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Journal articles on the topic 'Reduction with silanes'

Author: Grafiati

Published: 4 June 2021

Last updated: 2 February 2022

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1

Donath, Steffen, Holger Militz, and Carsten Mai. "Creating water-repellent effects on wood by treatment with silanes." Holzforschung 60, no. 1 (2006): 40–46. http://dx.doi.org/10.1515/hf.2006.008.

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Abstract Three types of silanes were tested for their ability to impart hydrophobicity to solid wood samples: a tetraalkoxy silane bearing four hydrolysable alkoxy groups; two alkyl-trialkoxy silanes; and two multifunctional oligomeric silane systems. The first two types were applied as monomeric silane solutions and pre-condensed sols. The water uptake of treated wood was considerably reduced, especially after treatment with multifunctional water-borne silane systems, while uptake of gaseous water was not changed. Initial water repellence was most pronounced when a fluoro-alkyl functional oli

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2

Wang, Danling, Fujun Ren, Chenxi Zhu, et al. "HYBRID SILANE TECHNOLOGY IN SILICA-REINFORCED TREAD COMPOUND." Rubber Chemistry and Technology 92, no. 2 (2018): 310–25. http://dx.doi.org/10.5254/rct.18.81563.

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ABSTRACT The use of a silane coupling agent in silica-reinforced tread can effectively improve silica dispersion in the rubber matrix and strengthen the interfacial interaction between the rubber and filler; this is beneficial to the enhancement of tire grip under wet conditions and reduces tire rolling resistance. The monofunctional silane n-octyltriethoxysilane (OTES) can react with the silanol group of the silica surface and hence improve silica dispersion. It can also suppress silica reaggregation during tire processing. Two hybrid silanes, OTES and 3-mercaptopropylethoxy-bis(tridecyl-pent

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3

Neves, Rodrigo S., Daiane P. B. Silva, and Artur J. Motheo. "Corrosion Protection of AA7075 Aluminium Alloy by Trimethoxy-Silanes Self-Assembled Monolayers." ISRN Electrochemistry 2013 (April 2, 2013): 1–9. http://dx.doi.org/10.1155/2013/142493.

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This study presents electrochemical data concerning the aluminium alloy AA7075 surface modified by self-assembled monolayers (SAMs) of octadecyl-trimethoxy-silane and propyl-trimethoxy-silane. Polarisation curves have shown SAMs blocking effect, as they partially block the oxygen reduction reaction and displace the corrosion potential to positive values. Electrochemical impedance spectroscopy experiments have suggested that the protective effect comes from the oxide layer stabilization by the organic monolayers, which block the corroding species diffusion to the surface. These results show the

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4

Lin, Chenchy, William L. Hergenrother, and Ashley S. Hilton. "Mooney Viscosity Stability and Polymer Filler Interactions in Silica Filled Rubbers." Rubber Chemistry and Technology 75, no. 2 (2002): 215–45. http://dx.doi.org/10.5254/1.3544974.

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Abstract The change in Mooney viscosity (ML1+4) with aging was followed for silica filled compounds containing various silanes and polar additives. Several mechanisms for the aging stability are postulated and evaluated through experimentation. The type of silane or polar additive used can cause the ML1+4 to increase or even decrease during aging. When bis(triethoxy silanes) are used in silica filled rubbers, the ML1+4 growth during aging is caused by hydrolysis. Silica-silica bridging was found to be responsible for the ML1+4 growth in rubber compounds containing a more thermally stable polys

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5

Kovacs, Tamara, and Gyorgy Keglevich. "The Reduction of Tertiary Phosphine Oxides by Silanes." Current Organic Chemistry 21, no. 7 (2017): 569–85. http://dx.doi.org/10.2174/1385272821666161108121532.

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6

Fernandes, Ana C., and Carlos C. Romão. "Reduction of amides with silanes catalyzed by MoO2Cl2." Journal of Molecular Catalysis A: Chemical 272, no. 1-2 (2007): 60–63. http://dx.doi.org/10.1016/j.molcata.2007.03.019.

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7

Donath, Steffen, Carsten Mai, and Holger Militz. "Untersuchungen zur Eignung von Silanen als Holzbehandlungsmittel | Examination of the usefulness of silanes to treat wood." Schweizerische Zeitschrift fur Forstwesen 156, no. 11 (2005): 411–13. http://dx.doi.org/10.3188/szf.2005.0411.

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The treatment of wood with the used monomer silanes, according to current research results, does not lead to a lasting stabilisation of dimension (reduction of moisture expansion and of shrinkage). Silanes are nevertheless useful to influence specific characteristics of wood. High water resistant effects with simultaneous low influence on absorption behaviour as well as increased resistance to biological degradation caused by a variety of micro-organisms is part of the efficiency profile of this treatment.

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8

Pramudita, Ria Ayu, and Ken Motokura. "Transformative reduction of carbon dioxide through organocatalysis with silanes." Green Chemistry 20, no. 21 (2018): 4834–43. http://dx.doi.org/10.1039/c8gc02052c.

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9

Rand, Alexander W., and John Montgomery. "Catalytic reduction of aryl trialkylammonium salts to aryl silanes and arenes." Chemical Science 10, no. 20 (2019): 5338–44. http://dx.doi.org/10.1039/c9sc01083a.

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10

Lin, Chenchy J., W. L. Hergenrother, E. Alexanian, and G. G. A. Böhm. "On the Filler Flocculation in Silica-Filled Rubbers Part I. Quantifying and Tracking the Filler Flocculation and Polymer-Filler Interactions in the Unvulcanized Rubber Compounds." Rubber Chemistry and Technology 75, no. 5 (2002): 865–90. http://dx.doi.org/10.5254/1.3547689.

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Abstract Filler flocculation was followed for silica filled compounds containing various alkoxy silanes and non-silane type polar additives. The methodology employed in this paper permitted a quantitative characterization of filler flocculation and polymer-filler interactions after heating the compound under conditions that simulated vulcanization. With the addition of trialkoxy silanes, the reduction of filler flocculation and the degree of polymer-filler interactions were found to depend on the type and the concentration of silane added, and on the mixing drop temperature (Td) used. Greater

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11

Dalko, Peter I., Janine Cossy, and Candice Menozzi. "Reduction of Olefins Using Ruthenium Carbene Catalysts and Silanes." Synlett, no. 16 (2005): 2449–52. http://dx.doi.org/10.1055/s-2005-872695.

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12

Nishibayashi, Yoshiaki, Akira Shinoda, Yoshihiro Miyake, Hiroshi Matsuzawa, and Mitsunobu Sato. "Ruthenium-Catalyzed Propargylic Reduction of Propargylic Alcohols with Silanes." Angewandte Chemie International Edition 45, no. 29 (2006): 4835–39. http://dx.doi.org/10.1002/anie.200601181.

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13

Nishibayashi, Yoshiaki, Akira Shinoda, Yoshihiro Miyake, Hiroshi Matsuzawa, and Mitsunobu Sato. "Ruthenium-Catalyzed Propargylic Reduction of Propargylic Alcohols with Silanes." Angewandte Chemie 118, no. 29 (2006): 4953–57. http://dx.doi.org/10.1002/ange.200601181.

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14

Lipshutz, Bruce, Ching-Tien Lee, and Benjamin Taft. "A Conjugate Reduction Pathway to Chiral Silanes Using CuH." Synthesis 2007, no. 20 (2007): 3257–60. http://dx.doi.org/10.1055/s-2007-983830.

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15

Zhang, Peng, Tie Jun Zhao, F. H. Wittmann, and Shao Chun Li. "Preparation and Characteristics of Integral Water Repellent Cement-Based Materials." Materials Science Forum 675-677 (February 2011): 1189–92. http://dx.doi.org/10.4028/www.scientific.net/msf.675-677.1189.

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Polymers are often applied in concrete for multiple purposes and aims. For instance, surface impregnation of concrete with silanes is a reliable technology to protect cement-based materials from ingress of aggressive solutions into the materials. An alternative method is to add silane emulsion into fresh concrete or mortar to produce integral water repellent materials. In this contribution integral water repellent concrete was prepared by adding 1 %, 2 %, 3 %, 4 % and 6 % of silane emulsion. The influence of silane emulsion on the compressive strength, porosity and pore size distribution, wate

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16

Luo, Nianhua, Jianhua Liao, Lu Ouyang, et al. "Highly Selective Hydroxylation and Alkoxylation of Silanes: One-Pot Silane Oxidation and Reduction of Aldehydes/Ketones." Organometallics 39, no. 1 (2019): 165–71. http://dx.doi.org/10.1021/acs.organomet.9b00716.

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17

Kumar, Akshai, Arun Kumar Pandiakumar, and A. G. Samuelson. "Titanium promoted reduction of imines with Grignards, silanes, and zinc: identification of a new mechanism with silanes." Tetrahedron 70, no. 19 (2014): 3185–90. http://dx.doi.org/10.1016/j.tet.2014.03.035.

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18

Cowie, Bradley E., Gary S. Nichol, Jason B. Love, and Polly L. Arnold. "Double uranium oxo cations derived from uranyl by borane or silane reduction." Chemical Communications 54, no. 31 (2018): 3839–42. http://dx.doi.org/10.1039/c8cc00341f.

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19

Molleo, Max, and James V. Crivello. "Redox-Initiated Cationic Polymerization: Reduction of Dialkylphenacylsulfonium Salts by Silanes." Macromolecules 42, no. 12 (2009): 3982–91. http://dx.doi.org/10.1021/ma900482d.

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20

Crivello, James V. "Redox Initiated Cationic Polymerization: Reduction of Triarylsulfonium Salts by Silanes." Silicon 1, no. 2 (2009): 111–24. http://dx.doi.org/10.1007/s12633-009-9007-1.

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21

Taori, Vijay P., and Michael R. Buchmeiser. "Tandem-reduction of DMF with silanes via necklace-type transition over Pt(0) nanoparticles: deciphering the dual Si–H effect as an extension of steric effects." Chem. Commun. 50, no. 94 (2014): 14820–23. http://dx.doi.org/10.1039/c4cc06979j.

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22

Jurado-Vázquez, Tamara, Carmen Ortiz-Cervantes, and Juventino J. García. "Catalytic reduction of CO2 with organo-silanes using [Ru3(CO)12]." Journal of Organometallic Chemistry 823 (November 2016): 8–13. http://dx.doi.org/10.1016/j.jorganchem.2016.08.032.

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23

Roa, Diego A., and Juventino J. Garcia. "Mild reduction with silanes and reductive amination of levulinic acid using a simple manganese catalyst." Inorganica Chimica Acta 516 (February 2021): 120167. http://dx.doi.org/10.1016/j.ica.2020.120167.

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24

Hackel, Taylor, and Nicholas A. McGrath. "Tris(pentafluorophenyl)borane-Catalyzed Reactions Using Silanes." Molecules 24, no. 3 (2019): 432. http://dx.doi.org/10.3390/molecules24030432.

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The utility of an electron-deficient, air stable, and commercially available Lewis acid tris(pentafluorophenyl)borane has recently been comprehensively explored. While being as reactive as its distant cousin boron trichloride, it has been shown to be much more stable and capable of catalyzing a variety of powerful transformations, even in the presence of water. The focus of this review will be to highlight those catalytic reactions that utilize a silane as a stoichiometric reductant in conjunction with tris(pentafluorophenyl) borane in the reduction of alcohols, carbonyls, or carbonyl-like der

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25

Fang, Shaoqin, Hongcai Chen, and Haiyan Wei. "Insight into catalytic reduction of CO2to methane with silanes using Brookhart's cationic Ir(iii) pincer complex." RSC Advances 8, no. 17 (2018): 9232–42. http://dx.doi.org/10.1039/c7ra13486j.

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The transformation of CO<sub>2</sub>and silanes to methane catalyzed by a cationic Ir–pincer complex is investigated and divided into four reducing steps. The first step is the rate-determining step of the overall catalytic cycle.

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26

Cai, Yudong, and Brian P. Roberts. "Formation of silanethiols by reaction of silanes with carbonyl sulfide: implications for radical-chain reduction of thiocarbonyl compounds by silanes." Tetrahedron Letters 42, no. 4 (2001): 763–66. http://dx.doi.org/10.1016/s0040-4039(00)02109-2.

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27

Liu, Jianhui, and Xingyang Wang. "Potassium Phenyltrifluoroborate-Catalyzed Reduction of Aldehydes and Ketones into Alcohol with Silanes." Chinese Journal of Organic Chemistry 39, no. 5 (2019): 1411. http://dx.doi.org/10.6023/cjoc201810010.

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28

Drew, Mark D., Nicholas J. Lawrence, William Watson, and Stephen A. Bowles. "The asymmetric reduction of ketones using chiral ammonium fluoride salts and silanes." Tetrahedron Letters 38, no. 33 (1997): 5857–60. http://dx.doi.org/10.1016/s0040-4039(97)01445-7.

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29

Sousa, Sara C. A., Carlos J. Carrasco, Mara F. Pinto, and Beatriz Royo. "A Manganese N‐Heterocyclic Carbene Catalyst for Reduction of Sulfoxides with Silanes." ChemCatChem 11, no. 16 (2019): 3839–43. http://dx.doi.org/10.1002/cctc.201900662.

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30

Li, Chao-Jun, Zhenhua Jia, Mingxin Liu, Xingshu Li, and Albert Chan. "Highly Efficient Reduction of Aldehydes with Silanes in Water Catalyzed by Silver." Synlett 24, no. 16 (2013): 2049–56. http://dx.doi.org/10.1055/s-0033-1339660.

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31

Pinto, Mara, Sofia Friães, Federico Franco, Julio Lloret-Fillol, and Beatriz Royo. "Manganese N-Heterocyclic Carbene Complexes for Catalytic Reduction of Ketones with Silanes." ChemCatChem 10, no. 13 (2018): 2734–40. http://dx.doi.org/10.1002/cctc.201800241.

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32

Pinto, Mara, Sofia Friães, Federico Franco, Julio Lloret-Fillol, and Beatriz Royo. "Manganese N-Heterocyclic Carbene Complexes for Catalytic Reduction of Ketones with Silanes." ChemCatChem 10, no. 13 (2018): 2711. http://dx.doi.org/10.1002/cctc.201800997.

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33

Cai, Yudong, and Brian P. Roberts. "ChemInform Abstract: Formation of Silanethiols by Reaction of Silanes with Carbonyl Sulfide: Implications for Radical-Chain Reduction of Thiocarbonyl Compounds by Silanes." ChemInform 32, no. 18 (2001): no. http://dx.doi.org/10.1002/chin.200118050.

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34

Aoyagi, Keiya, Yu Ohmori, Koya Inomata, et al. "Synthesis of hydrosilanes via Lewis-base-catalysed reduction of alkoxy silanes with NaBH4." Chemical Communications 55, no. 42 (2019): 5859–62. http://dx.doi.org/10.1039/c9cc01961h.

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Hydrosilanes were synthesized by reduction of alkoxysilanes with BH<sub>3</sub> in the presence of hexamethylphosphoric triamide (HMPA) as a Lewis-base catalyst. The reaction was also achieved using an inexpensive and easy-to-handle handled hydride source NaBH<sub>4</sub>, which reacted with EtBr as a sacrificial reagent to form BH<sub>3</sub>in situ.

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35

DREW, M. D., N. J. LAWRENCE, W. WATSON, and S. A. BOWLES. "ChemInform Abstract: Asymmetric Reduction of Ketones Using Chiral Ammonium Fluoride Salts and Silanes." ChemInform 28, no. 46 (2010): no. http://dx.doi.org/10.1002/chin.199746047.

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36

Lopes, Rita, Mariette M. Pereira, and Beatriz Royo. "Selective Reduction of Nitroarenes with Silanes Catalyzed by Nickel N-Heterocyclic Carbene Complexes." ChemCatChem 9, no. 15 (2017): 3073–77. http://dx.doi.org/10.1002/cctc.201700218.

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37

Szafraniec, Małgorzata, Danuta Barnat-Hunek, Małgorzata Grzegorczyk-Frańczak, and Maciej Trochonowicz. "Surface Modification of Lightweight Mortars by Nanopolymers to Improve Their Water-Repellency and Durability." Materials 13, no. 6 (2020): 1350. http://dx.doi.org/10.3390/ma13061350.

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The paper explores the possibility of covering the mortar with the lightweight aggregate by the nanopolymer silane and siloxane as surface hydrophobisation. The investigation involved the mortars with two types of hydrophobic agents diluted with water in a ratio of 1:4 and 1:8. Mortar wetting properties were determined by measuring the absorbability, water vapor diffusion, contact angle (CA) and surface free energy (SFE) of their structure. Surface micro-roughness and 2D topography were evaluated. Scanning electron microscopy (SEM) has shown the microstructure and distribution of pores in mort

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38

Zani, Paolo. "Biotransformations of organosilicon compounds: enantioselective reduction of acyl silanes by means of baker's yeast." Journal of Molecular Catalysis B: Enzymatic 11, no. 4-6 (2001): 279–85. http://dx.doi.org/10.1016/s1381-1177(00)00052-7.

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39

Jia, Zhenhua, Mingxin Liu, Xingshu Li, Albert S. C. Chan, and Chao-Jun Li. "ChemInform Abstract: Highly Efficient Reduction of Aldehydes with Silanes in Water Catalyzed by Silver." ChemInform 45, no. 8 (2014): no. http://dx.doi.org/10.1002/chin.201408037.

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40

Alcaide, Benito, Pedro Almendros, Cristina Aragoncillo та Gonzalo Gómez-Campillos. "Synthesis of Functionalized Azetidines through Chemoselective Zinc-Catalyzed Reduction of β-Lactams with Silanes". Advanced Synthesis & Catalysis 355, № 10 (2013): 2089–94. http://dx.doi.org/10.1002/adsc.201300320.

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41

Lopes, Rita, João M. S. Cardoso, Lorena Postigo, and Beatriz Royo. "Reduction of Ketones with Silanes Catalysed by a Cyclopentadienyl-Functionalised N-Heterocyclic Iron Complex." Catalysis Letters 143, no. 10 (2013): 1061–66. http://dx.doi.org/10.1007/s10562-013-1081-8.

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42

McGovern, Mark E., and Michael Thompson. "Article." Canadian Journal of Chemistry 77, no. 10 (1999): 1678–89. http://dx.doi.org/10.1139/v99-196.

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The immobilization of biomolecules on substrate surfaces for biosensor development requires linking molecules that must meet a specific set of criteria. Two such agents based on bifunctional alkyltrichlorosilane structures, 1-bromo-11-(trichlorosilyl)-undecane and 1-(thiotrifluoroacetato)-11-(trichlorosilyl)-undecane, are employed to generate thiol-functionalized surfaces either by nucleophilic substitution followed by reduction (bromine-containing derivative) or deprotection (fluorine-containing compound). Both molecules have been attached to the surfaces of silicon wafers in conjunction with

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43

Dautel, J., S. Abele, and W. Schwarz. "Synthese von 2,2-DiphenylethyI-substituierten Silanen -Molekülstruktur von Trichlor-2,2-diphenylethylsilan /Syntheses of 2,2-Diphenylethyl-Substituted Silanes -Molecular Structure of Trichloro-2,2-diphenylethylsilane." Zeitschrift für Naturforschung B 52, no. 7 (1997): 778–84. http://dx.doi.org/10.1515/znb-1997-0702.

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Abstract Hydrosilylation of 1,1-diphenylethylene with trichlorosilane leads in high yields to trichloro-2.2-diphenylethylsilane (1), which was investigated spectroscopically as well as by X-ray structure determination. The compound crystallizes monoclinically in the acentric space group Cc {a = 1002.4, b = 1573.8, c = 979.7 pm, β = 106.27°, Z = 4}; the bonding parameters show no special features. By fluorination with zinc(II) fluoride in diethylether and by reduction with “Red-Al” in toluene, the corresponding SiF3 (2) and SiH3 derivatives (3) are received, respectively.

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44

Matsuo, Jun-ichi, Yu Hattori, and Hiroyuki Ishibashi. "Brønsted Acid Catalyzed Asymmetric Reduction of Ketones and Acyl Silanes Using Chiralanti-Pentane-2,4-diol." Organic Letters 12, no. 10 (2010): 2294–97. http://dx.doi.org/10.1021/ol1006532.

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45

Ddungu, John L. Z., Simone Silvestrini, Alessandra Tassoni, and Luisa De Cola. "Shedding light on the aqueous synthesis of silicon nanoparticles by reduction of silanes with citrates." Faraday Discussions 222 (2020): 350–61. http://dx.doi.org/10.1039/c9fd00127a.

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46

Sousa, Sara C. A., Sara Realista, and Beatriz Royo. "Bench‐Stable Manganese NHC Complexes for the Selective Reduction of Esters to Alcohols with Silanes." Advanced Synthesis & Catalysis 362, no. 12 (2020): 2437–43. http://dx.doi.org/10.1002/adsc.202000148.

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47

Gevorgyan, V. N., L. M. Ignatovich, and E. Lukevics. "Reduction of alkoxysilanes, halo-silanes and -Germanes with lithium aluminium hydride under phase-transfer conditions." Journal of Organometallic Chemistry 284, no. 2 (1985): C31—C32. http://dx.doi.org/10.1016/0022-328x(85)87220-x.

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48

Riduan, Siti Nurhanna, Jackie Y. Ying, and Yugen Zhang. "Mechanistic Insights into the Reduction of Carbon Dioxide with Silanes over N-Heterocyclic Carbene Catalysts." ChemCatChem 5, no. 6 (2013): 1490–96. http://dx.doi.org/10.1002/cctc.201200721.

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49

Ji, Pengfei, Jeeyoung Park, Yang Gu, Douglas S. Clark, and John F. Hartwig. "Abiotic reduction of ketones with silanes catalysed by carbonic anhydrase through an enzymatic zinc hydride." Nature Chemistry 13, no. 4 (2021): 312–18. http://dx.doi.org/10.1038/s41557-020-00633-7.

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50

Pearce, Kyle G., Andryj M. Borys, Ewan R. Clark, and Helena J. Shepherd. "Exploring the Reactivity of Donor-Stabilized Phosphenium Cations: Lewis Acid-Catalyzed Reduction of Chlorophosphanes by Silanes." Inorganic Chemistry 57, no. 18 (2018): 11530–36. http://dx.doi.org/10.1021/acs.inorgchem.8b01578.

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