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Journal articles on the topic 'Seeded emulsion polymerization'

Author: Grafiati

Published: 20 February 2023

Last updated: 31 July 2025

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1

Duan, Yanping, Xia Zhao, Xiang Nan, et al. "Anisotropic Microparticles with a Controllable Structure via Soap-Free Seeded Emulsion Polymerization." Molecules 30, no. 1 (2025): 166. https://doi.org/10.3390/molecules30010166.

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Anisotropic particles have a wide range of applications in materials science such as emulsion stabilization, oil–water separation, and catalysis due to their asymmetric structure and properties. Nevertheless, designing and synthesizing large quantities of anisotropic particles with controlled morphologies continue to present considerable challenges. In this study, we successfully synthesized anisotropic microspheres using a soap-free seed emulsion polymerization method. This approach combines the benefits of seed emulsion polymerization with emulsion interfacial polymerization. By varying the

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2

Banetta, Luca, Giuseppe Storti, George Hoggard, Gareth Simpson, and Alessio Zaccone. "Predictive model of polymer reaction kinetics and coagulation behavior in seeded emulsion co- and ter-polymerizations." Polymer Chemistry 11, no. 41 (2020): 6599–615. http://dx.doi.org/10.1039/d0py01138j.

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3

Šňupárek, Jaromír, Jan Skoupil, Štêpán Podzimek, and Alois Kaštánek. "Non-seeded semi-continuous emulsion polymerization." Makromolekulare Chemie. Macromolecular Symposia 31, no. 1 (1990): 89–105. http://dx.doi.org/10.1002/masy.19900310109.

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4

Xu, Chun Lei, Yi Hu, Jin Qiang Liu, Sheng Peng Wang, Shao Min Qu, and Jian Hua Xu. "The Preparation of Core-Shell Type Acrylic-Polyurethane Composite Emulsions for Pigment Printing." Advanced Materials Research 332-334 (September 2011): 387–90. http://dx.doi.org/10.4028/www.scientific.net/amr.332-334.387.

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Vinyl-endblocked polyurethanes were prepared from polyether diols(N210), isophorone diisocyanate (IPDI), dimethylol propionic acid (DMPA) and 2-hydroxyethyl acrylate (HEA). The core-shell structure acrylic-polyurethane composite emulsion was prepared by seeded emulsion polymerization of methyl methacrylate (MMA) and butyl acrylate (BA) using the polyurethanes emulsions as seeded emulsions. The core and shell regions were occupied by acrylic polymer and polyurethane, respectively. Because polyurethanes were vinyl-endblocked, acrylic monomers could graft partially to them. The formation of core-

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5

Yu, Xiaotian, Yijing Sun, Fuxin Liang, Bingyin Jiang, and Zhenzhong Yang. "Triblock Janus Particles by Seeded Emulsion Polymerization." Macromolecules 52, no. 1 (2018): 96–102. http://dx.doi.org/10.1021/acs.macromol.8b02101.

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6

He, Min, Qiu Yu Zhang, and Ji Ying Guo. "Synthesis and Characterization of Water Based Acrylic Pressure Sensitive Adhesive of Surface Protection Tape." Advanced Materials Research 306-307 (August 2011): 1785–91. http://dx.doi.org/10.4028/www.scientific.net/amr.306-307.1785.

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The water based acrylic pressure sensitive adhesive was synthesized by seeded pre-emulsion polymerization, the influence of the amount of seeded pre-emulsion, and tri-functional aziridine crosslinker on the properties of the adhesive were studied. It was found that with the increase of the amount of seeded pre-emulsion, latex particle size decreases, contrasted with the increase of the viscosity, surface tension and contact angle of the emulsion; The aging performance of the adhesive can be significantly improved with the increase of the content of the crosslinker; compared with high temperatu

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7

Hamilton, Heather S. C., and Laura C. Bradley. "Probing the morphology evolution of chemically anisotropic colloids prepared by homopolymerization- and copolymerization-induced phase separation." Polymer Chemistry 11, no. 2 (2020): 230–35. http://dx.doi.org/10.1039/c9py01166h.

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Chemically anisotropic colloids prepared by polymerization-induced phase separation during seeded emulsion polymerization with non-crosslinked seeds reveals tunability in both surface and interior properties based on the morphology evolution.

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8

Mock, Eric B., Hank De Bruyn, Brian S. Hawkett, Robert G. Gilbert, and Charles F. Zukoski. "Synthesis of Anisotropic Nanoparticles by Seeded Emulsion Polymerization." Langmuir 22, no. 9 (2006): 4037–43. http://dx.doi.org/10.1021/la060003a.

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9

Plessis, Christophe, Gurutze Arzamendi, José R. Leiza, Harold A. S. Schoonbrood, Dominique Charmot, and José M. Asua. "Modeling of Seeded Semibatch Emulsion Polymerization ofn-BA." Industrial & Engineering Chemistry Research 40, no. 18 (2001): 3883–94. http://dx.doi.org/10.1021/ie000427e.

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10

Tobita, Hidetaka, and Yasunori Yoshihara. "Microgel formation in emulsion copolymerization: 2. Seeded polymerization." Journal of Polymer Science Part B: Polymer Physics 34, no. 8 (1996): 1415–22. http://dx.doi.org/10.1002/(sici)1099-0488(199606)34:8<1415::aid-polb3>3.0.co;2-r.

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11

Cheng, B., Y. R. Zhu, W. Q. Jiang, C. Y. Wang, and Z. Y. Chen. "Synthesis and Characterization of Nickel–Poly(St-co-AA)Composite Nanospheres by Ultraviolet Irradiation." Journal of Chemical Research 23, no. 8 (1999): 506–7. http://dx.doi.org/10.1177/174751989902300826.

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12

Keskin, Selime, Catalina N. Cheaburu-Yilmaz, Aylin Altinisik Tagac, Raluca Nicoleta Darie-Nita, and Onur Yilmaz. "Synthesis of Acrylic–Urethane Hybrid Polymer Dispersions and Investigations on Their Properties as Binders in Leather Finishing." Polymers 17, no. 3 (2025): 308. https://doi.org/10.3390/polym17030308.

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This study investigates the synthesis and application of acrylic–urethane hybrid polymer dispersions as advanced binders for leather finishing. Two polymerization techniques—seeded emulsion and miniemulsion—were used to produce hybrid polymer dispersions by varying the ratios of polyurethane (PU) and acrylic (AC). The synthesized dispersions, i.e., the hybrid polyurethanes, showed stable, uniform particle sizes, inferring good compatibility and interaction between the PU and AC phases, as confirmed by particle sizes, FTIR, and DSC analyses. The performance of the coating on leather surfaces wa

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13

Li, Jie, Zeting Huang, Mu Yang, et al. "Oriented immobilization of Au nanoparticles on C@P4VP core–shell microspheres and their catalytic performance." New Journal of Chemistry 39, no. 4 (2015): 2949–55. http://dx.doi.org/10.1039/c4nj02112f.

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14

Cong, Hailin, Bing Yu, Lilong Gao, et al. "Preparation of morphology-controllable PGMA-DVB microspheres by introducing Span 80 into seed emulsion polymerization." RSC Advances 8, no. 5 (2018): 2593–98. http://dx.doi.org/10.1039/c7ra13158e.

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15

Fei, Guiqiang, Yu Zhang, Xia Wang, Xiaorui Li, and Haihua Wang. "Effects of Continuous Phase and Crosslinking Agent on the Rheological Behaviors and Properties of Cationic Poly(urethane-acrylate) Emulsifier-Free Microemulsions." Journal of Nanoscience and Nanotechnology 18, no. 12 (2018): 8419–25. http://dx.doi.org/10.1166/jnn.2018.16423.

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Cationic poly(urethane-acrylate) emulsifier-free microemulsions are prepared by seeded emulsion polymerization (SPUA) or in-situ emulsion polymerization (IPUA) with (a) or without (b) crosslinking agent hydroxyethyl acrylate (HEA). Furthermore, no surfactant is introduced into the reaction system. The effect of continuous phase and HEA on the rheological behavior and properties of microemulsions are studied. The results show that IPUA using vinylmonomers as the continuous phase and with HEA (IPUAMB-b) has the highest ζ value, lowest coagulation ratio, smallest particle size of 48 nm and appare

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16

Kumar, Satish, Shayoraj Shayoraj, Neeru Devi, et al. "Preparation, Characterization and Properties of some Acrylic Base Latex: A Review." Oriental Journal Of Chemistry 37, no. 5 (2021): 1002–16. http://dx.doi.org/10.13005/ojc/370501.

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Acrylic polymer latex has versatile role in many academic and industrial applications like paint, adhesives, textile, paper industry, concrete, surface coating, synthetic rubber and many ones. Acrylic base polymer latex can be prepared by various polymerization methods like Batch emulsion, Seeded emulsion, Situ miniemulsion, Atom transfer radical, Free radical copolymerization, Pickering miniemulsion, Semi-continuous seeded emulsion, dispersion copolymerization, aqueous suspension polymerization etc. in different solvents i.e. 1,1,2-trichloroethane, water, deionized water, 1,4-dioxane, chlorof

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17

Spasevska, D., G. P. Leal, M. Fernández, J. Blazevska Gilev, M. Paulis, and R. Tomovska. "Crosslinked reduced graphene oxide/polymer composites via in situ synthesis by semicontinuous emulsion polymerization." RSC Advances 5, no. 21 (2015): 16414–21. http://dx.doi.org/10.1039/c4ra16406g.

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From aqueous dispersions of crosslinked polymer/reduced graphene oxide (rGO) composite nanoparticles, synthesized by semicontinuous seeded emulsion polymerization, to electrically conductive and reinforced composite films.

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18

Horn, Alexander G., Thomas C. Johnston, and Damien Guironnet. "Biphasic Seeded Emulsion Polymerization in a Tubular Flow Reactor." Industrial & Engineering Chemistry Research 59, no. 22 (2020): 10389–96. http://dx.doi.org/10.1021/acs.iecr.0c00961.

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19

Chern, C. S., and Y. N. Kuo. "Shear-induced coagulation kinetics of semibatch seeded emulsion polymerization." Chemical Engineering Science 51, no. 7 (1996): 1079–87. http://dx.doi.org/10.1016/s0009-2509(96)80007-8.

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20

Zhenqian, Zhang, Xie Bo, Wang Pei, and Yuan Ninyyi. "Hybrid latex particles preparation with seeded semibatch emulsion polymerization." Colloids and Surfaces A: Physicochemical and Engineering Aspects 482 (October 2015): 422–30. http://dx.doi.org/10.1016/j.colsurfa.2015.06.050.

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21

Lange, David M., Gary W. Poehlein, Sadao Hayashi, Akihiko Komatsu, and Toshihiro Hirai. "Kinetic analysis of seeded emulsion polymerization of vinyl acetate." Journal of Polymer Science Part A: Polymer Chemistry 29, no. 6 (1991): 785–92. http://dx.doi.org/10.1002/pola.1991.080290601.

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22

Subramaniam, Nadaraja, Michael J. Monteiro, Joshua R. Taylor, Anne Simpson-Gomes, and Robert G. Gilbert. "Novel graft copolymers from mechanistically-designed seeded emulsion polymerization." Macromolecular Symposia 152, no. 1 (2000): 43–53. http://dx.doi.org/10.1002/1521-3900(200003)152:1<43::aid-masy43>3.0.co;2-7.

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23

Tang, P. L., E. D. Sudol, M. Adams, M. S. El-Aasser, and J. M. Asua. "Seeded emulsion polymerization of n-butyl acrylate utilizing miniemulsions." Journal of Applied Polymer Science 42, no. 7 (1991): 2019–28. http://dx.doi.org/10.1002/app.1991.070420728.

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24

Chen, Liang, Liang Hong, Jui-Ching Lin, Greg Meyers, Joseph Harris, and Michael Radler. "Epoxy-acrylic core-shell particles by seeded emulsion polymerization." Journal of Colloid and Interface Science 473 (July 2016): 182–89. http://dx.doi.org/10.1016/j.jcis.2016.04.005.

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25

Zhang, Pei, Donald C. Sundberg, and John G. Tsavalas. "Polymerization Induced Phase Separation in Composite Latex Particles during Seeded Emulsion Polymerization." Industrial & Engineering Chemistry Research 58, no. 46 (2019): 21118–29. http://dx.doi.org/10.1021/acs.iecr.9b02964.

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26

Chang, Yanning, Mingwang Pan, Jinfeng Yuan, et al. "Morphology and film performance of phthalate-free plasticized poly(vinyl chloride) composite particles via the graft copolymerization of acrylate swelling flower-like latex particles." RSC Advances 5, no. 50 (2015): 40076–87. http://dx.doi.org/10.1039/c5ra04747a.

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Polyacrylate plasticized PVC composite particles without toxicity and migration were synthesized via a multistage seeded emulsion polymerization of BA swelling nonspherical PBA/PVC latex particles with a flower-like shell.

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27

Resende, Graciane, Gabriel V. S. Dutra, Maria S. B. Neta, Olacir A. Araújo, Sacha B. Chaves, and Fabricio Machado. "Well Defined Poly(Methyl Methacrylate)-Fe3O4/Poly(Vinyl Pivalate) Core–Shell Superparamagnetic Nanoparticles: Design and Evaluation of In Vitro Cytotoxicity Activity Against Cancer Cells." Polymers 12, no. 12 (2020): 2868. http://dx.doi.org/10.3390/polym12122868.

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The objective of this work is to develop and characterize polymeric nanoparticles with core–shell morphology through miniemulsion polymerization combined with seeded emulsion polymerization, aiming at the application in the treatment of vascular tumors via intravascular embolization. The synthesis of the core–shell nanocomposites was divided into two main steps: (i) Formation of the core structure, consisting of poly(methyl methacrylate)/magnetic oxide coated with oleic acid (OM-OA) via miniemulsion and (ii) shell structure produced through seeded emulsion polymerization of vinyl pivalate. Nan

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28

Harsono, I., H. Hindarso, and N. Indraswati. "Base case simulation of a semi-batch emulsion copolymerization process: application to styrene/ butadiene system." Jurnal Teknik Kimia Indonesia 4, no. 3 (2018): 304. http://dx.doi.org/10.5614/jtki.2005.4.3.6.

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It has been long recognized that emulsion polymerization is a complex heterogeneous process involving transport of monomers, free radicals, and other species between aqueous phase and organic phase. Though there are a number of models available in the literature, most of them deal only with specific aspects in emulsion polymerization and are far from being general. To simulate this complicated process and to achieve an adequate level of understanding, a Polymers Plus software from Aspen Technology. Inc. was used. The objective of this work is to illustrate the principle of use of Polymers Plus

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29

Vogel, Nicolas, Ulrich Ziener, Achim Manzke, et al. "Platinum nanoparticles from size adjusted functional colloidal particles generated by a seeded emulsion polymerization process." Beilstein Journal of Nanotechnology 2 (August 18, 2011): 459–72. http://dx.doi.org/10.3762/bjnano.2.50.

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The benefits of miniemulsion and emulsion polymerization are combined in a seeded emulsion polymerization process with functional seed particles synthesized by miniemulsion polymerization. A systematic study on the influence of different reaction parameters on the reaction pathway is conducted, including variations of the amount of monomer fed, the ratio of initiator to monomer and the choice of surfactant and composition of the continuous phase. Critical parameters affecting the control of the reaction are determined. If carefully controlled, the seeded emulsion polymerization with functional

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30

Tian, Lei, Xue Li, Wenyan Wang, Zafar Ali, and Qiuyu Zhang. "Self-stripping of free-standing microparticle gel membranes driven by asymmetric swelling." Journal of Materials Chemistry C 5, no. 31 (2017): 7830–36. http://dx.doi.org/10.1039/c7tc01235g.

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A series of free-standing superparticle-gel membranes are fabricated on various polymer substrates, which assembled with acidified microsized patchy particles synthetized by unique seeded emulsion polymerization. These membranes with remarkable swelling property possess self-stripping ability.

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31

Liu, Yan Ping, Xi Jun Liu, and Chun Hua Lou. "Study on Synthesis Technology and Recipe Optimization of Core (PBA) - Shell (PMMA) Latex Particles." Advanced Materials Research 631-632 (January 2013): 584–87. http://dx.doi.org/10.4028/www.scientific.net/amr.631-632.584.

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In this paper, a novel grafting poly(butyl methacry1ate)-poly(methyl methacrylate) (PBA/PMMA) latex particles with core-shell structure was successfully synthesized by the method of pre-emulsion semi-continuous seeded emulsion polymerization. PMMA shell layer was cross-linked structure, and it was almost grafted onto PBA core due to the presence of the grafting agent ALMA. The influences of the amount of emulsifier and initiator, and reaction time on PBA core emulsion properties were investigated by analyzing BA conversion and PBA core particles size distribution. The influence of the amount o

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32

Tian, Lei, Yanxing Liu, Dai Wang, et al. "Particle-click-particle: colloidal clusters from click seeded emulsion polymerization." Polymer Chemistry 13, no. 8 (2022): 1084–89. http://dx.doi.org/10.1039/d1py00360g.

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33

Adams, Mary E., Gregory T. Russell, Brendan S. Casey, Robert G. Gilbert, Donald H. Napper, and David F. Sangster. "Bimolecular termination events in the seeded emulsion polymerization of styrene." Macromolecules 23, no. 21 (1990): 4624–34. http://dx.doi.org/10.1021/ma00223a021.

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34

Verdurmen, Edwin M., Erik H. Dohmen, John M. Verstegen, Ian A. Maxwell, Anton L. German, and Robert G. Gilbert. "Seeded emulsion polymerization of butadiene. 1. The propagation rate coefficient." Macromolecules 26, no. 2 (1993): 268–75. http://dx.doi.org/10.1021/ma00054a004.

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35

Oliveira, Pedro C., A. Guimarães, Jean-Yves Cavaillé, Laurent Chazeau, Robert G. Gilbert, and Amilton M. Santos. "Poly(dimethylaminoethyl methacrylate) grafted natural rubber from seeded emulsion polymerization." Polymer 46, no. 4 (2005): 1105–11. http://dx.doi.org/10.1016/j.polymer.2004.11.048.

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36

Wichaita, Waraporn, Duangporn Polpanich, Teeraporn Suteewong, and Pramuan Tangboriboonrat. "Hollow core-shell particles via NR latex seeded emulsion polymerization." Polymer 99 (September 2016): 324–31. http://dx.doi.org/10.1016/j.polymer.2016.07.032.

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37

Lu, Shulai, Rongjun Qu, and Jacqueline Forcada. "Preparation of magnetic polymeric composite nanoparticles by seeded emulsion polymerization." Materials Letters 63, no. 9-10 (2009): 770–72. http://dx.doi.org/10.1016/j.matlet.2008.12.045.

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38

Li, Yifan, Shensheng Chen, Serkan Demirci, et al. "Morphology evolution of Janus dumbbell nanoparticles in seeded emulsion polymerization." Journal of Colloid and Interface Science 543 (May 2019): 34–42. http://dx.doi.org/10.1016/j.jcis.2019.01.109.

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39

Nuasaen, Sukanya, and Pramuan Tangboriboonrat. "Highly charged hollow latex particles prepared via seeded emulsion polymerization." Journal of Colloid and Interface Science 396 (April 2013): 75–82. http://dx.doi.org/10.1016/j.jcis.2013.01.012.

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40

Shim, Sang-Eun, Yoon-Jong Cha, Jae-Man Byun, and Soonja Choe. "Size control of polystyrene beads by multistage seeded emulsion polymerization." Journal of Applied Polymer Science 71, no. 13 (1999): 2259–69. http://dx.doi.org/10.1002/(sici)1097-4628(19990328)71:13<2259::aid-app17>3.0.co;2-5.

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41

Zhao, Zong Qian, Bu Qin Xu, Gui Long Xu, Yi Wang, and Jian Hu. "Preparation and Characterization of Soap-Free Cationic Polystyrene Microspheres Using a Water Soluble Monomer." Advanced Materials Research 988 (July 2014): 84–88. http://dx.doi.org/10.4028/www.scientific.net/amr.988.84.

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Soap-free Cationic polystyrene microspheres were prepared by emulsion polymerization using a water soluble monomer Methacrylatoethyl trimethyl ammonium chloride (MADAC). Experimental studies were performed in detail to check the effect of the synthesis process of the microspheres, the MADAC dosage, and initiator dosage on the particle size and distribution. The chemical structure of latex particles was characterized by Fourier transform infrared spectroscopy. The micro-morphology of latex particles were observed by Transmission electron microscope. The results show that different particle size

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42

Wang, Likui, Florian Ion Tiberiu Petrescu, Jing Liu, Hongping Li, and Gang Shi. "Synthesis of Dimpled Particles by Seeded Emulsion Polymerization and Their Application in Superhydrophobic Coatings." Membranes 12, no. 9 (2022): 876. http://dx.doi.org/10.3390/membranes12090876.

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Dimpled particles are synthesized through the seeded polymerization of fluoroacrylate and styrene on swelled polystyrene spheres. The morphologies of the particles can be controlled by the polymerization temperature, the amount of solvent swelling the seeds or the ratio of the fluoroacrylate monomer over styrene. Golf-ball-like particles with many small dimples on their surfaces are obtained at low polymerization temperatures or with a small amount of solvent. Particles with a large single dimple are formed at higher polymerization temperatures, with larger solvent amounts or a higher ratio of

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43

Vatankhah, Zahra, Elham Dehghani, Mehdi Salami-Kalajahi, and Hossein Roghani-Mamaqani. "Seed's morphology-induced core-shell composite particles by seeded emulsion polymerization for drug delivery." Colloids and Surfaces B: Biointerfaces 191 (July 2020): 111008. http://dx.doi.org/10.1016/j.colsurfb.2020.111008.

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44

Zhu, Zhewen, Chaoying Zhang, and Shuling Gong. "Preparation and Properties of Polyester Modified Waterborne High Hydroxyl Content and High Solid Content Polyacrylate Emulsion." Polymers 11, no. 4 (2019): 636. http://dx.doi.org/10.3390/polym11040636.

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A high hydroxyl content waterborne polyester-acrylate emulsion was successfully synthesized in two steps. Firstly, the carboxyl terminated unsaturated polyester was synthesized, then it was reacted as a monomer with acrylate monomer by emulsion polymerization using the semi-continuous seeded method. The effects of the amount of hydroxyethyl methacrylate (HEMA), the ratio of polyester/acrylic, the ratio of soft/hard monomer, and the content of chain transfer agent to the properties of the composite emulsion were investigated. Through a variety of tests, both the emulsion and film properties of

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45

Plessis, C., G. Arzamendi, J. R. Leiza, H. A. S. Schoonbrood, D. Charmot, and J. M. Asua. "Seeded Semibatch Emulsion Polymerization ofn-Butyl Acrylate. Kinetics and Structural Properties." Macromolecules 33, no. 14 (2000): 5041–47. http://dx.doi.org/10.1021/ma992053a.

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46

Kim, Jung-Hyun, In-Woo Cheong, and Do-Ik Lee. "Modeling and Simulation of Equal Density Seeded Emulsion Polymerization of Styrene." Polymer Reaction Engineering 8, no. 1 (2000): 95–114. http://dx.doi.org/10.1080/10543414.2000.10744540.

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47

Li, Wing Sze Jennifer, Vincent Ladmiral, Hisaaki Takeshima, et al. "Ferulic acid-based reactive core–shell latex by seeded emulsion polymerization." Polymer Chemistry 10, no. 23 (2019): 3116–26. http://dx.doi.org/10.1039/c9py00079h.

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48

TEMENG, KWAKU O., and F. JOSEPH SCHORK. "CLOSED-LOOP CONTROL OF A SEEDED CONTINUOUS EMULSION POLYMERIZATION REACTOR SYSTEM." Chemical Engineering Communications 85, no. 1 (1989): 193–219. http://dx.doi.org/10.1080/00986448908940356.

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49

Okubo, M., K. Kanaida, and T. Matsumoto. "Production of anomalously shaped carboxylated polymer particles by seeded emulsion polymerization." Colloid & Polymer Science 265, no. 10 (1987): 876–81. http://dx.doi.org/10.1007/bf01421815.

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50

Chern, Chorng-Shyan, Tseng-Jung Chen, Shinn-Yih Wu, Horng-Bin Chu, and Chun-Fu Huang. "Semibatch Seeded Emulsion Polymerization of Acrylic Monomers: Bimodal Particle Size Distribution." Journal of Macromolecular Science, Part A 34, no. 7 (1997): 1221–36. http://dx.doi.org/10.1080/10601329708009381.

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