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1

Ramadani, Tarikh Azis, Fadilatul Taufany, and Siti Nurkhamidah. "Study of packed sieve tray column in ethanol purification using distillation process." Malaysian Journal of Fundamental and Applied Sciences 15, no. 1 (February 4, 2019): 69–74. http://dx.doi.org/10.11113/mjfas.v15n2019.936.

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Sieve tray becomes a popular contacting device in distillation process because of its relative simplicity and low cost. There is one way to improve the contact performance, especially mass transfer by modifying the sieve tray into packed sieve tray. This study was aimed to investigate the effect of adding packing in each tray to ethanol content on ethanol purification. This research was conducted via experiment and simulation approaches. The experiment used packed sieve tray that contained 3 cm and 5 cm bed of steel wool with 16 trays in the column, with operating pressure about 760 mmHg and performed in batch condition. The simulation used a reduced rated base model with some modifications for operation in the packed sieve tray column. It was found that the use of packed sieve tray gave better distillate in the batch distillation process than the use of sieve tray. The packed sieve tray raised distillate content about 8.89% when using 3 cm of packing and 23.31% when using 5 cm of packing when it was compared with sieve tray. The use of packed sieve tray could increase the mass transfer and reduce bubble diameter in the batch distillation process.
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2

Taufany, Fadlilatul, Nonot Soewarno, Melvina Eliana Sutanto, and Indi Raisa Girsang. "Performance of Appended Wire Mesh Packing in Sieve Tray Distillation Column of Ethanol-Water System." Modern Applied Science 9, no. 7 (July 1, 2015): 148. http://dx.doi.org/10.5539/mas.v9n7p148.

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For the separation process in liquid-liquid mixture such as ethanol-water mixture, a sieve tray distillation columnis an alternatif for affordable process and maintenance. However to date, this sieve tray system is still currentlyhaving a lower Murphee efficiency and smaller interfacial area, as compared to other tray system, that is, either abubble cap or valve tray. Therefore it is of important to optimize the performance of sieve tray distillation bymeans of adding the wire mesh packing on that tray, as being the aim of the present study. This study isconducted by using a batch sieve tray distillation system, where the wire mesh packing is added on the third traythat is calculated from the top of the column, to avoid flooding inside the column. Here the resulting fermentedmolasses of containing a 10% volume of ethanol is used as a mixture distillation feed. The height of the wiremesh packing being studied is varied as 5 cm, 3 cm, and 2 cm. Our results showed that the Murphee efficiencyobtained by the variation of the packing height of 5 cm, 3 cm, 2 cm and without packing were 73.5%, 66.27%,56.86%, and 46.7% respectively, and were increased by subsequent level of the packing height. Thecorresponding hydrodynamic properties of this appended packing sieve tray distillation by means of theinterfacial area were 11.88 cm2/cm3, 0.48 cm2/cm3, and 0.32 cm2/cm3, while its pressure drop measured from thewater manometer height were 38.33 cm H2O/m, 30 cm H2O/m, 10 cm H2O/m for the packing height of 5 cm, 3cm, 2 cm height, respectively. The increasing of the performance of appended packing sieve tray distillation bymeans of the Murphee efficiency is explained by the increasing of the interfacial area for vapour-liquid than thetray itself. This preliminary study is expected to be a pioneer study of strategy to increase the performance ofconventional sieve tray distillation that is known as a kind of affordable distillation process.
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3

Taufany, Fadlilatul, Nonot Soewarno, Koko Yuwono, Dimas Ardiyanta, Melvina Eliana, and Indi Raisa Girsang. "Feed Plate and Feed Adsorbent Temperature Optimisation of Distillation – Adsorption Process to Produce Absolute Ethanol." Modern Applied Science 9, no. 7 (July 1, 2015): 140. http://dx.doi.org/10.5539/mas.v9n7p140.

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Two subsequent separation processes are required to produce absolute ethanol (at least purity of 99.5% v/v),namely the distillation and adsorption processes. Thus, it is important to find the optimum operation conditionfor those following processes. The aims of the present study are to optimize the feed plate of distillation and thetemperature of feed adsorbent. This study is conducted using a continuous sieve tray distillation system with thenumber of 16 trays, the length-diameter ratio of 80.64, the reflux ratio of 3.5, and the feed with ethanol contentof 10 % v/v ethanol, which is produced via the fermentation process of molasses. To conduct the first aim of thisstudy, the feed enters the distillation column with several of variable feed plate, i.e. 12, 13, 14, and 15. This feedplate location is calculated from the top of the column. On the other hand, the second aim of this study, isconducted using the subsequent combination of distillation and adsorbent columns, where the distillate (purity ofethanol around 95% v/v) from the distillation column is then flowed into the adsorbent column with various feedadsorbent temperature, i.e. 80 °C, 90 °C, 100 °C, and 110 °C, to be purified as an absolute ethanol. Here theadsorbent column is designed as a fix bed adsorption column with a molecular sieve of 3A (zeolite) is used as anadsorbent for that purification process. Our results showed that the optimum feed plate is 14, because at thisplate the ethanol distillate has the highest content among those various variables. Meanwhile, the optimumtemperature of feed adsorbent is 90° C, which requires the least energy for the distillation - adsorption process,i.e. at 18691 kJ/kg absolute ethanol. This primary study is expected to be an alternative way to optimize theoperating condition of the sieve tray distillation-molecular sieve adsorption system by means of acquiring aminimum energy involving in the process to achieve the highest purity of ethanol.
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4

Biddulph, Michael W. "Efficiencies in a ternary sieve tray distillation column." Gas Separation & Purification 1, no. 2 (December 1987): 90–93. http://dx.doi.org/10.1016/0950-4214(87)80016-6.

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5

Mortaheb, Hamid Reza, Yoichi Iimuro, Hitoshi Kosuge, and Koichi Asano. "Mass Transfer in Ternary Distillation with Sieve Tray Column." JOURNAL OF CHEMICAL ENGINEERING OF JAPAN 33, no. 4 (2000): 597–604. http://dx.doi.org/10.1252/jcej.33.597.

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6

Li, Qunsheng, Manxia Zhang, Zhigang Lei, Xiaofei Tang, Lun Li, and Baohua Wang. "A distillation tray with high efficiency and excellent operating flexibility for viscous mixture separation." Chemical Industry and Chemical Engineering Quarterly 20, no. 2 (2014): 223–31. http://dx.doi.org/10.2298/ciceq120918003l.

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The flow-guided sieve-valve tray(FGS-VT)with high efficiency was designed to overcome the shortcoming of low operating flexibility of the flow-guided sieve tray. Its dimensions and geometry, as well as structure characteristics, were presented. The hydrodynamics and mass transfer performance, including dry-plate pressure drop, wet plate-pressure drop, weeping, entrainment and tray efficiency, of two types of FGS-VTs (FGS-VTs with 14 and 8 valves, respectively) and one flow-guided sieve tray were tested in an air-water-oxygen cold model experiment with a 0.6 m diameter plexiglass column. The results demonstrate that FGS-VT with 14 valves works better than FGS-VT with 8 valves, and in comparison with the flow-guided sieve tray, the flow-guided sieve-valve tray with 14 valves has higher tray efficiency, bigger operating flexibility, and lower wet-plate pressure drop (when all the valves are opened fully).Additionally, two typical applications to separate the mixture with high viscosity, solid, powder, easy-to-foam or easy self-polymerization components proved the unique advantages of FGS-VT.
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7

Ray, S., and S. P. Sengupta. "Irreversibility analysis of a sieve tray in a distillation column." International Journal of Heat and Mass Transfer 39, no. 7 (May 1996): 1535–42. http://dx.doi.org/10.1016/0017-9310(95)00231-6.

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8

Mortaheb, H. "Hydrodynamics and mass transfer in heterogeneous distillation with sieve tray column." Chemical Engineering Journal 88, no. 1-3 (September 28, 2002): 59–69. http://dx.doi.org/10.1016/s1385-8947(01)00263-7.

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9

Ray, S., Asim K. Panja, and S. P. Sengupta. "Irreversibility analysis of a separation system using sieve tray distillation column." Chemical Engineering Science 49, no. 9 (May 1994): 1472–77. http://dx.doi.org/10.1016/0009-2509(94)85073-9.

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10

Rahimi, R., M. R. Rahimi, and M. Zivdar. "Efficiencies of Sieve Tray Distillation Columns by CFD Simulation." Chemical Engineering & Technology 29, no. 3 (March 2006): 326–35. http://dx.doi.org/10.1002/ceat.200500285.

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11

MORTAHEB, HAMID REZA, HITOSHI KOSUGE, and KOICHI ASANO. "Mass Transfer in Foam and Froth Regimes in Distillation with Sieve Tray Column." JOURNAL OF CHEMICAL ENGINEERING OF JAPAN 34, no. 4 (2001): 493–500. http://dx.doi.org/10.1252/jcej.34.493.

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12

KOSUGE, Hitoshi, and Koichi ASANO. "Simulation of performance of multicomponent distillation by sieve tray columns." Journal of The Japan Petroleum Institute 28, no. 5 (1985): 413–16. http://dx.doi.org/10.1627/jpi1958.28.413.

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13

Björn, Ingela Niklasson, Urban Grén, and Fredrik Svensson. "Simulation and experimental study of intermediate heat exchange in a sieve tray distillation column." Computers & Chemical Engineering 26, no. 4-5 (May 2002): 499–505. http://dx.doi.org/10.1016/s0098-1354(01)00796-7.

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14

Roshdi, Sepideh, Norollah Kasiri, Seyyed Hassan Hashemabadi, and Javad Ivakpour. "Computational fluid dynamics simulation of multiphase flow in packed sieve tray of distillation column." Korean Journal of Chemical Engineering 30, no. 3 (February 1, 2013): 563–73. http://dx.doi.org/10.1007/s11814-012-0166-1.

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15

Pudjiastuti, Lily, Tri Widjaja, Kornelius Kevin Iskandar, Fikran Sahid, Siti Nurkhamidah, Ali Altway, and Atha Pahlevi Putra. "Modelling and simulation of multicomponent acetone-butanol-ethanol distillation process in a sieve tray column." Heliyon 7, no. 4 (April 2021): e06641. http://dx.doi.org/10.1016/j.heliyon.2021.e06641.

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16

Ibragimova, Ramilya, Vitaliy Afanasenko, Gleb Kudryavtsev, and Denis Mazidullin. "Use of numerical modeling methods in desing of combined rectification column." MATEC Web of Conferences 298 (2019): 00070. http://dx.doi.org/10.1051/matecconf/201929800070.

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The article is devoted to the study of methods for modeling the operation of rectification columns using the HYSIS application software package. Such studies are very important not only for design, but also for the functioning of existing industries. The article proposes to use for combining nozzle devices in the concentration part of the column, and plate-shaped structures in the distant part of the column for more efficient and stable operation of distillation columns. To determine the hydrodynamic parameters of the operation of distillation column, a technique of determining the range of stable loads and the position of the operating point inside or outside the range of stable loads was taken. A column model was constructed using the HYSYS software package for separating gas mixtures with various contact devices: sieve trays, Rashig ring nozzles. Experiments for the same type and combined contact devices were carried out and their comparison was carried out in terms of hydraulic calculation and operating range. As a result of experiments with the use of the HYSYS software package, it was shown that the combined arrangement of contact devices can provide a stable hydraulic mode, in contrast to the use of similar contact devices.
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17

Elisante, Emrod. "Development of Pilot Plant for Bio-Ethanol Processing." Tanzania Journal of Engineering and Technology 33, no. 1 (June 30, 2010): 9–17. http://dx.doi.org/10.52339/tjet.v33i1.449.

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The paper outlines achievements obtained in developing a pilot bio-ethanol plant at the Department of Chemical and Mining Engineering (CME), University of Dar es Salaam. The pilot plant consists of: 30 L inoculums tank; 1,700 L fermenter; 1,500 L/day distillation column; and ancillary equipment. The prototype is a platform intended to be used for technology demonstration and research by graduate and undergraduate students studying the production of bio-ethanol using traditional and non-traditional raw materials like coffee mash, cashew fruit, and sisal inulin. The equipment has been developed using locally available engineering resources and the distillation column with 18 sieve tray measures 0.5m diameter 7 m high operates at atmospheric pressure. The condenser is cooled by 15 o C chilled water from utility lines and the reboiler is powered by 63 kW boiler installed at CME. Although the system includes biological, chemical and mechanical engineering details, only the important design issues are presented. A MATLAB code was developed forestimating the number of theoretical plates using the Mc Cabe-Thiele method. The water- ethanol vapour liquid equilibrium VLE data was obtained using relative volatilities estimated by Antoine equations for vapour pressure. The process design was done using various simulation packages and custom programs like Microsoft Excel for mass balance,Microsoft Visio for process and instrumentation (P&I) diagram AutoCAD software for mechanical engineering drawings. After performing hydraulic leak tests, the prototype was tested using blackstrap molasses 80 o brix which was prepared for fermentation using ilution and inoculums formulations developed in Microsoft Excel for water dilution, yeastand nutrients like (NH 4 ) 2 SO 4, KH 2 PO 4, MgCl 2. A batch mash boiling test conducted on the column showed that the response of tray temperatures exhibited first-order delay behavior with an average lag of 17 minutes and a delay of 50 -65 minutes depending on tray distance from the reboiler. Due to lack of feedback control equipment specifically on-linecomposition analyzers and suitable actuators, continuous control of ethanol composition could not be undertaken. It is planned to procure pertinent control hardware during the next phase of the project. However the batch test gave initial ethanol purity of 80% which decreased as the ethanol content in the still was continuously depleted.
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18

Gutiérrez-Oppe, Evelyn Edith, Wilson Miguel Salvagnini, and Maria Elena Santos Taqueda. "Comparison between the design of experiments and simulation in the three-phase distillation in a sieve tray column for glycerine dehydration." Chemical Engineering Research and Design 91, no. 7 (July 2013): 1186–202. http://dx.doi.org/10.1016/j.cherd.2013.01.011.

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19

Justi, Gabriel Henrique, Conrado Planas Zanutto, Gabriela Cantarelli Lopes, and José Antônio Silveira Gonçalves. "SIMULTANEOUS MOMENTUM AND ENERGY TRANSFER ANALYSIS IN A DISTILLATION COLUMN SIEVE TRAY USING CFD TECHNIQUES: STUDY OF INFLUENCE OF THE INLET DOWNCOMER." Enciclopédia Biosfera 13, no. 23 (June 24, 2016): 1668–83. http://dx.doi.org/10.18677/enciclopedia_biosfera_2016_150.

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20

Salem, Abu Bakr S. H. "Efficiency of Distillation Columns Containing Packed Sieve Trays." Separation Science and Technology 28, no. 13-14 (October 1993): 2255–72. http://dx.doi.org/10.1080/01496399308016748.

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21

Xu, Z. P., A. Afacan, and K. T. Chuang. "Prediction of Packed Sieve Tray Efficiency in Distillation." Chemical Engineering Research and Design 74, no. 8 (November 1996): 893–900. http://dx.doi.org/10.1205/026387696523193.

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22

Vennavelli, Anand N., James R. Whiteley, and Michael R. Resetarits. "New Fraction Jetting Model for Distillation Sieve Tray Efficiency Prediction." Industrial & Engineering Chemistry Research 51, no. 35 (August 24, 2012): 11458–62. http://dx.doi.org/10.1021/ie202997t.

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23

Chen, G. X., A. Afacan, C. Xu, and K. T. Chuang. "Performance of combined mesh packing and sieve tray in distillation." Canadian Journal of Chemical Engineering 68, no. 3 (June 1990): 382–86. http://dx.doi.org/10.1002/cjce.5450680305.

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24

Proctor, Sebastian J., Michael W. Biddulph, and Krish R. Krishnamurthy. "Effect of Liquid Channeling on a 1.8-m Distillation Sieve Tray." Industrial & Engineering Chemistry Research 37, no. 6 (June 1998): 2535–40. http://dx.doi.org/10.1021/ie970587z.

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25

Rocha, J. Antonio, J. Carlos Cardenas, Cesar Sosa, and Jorge Rosales. "Preliminary design of sieve tray extraction columns. 1. Determination of the column diameter. Flooding velocities in sieve tray extractors." Industrial & Engineering Chemistry Research 28, no. 12 (December 1989): 1873–78. http://dx.doi.org/10.1021/ie00096a020.

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26

Rocha, J. Antonio, J. Carlos Cardenas, and J. Antonio Garcia. "Preliminary design of sieve tray extraction columns. 2. Determination of the column height. Overall efficiency of sieve tray extractors." Industrial & Engineering Chemistry Research 28, no. 12 (December 1989): 1879–83. http://dx.doi.org/10.1021/ie00096a021.

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27

Singh, Amit Kumar, Barjeev Tyagi, and Vishal Kumar. "First Principle Modeling and Neural Network–Based Empirical Modeling with Experimental Validation of Binary Distillation Column." Chemical Product and Process Modeling 8, no. 1 (September 4, 2013): 53–70. http://dx.doi.org/10.1515/cppm-2013-0011.

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Abstract To get the better product quality and to decrease the energy consumption of the distillation column, an accurate and suitable nonlinear model is crucial important. In this work, two types of model have been developed for an existing experimental setup of continuous binary distillation column (BDC). First model is a theoretical tray-to-tray binary distillation model for describing the steady-state behavior of composition in response to changes in reflux flows and in reboiler duty. Another model is an artificial neural network (ANN)–based input/output data relationship model. In ANN-based model, temperature of first tray, feed flow rate, and column pressures have been taken in addition to reflux flow rate and reboiler heat duty as inputs to give the more accurate I/O relationship. The comparison of output of ANN model and the equation-based model with the real-time output of the experimental setup of BDC has been given for the validation of developed models.
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28

Zarei, Taleb, Reza Hamidi Jahromi, and Arash Mohammadi Karachi. "Experimental and computational fluid dynamics modeling of a novel tray humidifier column in humidification dehumidification desalination; evaluation of hydrodynamic and heat transfer characteristics." Proceedings of the Institution of Mechanical Engineers, Part E: Journal of Process Mechanical Engineering 234, no. 3 (April 8, 2020): 275–84. http://dx.doi.org/10.1177/0954408920916580.

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In this article, a novel tray humidifier column for humidification dehumidification desalination was proposed. The performance of the humidifier column has been investigated with experimental and computational fluid dynamics simulations. The hydrodynamics and heat transfer characteristics of this tray humidifier has been studied. A stainless steel sieve tray with a rectangular cross section with a dimension of 20 × 50 cm was used in the experimental study. In computational fluid dynamics modeling, a transient three-dimensional model has been developed based on the volume of fluid framework by using standard k-epsilon model. The effect of air and seawater flow rate and inlet seawater temperature on the exit air temperature has been investigated. The results show that the humidifier effectiveness of the tray humidifier column varies between 0.67 and 0.87 depending on operating conditions. Then, tray column can be used in humidification dehumidification desalination systems with advantages such as compact equipment, low-pressure drop, and handling solids or other sources of fouling.
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29

Sun, Lan Yi, Ru Jun Wang, Cheng Zhai, and Qing Song Li. "Hydrodynamic and Mass Transfer Performance of Bilayer Fixed Valve Tray." Advanced Materials Research 225-226 (April 2011): 107–10. http://dx.doi.org/10.4028/www.scientific.net/amr.225-226.107.

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Fixed valve trays have the advantages of low pressure drop, high efficiency, anti-fouling, simple structure, low manufacture cost and long runtime and therefore have been widely used abroad. This paper presents a new bilayer fixed valve (BFV) tray which has some improvements on traditional fixed valve trays. The hydrodynamic and mass transfer performance of BFV tray, sieve tray and F1 valve tray was experimentally studied with air-water-oxygen system in a 1.2m column. The results showed that the BFV tray possesses low pressure drop, high capacity, wide operating range and high efficiency.
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30

Ran, Wang, Tao Jinliang, Ling Yanli, Wei Feng, and Liu Jidong. "Total spray tray (TST) for distillation columns: A new generation tray with lower pressure drop." Chemical Industry and Chemical Engineering Quarterly 23, no. 4 (2017): 523–27. http://dx.doi.org/10.2298/ciceq160829005r.

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As a critical gas-liquid contact component, trays play an important role in the performance of distillation column. In this paper, the hydrodynamics of a new type of tray, the total spray tray (TST), were investigated. Taking air-water as the working medium, the pressure drop with different F0 was tested under atmospheric pressure. The results indicate that there is no flooding with the tray and thus the wider operation flexibility can be provided by TST. Furthermore, the pressure drop of TST is much lower than that of other trays. The above properties of TST would benefit the production expansion and energy decreasing in distillation operation greatly.
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31

HATORI, Shoichi, and Toshio MIYAUCHI. "Numerical Simulation of Flows in a Tray-Type Distillation Column." Transactions of the Japan Society of Mechanical Engineers Series B 58, no. 546 (1992): 463–70. http://dx.doi.org/10.1299/kikaib.58.463.

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32

Li, Jun, Lan Yi Sun, Zhan Hua Ma, Sha Xue, and Yang Dong Hu. "Hydrodynamic and Mass Transfer Performance of Enhanced Jet Tray." Advanced Materials Research 219-220 (March 2011): 697–700. http://dx.doi.org/10.4028/www.scientific.net/amr.219-220.697.

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In order to satisfy the revamping of refinery and chemical equipments, a new kind of tray, enhanced jet tray (EJT), was presented. The hydrodynamic and mass transfer performances of EJT and new vertical sieve tray (New VST) were investigated with air-water-oxygen system in a stainless steel column of 1200mm internal diameter. Correlations of hydrodynamic parameters such as pressure drop, weeping and entrainment of EJT were obtained. The experimental results show that EJT has lower pressure drop, fractional weeping, entrainment and higher efficiency compared with New VST because of its special geometry characteristics.
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33

Noriler, D., H. F. Meier, A. A. C. Barros, and M. R. Wolf Maciel. "Thermal fluid dynamics analysis of gas–liquid flow on a distillation sieve tray." Chemical Engineering Journal 136, no. 2-3 (March 2008): 133–43. http://dx.doi.org/10.1016/j.cej.2007.03.023.

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34

Biddulph, Michael W., and Christopher P. Thomas. "Effect of liquid surface tension on small hole distillation sieve tray pressure drop." AIChE Journal 41, no. 4 (April 1995): 819–27. http://dx.doi.org/10.1002/aic.690410409.

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35

Nobrega, M. B. M. M., A. S. Zimmermann, S. Mattedi, and O. Chiavone-Filho. "OPTIMIZATION OF A PETROLEUM FRACTIONAL DISTILLATION COLUMN USING DISTOP CALIBRATION AND STATISTICAL METHODS." Brazilian Journal of Petroleum and Gas 14, no. 04 (January 7, 2021): 221–37. http://dx.doi.org/10.5419/bjpg2020-0017.

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Distillation columns are important separation equipment that comprise most of the investment needed in a petroleum refining plant. Utilities and energy demands, though, are a concerning factor in the current economic and environmental scenario. The present work proposes a methodology to optimize the energy consumption of a crude oil distillation column using the Distop Calibration technique that allows faster convergence than the Tray-to-Tray method. The methodology presented involves process simulation, sensitivity analysis, factorial design, and the use of response surface methodology. Results show that it is possible to achieve significant gains by changing feed temperature and rectifying vapor flow, causing a relevant reduction in energy consumption. Hence, the methodology can be used as an optimization tool to increase energetic efficiency.
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36

Gnatyuk, Aleksey, and Mikhail Dunaev. "Structural model of binary mixture fractional distillation in a tray column." Proceedings of Irkutsk State Technical University 23, no. 6 (December 2019): 1203–11. http://dx.doi.org/10.21285/1814-3520-2019-6-1203-1211.

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37

Sudibyo, Sudibyo, Muhamad Nazri Murat, and Norashid Aziz. "Neural Wiener Based Model Predictive Control (NWMPC) for MTBE Catalytic Distillation Using Reduced Sequential Quadratic Programming (RSQP)." Advanced Materials Research 1113 (July 2015): 733–38. http://dx.doi.org/10.4028/www.scientific.net/amr.1113.733.

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Reactive distillation is a process that combines both reactor and distillation column in one unit process. The reactive distillation is normally applied in MTBE production in order to achieve high reaction conversion and purity of the MTBE. Controlling such reactive distillation is a challenging task due to its highly nonlinear behavior and the existence of strong interactions among control variables. In this work, a Neural Wiener based model predictive control (NWMPC) is designed and implemented to control the tray temperature of MTBE reactive distillation. The Reduced SQP (RSQP) has been embedded as an optimizer in the NWMPC proposed. The MTBE reactive distillation has been modeled using aspen dynamic and the control study has been simulated using Simulink (Matlab) which is integrated with Aspen dynamic model. The results achieved show that the NWMPC is able to maintain tray temperatures at desired set points, able to reject the disturbance and robust toward robustness test conducted.
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38

Malvin, Aldo, Andy Chan, and Phei Li Lau. "CFD study of distillation sieve tray flow regimes using the droplet size distribution technique." Journal of the Taiwan Institute of Chemical Engineers 45, no. 4 (July 2014): 1354–68. http://dx.doi.org/10.1016/j.jtice.2014.01.002.

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39

Garcia, J. Antonio, and James R. Fair. "A Fundamental Model for the Prediction of Distillation Sieve Tray Efficiency. 1. Database Development." Industrial & Engineering Chemistry Research 39, no. 6 (June 2000): 1809–17. http://dx.doi.org/10.1021/ie990875q.

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40

Uys, Ehbenezer C., Andries J. Burger, Louis J. Du Preez, and Johannes H. Knoetze. "The influence of gas physical properties on entrainment inside a sieve tray column." Chemical Engineering Research and Design 104 (December 2015): 429–39. http://dx.doi.org/10.1016/j.cherd.2015.08.031.

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41

Uys, Ehbenezer C., Andries J. Burger, Louis J. Du Preez, and Johannes H. Knoetze. "The influence of liquid physical properties on entrainment inside a sieve tray column." Chemical Engineering Research and Design 117 (January 2017): 205–17. http://dx.doi.org/10.1016/j.cherd.2016.10.027.

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42

Springer, P. A. M., R. Baur, and R. Krishna. "Composition Trajectories for Heterogeneous Azeotropic Distillation in a Bubble-Cap Tray Column." Chemical Engineering Research and Design 81, no. 4 (April 2003): 413–26. http://dx.doi.org/10.1205/026387603765173682.

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43

Røsjorde, A., and S. Kjelstrup. "The second law optimal state of a diabatic binary tray distillation column." Chemical Engineering Science 60, no. 5 (March 2005): 1199–210. http://dx.doi.org/10.1016/j.ces.2004.09.059.

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44

Hawaidi, Ebrahim Ali Mohamed, Mustafa T. Yagub, and Riyad Ageli Saleh. "ACETONE RECOVERY USING BATCH DISTILLATION." Scientific Journal of Applied Sciences of Sabratha University 2, no. 2 (September 27, 2019): 82–98. http://dx.doi.org/10.47891/sabujas.v2i2.82-98.

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This study focuses on determining the feasibility of obtaining maximum mole percentage of acetone (99 mole%) in the distillate stream from a 3 mole% acetone waste stream using batch distillation. The device which is used in this work has eight trays that will act as the stages of the batch distillation. The effects of varying reflux ratio and heat load (power) on acetone concentration were studied. Moreover, the operating conditions for the bath distillation column such as flooding and weeping with the extreme limits of operation were considered. The temperatures were also be recorded at each tray. The McCabe-Thiele method was used to determine the theoretical number of trays and compared with actual trays (column efficiency). For a chemical analysis of acetone/water compositions a refractometer was used for a chemical analysis, known acetone/water concentrations were analysed and used to construct a calibration curve. The results obtained showed that, the acetone concentration increases with increasing reflux ratio until a highest concentration was reached. Then, the concentration gradually decreases with increasing reflux ratio. However, the distillate stream with 99 mole % acetone was achieved at a reflux ratio of R=3 and at both powers 0.5 kw and 0.7 kw. Finally, the highest overall column efficiency reached by this work was about 75%.
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45

Tang, Meng, Shaofeng Zhang, Dewu Wang, Yan Liu, Yishuo Zhang, Hongkai Wang, and Kun Yang. "Hydrodynamics of the tridimensional rotational flow sieve tray in a countercurrent gas-liquid column." Chemical Engineering and Processing - Process Intensification 142 (August 2019): 107568. http://dx.doi.org/10.1016/j.cep.2019.107568.

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46

Attarakih, Menwer, Mazen Abu-Khader, and Hans-Jörg Bart. "Dynamic analysis and control of sieve tray gas absorption column using MATALB and SIMULINK." Applied Soft Computing 13, no. 2 (February 2013): 1152–69. http://dx.doi.org/10.1016/j.asoc.2012.10.011.

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47

Spasojevic, Momcilo, Milovan Jankovic, and Damir Djakovic. "Entropy production minimization in a multicomponent diabatic distillation column." Thermal Science 24, no. 3 Part B (2020): 2256–66. http://dx.doi.org/10.2298/tsci181206284s.

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This work presents a procedure for direct numerical minimization of entropy production in a diabatic tray column with heat exchanged on the trays as control variables, as opposed to previously used procedures with temperature on the trays as control variables. The procedure, which had previously been demonstrated on a binary mixture, was in this work applied to a multicomponent mixture, with minor modifications. The procedure comprised the complex optimization method and the Ishii-Otto method for solving the equations of a column model based on the iterative Newton-Raphson technique with partial linearization of the equations. The desired separation of the components was realized by the addition of a penalty function to the goal function, i.e. entropy production in the column. The required thermodynamic characteristics were calculated by the Soave equation of state. As an illustration, an industrial debutanizer with five components was used whose data, obtained by simulation, were compared with the optimization results of a diabatic column with the same desired separation and number of trays. After the diabatic column optimization procedure, the value of 91.91 J/Ks was obtained as the best result for entropy production. According to the best solution, entropy production in the diabatic column was 23.2% lower than in the adiabatic column. The heat to be removed from the column increased by 24.7%, while the heat to be added to the column increased by 28.8%.
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48

Sun, Dahai, Hui Tian, J. Sun, and W. Xu. "Reactive Distillation for the Production of Cyclohexanol." Chemical & biochemical engineering quarterly 34, no. 4 (2021): 223–32. http://dx.doi.org/10.15255/cabeq.2020.1863.

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Cyclohexanol is an organic chemical intermediate product widely used in chemical<br /> industry and commonly produced by cyclohexene hydration. Because of the low mutual<br /> solubility of cyclohexene and water, the reaction is limited by chemical equilibrium,<br /> which has the disadvantage of low conversion of cyclohexene. In this paper, the hydration reaction of cyclohexene catalysed by A-36 cation exchange resin catalyst was analysed by Aspen Plus V8.6 simulation software in the presence of isophorone as cosolvent.<br /> The process model of synthesising cyclohexanol by catalytic distillation was verified by<br /> process experiments. The simulation experiments were carried out using the process<br /> model, and suitable operating conditions of the catalytic distillation column were obtained. These are: ketene feed ratio 1.5, alkene/water ratio 0.5, distillation stage trays 5,<br /> reaction stage trays 12, stripping stage trays 6, cyclohexene feed at the 18th tray, water<br /> and isophorone feed at the 5th tray, reflux ratio 3, feed ratio (D/F) 0.25. Under these<br /> operating conditions, the conversion of cyclohexene can reach 40.63 %.
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Marangoni, Cintia, Geysa N. Mello, Ariovaldo Bolzan, and Ricardo A. F. Machado. "Dynamic Study of Distillation Column Operated with Tray Heat Source Combined with Reboiler." Chemical Engineering Communications 203, no. 3 (February 11, 2015): 364–71. http://dx.doi.org/10.1080/00986445.2014.1001888.

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50

Li, Hongshen, and Shizhong Li. "Optimization of Continuous Solid-State Distillation Process for Cost-Effective Bioethanol Production." Energies 13, no. 4 (February 15, 2020): 854. http://dx.doi.org/10.3390/en13040854.

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To improve the efficiency of bioethanol production, an advanced process was required to extract ethanol from solid-state fermented feedstock. With regard to the characteristics of no fluidity of solid biomass, a continuous solid-state distillation (CSSD) column was designed with a proprietary rotary baffle structure and discharging system. To optimize the operation condition, fermented sweet sorghum bagasse was prepared as feedstock for a batch distillation experiment. The whole distillation time was divided into heating and extracting period which was influenced by loading height and steam flow rate simultaneously. A total of 16 experiments at four loading height and four steam flow rate levels were conducted, respectively. Referring to packing, rectifying column, mass, and heat transfer models of the solid-state distillation heating process were established on the basis of analyzing the size distribution of sweet sorghum bagasse. The specific heat capacity and thermal conductivity value of fermented sweet sorghum bagasse were tested and served to calculate the ethanol yielding point and concentration distribution in the packing. The extracting process is described as the ethanol desorption from porous media absorbent and the pseudo-first-order desorption dynamic model was verified by an experiment. Benefit (profit/time) was applied as objective function and solved by successive quadratic programming. The optimal solution of 398 mm loading height and 8.47 m3/h steam flow rate were obtained to guide a 4 m in diameter column design. One heating and two extracting trays with 400 mm effective height were stacked up in an industrial CSSD column. The steam mass flow rate of 0.5 t/h was determined in each tray and further optimized to half the amount on the third tray based on desorption equation.
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