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Journal articles on the topic 'Silan'

Author: Grafiati

Published: 4 June 2021

Last updated: 12 February 2022

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1

Savitri, Savitri, Evi Triwulandari, Agus Haryono, and O. A. Syahputra. "PENGARUH SENYAWA SILAN TERHADAP SIFAT MEKANIK MATERIAL PELAPIS PADUAN HIBRID EPOKSI TERMODIFIKASI POLIURETAN." Jurnal Kimia Terapan Indonesia 17, no. 1 (December 10, 2015): 15–26. http://dx.doi.org/10.14203/jkti.v17i1.19.

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Preparation of hybrid coating material from modified epoxy polyurethane (ETP) and silan (Si) has been done. Epoxy and polyurethane were modified with silan using γ-Glisidoksil propil trimetoksisilan (GPTMS) and γ-aminopropyl triethoxysilane (γ-APS) and also dibutyltindilaurate (DBTL) as catalyst. Fourier Transform Infrared (FTIR) characterization indicated that the hybrid coating material has been formed. The results of the analysis of NCO percent and conversion rate of isocyanates (α) also verified that the ETP-Si hybrid coatings have been formed. The addition 30% of silane as Si-O group indicated the rest of NCO percent was the lowest for hybrid coating material with polyurethane concentration of 5% and 10. The composition of ETP5% - Si 30% was the optimum composition from the ETP-Si hybrid coating material based on the mechanical analysis.Key words: hybrid coating, polyurethane, epoxy, silane, ETP – Si

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2

Schenzel, Karla, Karl Hassler, and Günther Bauer. "Schwingungsspektren und Normalkoordinatenanalysen sterisch überladener Silane: Tetrakis(trimethylsilyl)silan und Hexakis(trimethylsilyl)disilan." Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 53, no. 14 (December 1997): 2435–43. http://dx.doi.org/10.1016/s1386-1425(97)00225-4.

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3

Haase, Martin, and Uwe Klingebiel. "Tris(silyl)silyl-chlorsilane und P-halogenierte Silylphosphane / Tris(silyl)silyl-chlorosilanes and P-Halogenated Silylphosphanes." Zeitschrift für Naturforschung B 41, no. 6 (June 1, 1986): 697–701. http://dx.doi.org/10.1515/znb-1986-0606.

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Lithium-tris(trimethylsilyl)silan reacts with chlorosilanes to give thermally stable compounds (1−3). The chlorination of 3 leads to the formation of the silane (Me3Si)3SiSi(Cl)(CMe3)2 4. The reaction of tetramethylpiperidinodihalogenophosphanes with (Me3Si)3SiSi(Cl)(Cme3)2 results in thermally stable compounds (Me3Si)3Si−P(Hal)N(CMe2)2(CH2)3, Hal = F (5). Cl (6), (Me3Si)3Si−P(Cl)N(CHMe2)2 (7) undergoes thermaly rearrangement via a silicon-chlorine exchange reaction to give (Me3Si)2Si(Cl)−P(SiMe3)N(CHMe2)2 (8). A byproduct − besides cyclic phosphanes - is the silylamine (Me3Si)2Si(Cl)N(CHMe2) (9). The formation of (9) can be explained via the elimination of the phosphinidene Me3SiP.

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4

Jansen, M., S. Rings, and H. P. Baldus. "Darstellung und Kristallstruktur von Tetrakis(pentafluorphenylamino)silan." Zeitschrift f�r anorganische und allgemeine Chemie 610, no. 4 (April 1992): 99–102. http://dx.doi.org/10.1002/zaac.19926100116.

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5

Özkütük, Ebru Birlik, Sibel Emir Diltemiz, Elif Özalp, Arzu Ersöz, and Rıdvan Say. "Silan based paraoxon memories onto QCM electrodes." Journal of Industrial and Engineering Chemistry 19, no. 6 (November 2013): 1788–92. http://dx.doi.org/10.1016/j.jiec.2013.02.021.

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6

Nyman, B. "Schutzbehandlung von Beton mit Silan- und Siloxanpräparaten / Protective Treatment of Concrete with Silane or Siloxane." Restoration of Buildings and Monuments 5, no. 3 (June 1, 1999): 307–10. http://dx.doi.org/10.1515/rbm-1999-5377.

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Abstract By means of laboratory experiments it is shown that the penetration depth of a treatment of concrete with Silane depends strongly on the duration of suction and on the moisture content of the concrete. The necessary duration of suction can be estimated for any required penetration depth.

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7

Czarnecki, L., and B. Chmielewska. "Bruchverhalten und Fraktographie eines Silan modifizierten Kunstharzmörtels / Fracture and Fractography of Silane Modified Resin Mortars." Restoration of Buildings and Monuments 9, no. 6 (December 1, 2003): 603–18. http://dx.doi.org/10.1515/rbm-2003-5806.

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8

Maskey, Rezisha, Marcel Schädler, Claudia Legler, and Lutz Greb. "Bis(perchlorocatecholato)silan - eine neutrale Silicium-Lewis-Supersäure." Angewandte Chemie 130, no. 6 (January 12, 2018): 1733–36. http://dx.doi.org/10.1002/ange.201712155.

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9

Omar, Mohamad Firdaus, NURIAH MOHAMAD, and Fathilah Ali. "PREPARATION AND CHARACTERIZATIONS OF LATEX/FILLER NANOCOMPOSITES." IIUM Engineering Journal 21, no. 2 (July 4, 2020): 230–38. http://dx.doi.org/10.31436/iiumej.v21i2.1388.

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Latex compounding which incorporates various types of clays as filler to the rubber can significantly give reinforcement in the rubber matrix when rubber/clay nanocomposites are formed, but the filler agglomerates. Thus, study was conducted by using Kaolin clay as the filler in the rubber nanocomposites with silane coupling agent to functionalize the surface of the filler. This study was done in order to investigate the mechanical properties of various functionalized Kaolin in latex nanocomposites, to prepare various ratios of Kaolin to rubber, and to characterize mechanical, thermal and morphological properties of the Kaolin in latex nanocomposites. To achieve these, six types of silane coupling agents was used for Kaolin filler surface functionalization purpose during the filler’s incorporation in latex compounding. The optimized coupling agent, USi-7301 (?-chloropropyltrimetoxysilane) – with tensile strength value of 32.77 MPa, elongation at break value of 632.589 % and force at break value of 6.737 N – was used to further functionalize Kaolin filler in different ratios so as to achieve the optimum mechanical, thermal and morphological properties of the filler in the polymer matrix. Universal tensile machine was used to analyze the mechanical properties of the nanocomposites, while the Scanning Electron Microscopy (SEM) and Differential Scanning Calorimetry (DSC) were used to observe the morphological and thermal properties of the nanocomposites, respectively. The results showed that reducing the Total Solids Content (TSC) of Kaolin filler to 26 % somehow showed the optimized properties of the nanocomposites, giving 34.00 MPa tensile strength, 576.494 % elongation at break and 6.564 N force at break. Rough surface morphology was observed under SEM suggesting the occurrence of phase separation between the hydrophilic filler and the hydrophobic rubber matrix. In the DSC plot, sample with USi-7301 and with functionalized Kaolin filler 26 % TSC showed glass transition temperature shifted to lower region compared to normal nitrile rubber. The reinforcement of nanocomposites formed will not only enhance the properties of the nanocomposites, but is also economically feasible thus brings advantages to the industry. ABSTRAK: Penyebatian lateks yang menggabungkan pelbagai jenis tanah liat sebagai pengisi dalam getah dapat memberi pengukuhan dalam matriks getah dengan ketara apabila nanokomposit getah / tanah liat terbentuk, tetapi pengisi mengagregat. Oleh itu, kajian dijalankan dengan menggunakan tanah liat Kaolin sebagai pengisi dalam nanokomposit getah dengan ejen gandingan silan untuk menambah-fungsi permukaan pengisi tersebut. Kajian ini dilakukan untuk mengenalpasti sifat mekanik pelbagai Kaolin (yang berfungsi) dalam nanokomposit lateks, untuk menyediakan pelbagai nisbah Kaolin terhadap getah, dan untuk mencirikan sifat mekanik, haba dan morfologi Kaolin dalam nanokomposit lateks. Untuk mencapainya, enam jenis ejen gandingan silan digunakan untuk tujuan menambah-fungsi permukaan pengisi Kaolin semasa penggabungan pengisi dalam penyebatian lateks. Ejen gandingan silan yang paling optimum, USi-7301 (?-silan kloropropiltrimetoksi) - dengan nilai kekuatan tegangan 32.77 MPa, nilai pemanjangan ketika pemutusan 632.589% dan kekuatan daya ketika pemutusan 6.737 N - digunakan dengan lebih lanjut untuk menambah-fungsi pengisi Kaolin dalam nisbah yang berbeza untuk lebih mencapai sifat mekanikal, haba dan morfologi optimum pengisi dalam matriks polimer lateks. Mesin tegangan universal digunakan untuk menganalisis sifat mekanik nanokomposit, sementara Mikroskopi Elektron Pengimbasan (SEM) dan Kalorimetri Pengimbasan Berbeza (DSC) digunakan untuk menganalisa sifat morfologi dan haba nanokomposit tersebut. Hasil kajian menunjukkan bahawa pengurangan Jumlah Kandungan Pepejal (TSC) pengisi Kaolin kepada 26% menunjukkan sifat optimum nanokomposit, dengan kekuatan tegangan 34.00 MPa, pemanjangan ketika pemutusan sebanyak 576.494% dan daya ketika pemutusan sebanyak 6.564 N. Morfologi permukaan kasar diperhatikan di bawah SEM dan ia menunjukkan berlakunya pemisahan fasa antara pengisi hidrofilik dan matriks getah hidrofobik. Dalam plot DSC, sampel dengan USi-7301 dan dengan pengisi Kaolin yang difungsikan dengan 26% TSC menunjukkan suhu peralihan kaca beralih ke kawasan yang lebih rendah berbanding getah nitril biasa. Pengukuhan nanokomposit yang terbentuk bukan sahaja akan meningkatkan sifat nanokomposit, tetapi juga dapat dilaksanakan secara ekonomi sehingga memberi banyak kelebihan kepada industri.

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10

Kühne, Heinz. "Reaktionskontrollierte chemische Gasphasenabscheidung von Silicium durch Pyrolyse von Silan." Chemie Ingenieur Technik 64, no. 3 (March 1992): 302–3. http://dx.doi.org/10.1002/cite.330640330.

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11

Baki, Mohammed Fazle. "Error Noted in a Paper by Jacobs, Silan, and Clemson." Interfaces 28, no. 2 (April 1998): 121–22. http://dx.doi.org/10.1287/inte.28.2.121.

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12

DrieΒ, Matthias, Hans Pritzkow, and Michael Reisgys. "Zur Kenntnis neuer 1,3,2,4-Diphosphadisiletan- und Diorganodi(phosphino)silan-Derivate." Chemische Berichte 124, no. 9 (September 1991): 1931–39. http://dx.doi.org/10.1002/cber.19911240908.

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13

Schroth, Werner, and Ullrich Jahn. "Erzeugung vonN,N-disubstituierten Iminiumsalzen mit Hilfe von Silan-Reagenzien." Journal f�r Praktische Chemie/Chemiker-Zeitung 340, no. 4 (1998): 287–99. http://dx.doi.org/10.1002/prac.19983400402.

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14

Cornils, Boy. "Buchbesprechung: Benzin aus Sand. Die Silan-Revolution. Von Peter Plichta." Angewandte Chemie 114, no. 8 (April 15, 2002): 1503. http://dx.doi.org/10.1002/1521-3757(20020415)114:8<1503::aid-ange1503>3.0.co;2-0.

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15

EVCİN, Atilla, Harun GÜNEY, and Nalan BEZİR. "Sol-gel Preparation of Silan based Zirconia Hybrid Thin Film." International Journal of Computational and Experimental Science and Engineering 7, no. 1 (March 31, 2021): 9–12. http://dx.doi.org/10.22399/ijcesen.727304.

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16

Gui-hong, Zhu, F. H. Wittmann, and Zhao Tie-jun. "Surface Impregnation of Chloride-contaminated and Humid Concrete with Silane / Oberflächenimprägnierung von Chlorid belastetem und feuchtem Beton mit Silan." Restoration of Buildings and Monuments 14, no. 1 (February 1, 2008): 3–14. http://dx.doi.org/10.1515/rbm-2008-6189.

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17

Buijink, Jan-Karel, Mathias Noltemeyer, and Frank T. Edelmann. "Synthese und Struktur von Difluor-bis[2,4,6-tris(trifluormethyl)phenyl]silan." Journal of Fluorine Chemistry 61, no. 1-2 (March 1993): 51–56. http://dx.doi.org/10.1016/s0022-1139(00)80416-9.

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18

Wiberg, Nils, Gerhard Preiner, Petros Karampatses, Chung-Kyun Kim, and Klaus Schurz. "Reaktivität von Silan- und Germaniminen Me2ENR (ESi, Ge)1)." Chemische Berichte 120, no. 8 (August 1987): 1357–68. http://dx.doi.org/10.1002/cber.19871200814.

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19

Hesse, Michael, and Uwe Klingebiel. "Diisopropyl-(2,4,6-tri-tert-butylphenylimino)silan – ein sehr stabiles, freies Silaimin." Angewandte Chemie 98, no. 7 (July 1986): 638–39. http://dx.doi.org/10.1002/ange.19860980713.

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20

Wiedemann, Jürgen, Thomas Heiner, Gregorz Mloston, G. K. Surya Prakash, and George A Olah. "Direkte Synthese von Trifluormethylketonen aus Carbonsäureestern: Trifluormethylierung mit Trimethyl(trifluormethyl)silan." Angewandte Chemie 110, no. 6 (March 16, 1998): 880–81. http://dx.doi.org/10.1002/(sici)1521-3757(19980316)110:6<880::aid-ange880>3.0.co;2-0.

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21

İstek, Abdullah, Hasan TUNÇ, and ismail ÖZLÜSOYLU. "Silan İlavesinin Yönlendirilmiş Yonga Levhaların (OSB) Bazı Fiziksel Ve Mekanik Özelliklerine Etkisi." Bartın Orman Fakültesi Dergisi 18, no. 2 (December 15, 2016): 1. http://dx.doi.org/10.24011/barofd.237949.

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22

Ramisch, E., A. Mutzke, R. Schneider, and U. Stroth. "Mechanisms of layer growth in microwave-PECVD silan plasmas – Experiment and simulation." Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms 316 (December 2013): 249–56. http://dx.doi.org/10.1016/j.nimb.2013.09.013.

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23

Mickoleit, Martin, Kathleen Schmohl, Rhett Kempe, and Hartmut Oehme. "Reaktion von Dichlormethyltris(trimethylsilyl)silan mit Organolithiumreagentien: Synthese eines intramolekular donorstabilisierten Silens." Angewandte Chemie 112, no. 9 (May 2, 2000): 1679–81. http://dx.doi.org/10.1002/(sici)1521-3757(20000502)112:9<1679::aid-ange1679>3.0.co;2-q.

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24

Hermannsdorfer, André, and Matthias Driess. "Siliciumtetrakis(trifluormethansulfonat): Ein einfaches, neutrales Silan als weiche und harte Lewis‐Supersäure." Angewandte Chemie 133, no. 24 (May 2, 2021): 13769–73. http://dx.doi.org/10.1002/ange.202103414.

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25

Schmidbaur, Hubert, and Jan Ebenhöch. "Synthese und Eigenschaften einiger Silylethinylsilane; Molekülstruktur von Tetrakis(trimethylsilylethinyl)silan / Synthesis and Properties of Some Silylethynylsilane; Molecular Structure of Tetrakis(trimethylsilylethynyl)silane." Zeitschrift für Naturforschung B 43, no. 1 (January 1, 1988): 49–52. http://dx.doi.org/10.1515/znb-1988-0109.

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Abstract Trimethylsilylethine (1) has been prepared from C2H2, sodium and Me3SiCl in anisole. The product can be converted into a Grignard reagent Me3SiC≡CMgCl using iPrMgCl. This reagent yields the compounds Me3SiC≡CSiH3, (Me3SiC≡C)2SiH2, (Me3SiC≡C)3SiH, and (Me3SiC≡C)4Si (2-5) when treated with equivalent amounts of H3SiBr, H2SiBr2, HSiCl3, or SiCl4. respectively. The new silanes have been characterized by NMR data. The crystal structure of (Me3SiC≡C)4Si has been determined by single crystal X-ray diffraction. It shows the expected tetrahedral geometry at he central silicon atom with four linear SiC≡CSi linkages.

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26

Meier, S. J., and M. F. Bäuml. "Massenhydrophobierung von Beton mit Silan / Internal Impregnation of Concrete by Means of Silanes." Restoration of Buildings and Monuments 12, no. 1 (February 1, 2006): 43–52. http://dx.doi.org/10.1515/rbm-2006-6022.

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27

Tropin, D. A., and E. S. Bochenkov. "Influence of inert particles on the ignition processes of hydrogen-silan-air mixtures." International Journal of Hydrogen Energy 45, no. 35 (July 2020): 17953–60. http://dx.doi.org/10.1016/j.ijhydene.2020.04.220.

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28

Mohamed, Amina L., Mehrez E. El-Naggar, Th I. Shaheen, and Ahmed G. Hassabo. "Laminating of chemically modified silan based nanosols for advanced functionalization of cotton textiles." International Journal of Biological Macromolecules 95 (February 2017): 429–37. http://dx.doi.org/10.1016/j.ijbiomac.2016.10.082.

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29

Qi, Long Fei, Zhi Hua Ning, and Le Nian He. "A Design of Powered Device Interface Chip under PoE System." Applied Mechanics and Materials 716-717 (December 2014): 1277–82. http://dx.doi.org/10.4028/www.scientific.net/amm.716-717.1277.

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This paper proposes a design of powered device interface chip compatible with communication protocol IEEE 802.at standard, for Ethernet control of power supply. This design has all the features IEEE 802.at standard requires, including the detection, classification, under-voltage lockout and inrush current control, support of not less than 25.5W of power. The circuit of the chip is designed with Hangzhou Silan BCD process technique. Specific features of the design are 140mA inrush-current-limiting, complementary-output-enable-signal, under-voltage, overvoltage, over temperature protection, an optional external power adapter input, IEEE 802.3at type2 display signals by new electrical equipment, as well as two-event classification logic implementation.

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30

HINO, Makoto, Minoru HIRAMATSU, Koji MURAKAMI, Keiko CHEN, Masao TAKAMIZAWA, and Teruto KANADANI. "Zn-Ni-SiO2 Composite Coating from Sulfate Solution and Application of Silan Coupling Treatment." Journal of The Surface Finishing Society of Japan 55, no. 6 (2004): 434–38. http://dx.doi.org/10.4139/sfj.55.434.

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31

Kartal, İlyas, and Mustafa Çakır. "Floro Silan İçerikli Hibrid Kaplama ile Kaplanmış Alüminyum Levhaların Aşınma ve Termal Özelliklerinin İncelenmesi." Marmara University 1, no. 2 (January 1, 2020): 1–6. http://dx.doi.org/10.35333/porta.2019.96.

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32

Wiberg, Nils, Petros Karampatses, and Chung-Kyun Kim. "Erzeugung von Silan- und Germaniminen Me2ENR (ESi, Ge) aus Sila- und Germadihydrotriazolen1)." Chemische Berichte 120, no. 7 (July 1987): 1203–12. http://dx.doi.org/10.1002/cber.19871200716.

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33

Weidenbruch, Manfred, Youlin Pan, Karl Peters, and Hans Georg Von Schnering. "Silicium-Verbindungen mit starken intramolekularen sterischen Wechselwirkungen, 391) Ein spirocyclisches Silan aus einem 2,2-Dimesityldisilan." Chemische Berichte 123, no. 4 (April 1990): 795–96. http://dx.doi.org/10.1002/cber.19901230424.

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34

Rakebrandt, H. J., U. Klingebiel, and M. Noltemeyer. "Tetrameres Di(-tert-butylamino)di(-N-lithiummethylamino)silan, (Me3CHN)2Si(NLiMe)2 - Darstellung und Kristallstruktur." Zeitschrift f�r anorganische und allgemeine Chemie 623, no. 1-6 (1997): 288–91. http://dx.doi.org/10.1002/zaac.19976230146.

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35

Ivanova, Yordanka, Yanko Dimitriev, Tsvetelina Gerganova, Raina Bryaskova, Maria Fernandes, and Isabel Miranda Salvado. "Organic-inorganic hybrid materials based on N=C=O functionalised silan modified with titanium and zirconium." Open Chemistry 3, no. 3 (September 1, 2005): 452–69. http://dx.doi.org/10.2478/bf02479275.

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AbstractThis work investigates the influence of the precursor trimethylsilil isocyanate on the sol-gel synthesis of hybrid materials. The obtained Si−O−C−N network is additionally modified by titanium and zirconium alcoxypropoxides in the range of 10 to 30 wt. %. The structure of the obtained hybrid materials before and after pyrolysis up to 1100°C was investigated by methods of XRD, FTIR and 29Si MAS NMR. We established that the hybrid structure was stable up to 600°C based on IR study. The structural transformation of the hybrid materials into oxycarbonitrogen system started at 800°C. The network of the hybrids modified by titanium remained stable and amorphous up to the final temperature of the pyrolysis (1100°C) compared to the gels modified by more than 10 wt.% Zr. It was confirmed by XRD analysis that the last mentioned are nanocomposite materials, built from carbooxynitrogen vitreous matrix and ZrO2-nanocrystals (tetragonal). The NMR method verified the presence of heterometallic bonds (Si−O−Ti and Si−O−Zr) and Q4, ZrQ3 or TiQ3, NSiO3 and D structural units in the gels.

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36

Wiberg, Nils, Petros Karampatses, and Chung-Kyun Kim. "Speicherung von Silan- und Germaniminen Me2ENR (ESi, Ge) in Form von Sila- und Germadihydrotetrazolen1)." Chemische Berichte 120, no. 7 (July 1987): 1213–21. http://dx.doi.org/10.1002/cber.19871200717.

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37

Bauer, Jonathan O., and Carsten Strohmann. "Von einem α-funktionalisierten siliciumstereogenen N,O-Silan zu einem monomeren tetrakoordiniertentBuLi-Addukt mit lithiumzentrierter Chiralität." Angewandte Chemie 126, no. 31 (June 18, 2014): 8306–10. http://dx.doi.org/10.1002/ange.201404255.

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38

Bibber, J. W., C. L. Barnes, D. van der Helm, and Jerry J. Zuckerman. "Kristall- und Molekülstruktur von Bis(1,8-naphthalindioxy)silan - zur Kontroverse über planar tetrakoordiniertes Silicium in Orthokieselsäureestern." Angewandte Chemie 95, no. 6 (January 17, 2006): 498–99. http://dx.doi.org/10.1002/ange.19830950609.

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39

Gaertner, Benjamin, and Hans-Jörg Himmel. "Charakterisierung und Photochemie des Silan-Aluminium-Komplexes Al⋅SiH4und der Photoprodukte HAlSiH3und AlSiH3in einer festen Argonmatrix." Angewandte Chemie 114, no. 9 (May 2, 2002): 1602–6. http://dx.doi.org/10.1002/1521-3757(20020503)114:9<1602::aid-ange1602>3.0.co;2-3.

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40

Wrackmeyer, Bernd, and Klaus Horchler. "Trimethylblei-Lithium in Tetrahydrofuran: Synthese von Trimethyl(trimethylplumbyl)silan und des Trimethylplumbyltrihydridoborat-Anions / Trimethyllead-Lithium in Tetrahydrofuran: Synthesis of Trimethyl(trimethylplumbyl)silane and of the Trimethylplumbyltrihydridoborate Anion." Zeitschrift für Naturforschung B 44, no. 10 (October 1, 1989): 1195–98. http://dx.doi.org/10.1515/znb-1989-1008.

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Solutions of trimethyllead-lithium, [Me3Pb]Li (1), in tetrahydrofuran (THF) (-0.5 M) can be obtained from trimethyllead bromide and an excess of lithium at –78°C. 1H. 13C and 207Pb NMR are used for monitoring the formation of the reagent. Extensive decomposition into lead and tetramethyllead is observed at –20°C within minutes. The application of this reagent is demonstrated by the synthesis of trimethyl(trimethylplumbyl)silane (2) and by its stoichiometric 1:1 reaction with BH3–THF at –78°C, leading to lithium trimethylplumbyltrihydridoborate [Me3PB–BH3]Li (3). The composition of the products in solution follows conclusively from their 1H, 11B13C, 29B, 13C, 29Si, and 207Pb NMR data. The silane 2 decomposes slowly at ambient temperature into Me4Si, Me4Pb and lead. The borate is even less stable, decomposing at temperatures above –30°C mainly into lead, Me4Pb, [H4B]Li and [Me4B]Li.

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41

Schumann, Herbert, Mario Glanz, and Holger Hemling. "Metalloragnische Verbindungen der Lanthanoide, 90[1] [(tert-Butylcyclopentadienyl)dimethyl(tetramethylcyclopentadienyl)silan]-Komplexe von Lanthan, Neodym und Lutetium." Chemische Berichte 127, no. 12 (December 1994): 2363–67. http://dx.doi.org/10.1002/cber.19941271204.

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42

Kosse, P., and E. Popowski. "Untersuchungen zur Umsetzung von [Lithium(trimethylsilyl)amido]-methyl-trimethylsilylamino-silan Me(Me3SiNLi)(Me3SiNH)SiH mit verschiedenen Elektrophilen." Zeitschrift f�r anorganische und allgemeine Chemie 619, no. 3 (March 1993): 613–16. http://dx.doi.org/10.1002/zaac.19936190330.

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43

Tacke, Reinhold, Kirsten Fritsche, Andrea Tafel, and Frank Wuttke. "Synthese von racemischem Acetyl(t-butyl)methylphenylsilan und Acetylmethylphenyl[(trimethylsilyl)methyl]silan: Substrate für stereoselektive mikrobielle Reduktionen." Journal of Organometallic Chemistry 388, no. 1-2 (May 1990): 47–55. http://dx.doi.org/10.1016/0022-328x(90)85345-y.

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44

Raissi, Heidar, Mehdi Yoosefian, Fariba Mollania, and Samaneh Khoshkhou. "Electronic structures, intramolecular interactions, and aromaticity of substituted 1-(2-iminoethylidene) silan amine: a density functional study." Structural Chemistry 24, no. 1 (May 19, 2012): 123–37. http://dx.doi.org/10.1007/s11224-012-0038-7.

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45

Lin, Qin, Zhen Jiang Song, and Jian Liang Xie. "Preparation and Thermal Stability Properties of Epoxy Matrix/Nano-SiO₂ Composites." Materials Science Forum 788 (April 2014): 588–92. http://dx.doi.org/10.4028/www.scientific.net/msf.788.588.

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The addition of nanoparticles has been proven to a high potential application for improving polymer thermal stability properties. In this paper, the nanocomposites based on epoxy matrix modified with different mass ratio of silica nanoparticles were investigated. In order to disperse and incorporate silica nanoparticles into epoxy matrix, silica nanoparticles were modified with coupling agent (Gamma-glycidoxy propyl trimethoxy silan, KH-560). FTIR spectra showed that KH-560 was absorbed on the surface of SiO2 nanoparticles. The thermo gravimetric traces indicated that the addition of silica nanoparticles has improved the thermal stability properties of epoxy matrix significantly. The decomposition temperature of nanocomposite increased with the addition of nanoSiO2, and the temperatures of the maximum rate of degradation of the unmodified nanocomposite with 0wt%, 1wt%, 3wt%, 5wt% nanoSiO2 were 401oC, 405oC, 411oC, 421oC, respectively. The temperatures for 50% weight loose of the modified nanocomposite with 1wt% and 3wt% nanoSiO2 were 389oC and 405oC, respectively.

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46

Vũ, Phạm Gia, Vũ Kế Oánh, Tô Thị Xuân Hằng, Trịnh Anh Trúc, Nguyễn Anh Sơn, Nguyễn Thùy Dương, and Thái Thu Thủy. "Nghiên cứu khả năng bảo vệ chống ăn mòn của màng sơn polyuretan biến tính với trietoxyphenyl silan." Vietnam Journal of Chemistry 56, no. 1 (February 2018): 54–59. http://dx.doi.org/10.15625/vjc.2018-0004.

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47

Hassler, K., and U. Katzenbeisser. "Bis(bis(trimethylsilyl)phosphino)silan [(Me3Si)2P]2SiH2 und 1,2-Bis(bis(trimethylsilyl)phosphino)disilan [(Me3Si)2PSiH2]2." Journal of Organometallic Chemistry 399, no. 3 (December 1990): C18—C20. http://dx.doi.org/10.1016/0022-328x(90)85502-p.

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48

Ragaišytė, Ieva, Mindaugas Daukšys, and Albertas Klovas. "PROPERTIES OF HARDENED CEMENT PASTE DEPENDING ON SILANE BASED CHEMICAL ADMIXTURES / CHEMINIŲ PRIEDŲ SILANŲ PAGRINDU ĮTAKA CEMENTINIO AKMENS SAVYBĖMS." Engineering Structures and Technologies 4, no. 1 (April 18, 2012): 29–36. http://dx.doi.org/10.3846/2029882x.2012.677409.

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The article focuses on the influence of water repellent, silane based concrete admixtures on the physical, mechanical and porosity properties of hardened cement paste. To obtain the expected results, six compositions of cement slurries were designed changing the amount and type of the silane based chemical admixture. In order to obtain technological, physical and mechanical properties of cement (slurry) stone, the following experiments, including a test on the flow characteristics of cement slurries, a test on compression and bending strength as well as the analysis of porosity and resistance to frost were accomplished. On the basis of the achieved results and using a different amount and type of silane based chemical admixtures, the flow characteristics of cement slurry has increased up to 1,47 times in respect to the control specimen. On the other hand, when using the above introduced silane based chemical admixtures, the obtained results show a decrease in the density and strength of compression and bending. By adding chemical admixture “WACKER BS 1701” 0,2% and taking into account the amount of cement, a decrease in density goes up to 2,4%. The most noticeable decrease in bending strength (26%) is obtained by using WACKER BS SMK 2101 (0,1% in respect to the amount of cement). In addition, the biggest decrease in compression strength (34,6%), considering the control specimen, can be noticed when using SILRES BS 290 (0,2%) as a silane based chemical admixture. Water absorption of the control specimen with no silane based chemical admixtures is very similar to those containing them (vary around 1). The properties of porosity (opened and closed) are also very close and vary around 2% at the maximum. The indicator of medium pore size-λ shows that the control specimen include large pores (λ = 7,92). In most cases, by using the silane based chemical admixture, minor pores are obtained (λ = 0,94 – 3,66). The results received following 100 cycles of freezing-thaw show that all specimens have passed the test. Their surfaces did not contain any cracking. Santrauka Straipsnyje nagrinėjama cheminių priedų silanų/siloksanų pagrindu įtaka cementinio akmens fizikinėms ir mechaninėms savybėms bei poringumui. Tyrimams buvo paruoštos šešios cemento tešlos, naudojant skirtingos koncentracijos silanų/siloksanų pagrindu pagamintus cheminius priedus. Tyrimo metu nustatytas cemento tešlos sklidumas, cementinio akmens tankis, lenkimo ir gniuždymo stipriai, poringumo parametrai bei atsparumas šalčiui. Nustatyta, kad naudojant skirtingos koncentracijos silanų/siloksanų pagrindu pagamintus cheminius priedus, cemento tešlos sklidumas padidėjo iki 46,3%, lyginant su kontroline tešla. Cementinio akmens tankis sumažėjo iki 2,4%, lenkimo stipris – iki 21,0%, gniuždymo stipris – iki 34,6%, lyginant su kontroliniu bandiniu be silanų/siloksanų pagrindu pagamintų priedų. Cementinio akmens be cheminių priedų silanų/siloksanų pagrindu vandens įgėris (12,16%), atviras ir uždaras poringumai yra panašūs kaip ir cementinio akmens su cheminiais priedais silanų/siloksanų pagrindu. Cementinio akmens bandiniai išlaikė 100 užšaldymo ir atšildymo ciklų atsparumo šalčiui bandymą.

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Rosatto, Camila Maria Peres de, Marina Guimarães Roscoe, Veridiana Resende Novais, Murilo de Sousa Menezes, and Carlos José Soares. "Effect of Silane Type and Air-Drying Temperature on Bonding Fiber Post to Composite Core and Resin Cement." Brazilian Dental Journal 25, no. 3 (July 2014): 217–24. http://dx.doi.org/10.1590/0103-6440201300005.

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This study evaluated the influence of silane type and temperature of silane application on push-out bond strength between fiberglass posts with composite resin core and resin cement. One hundred and sixty fiberglass posts (Exacto, Angelus) had the surface treated with hydrogen peroxide 24%. Posts were divided in 8 groups according to two study factors: air-drying temperature after silane application (room temperature and 60 ºC) and silane type: three pre-hydrolyzed - Silano (Angelus), Prosil (FGM), RelyX Ceramic Primer (3M ESPE) and one two-component silane - Silane Coupling Agent (Dentsply). The posts (n=10) for testing the bond strength between post and composite core were centered on a cylindrical plastic matrix and composite resin (Filtek Z250 XT, 3M ESPE) that was incrementally inserted and photoactivated. Eighty bovine incisor roots (n=10) were prepared for testing the bond strength between post and resin cement (RelyX U100, 3M ESPE) and received the fiberglass posts. Push-out test was used to measure the bond strength. Data were analyzed by two-way ANOVA followed by Tukey's test (a=0.05). ANOVA revealed that temperature and silane had no influence on bond strength between composite core and post. However, for bond strength between post and resin cement, the temperature increase resulted in a better performance for Silane Coupling Agent, Silano and RelyX Ceramic Primer. At room temperature Silane Coupling Agent showed the lowest bond strength. Effect of the warm air-drying is dependent on the silane composition. In conclusion, the use of silane is influenced by wettability of resinous materials and pre-hydrolyzed silanes are more stable compared with the two-bottle silane.

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Friedel, M., M. Büchler, and P. Albers. "Verwendung von Betonzusatzmitteln und Oberflächenschutzsystemen auf der Basis von Silan und Siloxan als Korrosionsinhibitor für den Bewehrungsstahl in Beton / Silane and Siloxane Based Formulations for the Corrosion Inhibition of Steel Reinforcement in Concrete." Restoration of Buildings and Monuments 16, no. 2 (April 1, 2010): 99–108. http://dx.doi.org/10.1515/rbm-2010-6360.

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