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Dissertations / Theses on the topic 'Rhodium iii complexes'

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Published: 4 June 2021

Last updated: 1 February 2022

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1

Pater, Boke Chan de. "Terpyridine complexes of rhodium (I, III)." [S.l. : Amsterdam : s.n.] ; Universiteit van Amsterdam [Host], 2003. http://dare.uva.nl/document/70850.

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2

Goswami, Niranjan. "105Rh(III) complexes with acyclic tetrathioether ligands : potential radiotherapeutic agents /." free to MU campus, to others for purchase, 1996. http://wwwlib.umi.com/cr/mo/fullcit?p9812951.

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3

Karpin, George W. "Synthesis and Antimicrobial Activity of Half-Sandwich Ir(III), Rh(III), and Co(III) Complexes." Diss., Virginia Tech, 2017. http://hdl.handle.net/10919/79414.

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This dissertation describes the synthesis and antimicrobial use of a series of half-sandwich Ir(III), Rh(III), Co(III) amino acid and ethylenediamine complexes. This investigation focuses on the formulation (ηn-arene)M(L)X, (L = ethylenediamine or α-amino carboxylate), (M= Ir, Rh, Ru, Co). Arene, Ligand and metal center variations were designed to tailor antimicrobial activity specific for each organism studied (Staphylococcus aureus or Mycobacteria). Each of the D/L-amino acids formed a diasteromeric complex with chiral centers on both the metal center and amino acid ligand. The unique chira

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4

Anderson, Margaret. "An electrochemical and kinetic investigation of some rhodium (III) complexes." Thesis, University of the West of Scotland, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.294070.

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5

Matharu, Daljit. "Synthesis and applications of rhodium (III) complexes for asymmetric catalysis." Thesis, University of Warwick, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.445516.

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6

Bonnington, Kevin John. "Reactive rhodium (III) methyl complexes : kinetics, mechanisms and polymerisation catalysis." Thesis, University of Sheffield, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.419638.

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7

Vitorino, Susana Ricardo. "Rhodium(III) supramolecular complexes : synthesis, DNA binding and biological studies." Thesis, University of Birmingham, 2011. http://etheses.bham.ac.uk//id/eprint/2814/.

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The work described in this thesis concerns the synthesis, DNA binding and cytotoxicity studies of new Rh(III) supramolecular complexes. Chapter 1 reviews DNA molecular recognition by synthetic agents; exploring the different DNA binding modes and their importance in the anticancer properties of several metallodrugs. Special attention is given to the exciting cylinder agents, which underpin the work in this thesis and to the work with rhodium complexes and their studies with DNA and as anticancer drugs. Chapter 2 describes the synthesis, purification and characterization of Rh(III) mononuclear,

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8

Ballard, Beau Jurisson Silvia S. "Synthesis and evaluation of ¹⁰⁵Rhodium (III) complexes of phosphine chelate systems." Diss., Columbia, Mo. : University of Missouri--Columbia, 2008. http://hdl.handle.net/10355/6693.

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Title from PDF of title page (University of Missouri--Columbia, viewed on Feb 25, 2010). The entire thesis text is included in the research.pdf file; the official abstract appears in the short.pdf file; a non-technical public abstract appears in the public.pdf file. Dissertation advisor: Dr. Silvia Jurisson. Vita. Includes bibliographical references.

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9

Akgun, Zeynep. "Synthesis and evaluation of 105Rhodium(III) complexes derived from diaminodithioether (DADTE) ligands." Diss., Columbia, Mo. : University of Missouri-Columbia, 2006. http://hdl.handle.net/10355/4340.

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Thesis (Ph. D.) University of Missouri-Columbia, 2006.<br>The entire dissertation/thesis text is included in the research.pdf file; the official abstract appears in the short.pdf file (which also appears in the research.pdf); a non-technical general description, or public abstract, appears in the public.pdf file. Title from title screen of research.pdf file (viewed on July 30, 2006). Includes bibliographical references.

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10

Nallas, Girlie Naomi A. "Heteronuclear trimetallic polyazine complexes of iridium (III) or rhodium (III) as electrocatalysts for the reduction of CO2." Diss., Virginia Tech, 1996. http://hdl.handle.net/10919/40465.

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11

Simonato, Jean-Pierre. "Chimie de coordination de la tétraméthylchiroporphyrine avec le fer(III), le cobalt(III) et le rhodium(III) : applications à l'analyse d'énantiomères d'amines, à la complexation énantiosélective d'aminoalcools, et à la catalyse d'aziridination asymétrique." Université Joseph Fourier (Grenoble), 1999. http://www.theses.fr/1999GRE10051.

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Des complexes metalliques de la tetramethylchiroporphyrine, de symetrie et possedant des groupements meso derives du biocartol, ont ete synthetises, caracterises, et utilises dans quatre axes de recherches. _la caracterisation du complexe bis-ethanol de la tetramethylchiroporphyrine de fer(iii), en solution et en phase solide, revele que ce compose presente un etat de spin inhabituel : le spin intermediaire pur (s = 3/2). _l'insertion d'un metal diamagnetique, le cobalt(iii), coordonnant les amines au cur de la porphyrine, a permis l'analyse qualitative et quantitative de la composition de der

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12

Caix, Chrystelle. "Propriétés électrochimiques des complexes du type ((eta5-Me5C5)M(L)Cl)+ (M=Ir(III), Rh(III)) en solution et immobilisés dans des films de polymère : application à l'électrocatalyse." Université Joseph Fourier (Grenoble), 1996. http://www.theses.fr/1996GRE10154.

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Ce memoire est consacre a l'evaluation des possibilites offertes par les complexes de coordination de rhodium (iii) et d'iridium (iii) du type (#5-me#5c#5)m(l)x#+ en electrocatalyse. Nous nous sommes plus particulierement interesses a leur application (en phase homogene ou immobilises a la surface d'une electrode sous forme de films polypyrroliques) a l'electroreduction catalytique des protons en hydrogene moleculaire, a l'hydrogenation electrocatalytique de substrats organiques insatures, et a la reduction electrocatalytique du dioxyde de carbone. Une partie de ce travail a consiste a etudier

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13

La, PenseÌe Annemarie Agnes. "Homoleptic diarsine and diphosphine complexes of iron(II), ruthenium(II) and rhodium(III) : synthesis and electrochemistry." Thesis, University of Liverpool, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.250371.

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14

Menu, Marie-Joëlle. "Nouveaux reactifs dans la chimie des complexes du rhodium, du chrome et du tungstene : les anions diazo rc(n::(2))**(-)." Toulouse 3, 1988. http://www.theses.fr/1988TOU30068.

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Synthese des complexes de rh, cr et w contenant le coordinat diazo en faisant reagir les sels de li des anions rc(n::(2))**(-) sur les complexes metalliques. On a isole: (pme::(3))::(4) rhc(n::(2))sime::(3) (pet::(3))::(3) rhc(n::(2))sime::(3), (pme::(3))::(2) rhc(n::(2))(s)p(n-ipr::(2))::(2). On a mis en evidence un complexe carbenique dimere possedant un groupe ylure, lors de la photolyse de (pet::(3))::(3) rhc(n::(2))sime::(3)

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15

Thu, Hung-yat. "Catalytic C-H bond functionalization reactions catalyzed by rhodium(III) porphyrin, palladium(II) and platinum(II) acetate complexes." View the Table of Contents & Abstract, 2006. http://sunzi.lib.hku.hk/hkuto/record/B38027872.

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16

Lee, Wei-Tsung. "Tris(guanidinato)complexes of iridium and rhodium in the oxidation states +III and +IV: synthesis, characterization, and reactivity." Diss., University of Iowa, 2011. https://ir.uiowa.edu/etd/2736.

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Mononuclear [Ir{ArNC(NR2)NAr}(C8H14)2] complexes (where R = Me or Et; Ar = Ph or 4-MeC6H4; and C8H14 = cis-cyclooctene) were synthesized from the neutral N,N-dialkyl-N′,N′′-diarylguanidines via deprotonation and transmetalation. As confirmed by single-crystal structure determination, the guanidinato(1−) ligands coordinate the low-valent d8 IrI center in an N,N′-chelating binding mode, and the C–N distances of the CN3 core suggest that these ligands function as stronger donors than related monoanionic, bidentate nitrogen-based ligands. In the reaction of the complexes with O2, new [Ir{ArNC(NR2)

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17

Morris, David. "Design and Modification of Half-Sandwich Ir(III), Rh(III), and Ru(II) Amino Acid Complexes for Application in Asymmetric Transfer Hydrogenation Reactions." Diss., Virginia Tech, 2015. http://hdl.handle.net/10919/71819.

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This dissertation describes the design and synthesis of a series of half-sandwich amino acid complexes of the form), (aa = α-amino carboxylate), and their utility as asymmetric transfer hydrogenation catalysts of ketones. Variation of the metal center, the n-ring, and the aa was used to tune these systems for specific sets of ketones. Upon reaction with homochiral]s, the ligand environment in all of these complexes is pseudotetrahedral, leading to stereogenic metal ions (SM, RM). The addition of another stereogenic center from the amino acid ligand (the carbon, RC or SC;glycine) gives rise to

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18

Nkabyo, Henry Ane. "A study on the reversible photo-induced isomerisation of platinum(II) and palladium(II) complexes of the N,N-dialkyl-N’-acyl(aroyl)thioureas with reversed-phase HPLC separation from related rhodium(III), ruthenium(III) and iridium(III) complexes." Thesis, Stellenbosch : Stellenbosch University, 2014. http://hdl.handle.net/10019.1/86773.

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19

Oliveira, Ione Maria Ferreira de. "Films de polypyrroles fonctionnalisés contenant des microparticules de métaux nobles ou des complexes du rhodium (III) : application de ces matériaux moléculaires d'électrode en hydrogénation électrocatalytique." Grenoble 1, 1992. http://www.theses.fr/1992GRE10075.

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Ce travail est consacré à la préparation, à la caractérisation et aux applications dans le domaine de l'hydrogénation électrocatalytique d'électrodes modifiées (em) par des films de polypyrroles fonctionnalisés. Les em par des films de polypyrroles substitues par des groupes cationiques (groupes alkylamonium ou pyridinium) et dans lesquels des microparticules d'un catalyseur hétérogène (pd(0) ou rh(0)) ont été incorporées, présentent une grande stabilité et une forte efficacité catalytique pour l'hydrogénation de substrats organiques, malgré les très faibles quantités de métaux déposées. Une é

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20

Davis, John Christopher. "Understanding the origin of 35/37Cl and 16/18O isotope effects on 195Pt and 103Rh NMR nuclear shielding in selected Pt(IV) and Rh(III) complexes : a DFT study." Thesis, Stellenbosch : Stellenbosch University, 2013. http://hdl.handle.net/10019.1/95484.

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21

Ourari, Ali. "Étude de deux réactions d'électrocatalyse : hydrogénation électrocatalytique sur des films de polymères contenant des microparticules de métaux nobles et activation de l'oxygène par des complexes Mn(III) - bases de Schiff." Université Joseph Fourier (Grenoble ; 1971-2015), 1995. http://www.theses.fr/1995GRE10171.

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Ce travail est relatif a l'etude de deux reactions d'electrocatalyse. La premiere partie concerne la mise au point de cathodes moleculaires, realisees par l'inclusion de microparticules de metaux nobles dans des films de polypyrrole fonctionnalise et a leur application en hydrogenation electrocatalytique. L'etude de l'hydrogenation de deux substrats test, le limonene et la carvone, a montre qu'il est possible d'orienter la selectivite de ces electrodes modifiees selon la nature du metal incorpore (pt, pd ou rh). Le resultat le plus significatif est que l'incorporation dans le meme film de poly

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22

Boudreau, Josée. "SYNTHÈSE ET RÉACTIVITÉ D’UN COMPLEXE DE RHODIUM(III) POSSÉDANT UN LIGAND AMBIPHILE PHOSPHINE-ALANE." Thesis, Université Laval, 2011. http://www.theses.ulaval.ca/2011/28809/28809.pdf.

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23

Boudreau, Josée. "Synthèse et réactivité d'un complexe de rhodium(iii) possédant un ligand ambiphile phosphine-alane." Doctoral thesis, Université Laval, 2011. http://hdl.handle.net/20.500.11794/23197.

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Cet ouvrage démontre le potentiel qu'ont les ligands ambiphiles pour des applications dans des systèmes d'intérêt en activation du lien C-H d'alcanes. La synthèse du complexe Cp*RhMe2(PMe2CH2AlMe2) (Cp* = r*5-C5Me5) est présentée et l'étude de sa réactivité démontre que l'incorporation d'un fragment acide de Lewis dans la sphère de coordination secondaire de l'atome de rhodium influence significativement la réactivité au niveau de ce métal de transition. Celle-ci est enrichie par la capacité du fragment acide de Lewis d'abstraire un ligand méthylé pour former le zwitterion transitoire Cp*Rh+M

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24

Yu, Yu-Cheng, and 游育晟. "Photophysical, Electrochemical and Theoretical Studies of Cyclometalated Rhodium(III) and Iridium(III) Complexes." Thesis, 2007. http://ndltd.ncl.edu.tw/handle/92101106029709879632.

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碩士<br>國立成功大學<br>化學系碩博士班<br>95<br>The research performed in this work constitutes two major parts. The first section involves photophysical and electrochemical properties of six new cyclometalated rhodium(III) complexes. Six new cyclometalated rhodium(III) complexes of the formula [Rh(ppy)2(L)], ppy = 2-phenylpyridine and L = 2,2'-dipyridylamine (HDPA) (1), deprotonated form of 2,2'-dipyridylamine (DPA) (2), 2,2'-dipyridylketone (dpk) (3), acetyl acetone (acac) (4), 2,2'-bipyrimidine (bpym) (5), and 2,3-di-pyridin-2-yl-pyrazine (dpp) (6) have been synthesized and subjected to X-ray diffraction

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25

Tseng, Mei-Ching, and 曾梅菁. "Synthesis, structure, photophysical and electrochemical studies of rhodium(III) and iridium(III) complexes." Thesis, 2006. http://ndltd.ncl.edu.tw/handle/49494277653095504801.

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博士<br>國立成功大學<br>化學系碩博士班<br>94<br>The research performed in this works constitutes three major parts. The synthesis, X-ray crystal structure, luminescence and electrochemical properties of four bis-cyclometalated heteroleptic Ir(III) complexes, [Ir(ppy)2(HDPA)](PF6) (1), [Ir(ppy)2(DPA)] (2), [Ir(ppy)2(dpk)](PF6) (3), and [Ir(ppy)2(pik)](PF6) (4) (where ppy = 2-phenylpyridine, HDPA = 2,2'-dipyridylamine, DPA = the deprotonated form of 2,2'-dipyridylamine, dpk = di-2-pyridyl ketone, and pik = 2-pyridyl N-methyl-2-imidazolyl ketone ) are reported in the first part. Each complex exhibits strong abs

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26

Chung, George, and 張喬智. "Photophysical, Electrochemical and Density Functional Theory Studies of Cyclometalated Rhodium(III) and Iridium(III) Complexes Containing Bridge Ligands." Thesis, 2008. http://ndltd.ncl.edu.tw/handle/18857269245941695638.

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碩士<br>國立成功大學<br>化學系碩博士班<br>96<br>The research performed in this work involved two kind of bridge ligands, 2,3-bis(2-pyridiyl)-pyrazine (dpp) and 2,2'-bipyrimidine (bpym). Dinuclear cyclometalated complexes of [Ir2(ppy)4(dpp)]2+ (1), [Rh2(ppy)4(dpp)]2+ (2), [IrRh(ppy)4(dpp)]2+ (3), [Ir2(ppy)4(bpym)]2+ (5), [Rh2(ppy)4(bpym)]2+ (6), and [IrRh(ppy)4(bpym)]2+ (7) and mononuclear cyclometalated complexes of [Ir(ppy)2(dpp)]+ (4) and [Ir(ppy)2(bpym)]+ (8) were synthesized with bridge ligand. The structure of these cyclometalated complexes were identified by X-ray diffraction crystallography and spect

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27

Sitlani, Ayesha. "Sequence specific recognition and photocleavage of DNA by phenanthrenequinone diimine complexes of rhodium(III)." Thesis, 1993. https://thesis.library.caltech.edu/7388/1/Sitlani-a-1993.pdf.

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<p>Sequence-specific recognition and photocleavage of DNA by a series of 9,10- phenanthrenequinone diimine (phi) complexes of rhodium(III) was studied. [Rh(phi)]^(3+) complexes bind to DNA via intercalation of their phi ligand and upon photoactivation promote strand scission. The DNA degradation products formed are consistent with photoreaction of [Rh(phi)]^(3+) intercalated in the major groove of DNA, via abstraction of the C3'-H atom of the deoxyribose. For the complex [Rh(phen)2phi]^(3+) and its derivatives [Rh(X)2phi]^(3+), the primary products are 5' and 3' phosphate termini and nucleic a

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28

Stern, Gary Avery. "Mass spectrometric and NMR studies of some [beta]-ketoenolate and monothio-[beta]-ketoenolate complexes of rhodium(III) and iridium(III)." 1991. http://hdl.handle.net/1993/18353.

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29

"1,2-rearrangements of porphyrinato rhodium (III) alkyls- mechanistic investigation." 1998. http://library.cuhk.edu.hk/record=b6073084.

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by Kin Wah Mak.<br>Thesis (Ph.D.)--Chinese University of Hong Kong, 1998.<br>Includes bibliographical references (p. 180-195).<br>Electronic reproduction. Hong Kong : Chinese University of Hong Kong, [2012] System requirements: Adobe Acrobat Reader. Available via World Wide Web.<br>Mode of access: World Wide Web.

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30

Huang, Jen-Hsing, and 黃任興. "Electrochemical studies of mixed-ligand complexesof rhodium(III) containing N,N''—dipyridylamine." Thesis, 2002. http://ndltd.ncl.edu.tw/handle/98299401685896308629.

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碩士<br>國立成功大學<br>化學系碩博士班<br>90<br>Abstract Cyclic voltametric data have been obtained for mixed-ligand complexes of rhodium(III) containing N,N'–dipyridylamine，cis-[Rh(L-L)(HDPA)Cl2]Cl、cis-Rh(L-L)(DPA)Cl2（L-L=bipy or phen）and cis-[Rh(HDPA)2Cl2]Cl in acetonitrile. For cis-[Rh(L-L)(HDPA)Cl2] Cl，between 0∼+1.80 V vs. SCE there is a reversible oxidation peak which is +1.07∼+1.08 V and reduction peak is +0.85∼+0.87 V. This is attributed to oxidation of chloride ion. There are two irreversible reduction peaks between 0∼-1.80 V vs. SCE. Each of the reductions is one-electron reduction step followed b

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