Joshi, J. Howard Rytting, Michel Warny, and C. Russell Middaugh. "Preformulation Studies of Clostridium difficile Toxoids A and B." Journal of Pharmaceutical Sciences 97, no. 10 (2008): 4194–207. http://dx.doi.org/10.1002/jps.21300.

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44

Nep, Elijah I., and Barbara R. Conway. "Preformulation studies on grewia gum as a formulation excipient." Journal of Thermal Analysis and Calorimetry 108, no. 1 (2011): 197–205. http://dx.doi.org/10.1007/s10973-011-1782-4.

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45

Longer, Mark, Irina Zamansky, Praveen Tyle, and Bhasker Shetty. "Preformulation Studies of a Novel HIV Protease Inhibitor, AG1343." Journal of Pharmaceutical Sciences 84, no. 9 (1995): 1090–93. http://dx.doi.org/10.1002/jps.2600840911.

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46

Peña, M. A. "Solubilization and Controlled Release Strategy of Poorly Water-Soluble Drugs." Pharmaceuticals 15, no. 11 (2022): 1353. http://dx.doi.org/10.3390/ph15111353.

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47

Chiş, Adriana Aurelia, Isabela Crăciun, Carmen Maximiliana Dobrea, Felicia Gabriela Gligor, Angela Bărbat, and Luca Liviu Rus. "Preformulation and preliminary formulation studies of mesalazine gastro-resistant tablets." Romanian Journal of Pharmaceutical Practice 13, no. 4 (2020): 207–13. http://dx.doi.org/10.37897/rjphp.2020.4.5.

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48

Chouksey, Khushi, Kuldeep Ganju, and Ganesh Prasad Patel. "Preformulation Studies of Econazole: A Vital Part of Formulation Design." Scholars Academic Journal of Pharmacy 9, no. 9 (2020): 253–56. http://dx.doi.org/10.36347/sajp.2020.v09i09.001.

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49

Saini, Mohit, Amit Kumar, Jitender Malik, Pankaj Singh Painwal, and Bipin Prakash Tamta. "Tramadol HCL: Preformulation Studies of Imperative Part of Formulation Design." Scholars Academic Journal of Pharmacy 9, no. 9 (2020): 257–62. http://dx.doi.org/10.36347/sajp.2020.v09i09.002.

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50

Sripetch, Suppakan, Alexey Ryzhakov, and Thorsteinn Loftsson. "Preformulation studies of dovitinib free base: Solubility, lipophilicity and stability." International Journal of Pharmaceutics 619 (May 2022): 121721. http://dx.doi.org/10.1016/j.ijpharm.2022.121721.

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