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Reshetyuk, Yuriy. "Investigation and calibration of pulsed time-of-flight terrestrial laser scanners." Licentiate thesis, Stockholm : Division of Geodesy, Royal Institute of Technology, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-4126.
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Qu, Guangzhi. "Resolution Limits of Time-of-Flight Mass Spectrometry with Pulsed Source." W&M ScholarWorks, 2016. https://scholarworks.wm.edu/etd/1477068405.
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Matrix Assisted Laser Desorption/Ionization (MALDI) is a time-of-flight mass spectrometry commonly used to detect a wide mass range of biomarkers. However, MALDI requires a high laser pulse energy to create ions with a mass higher than 50,000 Daltons. That high laser energy increases the net ion production but it also degrades the instrument's mass resolution. This project uses a Room Temperature Ionization Liquid (RTIL) as a liquid matrix with a self healing surface instead of a standard crystal matrix to increase shot to shot reproducibility, enabling a systematic study of the origin of the resolution degradation. This study shows that the main source of the resolution degradation is the ionic space charge which delays the ejection of ions into the acceleration region, essentially increasing the ionization pulse time to be as long as hundreds of nanoseconds. This study includes simulation and experimental results to document this effect.
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Hallman, L. (Lauri). "Single photon detection based devices and techniques for pulsed time-of-flight applications." Doctoral thesis, Oulun yliopisto, 2015. http://urn.fi/urn:isbn:9789526210445.
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Abstract In this thesis, a new type of laser diode transmitter using enhanced gain-switching suitable for use with a single photon avalanche diode (SPAD) detector was developed and tested in the pulsed time-of-flight laser range finding (lidar) application. Several laser diode versions were tested and the driving electronics were developed. The driving electronics improvements enabled a pulsing frequency of up to 1 MHz, while the maximum laser output power was about 5–40 W depending on the laser diode dimensions. The large output power is advantageous especially in conditions of strong photon noise emerging from ambient light outdoors. The length of the laser pulse matches the jitter of a typical SPAD detector providing several advantages. The new laser pulser structure enables a compact rangefinder for 50 m distance measurement outdoors in sunny conditions with sub-centimeter precision (σ-value) at a valid distance measurement rate of more than 10 kHz, for example. Single photon range finding techniques were also shown to enable a char bed level measurement of a recovery boiler containing highly attenuating and dispersing flue gas. In addition, gated single photon detector techniques were shown to provide a rejection of fluorescent photons in a Raman spectroscope leading to a greatly improved signal-to-noise ratio. Photonic effects were also studied in the case of a pulsed time-of-flight laser rangefinder utilizing a linear photodetector. It was shown that signal photon noise has an effect on the optimum detector configuration, and that pulse detection jitter can be minimized with an appropriate timing discriminatorTiivistelmä Tässä työssä kehitettiin uudentyyppinen, tehostettua "gain-switchingiä" hyödyntävä laserdiodilähetin käytettäväksi yksittäisten fotonien avalanche-ilmaisimien (SPAD) kanssa, ja sitä testattiin pulssin lentoaikaan perustuvassa laseretäisyysmittaussovelluksessa. Useita laserdiodiversioita testattiin ja ohjauselektroniikkaa kehitettiin. Ohjauselektroniikan parannukset mahdollistivat jopa 1 MHz pulssitustaajuuden, kun taas laserin maksimiteho oli noin 5–40 W riippuen laserdiodin dimensioista. Suuri lähtöteho on edullinen varsinkin vahvoissa taustafotoniolosuhteissa ulkona. Laserpulssin pituus vastaa tyypillisen SPAD-ilmaisimen jitteriä tarjoten useita etuja. Uusi laserpulssitinrakenne mahdollistaa esimerkiksi kompaktin etäisyysmittarin 50 m mittausetäisyydelle ulkona aurinkoisessa olosuhteessa mm–cm -mittaustarkkuudella (σ-arvo) yli 10 kHz mittaustahdilla. Yksittäisten fotonien lentoaikamittaustekniikan osoitettiin myös mahdollistavan soodakattilan keon korkeuden mittauksen, jossa on voimakkaasti vaimentavaa ja dispersoivaa savukaasua. Lisäksi portitetun yksittäisten fotonien ilmaisutekniikan osoitettiin hylkäävän fluoresenssin synnyttämiä fotoneita Raman-spektroskoopissa, joka johtaa selvästi parempaan signaali-kohinasuhteeseen. Fotoni-ilmiöitä tutkittiin myös lineaarista valoilmaisinta hyödyntävän pulssin kulkuaikamittaukseen perustuvan lasertutkan tapauksessa. Osoitettiin, että signaalin fotonikohina vaikuttaa optimaaliseen ilmaisinkonfiguraatioon, ja että pulssin ilmaisujitteri voidaan minimoida sopivalla ajoitusdiskriminaattorilla
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Moser, Matthew A. "Micro-and pulsed-plasmas fine tuning plasma energies for chemical analysis /." Morgantown, W. Va. : [West Virginia University Libraries], 2002. http://etd.wvu.edu/templates/showETD.cfm?recnum=2534.
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Thesis (Ph. D.)--West Virginia University, 2002.Title from document title page. Document formatted into pages; contains ix, 99 p. : ill. (some col.). Includes abstract. Includes bibliographical references.
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Hintikka, M. (Mikko). "Integrated CMOS receiver techniques for sub-ns based pulsed time-of-flight laser rangefinding." Doctoral thesis, Oulun yliopisto, 2019. http://urn.fi/urn:isbn:9789526221625.
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Abstract The goal of this work was to develop a CMOS receiver for a time-of-flight (TOF) laser rangefinder utilizing sub-ns pulses produced by a laser diode operating in gain switching mode (~ 1 nJ transmitter energy). This thesis also discusses the optical detector components and their usability with sub-ns optical pulses in laser rangefinding and the effect of the laser driver electronics on the shape of the sub-ns laser output, and eventually on the timing walk error of the laser rangefinder. The thesis presents the design of an integrated receiver channel IC intended for use in the pulsed TOF rangefinder. This is realized in a low-cost and consumer electronics-friendly CMOS technology (0.18 μm) and is based on a linear receiver and leading edge time discrimination. The measured walk error of the receiver is ~ 500 ps (4.5 cm in distance) within a 1:21,000 dynamic range. The measured jitter of the leading edge, affecting the single-shot precision of the radar, was ~ 12 ps (1.6 mm in distance) at an SNR > 200. In addition, a pulsed TOF rangefinder using the receiver IC developed here was designed and used for demonstrating the possibility of measuring tiny vibrations in a distant non-cooperative target. The radar was used successfully to observe 10 Hz vibrations in a non-cooperative target with an amplitude of 1.5 mm (sub-mm precision after averaging) at a distance of ~ 2 m. One important result was the demonstration of a difference in walk error behaviour between MOSFET and avalanche BJT-based laser pulse transmitters. The practicability of an integrated CMOS AP detector in sub-ns laser rangefinding was also studiedTiivistelmä Työn tavoitteena oli kehittää CMOS-vastaanotin valon kulkuaikamittaukseen perustuvaan laseretäisyysmittariin, joka hyödyntää ”gain-switching”-tekniikalla toimivan laserdiodin (~ 1 nJ energia) tuottamia alle nanosekuntiluokan laserpulsseja. Väitöskirja tutkii myös valovastaanotinkomponenttien käyttökelpoisuutta alle nanosekuntiluokan laserpulsseja hyödyntävässä laseretäisyysmittauksessa. Työssä tutkitaan myös laserdiodilähettimen elektroniikan vaikutusta alle nanosekuntiluokan laserpulssien muotoon ja lopulta niiden vaikutusta systemaattiseen ajoitusvirheeseen laseretäisyysmittauksessa. Väitöskirja esittelee suunnitellun valopulssin kulkuaikamittaukseen perustuvaan laseretäisyysmittariin soveltuvan integroidun vastaanotinkanavan IC-piirin. Se on toteutettu halvalla, kulutuselektroniikkaan soveltuvalla CMOS tekniikalla (0,18 μm) ja se perustuu lineaariseen vastaanottimeen ja nousevan reunan ilmaisuun. Vastaanottimen mitattu systemaattinen ajoitusvirhe on ~ 500 ps (4,5 cm matkassa) 1:21 000 signaalivoimakkuuden vaihtelualueella. Vastaanottimesta mitattu laseretäisyysmittarin kertamittaustarkkuuteen vaikuttava nousevan reunan satunnainen ajoitusepävarmuus oli ~ 12 ps (1.6 mm matkassa) signaalikohinasuhteella > 200. Lisäksi tässä työssä toteutettiin kehitettyä vastaanotin-IC piiriä hyödyntävä valopulssin kulkuaikamittaukseen perustuva etäisyysmittari, jolla kyettiin havainnollistamaan mahdollisuutta mitata pientä tärinää kaukaisessa passiivisessa kohteessa. Tutkalla onnistuttiin havainnoimaan 1,5 mm vaihteluväliltään olevaa 10 Hz tärinä ~ 2 m etäisyydellä olevasta kohteesta. Väitöskirjan yksi tärkeä tulos oli havainnollistaa systemaattisessa ajoitusvirheessä havaittava ero MOSFET-transistoriin ja vyöry-BJT-transistoriin perustuvan laserpulssilähettimen välillä. Integroidun CMOS AP vastaanotinkomponentin käyttökelpoisuus alle nanosekuntiluokan laseretäisyysmittauksessa tutkittiin myös
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Nissinen, I. (Ilkka). "CMOS time-to-digital converter structures for the integrated receiver of a pulsed time-of-flight laser rangefinder." Doctoral thesis, Oulun yliopisto, 2011. http://urn.fi/urn:isbn:9789514295478.
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Abstract The aim of this thesis was to develop time-to-digital converters (TDC) for the integrated receiver of a pulsed time-of-flight (TOF) laser rangefinder aiming at cm-level accuracy over an input range of 10 m – 15 m. A simple structure, a high integration level and low power consumption are the desired features for such a TDC. From the pulsed TOF laser rangefinder point of view an integrated receiver consisting of both the TDC and the receiver channel on the same die offers the possibility of manufacturing these laser rangefinders with a high integration level and at a low price to fulfil the needs of mass industrial markets. The heart of the TDC is a CMOS ring oscillator, the clock frequency of which is used to calculate the full clock cycles between timing signals, the positions of the timing signals inside the clock period being determined by storing the state of the phase of the ring oscillator for each timing signal. This will improve the resolution of the TDC. Also, additional delay lines are used to generate multiple timing signals, each having a time difference of a fraction of that of the ring oscillator. This will further improve the resolution of the whole TDC. To achieve stable results regardless of temperature and supply voltage variations, the TDC is locked to an on-chip reference voltage, or the resolution of the TDC is calibrated before the actual time interval measurement. The systematic walk error in the receiver channel caused by amplitude variation in the received pulse is compensated for by the TDC measuring the slew rate of the received pulse. This time domain compensation method is not affected by the low supply voltage range of modern CMOS technologies. Three TDC prototypes were tested. A single-shot precision standard deviation of 16 ps (2.4 mm) and a power consumption of 5.3 mW/channel were achieved at best over an input range of 100 ns (15 m). The temperature drifts of an on-chip voltage reference-locked TDC and a TDC based on the calibration method were 90 ppm/°C and 0.27 ps/°C, respectively. The results also showed that a pulsed TOF laser rangefinder with cm-level accuracy over a 0 – 15 m input range can be realized using the integrated receiver with the time domain walk error compensation described hereTiivistelmä Väitöskirjatyön tavoitteena oli kehittää aika-digitaalimuunninrakenteita valopulssin kulkuajan mittaukseen perustuvan lasertutkan integroituun vastaanottimeen. Tavoitteena oli saavuttaa senttimetriluokan tarkkuus 10 m – 15 m mittausalueella koko lasertutkan osalta. Aika-digitaalimuuntimelta vaaditaan yksinkertaista rakennetta, korkeaa integroimisastetta ja matalaa tehonkulutusta. Integroitu vastaanotin sisältää sekä aika-digitaalimuuntimen että vastaanotinkanavan ja tarjoaa mahdollisuuden korkeasti integroidun lasertutkan valmistukseen halvalla teollisuuden massamarkkinoiden tarpeisiin. Aika-digitaalimuuntimen ytimenä toimii monivaiheinen CMOS-rengasoskillaattori. Aika-digitaalimuunnos perustuu rengasoskillaattorin täysien kellojaksojen laskentaan laskurilla ajoitussignaalien välillä. Lisäksi rengasoskillaatorin jokaisesta vaiheesta otetaan näyte ajoitussignaaleilla niiden paikkojen määrittämiseksi kellojakson sisällä, jolloin aika-digitaalimuuntimen erottelutarkkuutta saadaan parannettua. Erottelutarkkuutta parannetaan lisää viivästämällä ajoitussignaaleja viive-elementeillä ja muodostamalla näin useita erillisiä ajoitussignaaleja, joiden väliset viive-erot ovat murto-osa rengasoskillaattorin viive-elementin viiveestä. Aika-digitaalimuunnin stabiloidaan käyttöjännite- ja lämpötilavaihteluja vastaan lukitsemalla se integroidun piirin sisäiseen jännitereferenssiin, tai sen erottelutarkkuus määritetään ennen varsinaista aikavälinmittausta erillisellä kalibrointimittauksella. Vastaanotetun valopulssin amplitudivaihtelun aiheuttama systemaattinen ajoitusvirhe integroidussa vastaanotinkanavassa kompensoidaan mittaamalla vastaanotetun valopulssin nousunopeus aika-digitaalimuuntimella. Tällainen aikatasoon perustuva kompensointimetodi on myös suorituskykyinen nykyisissä matalakäyttöjännitteisissä CMOS-teknologioissa. Työssä valmistettiin ja testattiin kolme aika-digitaalimuunninprototyyppiä. Muuntimien kertamittaustarkkuuden keskihajonta oli parhaimmillaan 16 ps (2,4 mm) ja tehonkulutus alle 5,3 mW/kanava mittausetäisyyden olessa alle 100 ns (15 m). Sisäiseen jännitereferenssiin lukitun aika-digitaalimuuntimen lämpötilariippuvuudeksi mitattiin 90 ppm/°C ja kalibrointimenetelmällä saavutettiin 0,27 ps/°C lämpötilariipuvuus. Työssä saavutetut tulokset osoittavat lisäksi, että valopulssin kulkuajan mittaukseen perustuvalla lasertutkalla on saavutettavissa senttimetriluokan tarkkuus 0 – 15 m mittausalueella käyttämällä tässä työssä esitettyä integroitua vastaanotinta ja aikatason ajoitusvirhekompensointia
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Kilpelä, A. (Ari). "Pulsed time-of-flight laser range finder techniques for fast, high precision measurement applications." Doctoral thesis, University of Oulu, 2004. http://urn.fi/urn:isbn:9514272625.
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Abstract
This thesis describes the development of high bandwidth (~1 GHz) TOF (time-of-flight) laser range finder techniques for industrial measurement applications in the measurement range of zero to a few dozen metres to diffusely reflecting targets. The main goal has been to improve single-shot precision to mm-level in order to shorten the measurement result acquisition time.
A TOF laser range finder consists of a laser transmitter, one or two receivers and timing discriminators, and a time measuring unit. In order to improve single-shot precision the slew-rate of the measurement pulse should be increased, so the optical pulse of the laser transmitter should be narrower and more powerful and the bandwidth of the receiver should be higher without increasing the noise level too much.
In the transmitter usually avalanche transistors are used for generating the short (3–10 ns) and powerful (20–100 A) current pulses for the semiconductor laser. Several avalanche transistor types were compared and the optimization of the switching circuit was studied. It was shown that as high as 130 A current pulses are achievable using commercially available surface mount avalanche transistors.
The timing discriminator was noticed to give the minimum walk error, when high slew rate measurement pulses and a high bandwidth comparator were used. A walk error of less than +/- 1 mm in an input amplitude dynamic range higher than 1:10 can be achieved with a high bandwidth receiver channel. Adding an external offset voltage between the input nodes of the comparator additionally minimized the walk error.
A prototype ~1 GHz laser range finder constructed in the thesis consists of a laser pulser and two integrated ASIC receiver channels with silicon APDs (avalanche photodiodes), crossover timing discriminators and Gilbert cell attenuators. The laser pulser utilizes an internal Q-switching mode of a commercially available SH-laser and produces optical pulses with a pulse peak power and FWHM (full-width-at-half-maximum) of 44 W and 74 ps, respectively. Using single-axis optics and 1 m long multimode fibres between the optics and receivers a total accuracy of +/-2 mm in the measurement range of 0.5–34.5 m was measured. The single-shot precision (σ-value) was 14 ps–34 ps (2–5 mm) in the measurement range. The single-shot precision agrees well with the simulations and is better with a factor of about 3-5 as compared to earlier published pulsed TOF laser radars in comparable measuring conditions.
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Palojärvi, P. (Pasi). "Integrated electronic and optoelectronic circuits and devices for pulsed time-of-flight laser rangefinding." Doctoral thesis, University of Oulu, 2003. http://urn.fi/urn:isbn:9514269667.
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Abstract
The main focus of this work concerned with the development of integrated electronic and optoelectronic circuits and devices for pulsed time-of-flight laser rangefinding is on the construction of the receiver channel, system level integration aimed at realisation of the laser radar module and in integration of all the receiver functions of laser radar on one chip.
Since the timing discriminator is a very important part of a pulsed
time-of-flight laser rangefinder, two timing discrimination methods are presented and verified by means of circuit implementations, a leading edge discriminator and a high-pass timing discriminator. The walk error of the high-pass timing discriminator is ±4 mm in a dynamic range of 1:620 and the uncompensatable walk error of the leading edge discriminator is ±30 mm in a dynamic range of 1:4000. Additionally a new way of combining the timing discriminator with time interval measurement is presented which achieves a walk error of ±0.5 mm in a dynamic range of 1:21.
The usability of the receiver channel chip is verified by constructing three prototypes of pulsed TOF laser radar module. The laser
radar achieves mm-level accuracy in a measurement range from 4 m to 34 m with non-cooperative targets. This performance is similar to that of earlier realisations using discrete components or even better and has markedly reduced power consumption and size.
The integration level has been increased further by implementing a photodetector on the same chip as the rest of the receiver electronics. The responsivity of the photodetector is about 0.3 A/W at 850 nm wavelength and the noise of the receiver is reduced by a factor of about two relative to realisations using an external photodetector, because of the absence of parasitic capacitances and inductances caused by packages, PCB wiring, bond wires and ESD and I/O cell structures.
The functionality of a multi-channel pulsed TOF laser radar chip is demonstrated using the photodiode structure investigated here. The chip includes four photodetectors with receiver channels and a three-channel time-to-digital converter. The chip together with external optics and a laser pulse transmitter enables distances to be measured in three directions with a single optical pulse, thus showing the feasibility of implementing all the receiver functions of a pulsed time-of-flight imager on a single chip using a current semiconductor process.
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Ruotsalainen, T. (Tarmo). "Integrated receiver channel circuits and structures for a pulsed time-of-flight laser radar." Doctoral thesis, University of Oulu, 1999. http://urn.fi/urn:isbn:9514252160.
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This thesis describes the development of integrated structures and circuit implementations for the receiver channel of portable pulsed time-of-flight laser rangefinders for industrial measurement applications where the measurement range is from ∼1 m to ∼100 m to noncooperative targets and the required measurement accuracy is from a few millimetres to a few centimetres. The receiver channel is used to convert the current pulse from a photodetector to a voltage pulse, amplify it, discriminate the timing point and produce an accurately timed logic-level pulse for a time-to-digital converter.
Since the length of the laser pulse, typically 5 ns, is large compared to the required accuracy, a specific point in the pulses has to be discriminated. The amplitude of the input pulses varies widely as a function of measurement range and the reflectivity of the target, typically from 1 to 100 ... 1000, so that the gain of the amplifier channel needs to be controlled and the discrimination scheme should be insensitive to the amplitude variation of the input signal. Furthermore, the amplifier channel should have low noise in order to minimize timing jitter.
Alternative circuit structures are discussed, the treatment concentrating on the preamplifier, gain control circuitry and timing discriminator, which are the key circuit blocks from the performance point of view. New circuit techniques and structures, such as a fully differential transimpedance preamplifier and a current mode gain control scheme, have been developed. Several circuit implementations for different applications are presented together with experimental results, one of them being a differential BiCMOS receiver channel with a bandwidth of 170 MHz, input referred noise of 6 pA/√Hz
and maximum transimpedance of 260 kW. It has an accuracy of about +/- 7 mm (average of 10000 measurements), taking into account walk error with an input signal range of 1:624 and jitter (3s).
The achievable performance level using integrated circuit technology is comparable or superior to that of the previously developed commercially available discrete component implementations, and the significantly reduced size and power consumption open up new application areas.
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Kurtti, S. (Sami). "Integrated receiver channel and timing discrimination circuits for a pulsed time-of-flight laser rangefinder." Doctoral thesis, Oulun yliopisto, 2013. http://urn.fi/urn:isbn:9789526200460.
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Abstract In this thesis integrated receiver channel techniques and circuit implementations for a pulsed time-of-flight (TOF) laser rangefinder are developed with the aim to achieve centimetre level accuracy within the dynamic range of > 1:10 000 of the input pulse amplitudes. The receiver channel converts the input current pulses produced by the photo detector to voltage pulses and produces a logic-level timing pulse for the time interval measurement. In addition to the minimization of noise, the main design challenge is the minimization of the timing walk error resulting from the varying amplitude of the received optical echo. In automotive perception laser radar application, which was the target application of this work, the input amplitude of the received echo varies in a range of 1:10 000 or even more due to changes in the measured distance and reflectivity and orientation of the target. Two receiver channel and timing discriminator architectures were developed and realized as integrated circuits in 0.35 μm BiCMOS technology, and finally verified by measurements. One of the receiver channels is based on the detection of the zero-crossing of the timing pulse produced with a unipolar-to-bipolar conversion at the input of the receiver. It achieved a timing walk error of ±8 mm in a dynamic range of 1:3000. Another receiver channel is based on the leading edge timing discrimination, in which the timing walk error is being compensated for in time domain by measuring the width of the timing pulse simultaneously with its leading edge time position. An important feature of this technique, suggested in this thesis, is that it is operative also beyond the linear range of the receiver channel, which is typically limited to < 1:100. The receiver channel with leading edge detection and pulse width compensation achieved a compensated walk error of ± 2–3 mm in a dynamic range of ~ 1:100 000. The bandwidth and input referred current noise of the channel were 230 MHz and <100 nArms, respectively. The single-shot timing precision was 120 ps (20 mm in distance) at the SNR of 10. The feasibility of the receiver electronics was verified by two laser radar prototypes. An accuracy of < ± 5 mm was measured in a measurement range from 1 to 55 m, which corresponds to the receiver dynamic range of > 1:10 000 taking into consideration the varying reflectivity of the target materials usedTiivistelmä Väitöskirjatyössä on suunniteltu integroituja vastaanotintekniikoita ja –piirejä valopulssin kulkuaikamittaustekniikkaan perustuvaan laseretäisyysmittaukseen. Tavoitteena on ollut saavuttaa senttimetriluokan tarkkuus laajalla tulopulssin amplitudin dynaamisella alueella > 1:10 000. Vastaanotinkanava muuntaa valoilmaisimelta saadun tulovirtapulssin jännitepulssiksi ja muodostaa siitä logiikkatasoisen ajoituspulssin aikavälimittauspiirille. Kohinan minimoimisen lisäksi toinen suuri suunnitteluhaaste on minimoida ajoitusvirhe, jota syntyy vastaanotetun optisen tulosignaalin amplitudin vaihdellessa laajalla alueella. Työssä kehitettyjen vastaanotinkanavien yksi sovelluskohdetavoitteista on ollut autoteollisuudessa käytettävät etäisyysmittarit. Näissä tulosignaalin taso vaihtelee erittäin laajalla dynaamisella alueella, joka voi olla > 1:10 000, johtuen laajasta etäisyysmittausalueesta sekä kohteen heijastavuuden ja orientaation vaihteluista. Väitöskirjatyössä kehitettiin ja valmistettiin kaksi vastaanotin- ja ajoitusilmaisurakennetta. Piirit valmistettiin 0,35 μm BiCMOS- teknologialla, ja niiden toiminta varmistettiin mittauksilla. Ensimmäinen vastaanotinkanava-arkkitehtuuri perustuu kanavan tulossa tapahtuvaan unipolaari-bipolaari muutokseen ja sen jälkeiseen nollaylityskohdan ilmaisuun. Piirillä saavutettiin ±8 mm ajoitusvirhe 1:3000 dynaamisella alueella. Toinen vastaanotinkanava-arkkitehtuuri perustuu etureunanilmaisuun, jossa ajoitusvirhe korjataan aikatasossa mittaamalla samanaikaisesti ajoituspulssin paikka ja leveys. Ajoitusvirheenkorjausmenetelmän tärkeä ominaisuus on, että se toimii laajemmalla kuin vastaanottimen lineaarisella alueella (< 1:100). Etureunanilmaisuun ja pulssinleveyden korjaukseen perustuvalla vastaanotinkanavalla saavutettiin korjattu ajoitusvirhe ± 2–3 mm 1:100 000 dynaamisella alueella. Kanavan kaistanleveys oli 230 MHz ja tulon redusoitu virtakohina < 100 nArms. Signaalikohinasuhteella 10 laseretäisyysmittauksen kertamittaustarkkuudeksi mitattiin 120 ps (20 mm etäisyydessä). Väitöskirjatyön yhteydessä valmistettiin lisäksi kaksi prototyyppilasertutkaa, joilla varmistettiin vastaanotinelektroniikan toiminta laajalla > 1:10 000 dynaamisella tulopulssin amplitudin vaihtelualueella. Lasertutkan ajoitusvirheeksi mitattiin < ± 5 mm 1–55 m:n mittausalueella
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Lyöri, V. (Veijo). "Structural monitoring with fibre-optic sensors using the pulsed time-of-flight method and other measurement techniques." Doctoral thesis, University of Oulu, 2007. http://urn.fi/urn:isbn:9789514287022.
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Abstract
This thesis deals with the developing of fibre-optic instruments for monitoring the health of civil engineering and composite structures. A number of sensors have been tested for use with different road structures, concrete bridges, fibre reinforced polymer (FRP) containers and other composite specimens, the interrogation methods being mainly based on measuring optical power and time-of-flight (TOF). The main focus is on the development of a fibre-optic TOF measurement system and its applications, but different sensing needs and fibre-optic measurement systems are also reviewed, with the emphasis on commercial devices.
Deformation in a road structure was studied with microbending sensors of gauge-length about 10 cm and a commercial optical time domain reflectometer (OTDR) in a quasi-distributed fashion. The responses of the optical fibre sensors during the one-year measurement period were similar in shape to those obtained with commercial strain gauges but the absolute measurement values typically deviated by several tens of per cent. Low dynamic range, crosstalk and poor signal-to-noise ratio proved to be the main problem when measuring several successive sensors with an OTDR. In another road investigation, microbending and speckle sensors were found useful for providing on/off-type information for traffic control applications.
FRP composite containers were investigated with the focus on developing a continuous monitoring system for improving yield and quality by evaluating the state of cure during the manufacturing process and for assessing damage, e.g. delaminations, during service life. Standard multi-mode and single mode fibres with a typical length of a few hundreds of metres were embedded inside the walls of containers during the normal manufacturing process, and the measurements were carried out using an optical through-power technique and an OTDR. This largely empirical investigation revealed that the coating material and its thickness have an effect on loading sensitivity and on the applicability of the method for cure monitoring. The measurement data also indicated that the end-of-curing process and the location of external damage can be determined with a distributed optical fibre sensor and an OTDR.
Several versions of a pulsed time-of-flight measurement system were developed for interrogating sensor arrays consisting of multiple long gauge-length sensors. The early versions based on commercial electronics were capable of producing relevant measurement data with a reasonable precision, but they suffered especially from poor spatial resolution, low sampling rate and long-term drift.
The high precision TOF system developed in this thesis is capable of measuring time delays between a number of wideband reflectors, such as connectors or fibre Bragg gratings (FBG), along a fibre path with a precision of about 280 fs (rms-value) and a spatial resolution of about 3 ns (0.30 m) in a measurement time of 25 milliseconds. By using a fibre loop sensor with a reference fibre, a strain precision below 1 με and a measurement frequency of 4 Hz can be achieved. The system has proved comparable in performance to a commercial FBG interrogation system in monitoring the behaviour of a bridge deck, while the fact that it allows static and dynamic measurements with a number of long gauge-length sensors, also embedded in FRP composite material, makes this TOF device unique relative to other measurement systems.
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Fani-Pakdel, Farzad. "Microsecond pulsed Grimm glow discharge time-of-flight mass spectrometry study of aerosols generated by nebulization and laser ablation." [Gainesville, Fla.] : University of Florida, 2009. http://purl.fcla.edu/fcla/etd/UFE0024978.
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Kinnunen, M. (Matti). "Comparison of optical coherence tomography, the pulsed photoacoustic technique, and the time-of-flight technique in glucose measurements in vitro." Doctoral thesis, University of Oulu, 2006. http://urn.fi/urn:isbn:9514281462.
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Abstract
The development of a non-invasive glucose monitoring technique is very important because it would tremendously diminish the need to puncture the skin when taking blood samples and help diabetic patients in controlling their blood glucose levels and in treating Diabetes Mellitus. The focus of this thesis is on measuring the effect of glucose on the light scattering properties of a tissue-simulating phantom and biological tissues in vitro. Optical coherence tomography (OCT), the pulsed photoacoustic (PA) technique, and the time-of-flight (TOF) technique are used in the measurements and their capabilities for detecting changes in the scattering properties are evaluated and compared with each other. The theoretical background of the techniques, light propagation and PA wave generation are briefly explained. The glucose-induced changes in light scattering are also reviewed.
The measurement results with the OCT and the PA technique from Intralipid, pig whole blood, and mouse skin tissue samples show that the glucose-induced changes are larger in the biological tissues than in the Intralipid phantom. The PA measurements show that although the PA signals are stronger at a wavelength of 532 nm than at 1064 nm, the glucose-induced change in the peak-to-peak value of the PA signal measured from pig whole blood is larger at a wavelength of 1064 nm than at 532 nm. The TOF measurements with a streak camera show that the scattering-related changes in the registered pulse shapes occur mainly in the rising part of the pulses. The utilization of fiber-optic measurement heads enabled the detection of back-scattered photons at different distances from the emitting fiber.
Although all the techniques are able to detect changes induced by large glucose concentrations (0–5000 mg/dl) in Intralipid, the effect of glucose on the scattering properties of Intralipid is so weak that the techniques failed to detect changes with lower (50–500 mg/dl) concentrations. The measurements of biological samples with the PA technique and with the OCT also demonstrate capabilities to measure glucose concentrations in the physiologically relevant range (18–450 mg/dl) as well. The results compare well with earlier literature and also confirm some earlier findings.
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Alm, Johanna. "Method development for identification of N-linked glycans by high performance anion exchange chromatography with pulsed amperometric detection and time of flight mass spectrometry." Thesis, Linköpings universitet, Institutionen för fysik, kemi och biologi, 2011. http://urn.kb.se/resolve?urn=urn:nbn:se:liu:diva-66232.
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In the biopharmaceutical industry, identification of glycans in a glycoprotein is a regulatory requirement and is a part of the characterization of the protein. Glycans are constructed of several monosaccharides linked together. N-linked glycans, which have been studied in this project, are attached to the nitrogen atom in asparagine. A method for separating N-linked glycans by high performance anion exchange chromatography had already been developed at the department. To develop a method for identification of the N-glycans by mass spectrometry, a desalting method on porous graphitic carbon (PGC) columns was used and optimized resulting in the eluents A (0,05% TFA in ACN:water 5:95 v/v) and B (0,05% TFA in ACN:water 50:50 v/v). Also the sample introduction on the mass spectrometer was optimized and resulted in a sensitive on-line liquid chromatography mass spectrometry (LC-MS) approach which gave mass spectrometric peaks with high signal to noise ratios and with high mass accuracy. The developed procedure was then successfully used on glycans cleaved from a glycoprotein separated by high performance anion exchange chromatography with pulsed amperometric detector.
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Lanz, B. (Brigitte). "Compact current pulse-pumped GaAs–AlGaAs laser diode structures for generating high peak-power (1–50 watt) picosecond-range single optical pulses." Doctoral thesis, Oulun yliopisto, 2016. http://urn.fi/urn:isbn:9789526213569.
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Abstract Although gain-switching is a simple, well-established technique for obtaining ultrashort optical pulses generated with laser diodes, the optical energy in a pulse achievable from commercial structures using this technique is no more than moderate and the ‘spiking’ behaviour seen at turn-on is likely to evolve into trailing oscillations. This thesis investigates, develops and improves laser diodes in order to offer experimentally verified solutions for maximizing the optical energy so as to achieve a peak power of several watts in a single optical pulse of picosecond-range duration in the gain-switching operation regime, and for suppressing the energy located in any trailing pulses to a negligible level relative to the total optical pulse energy. This was addressed by means of either (i) an ultrashort pump current pulse with an amplitude range ~(1–10) A or (ii) custom laser diode structures, both options being capable of operating uncooled at room temperature (23±3°C). For the first solution a unique superfast gallium arsenide (GaAs) avalanche transistor was utilized as a switch in order to achieve an injection current pulse with a duration of < 1 ns, which is short enough to generate only a first optical ‘spike’ when pumping a commercial laser diode. The most promising structure with regard to the second solution was an edge-emitting semiconductor laser having a strongly asymmetric broadened double heterostructure with a relatively thick active layer. Laser pulses with full width at half maximum (FWHM) of ~100 ps and an optical energy of >3 nJ but with some trailing oscillations were achieved in experiments employing injection current pulses in the nanosecond range with an amplitude of ≤17 A, generated using inexpensive silicon (Si) electronics. The performance was improved by introducing a saturable absorber (SA) into the laser cavity, which suppressed the formation of trailing oscillations, resulting in a single optical pulseTiivistelmä ”Gain switching” (vahvistuskytkentä) on tunnettu tekniikka lyhyiden (<100 ps) optisten pulssien generoimiseen laserdiodeilla. Kaupallisia laserdiodirakenteita käyttäen optinen energia rajoittuu kuitenkin 10…100 pJ:n tasolle. Tällöinkin, erityisesti suurilla energiatasoilla, optisessa pulssissa ilmenee voimakkaita jälkioskillaatioita. Tässä väitöskirjassa tutkittiin ja kehitettiin kokeellisesti varmennettuja laserdiodilähetinrakenteita tavoitteena saavuttaa >1 nJ:n optisen pulssin energia ja ~100 ps:n pulssinpituus gain-switching -toimintamoodissa. Tavoitteena oli myös minimoida jälkipulssien energia. Tutkimuksen pääsisältönä on kaksi toimintaperiaatetta: Toisessa tekniikassa päähuomio kohdistuu laseridiodin virta-ajuriin, johon kehitettiin elektroniikka, joka kykenee tuottamaan nopeita virtapulsseja laajalla pulssivirta-alueella. Virtapulssin nopeuden kasvattamisen (<1 ns) osoitettiin edistävän gain switching -ilmiötä. Toisena tekniikkana tutkittiin räätälöityä laserdiodirakennetta, joka sisäisen toimintansa perusteella tuottaa dynaamisessa ohjaustilanteessa tehokkaan ja nopean laserpulssin. Kummankin periaatteen osoitettiin toimivan huonelämpötilassa (23±3°C) ilman erillistä jäähdytystä. Ensimmäisessä ratkaisussa käytettiin nopeaa gallium-arsenidi (GaAs) -avalanchetransistoria virtakytkimenä, jolla saavutettiin <1 ns FWHM injektiovirtapulssi 10 A:n virtatasolla. Tällainen virtapulssi on riittävän lyhyt virittämään ”gain switching” -ilmiön nJ-energiatasolla. Lupaavin rakenne toiseksi ratkaisuksi oli reunaemittoiva puolijohdelaseri, jossa epäsymmetrinen aaltoputki ja aktiivinen alue ovat sijoitettu normaalista laserdiodirakenteesta poiketen rinnakkain. Tällä rakenteella voitiin tuottaa ~100 ps levyisiä (FWHM) ja >3 nJ optisen kokonaisenergian omavia laserpulsseja edullisella pii-pohjaisella (Si) elektroniikalla luoduilla 1.5–2 ns:n (FWHM) ≤17 A injektiovirtapulsseilla. Suorituskykyä saatiin edelleen parannettua istuttamalla saturoiva absorbaattori (SA) laserin optiseen onteloon. Tämän osoitettiin vähentävän jälkioskillaatioiden muodostumista
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Timilsina, Pratap. "Development of an electron time of flight spectrometer for ultrafast pulse characterization and ultrafast dynamics studies." Kansas State University, 2016. http://hdl.handle.net/2097/32598.
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Master of ScienceDepartment of Physics
Carlos Trallero
This report presents the details of an electron time-of-flight (ETOF) spectrometer to be used for characterizing ultrafast electric field pulses. The pulses will range in pulse-duration from femtosecond to attoseconds and in wavelength from the far infrared (FIR) to the extreme ultra violet (XUV). By measuring the photoelectrons in the presence of two electric fields and their quantum interference we will be able to extract the amplitude and phase of the electric field. For XUV pulses this is the well-known streaking and Reconstruction of Attosecond Beating by Interference of Two-Photon Transition (RABITT) method. The ETOF is based on a set of tunable electrostatic lenses capable of detecting 0-150 eV electrons. In addition, we can selectively increase the photoelectron yield of the spectrum. The precise tuning of the electrostatic lens system is done with a Genetic Algorithm (GA) with an intensity fluctuation discriminator in the fitness.
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Nakamura, Shu. "Real-time time-of-flight measurement of proton beam produced by an intense short-pulse laser." 京都大学 (Kyoto University), 2007. http://hdl.handle.net/2433/136761.
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Mollén, Katarina. "Water Depth Estimation Using Ultrasound Pulses for Handheld Diving Equipment." Thesis, Linköpings universitet, Institutionen för systemteknik, 2015. http://urn.kb.se/resolve?urn=urn:nbn:se:liu:diva-117061.
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This thesis studies the design and implementation of an ultra-sonic water depth sounder. The depth sounder is implemented in a hand-held smart console used by divers. Since the idea of echo sounding is to measure the flight time between transmitting the signal and receiving the echo, the main challenge of this task is to find a time-of-flight (ToF) estimation for a signal in noise. It should be suitable for this specific application and robust when implemented in the device. The thesis contains an investigation of suitable ToF methods. More detailed evaluations of the matched filter, also known as the correlation method, and the linear phase approach are done. Aspects like pulse frequency and duration, speed of sound in water and underwater noise are taken into account. The ToF-methods are evaluated through simulation and experiments. The matched filter approach is found suitable based on these simulations and tests with signals recorded by the console. This verification leads to the implementation of the algorithm on the device. The algorithm is tested in real time, the results are evaluated and improvements suggested.Denna rapport behandlar skattning av vattendjup med hjälp av ultraljudspulser och implementation av detta. Djupmätaren implementeras i en handhållen dykarkonsoll. Eftersom grundidén i ekolodning är att mäta tiden mellan att pulsen skickas iväg och att ekot tas emot är en stor del av utmaningen att hitta en lämplig metod för att skatta flykttiden för en signal i brus. Metoden ska passa för detta användingsområde och vara robust. Rapporten tar upp tidigare forskning gjord inom flykttidsestimering. De metoder som utvärderas för implementation är det matchade filtret, också kallad korrelationsmetoden, och linjär fas-metoden. Andra aspekter som avvägs och utreds är pulsfrekvens och pulsvaraktighet, ljudets hastighet och brus under vattnet. Metoderna för att skatta flykttid utvärderas genom simuleringar. Det matchade filtret bedöms vara lämpligt baserat på dessa simuleringar och experiment med data inspelad med konsollen. Denna verifikation leder till att algoritmen implementeras på konsollen. Den implementerade algoritmen testas i realtid, resultaten utvärderas och förbättringar föreslås.
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Billings, Don, Mei Wei, Joseph Leung, Michio Aoyagi, Fred Shigemoto, and Rob Honeyman. "REAL-TIME INTEGRATION OF RADAR INFORMATION, AND GROUND AND RADIOSONDE METEOROLOGY WITH FLIGHT RESEARCH DATA." International Foundation for Telemetering, 1998. http://hdl.handle.net/10150/607368.
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International Telemetering Conference Proceedings / October 26-29, 1998 / Town & Country Resort Hotel and Convention Center, San Diego, CaliforniaAlthough PCM/TDM framed data is one of the most prevalent formats handled by flight test ranges, it is often required to acquire and process other types. Examples of such non-standard data types are radar position information and meteorological data from both ground based and radiosonde systems. To facilitate the process and management of such non-standard data types, a micro-processor based system was developed to acquire and transform them into a standard PCM/TDM data frame. This obviated the expense of developing additional special software and hardware to handle such non-standard data types.
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Valldor-Blücher, Johan. "Upgrading the Control and Monitoring system for the TOFOR neutron time-of-flight spectrometer at JET." Thesis, Uppsala universitet, Institutionen för fysik och astronomi, 2013. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-197586.
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This report describes the development and testing of the upgraded Control and Monitoring (C&Mu) system for the TOFOR neutron spectrometer. TOFOR is currently performing plasma diagnostics for the JET experimental fusion reactor. The purpose of the C&Mu system is to enable monitoring of the amplitude dependent time delays of TOFOR. In order to perform this monitoring function the C&Mu system must comprise a pulsed light source with variable intensity and a reference time signal. In this work a reference time signal has been retrieved from a laser comprising a motorized polarizer. This has been accomplished by installing a photomultiplier tube and a beamsplitter cube. The beamsplitter cube splits the laser light into two parts and directs one part into the photomultiplier tube. The photomultiplier tube converts the light into an electrical reference time signal. A control program has been developed for the motorized polarizer, enabling the user to vary the intensity of the light over the interval from 0% to 100%. The C&Mu system has been performance tested and it was found that the time resolution of the system is about 0.1ns and the time stability of the system is about 0.12ns over 27 hours. The system is more than adequate to monitor variations in time delays at TOFOR of several nanoseconds, over a full JET day. The C&Mu system is ready to be installed on TOFOR.
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Elkhalili, Omar. "Entwicklung von opischen 3D CMOS-Bildsensoren auf der Basis der Pulslaufzeitmessung / Development of optical 3D CMOS image sensors based on pulse time of flight measurement." Gerhard-Mercator-Universitaet Duisburg, 2005. http://www.ub.uni-duisburg.de/ETD-db/theses/available/duett-05072005-130542/.
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In this thesis, a 3D CMOS imager based on time-of-flight (TOF) has been developed and successfully tested. It uses an active pulsed class 1 laser operating at 910nm to illuminate a 3D scene. The scene depth is determined by measurement of the travel time of reflected pulses by employing a fast on-chip synchronous shutter. A so-called Multiple Double Short Time Integration (MDSI) enables suppression of the background illumination and correction for reflectivity variations in the scene objects. The sensor chip contains two pixel lines with each pixel containing twin photodiodes, thus the chip contains 4´64 sensors. The chip allows tow operating modes; the first is the binning mode, where the twin pixels are short-circuited (tow lines on the die) and the average signal is measured. The second mode is the high-resolution mode. In this mode the pixels operate separately (four lines on the die). The chip has been realized in 0.5mm n-well standard CMOS process. The pixel pitch is 130mm. To get a good fill factor, the readout circuitry is located at the sides of the chip.
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Terschlüsen, Joachim A. "Constructing and Commissioning HELIOS – A High Harmonic Generation Source for Pump-Probe Measurements with sub 50 fs Temporal Resolution : The Development of Experimental Equipment for Extreme Ultraviolet Spectroscopy." Doctoral thesis, Uppsala universitet, Molekyl- och kondenserade materiens fysik, 2016. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-281298.
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This thesis presents HELIOS, an in-house laboratory for time-resolved pump-probe spectroscopy with extreme-ultraviolet (XUV) probe radiation. A wide span of pump wavelengths can be generated using commercial laser equipment while XUV probe radiation is generated via a high harmonic generation process in a noble gas delivering probe photons with energies between 20 eV and 72 eV. The XUV beam path features a time-preserving monochromator and was constructed and built in-house. HELIOS features an overall time resolution of about 50 fs when using 800 nm pump and 41 eV probe photons. An energy resolution of 110 meV at 41 eV photon energy can be achieved. HELIOS features two beamlines. One µ-focus beamline with an XUV focal size of about 20 µm can be used with experiments that require such a small XUV focal size as well as with different end stations. The other beamline features a semi-permanently mounted end station for angle-resolved photoelectron spectroscopy under ultra-high vacuum conditions. Experiments demonstrating the usability of HELIOS and the two beamlines are presented. A pump-probe measurement on graphene demonstrates the capability of determining a large part of the k-space in only one measurement due to the use of an ARTOF angle-resolved time-of-flight electron spectrometer. A non-angle-resolved pump-probe measurement on the conducting polymer PCPDTBT demonstrates the high signal-to-noise ratio achievable at this beamline in non-angle-resolved photoelectron-spectroscopy pump-probe measurements. The usability of the µ-focus beamline is demonstrated with time-resolved measurements on magnetic samples employing an in-house-designed spectrometer. These experiments allow the retrieval of element-specific information on the magnetization within a sample employing the transversal magneto-optical Kerr effect (T-MOKE). Additionally, a Fourier transform spectrometer for the XUV is presented, the concept was tested at a synchrotron and it was used to determine the longitudinal coherence of the XUV radiation at HELIOS.
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Ljungvall, Joa. "Characterisation of the Neutron Wall and of Neutron Interactions in Germanium-Detector Systems." Doctoral thesis, Uppsala University, Department of Nuclear and Particle Physics, 2005. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-5845.
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A Monte Carlo simulation of the Neutron Wall detector system has been performed using Geant4, in order to define optimum conditions for the detection and identification of multiple neutrons. Emphasis was put on studying the scattering of neutrons between different detectors, which is the main source of the apparent increase of the number of detected neutrons. The simulation has been compared with experimental data. The quality of neutron gated γ-ray spectra was improved for both two- and three-neutron evaporation channels. The influence of small amounts of γ rays mis-interpreted as neutrons was investigated. It was found that such γ rays dramatically reduce the quality of neutron gated γ-ray spectra.
The interaction properties of fast neutrons in a closed-end coaxial and a planar high-purity germanium detector (HPGe) were studied. Digitised waveforms of HPGe preamplifier signals were recorded for time-of-flight separated neutrons and γ rays, emitted by a 252Cf source. The experimental waveforms from the detectors were compared to simulated pulse shapes. In the analysis, special emphasis was given to the detection of elastically scattered neutrons, which may be an important effect to take into account in future spectrometers based on γ-ray tracking. No differences between neutron and γ-ray induced pulse shapes were found in this work.
A Monte Carlo simulation of the interactions of fast neutrons in the future 4π γ-ray spectrometer AGATA was also performed, in order to study the influence of neutrons on γ-ray tracking. It was shown that although there is a large probability of detecting neutrons in AGATA, the neutrons decrease the photo-peak efficiency of AGATA by only about 1% for each neutron emitted in coincidence with γ rays. The peak-to-background ratios in γ-ray spectra are, however, reduced to a much larger extent. The possibility of using AGATA as a neutron detector system was also investigated.
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Carbol, Ladislav. "Měření akustických vlastností stavebních materiálů pomocí pseudonáhodné sekvence." Doctoral thesis, Vysoké učení technické v Brně. Fakulta stavební, 2017. http://www.nusl.cz/ntk/nusl-355599.
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The thesis deals with research of pulse compression of the acoustic signal in terms of applications in civil engineering. Based on the study and analysis of these methods, automated measuring equipment for non-destructive testing with pseudorandom sequence of maximum length and automated signal analysis, have been designed and implemented. In a single test cycle are obtained three parameters that characterize the linear and nonlinear behavior of the sample. A nonlinear parameter, Time of Flight of ultrasonic wave in the sample is further in the work compared with the conventional pulse measuring, and spectral analysis is compared with the method impact-echo. Functionality and optimization of the testing method was performed on a total of three sets of test pieces made of various building materials. The experiments proved simple result interpretation, and high sensitivity to structural damage associated with temperature loading. The results were correlated with conventional nondestructive methods and by destructive testing was measured change in compressive strength and flexural strength. This work also includes continual measurement of fundamental frequency influenced by moisture on a mortar sample. Use of pulse compression signal is in the civil engineering quite unusual. Only in recent years this topic is discussed in scientific articles with increasing frequency. Great potential lies in the association of three test methods into a single. Beneficial is high test speed and measurement reproducibility, but also theoretical possibility of testing massive test elements.
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Li, Ji-Shiang, and 李冀翔. "Low Walk Error Receiver Channel with Leading Edge Timing Discriminator for a Pulsed Time-of-Flight Laser Rangefinder." Thesis, 2009. http://ndltd.ncl.edu.tw/handle/97934546614957485271.
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Hu, Anming. "Interaction of Nanosecond and Femtosecond Laser Pulses with Carbon: Deposition of Carbon Films having Novel Compositions." Thesis, 2008. http://hdl.handle.net/10012/3742.
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A comparison of the composition and structure of carbon films deposited by ns and fs laser ablation of graphite is the subject of this thesis. In addition, the effect of irradiation on the surface of graphite has been investigated in detail. Laser-induced phase transitions from graphite to sp-bonded carbon and trans-polyacetylene chains as well as the formation of nano-diamond have been observed after irradiation with fs pulses. An optical orientation mechanism involving both electric and magnetic interactions is proposed to understand the formation of nano-stripes and other structures on irradiated graphite surfaces. These phenomena are not observed after nanosecond laser irradiation.
Tetrahedral carbon (ta-C) films deposited at cryogenic temperatures using ns laser radiation consist of sub-micron graphitized grains embedded in a matrix of sp3-hybridized bonded carbon. Nano-buckling is evident in ta-C films deposited by fs ablation where the composition is found to consist of mixed sp, sp2, and sp3 – hybridized carbons species. It is found that the concentration of sp-bonded chains is negligible in ns-C films. Surface enhanced Raman spectroscopy has been used to characterize molecular species in ns and fs carbon films. Time of flight mass spectroscopy has been used to study plume species produced by laser ablation.
It is also found that polyyne molecules can be formed by fs laser dissociation of small molecules in organic solvents. This process is accompanied by the deposition of hexagonal nano-diamond films on substrates placed near the laser focus during irradiation. This opens a new path in the synthesis of 1D conducting molecules and nano-diamond materials for nano-science applications.
Quantum chemical calculations involving density functional theory (Gaussian '03) have been carried out in support of this work and have been used to study Raman and IR vibrational modes of several novel carbon molecules synthesized in ta-C films and in the liquid phase. These studies have been extended to assist in the identification of astronomical spectra.
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Nahler, Nils Hendrik. "Photodissoziation von Halogenwasserstoff- und orientierten Wasserstoff-Edelgas-Halogen-Molekülen in Clusterumgebungen." Doctoral thesis, 2002. http://hdl.handle.net/11858/00-1735-0000-0006-B431-7.
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