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Relevant bibliographies by topics / Resolution of racemic mixture

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Academic literature on the topic 'Resolution of racemic mixture'

Author: Grafiati

Published: 4 June 2021

Last updated: 17 February 2022

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Journal articles on the topic "Resolution of racemic mixture"

1

Baregama, Chetna. "STEREOCHEMISTRY - RACEMIC MODIFICATION, RESOLUTION, AND ITS IMPORTANCE WITH RECENTLY USED OPTICALLY ACTIVE DRUGS." Asian Journal of Pharmaceutical and Clinical Research 11, no. 1 (2018): 3. http://dx.doi.org/10.22159/ajpcr.2017.v11i1.23090.

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Stereochemistry involves the study of the relative spatial arrangement of atoms that form the structure of molecules and their manipulation. An important branch of stereochemistry is the study of chiral molecules. Optical activity is the ability of a chiral molecule to rotate the plane of plane-polarized light, measured using a polarimeter. Racemic modification and resolution, both processes are very important in stereochemistry. A mixture of equal parts of enantiomers is called a racemic modification. The process of separating a racemate into pure enantiomers is known as resolution. Recently,

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Baregama, Chetna. "STEREOCHEMISTRY - RACEMIC MODIFICATION, RESOLUTION, AND ITS IMPORTANCE WITH RECENTLY USED OPTICALLY ACTIVE DRUGS." Asian Journal of Pharmaceutical and Clinical Research 11, no. 1 (2018): 3. http://dx.doi.org/10.22159/ajpcr.2018.v11i1.23090.

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Stereochemistry involves the study of the relative spatial arrangement of atoms that form the structure of molecules and their manipulation. An important branch of stereochemistry is the study of chiral molecules. Optical activity is the ability of a chiral molecule to rotate the plane of plane-polarized light, measured using a polarimeter. Racemic modification and resolution, both processes are very important in stereochemistry. A mixture of equal parts of enantiomers is called a racemic modification. The process of separating a racemate into pure enantiomers is known as resolution. Recently,

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Bosits, Miklós Hunor, Emese Pálovics, János Madarász, and Elemér Fogassy. "New Discoveries in Enantiomeric Separation of Racemic Tofisopam." Journal of Chemistry 2019 (April 7, 2019): 1–10. http://dx.doi.org/10.1155/2019/4980792.

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Resolution process of tofisopam has been re-evaluated now based on our new investigations. Originally, it was carried out in the water-chloroform system, where the intermediate salt of high diastereomeric excess was described as (R)-TOF·(R,R)-DBTA·(H2O)3. Opposed to previous assumptions, we have actually found that a different solvate composition, (R)-TOF‐(R,R)-DBTA-CHCl3, forms with chloroform, in which molecules of CHCl3 are captured and held with different strengths. Moreover, resolution of TOF with (R,R)-DBTA is possible (and favourable) in water-free solvent and solvent mixture. However,

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Dachwitz, E., and M. Stockhausen. "On the Occurance of Stereoisomeric Effects in the Dielectric Relaxation Behaviour of Pure Liquid." Zeitschrift für Naturforschung A 43, no. 5 (1988): 476–80. http://dx.doi.org/10.1515/zna-1988-0512.

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In order to find out whether liquids consisting of pure enantiomers of a chiral molecule differ in their dielectric relaxation behaviour from that of corresponding racemic mixtures, the complex permittivity of the following pure substances was measured over a broad frequency range (3 MHz to 72 GHz) at 20° CC: Phenylethylisocyanate, carvone, fenchone, 2-octanol, 2-amino-l-butanol, diethyltartrate and diisopropyltartrate. With the achieved experimental resolution, no stereoisomers effect could be observed with the exception of the tartrates, where there are clear differences in the low frequency

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Maharani, Rani, Ace Tatang Hidayat, Dadan Sumiarsa, Achmad Zainuddin, and Ika Wiani Hidayat. "RESOLUTION OF A RACEMIC ISOLEUCINE MIXTURE BY USING METHYL L-MANDELATE." Chimica et Natura Acta 4, no. 3 (2016): 156. http://dx.doi.org/10.24198/cna.v4.n3.10991.

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A methyl ester of L-mandelic acid was found to be an effective resolving agent for resolution of commercial DL-isoleucine. The resolution was based on Steglich esterification between methyl L-mandelate and Boc-DL-isoleucine. The two resolved isomers were easily separated by using a conventional flash-column chromatography, giving quantitatively good yields. Unfortunately, the methyl L-mandelate was found to be ineffective to resolve four stereoisomers of Fmoc- isoleucine.

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Tomioka, Kiyoshi. "Catalytic asymmetric reactions using environmentally friendly reagents and catalyst: Asymmetric synthesis versus kinetic resolution." Pure and Applied Chemistry 78, no. 11 (2006): 2029–34. http://dx.doi.org/10.1351/pac200678112029.

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Kinetic resolution of racemic compounds is a familiar method for the preparation of optically active compounds. However, an inevitable and critical drawback from the point of view of green chemistry is the consequent wastage of half of the starting compound. A catalytic asymmetric synthesis of 5-arylcyclohex-2-enones was developed starting from racemic 5-(trimethylsilyl)cyclohex-2-enone, which overcomes the drawback of kinetic resolution. A chiral amidophosphane- or BINAP-Rh(I)-catalyzed asymmetric conjugate arylation of racemic 5-(trimethylsilyl)cyclohex-2-enone with arylboronic acids in diox

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Singh, Kripal, Pravin G. Ingole, Jayesh Chaudhari, Harshad Bhrambhatt, Amit Bhattacharya та Hari C. Bajaj. "Resolution of racemic mixture of α-amino acid derivative through composite membrane". Journal of Membrane Science 378, № 1-2 (2011): 531–40. http://dx.doi.org/10.1016/j.memsci.2011.05.049.

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Drauz, Karlheinz, Wilfried Jahn, and Michael Schwarm. "Synthesis of (R)-tert-Leucinol by Classical Resolution of the Racemic Mixture." Chemistry - A European Journal 1, no. 8 (1995): 538–40. http://dx.doi.org/10.1002/chem.19950010807.

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9

Mamaghani, Manouchehr, and Alireza Alizadehnia. "Enzyme Catalysed Kinetic Resolution of Racemic Methyl 3-acethylbicyclo [2.2.1] hept-5-ene-2-carboxylate using pig's liver esterase†." Journal of Chemical Research 2002, no. 8 (2002): 386–87. http://dx.doi.org/10.3184/030823402103172400.

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Racemic methyl 3- endo-acetylbicyclo[2.2.1]hept-5-ene-2- exo-carboxylate and methyl 3- exo-acetylbicyclo[2.2.1]hept-5-ene-2- endo-carboxylate were prepared (as a 1:1 mixture in 98% yield) from (E)-methyl 4- oxo-2-pentenoate, using Diels–Alder methodology. The mixture was separated chromatographically and resolved into the enantiomers by pig liver esterase (PLE) with low to high ee's (98%).

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Park, Songsoon, and Hyeon-Kyu Lee. "Efficient kinetic resolution in the asymmetric transfer hydrogenation of 3-aryl-indanones: applications to a short synthesis of (+)-indatraline and a formal synthesis of (R)-tolterodine." RSC Advances 11, no. 37 (2021): 23161–83. http://dx.doi.org/10.1039/d1ra04538e.

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Efficient kinetic resolution occurs in ATH of racemic 3-arylindanones using (R,R)-or (S,S)-Ts-DENEB catalyst and HCO<sub>2</sub>H/Et<sub>3</sub>N mixture providing near equal yields of cis-3-arylindanols and unreacted 3-arylindanones with excellent stereoselectivities.

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Dissertations / Theses on the topic "Resolution of racemic mixture"

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Campbell, Matthew 1980. "Resolution of racemic glutamic acid mixtures." Thesis, McGill University, 2005. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=83854.

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Optical isomers (enantiomers) are chiral molecules, which are commonly used in the drug and food industry. The major difference between the two D and L enantiomers is the spatial arrangement of atoms around a central carbon. During normal chemical synthesis a mixture of L and D enantiomers are formed in equally proportion (racemic mixture). Currently, the most common technique for resolution of a racemic mixture is chromatography using chiral specific columns. However, this method is limited in scale and is rather costly. This work studies the possibility for the resolution of racemic g

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Piamtongkam, Rungtiwa. "Expression and evolution of lipases from Candida rugosa and Yarrowia lipolytica to modify their activities and specificities." Thesis, Toulouse, INSA, 2010. http://www.theses.fr/2010ISAT0015/document.

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Les lipases, protéines ubiquitaires, sont les enzymes les plus étudiées et les plus utilisées dans l’industrie. Elles catalysent un très grand nombre de réactions, d’hydrolyse et de synthèse, conduisant à une grande diversité de molécules, acides, esters, amides…. Les domaines d’applications sont nombreux : les bio-énergies, les arômes, bio-lubrifiants, bio-plastifiants, émulsifiants, produits phytosanitaires et détergents, cosmétiques, synthons pour la chimie fine, produits pharmaceutiques… Aujourd’hui, grâce aux outils génétiques, il est possible de modifier leur activité, spécificité et the

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Canbolat, Eylem. "Organocatalytic Resolution Of Racemic Alpha Azido Ketones." Master's thesis, METU, 2012. http://etd.lib.metu.edu.tr/upload/12614602/index.pdf.

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Chiral cyclic alpha azido ketones are very important compounds in organic chemistry. Because, the reduced forms of them are amino alcohols and these amino alcohols are interesting compounds for their biological activities. They have some pharmaceutical activities such as: potassium channel open up properties, treatment of central nervous system, antihypertensive properties, the agent of dopamin receptor activator, hypolipemic agent and dopamine agonist. These types of compounds have highly acidic alpha-protons, and many kinds of reactions can be performed with them. In this study, mainly, sel

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Lekuni, Olivia. "Cost-Effectiveness of selecting an Enantiopure formulation over a racemic mixture." University of the Western Cape, 2017. http://hdl.handle.net/11394/6437.

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Magister Scientiae - MSc (Pharmacy Administration and Policy Regulation)<br>The aim of this study is to provide more information in terms of the cost-effectiveness of selecting an enantiopure formulation over a racemic mixture in the context of promoting rational use of medicines. This was done by comparing costs and efficacy of escitalopram versus citalopram and esomeprazole versus omeprazole since they are the most commonly used medicines with both racemate and enantiopure products registered.

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Kavurt, Ulku Bade. "Enzyme Enhanced Ultrafiltration For The Resolution Of Racemic Mandelic Acid." Master's thesis, METU, 2011. http://etd.lib.metu.edu.tr/upload/12613483/index.pdf.

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In this study, resolution of racemic mandelic acid by enyzme enhanced ultrafiltration (EEUF) was studied. In order to develop a methodology, bovine serum albumin (BSA) was used as a model protein for polymer enhanced ultrafiltration (PEUF) experiments and the enzyme S-mandelate dehydrogenase was used for EEUF experiments. To be used for enzyme enhanced ultrafiltration experiments, the gene which is responsible from the production of S-mandelate dehydrogenase was isolated from Pseudomonas putida, expressed in Escherichia coli and the recombinant enzyme was produced. For PEUF experiments, effect

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Swain, Simon A. "The enzymatic resolution of racemic enol acetates derived from prochiral oxabicyclic ketones." Thesis, University of Liverpool, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.367792.

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Pinto, José Jorge Baeta Fontinha. "One-pot enzymatic resolution/separation of enantiomers using green solvents." Master's thesis, Faculdade de Ciências e Tecnologia, 2013. http://hdl.handle.net/10362/10824.

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Dissertação para obtenção do Grau de Mestre em Biotecnologia<br>In the context of “green” chemistry and sustainable processes, the main goal of this work is to develop a process that would circumvent the current complications of racemic sec-alcohol separation, using alternative solvents and selective enzymatic resolution. In this work the ability of enzymes to perform the resolution of sec-alcohols to obtain high added-value enantiomers is advantageously exploited in the production of pure chiral compounds. Candida rugosa lipase is capable of selectively converting one of the enantiomers of

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Castro, João Tiago Duarte Ferreira de. "Benefícios dos estereoisómeros na terapêutica medicamentosa." Master's thesis, [s.n.], 2014. http://hdl.handle.net/10284/4514.

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Projeto de Pós-Graduação/Dissertação apresentado à Universidade Fernando Pessoa como parte dos requisitos para obtenção do grau de Mestre em Ciências Farmacêuticas<br>A maioria dos fármacos comercializados atualmente são estereoisómeros, podendo estes apresentar-se na forma de enantiómeros ou diastereómeros. Desde que ocorreu o desastre da talidomida nos anos 60, a indústria química e farmacêutica apercebeu-se da importância do estudo da quiralidade dos fármacos e das suas propriedades estereoquímicas. A análise da correlação entre a quiralidade e as propriedades toxicológicas e farmacológicas

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Vieira, Mariano George Sousa. "Chemical study of two Xylopia species and resolution of natural products by matrix assisted diffusion ordered spectroscopy (MAD)." Universidade Federal do CearÃ, 2014. http://www.teses.ufc.br/tde_busca/arquivo.php?codArquivo=13132.

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CoordenaÃÃo de AperfeiÃoamento de Pessoal de NÃvel Superior<br>Conselho Nacional de Desenvolvimento CientÃfico e TecnolÃgico<br>Xylopia nitida and Xylopia sericea are commonly known as âembira-brancaâ and âpimenta do sertÃoâ, respectively, belonging to Annonaceae family. The chromatographic analysis of X. nitida roots allowed isolation of a trachlyobane diterpene, ent-trachlyoban-18,19-diol and its acetylated product, ent-18,19-diacetoxy-trachylobane, a kaurene diterpene, ent-kaur-16-en-18,19-diol, two aporphinic alkaloids, 5,6,6a,7-tetrahydro-1-methoxy-(6aS)-4H-benzo[de][1,3]benzodioxolo[5,6-

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Ranjbar, Mohammad. "Optimal Signaling Strategies and Fundamental Limits of Next-Generation Energy-Efficient Wireless Networks." University of Akron / OhioLINK, 2019. http://rave.ohiolink.edu/etdc/view?acc_num=akron1564677171677636.

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Books on the topic "Resolution of racemic mixture"

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Olness, D. U. Mixture resolution of chemical vapors using a piezoelectricmultisensor array. 1987.

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Capogna, Giorgio. Labour analgesia: choice of local anaesthetics. Oxford University Press, 2016. http://dx.doi.org/10.1093/med/9780198713333.003.0016.

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In this chapter, the rationale for the choice of commonly used local anaesthetics—racemic bupivacaine, ropivacaine, and levobupivacaine—is reviewed, particularly with respect to their potency and differential block. Epidural and spinal dosing for labour analgesia and the role of ‘up–down’ studies to determine the minimum local anaesthetic concentration (MLAC) for labour analgesia is explained. Applying the MLAC model has enabled clinical comparisons at equipotent concentrations and doses. It has also quantified what contribution opioids have on the overall effectiveness of the analgesic mixtur

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Book chapters on the topic "Resolution of racemic mixture"

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Matsuoka, M. "Purity Drop in Optical Resolution of Racemic Mixtures." In Separation and Purification by Crystallization. American Chemical Society, 1997. http://dx.doi.org/10.1021/bk-1997-0667.ch006.

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Russell, Trisha A., and Edwin Vedejs. "Enantiodivergent Reactions: Divergent Reactions on a Racemic Mixture and Parallel Kinetic Resolution." In Separation of Enantiomers. Wiley-VCH Verlag GmbH & Co. KGaA, 2014. http://dx.doi.org/10.1002/9783527650880.ch6.

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Bada, Jeffrey. "Racemic (Mixture)." In Encyclopedia of Astrobiology. Springer Berlin Heidelberg, 2011. http://dx.doi.org/10.1007/978-3-642-11274-4_1329.

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Bada, Jeffrey. "Racemic Mixture." In Encyclopedia of Astrobiology. Springer Berlin Heidelberg, 2014. http://dx.doi.org/10.1007/978-3-642-27833-4_1329-3.

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Bada, Jeffrey. "Racemic Mixture." In Encyclopedia of Astrobiology. Springer Berlin Heidelberg, 2015. http://dx.doi.org/10.1007/978-3-662-44185-5_1329.

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Hengartner, Urs, and Johann Riegl. "Optical Resolution of Racemic α-Ionone." In Carotenoids. Birkhäuser Basel, 1996. http://dx.doi.org/10.1007/978-3-0348-9323-7_23.

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Ohuchi, Shokichi, Hiroyuki Nakamura, Hiroto Sugiura, Mitsuaki Narita, and Koji Sode. "An Optical Resolution of Racemic Organophosphorous Esters by Phosphotriesterase-Catalyzing Hydrolysis." In Biotechnology for Fuels and Chemicals. Humana Press, 1997. http://dx.doi.org/10.1007/978-1-4612-2312-2_58.

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Messina, Maria Teresa, Pierangelo Metrangolo, and Giuseppe Resnati. "Resolution of Racemic Perfluorocarbons through Self-Assembly Driven by Electron Donor-Acceptor Intermolecular Recognition." In ACS Symposium Series. American Chemical Society, 1999. http://dx.doi.org/10.1021/bk-2000-0746.ch017.

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Hopke, Philip K. "The Mixture Resolution Problem Applied to Airborne Particle Source Apportionment." In The Handbook of Environmental Chemistry. Springer Berlin Heidelberg, 1995. http://dx.doi.org/10.1007/978-3-540-49150-7_3.

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El-Din, Yomna Safaa, Mohamed N. Moustafa, and Hani Mahdi. "Gender Classification Using Mixture of Experts from Low Resolution Facial Images." In Multiple Classifier Systems. Springer Berlin Heidelberg, 2013. http://dx.doi.org/10.1007/978-3-642-38067-9_5.

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Conference papers on the topic "Resolution of racemic mixture"

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Lemercier, Gilles, Magali Alexandre, Chantal Andraud, et al. "All-optical induction of enantiomer resolution in a racemic mixture." In Optical Science and Technology, SPIE's 48th Annual Meeting, edited by Mark G. Kuzyk, Manfred Eich, and Robert A. Norwood. SPIE, 2003. http://dx.doi.org/10.1117/12.507994.

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Bhushan, Indu. "Efficient media for high production of microbial lipase from Bacillus subtilis (BSK-L) using response surface methodology for enantiopure synthesis of drug molecules." In 2nd International Scientific Conference "Plants and Microbes: the Future of Biotechnology". PLAMIC2020 Organizing committee, 2020. http://dx.doi.org/10.28983/plamic2020.044.

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Lipases are a multipurpose enzyme that holds a significant position in industrial applications due to its ability to catalyse a large number of reactions such as hydrolysis, esterification, interesterification, transesterification which makes it a potential candidate. It is also used for the separation of chiral drugs from the racemic mixture and this property of lipase is considered very important in pharmaceutical industries for the synthesis of enantiopure bioactive molecules. Assuming the tremendous importance of lipases, as stereoselective biocatalysts, in pharmaceuticals and various othe

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Rincón, D. A., M. C. Daza, and M. Doerr. "Application of the quantum theory of atoms in molecules (QTAIM) to the study of the enzymatic kinetic resolution of propranolol, an amino alcohol with pharmaceutical applications." In VIII Simpósio de Estrutura Eletrônica e Dinâmica Molecular. Universidade de Brasília, 2020. http://dx.doi.org/10.21826/viiiseedmol2020135.

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Propranolol, ((R,S)-1-iso-propylamino-3-(1-naphthoxy)-2-propanol), is a β-adrenergic antagonist and is commercially available as a racemic mixture. Only the S-enantiomer has the desired therapeutic effect. Therefore, many researchers have been working on strategies to obtain S-propranolol with high enantiomeric purity. One approach to carry out the acetylation of (R,S)-Propranolol using Candida antarctica lipase B, CalB. This reaction leads to an enantiomeric purity of 96% at a relatively low conversion rate of 30 %. In our research group, we have been studying this reaction. The CalB active s

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Bychkov, Stanislav S., Boris A. Grishanin, and Victor N. Zadkov. "Laser distillation of enantiomers from an isotropic racemic mixture." In International Seminar on Novel Trends in Nonlinear Laser Spectroscopy and High-Precision Measurements in Optics, edited by Sergei N. Bagaev, Victor N. Zadkov, and Sergei M. Arakelian. SPIE, 2001. http://dx.doi.org/10.1117/12.428338.

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Eames, Jason, Gregory Coumbarides, Marco Dingjan, Tony Flinn, Northern Northen, and Yonas Yohannes. "Probing the Parallel Kinetic Resolution of Racemic Oxazolidinones using Quasi-enantiomeric Profens." In The 10th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2006. http://dx.doi.org/10.3390/ecsoc-10-01417.

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Liu, Yan, Yin Feng, and Jing-Xi Ma. "Different Immobilized Method of CRL to Influence on Chiral Resolution of Racemic Paroxol." In 2016 Eighth International Conference on Measuring Technology and Mechatronics Automation (ICMTMA). IEEE, 2016. http://dx.doi.org/10.1109/icmtma.2016.63.

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Huang, Dushu, Yunhui Long, Wei Liu, Yong Hong, Ming Zhong, and Shijuan Xu. "Resolution of racemic a#945;-cyclohexyl mandelic acid using chiral micromicroemulsion liquid membrane." In 5th International Conference on Information Engineering for Mechanics and Materials. Atlantis Press, 2015. http://dx.doi.org/10.2991/icimm-15.2015.100.

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JEON, S. J., and W. H. HONG. "SEPARATION OF ETHYL (R) 4-CHLORO-3-HYDROXYBUTYRATE FROM RACEMIC MIXTURE BY USING BULK LIQUID MEMBRANE." In Proceedings of the 4th International Conference. WORLD SCIENTIFIC, 2004. http://dx.doi.org/10.1142/9789812702623_0109.

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Shen, Jun, Shuangyan Liu, Pengfei Li, Xiande Shen, and Yoshio Okamoto. "Optical resolution of racemic compounds by chiral HPLC on immobilized amylose derivatives with regioselective substituents." In 2011 IEEE/ICME International Conference on Complex Medical Engineering - CME 2011. IEEE, 2011. http://dx.doi.org/10.1109/iccme.2011.5876694.

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Pearlman, Justin D., and Vivek V. Sukhatme. "High-resolution atheroma mixture-modeled MRI." In Photonics West '98 Electronic Imaging, edited by Robert F. Erbacher and Alex Pang. SPIE, 1998. http://dx.doi.org/10.1117/12.309545.

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