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Journal articles on the topic 'Silylamine'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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1

Huber, Gerald, and Hubert Schmidbaur. "The Basicity of Silylamines and Alkylamines: An Equilibrium Study of the Competitive Borane Adduct Formation." Zeitschrift für Naturforschung B 53, no. 10 (October 1, 1998): 1103–8. http://dx.doi.org/10.1515/znb-1998-1005.

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AbstractIn order to investigate the Lewis acid/base chemistry of silylamines in solution, the equilibrium reactions of Me3SiNMe2 / Me3SiNMe2(BH3) and different amines NR3 / amineboranes NR3(BH3) were monitored by 1H NMR spectroscopy in C6D6 and CDCI3 at 60 °C. For the equilibrium of the reference silylamine/-borane and Me3CNMe2 / Me3CNMe2(BH3) values K = 0.35 (AG = 3.1 kJ mol-1) in C6D6 and K = 0.50 (AG = 2.0 kJ mol-1) in CDCl3 have been estimated, showing that both the silylamine and the C/Si-analogous organic amine have very similar donor properties. Small amines like NMe3 proved to be much more powerful donors than the silylamine Me3SiNMe2, whereas bulky amines are less efficient donors, indicating that steric effects play an important role. The formation of BH3 adducts of Me2NSiH3 and (H3Si)3N which could not be followed experimentally owing to the low stability of the products, has been studied by quantum chemical calculations. A comparison with data for Me3N(BH3) shows that the silylamines are poorer donors, but the reason for this remains unclear

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2

Morgenstern, Uwe, Christoph Wagner, and Kurt Merzweiler. "Synthesis and crystal structure of the copper silylamide cluster compound [Cu9{MesSi(NPh)3}2 (PhCO2)3]." Zeitschrift für Naturforschung B 73, no. 11 (November 27, 2018): 953–57. http://dx.doi.org/10.1515/znb-2018-0103.

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AbstractThe trifunctional silylamine MesSi(NHPh)3 (Mes: 2,4,6-trimethylphenyl) was prepared by standard methods from MesSiCl3 and LiNHPh. Lithiation of MesSi(NHPh)3 and subsequent reaction with copper(I) benzoate afforded the nonanuclear cluster complex [Cu9{MesSi(NPh)3}2 (PhCO2)3]·2toluene. The cluster core consists of three copper atoms which are coordinated almost linearly by the nitrogen atoms of two adjacing MesSi(NPh)3 units. Additionally, each of the silylamide nitrogen atoms is connected to a peripheral copper atom and the peripheral copper atoms are linked by μ2-κ(O,O′) bridging benzoate groups. The observed Cu–N distances are in the range 189.6(4)–196.7(3) pm.

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3

Gordon, Mark S. "The molecular structure of silylamine." Chemical Physics Letters 126, no. 5 (May 1986): 451–54. http://dx.doi.org/10.1016/s0009-2614(86)80134-8.

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4

Ruhlandt-Senge, Karin, Ruth A. Bartlett, Marilyn M. Olmstead, and Philip P. Power. "Silylamine mit pyramidal umgebenem Stickstoff." Angewandte Chemie 105, no. 3 (March 1993): 459–61. http://dx.doi.org/10.1002/ange.19931050334.

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5

Soderquist, John A., Jesus R. Medina, and Ramon Huertas. "Novel hydroborating agents from silylamine-boranes." Tetrahedron Letters 39, no. 34 (August 1998): 6119–22. http://dx.doi.org/10.1016/s0040-4039(98)01261-1.

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6

Takeda, Youhei, Kaoru Shibuta, Shohei Aoki, Norimitsu Tohnai, and Satoshi Minakata. "Catalyst-controlled regiodivergent ring-opening C(sp3)–Si bond-forming reactions of 2-arylaziridines with silylborane enabled by synergistic palladium/copper dual catalysis." Chemical Science 10, no. 37 (2019): 8642–47. http://dx.doi.org/10.1039/c9sc02507c.

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A Pd/Cu catalyst-controlled regiodivergent and stereospecific ring-opening C(sp³)–Si cross-coupling of 2-arylaziridines with silylborane has been developed and a new tandem reaction to give another regioisomer of silylamine has been discovered.

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7

Soderquist, John A., Ramon Huertas, and Jesus R. Medina. "Mono- and dialkylborane reagents from silylamine-boranes." Tetrahedron Letters 39, no. 34 (August 1998): 6123–26. http://dx.doi.org/10.1016/s0040-4039(98)01262-3.

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8

SODERQUIST, J. A., J. R. MEDINA, and R. HUERTAS. "ChemInform Abstract: Novel Hydroborating Agents from Silylamine-Boranes." ChemInform 29, no. 44 (June 19, 2010): no. http://dx.doi.org/10.1002/chin.199844077.

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9

Mitzel, Norbert W., and Heinz Oberhammer. "A Steeply Pyramidal Silylamine: N,O-Dimethyl-N-silylhydroxylamine." Inorganic Chemistry 37, no. 14 (July 1998): 3593–98. http://dx.doi.org/10.1021/ic980323k.

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10

SODERQUIST, J. A., R. HUERTAS, and J. R. MEDINA. "ChemInform Abstract: Mono- and Dialkylborane Reagents from Silylamine-Boranes." ChemInform 29, no. 44 (June 19, 2010): no. http://dx.doi.org/10.1002/chin.199844166.

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11

Vasisht, S. K., and G. Singh. "Redox and oxo-abstraction Reactions of Silylamine with MoOCl4." Zeitschrift f�r anorganische und allgemeine Chemie 526, no. 7 (June 1985): 161–67. http://dx.doi.org/10.1002/zaac.19855260719.

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12

Klingebiel, Uwe, Sabine Pohlmann, Lutz Skoda, Cornelia Lensch, and George M. Sheldrick. "Vom Fluorsilan zum Siloxan — 1,3-Silylgruppenwanderung am Si3CSiO-Gerüst/ From a Fluorosilane to a Siloxane — 1,3-Migration of Silyl Groups in the Si3CSiO System." Zeitschrift für Naturforschung B 40, no. 8 (August 1, 1985): 1023–28. http://dx.doi.org/10.1515/znb-1985-0806.

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AbstractThe nature of the products which are formed in the reaction of tris(trimethylsilyl)Methylfluorosilanes (Me3Si)3C -SiF2R with KOH depends on the bulkiness of the substituents R. The condensed siloxane is obtained for R = F . The crystal structure determination of this siloxane (Me3Si)3C -SiF2-O -SiF2-C (SiMe3)3 shows that the Si -O - Si unit is linear. A fluorosilanol as well as a siloxane could be isolated for R = Me. 1,3-Migration of one or two trimethylsilyl groups from the carbon to the oxygen takes place for R = phenyl, rm-butyl or silylamine, with formation of siloxanes which are isomeres o f the expected silanols.

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13

Kawakami, Ryosuke, Shogo Kuriyama, Hiromasa Tanaka, Asuka Konomi, Kazunari Yoshizawa, and Yoshiaki Nishibayashi. "Iridium-catalyzed Formation of Silylamine from Dinitrogen under Ambient Reaction Conditions." Chemistry Letters 49, no. 7 (July 5, 2020): 794–97. http://dx.doi.org/10.1246/cl.200254.

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14

Haase, Martin, and Uwe Klingebiel. "Tris(silyl)silyl-chlorsilane und P-halogenierte Silylphosphane / Tris(silyl)silyl-chlorosilanes and P-Halogenated Silylphosphanes." Zeitschrift für Naturforschung B 41, no. 6 (June 1, 1986): 697–701. http://dx.doi.org/10.1515/znb-1986-0606.

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Lithium-tris(trimethylsilyl)silan reacts with chlorosilanes to give thermally stable compounds (1−3). The chlorination of 3 leads to the formation of the silane (Me3Si)3SiSi(Cl)(CMe3)2 4. The reaction of tetramethylpiperidinodihalogenophosphanes with (Me3Si)3SiSi(Cl)(Cme3)2 results in thermally stable compounds (Me3Si)3Si−P(Hal)N(CMe2)2(CH2)3, Hal = F (5). Cl (6), (Me3Si)3Si−P(Cl)N(CHMe2)2 (7) undergoes thermaly rearrangement via a silicon-chlorine exchange reaction to give (Me3Si)2Si(Cl)−P(SiMe3)N(CHMe2)2 (8). A byproduct − besides cyclic phosphanes - is the silylamine (Me3Si)2Si(Cl)N(CHMe2) (9). The formation of (9) can be explained via the elimination of the phosphinidene Me3SiP.

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15

Lakshmi Kantam, M., Tapasree Bandyopadhyay, Ateeq Rahman, N. Mahender Reddy, and B. M. Choudary. "Reduction of nitroaromatics with a new heterogenised MCM–silylamine palladium (II) catalyst." Journal of Molecular Catalysis A: Chemical 133, no. 3 (August 1998): 293–95. http://dx.doi.org/10.1016/s1381-1169(98)00137-x.

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16

Imayoshi, Ryuji, Kazunari Nakajima, and Yoshiaki Nishibayashi. "Vanadium-catalyzed Reduction of Molecular Dinitrogen into Silylamine under Ambient Reaction Conditions." Chemistry Letters 46, no. 4 (April 5, 2017): 466–68. http://dx.doi.org/10.1246/cl.161165.

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17

Imayoshi, Ryuji, Hiromasa Tanaka, Yuki Matsuo, Masahiro Yuki, Kazunari Nakajima, Kazunari Yoshizawa, and Yoshiaki Nishibayashi. "Cobalt-Catalyzed Transformation of Molecular Dinitrogen into Silylamine under Ambient Reaction Conditions." Chemistry - A European Journal 21, no. 24 (May 5, 2015): 8905–9. http://dx.doi.org/10.1002/chem.201501088.

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18

Kantam, M. Lakshmi, N. Sreeniwasa Chowdari, Ateeq Rahman, and B. M. Choudary. "MCM-Silylamine Pd(II)Complex: A Heterogeneous Catalyst for Selective Azide Reductions." Synlett 1999, no. 9 (September 1999): 1413–14. http://dx.doi.org/10.1055/s-1999-2846.

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19

Tecklenburg, Brigitte, Uwe Klingebiel, Mathias Noltemeyer, and Dieter Schmidt-Bäse. "Tetrafluorcyclodi- und Hexafluorcyclotrisilazane / Tetrafluorocyclodi- and Hexafluorocyclotrisilazanes." Zeitschrift für Naturforschung B 47, no. 6 (June 1, 1992): 855–60. http://dx.doi.org/10.1515/znb-1992-0615.

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Bis(silylamino)difluorosilanes (1,2) are prepared in the reaction of lithiated di-tert-butylmethyl- and tert-butyl-dimethylsilylamine with tetrafluorosilane. The dilithium derivative of 1 reacts with SiF4 to give the tetrafluoro-substituted four-membered (Si-N) ring system [(CMe3)2MeSiN-SiF2]2 (3). Two four-membered rings [(RN-SiF2)2 (4), (RN-SiFNRSiF3)2 (5), R=CMe3SiMe2] are obtained in the reaction of dilithiated 2 with SiF4. The dilithiated silylamines and SiF4 also react with formation of 3 and 4. However, besides 4 the six-membered ring (CMe3SiMe2N-SiF2)3(6) is obtained. Crystal structures of 3,5, and 6 were determined. A transannular Si ··· Si ring distance of 237,5 pm is found in 3.

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20

Liao, Qian, Nathalie Saffon-Merceron, and Nicolas Mézailles. "N2 Reduction into Silylamine at Tridentate Phosphine/Mo Center: Catalysis and Mechanistic Study." ACS Catalysis 5, no. 11 (October 20, 2015): 6902–6. http://dx.doi.org/10.1021/acscatal.5b01626.

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21

Park, Jae-Min, Se Jin Jang, Luchana L. Yusup, Won-Jun Lee, and Sang-Ick Lee. "Plasma-Enhanced Atomic Layer Deposition of Silicon Nitride Using a Novel Silylamine Precursor." ACS Applied Materials & Interfaces 8, no. 32 (August 4, 2016): 20865–71. http://dx.doi.org/10.1021/acsami.6b06175.

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22

Feng, Ke, and Yitbarek H. Mariam. "Controlled synthesis and spectroscopic characterization of multifunctional hybrid silazane/silylamine preceramic telechelic oligomers." Macromolecules 24, no. 16 (August 1991): 4729–32. http://dx.doi.org/10.1021/ma00016a039.

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23

Rhodes, Christopher J. "Direct EPR evidence for Si–N dπ–pπ bonding in silylamine radical cations." J. Chem. Soc., Perkin Trans. 2, no. 2 (1992): 235–41. http://dx.doi.org/10.1039/p29920000235.

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24

Eppinger, Jörg, Michael Spiegler, Wolfgang Hieringer, Wolfgang A. Herrmann, and Reiner Anwander. "C2-Symmetricansa-Lanthanidocene Complexes. Synthesis via Silylamine Elimination and β-SiH Agostic Rigidity." Journal of the American Chemical Society 122, no. 13 (April 2000): 3080–96. http://dx.doi.org/10.1021/ja992786a.

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25

Jimenez, Juan D., Sungyup Jung, and Elizabeth J. Biddinger. "Ionicity Analysis of Silylamine-Type Reversible Ionic Liquids as a Model Switchable Electrolyte." Journal of The Electrochemical Society 162, no. 7 (2015): H460—H465. http://dx.doi.org/10.1149/2.0521507jes.

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26

Anwander, Reiner, Jörg Eppinger, Iris Nagl, Wolfgang Scherer, Maxim Tafipolsky, and Peter Sirsch. "Yttrium Calix[4]arene Complexes. Silylation and Silylamine Elimination Reactions on Model Oxo Surfaces." Inorganic Chemistry 39, no. 21 (October 2000): 4713–20. http://dx.doi.org/10.1021/ic000147r.

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27

Yoon, Ung Chan, Jin Uk Kim, Eietsu Hasegawa, and Patrick S. Mariano. "Electron-transfer photochemistry of .alpha.-silylamine-cyclohexenone systems. Medium effects on reaction pathways followed." Journal of the American Chemical Society 109, no. 14 (July 1987): 4421–23. http://dx.doi.org/10.1021/ja00248a063.

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28

Urgaonkar, Sameer, Joseph F. Cortese, Robert H. Barker, Mandy Cromwell, Adelfa E. Serrano, Dyann F. Wirth, Jon Clardy, and Ralph Mazitschek. "A Concise Silylamine Approach to 2-Amino-3-hydroxy-indoles with Potentin vivoAntimalaria Activity." Organic Letters 12, no. 18 (September 17, 2010): 3998–4001. http://dx.doi.org/10.1021/ol101566h.

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29

Lakshmi Kantam, M., Ateeq Rahman, Tapasree Bandyopadhyay, and Y. Haritha. "ChemInform Abstract: Efficient Hydrodehalogenation of Aryl Halides by Heterogenized MCM-Silylamine Palladium(II) Catalyst." ChemInform 30, no. 21 (June 15, 2010): no. http://dx.doi.org/10.1002/chin.199921060.

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30

Kantam, M. Lakshmi, N. Sreenivasa Chowdari, Ateeq Rahman, and B. M. Choudary. "ChemInform Abstract: MCM-Silylamine Pd(II) Complex: A Heterogeneous Catalyst for Selective Azide Reductions." ChemInform 30, no. 49 (June 12, 2010): no. http://dx.doi.org/10.1002/chin.199949056.

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31

Sch�tte, S., F. Pauer, U. Klingebiel, D. Stalke, and G. M. Sheldrick. "Synthesen, Halogenaustausch-Reaktionen und Kristallstrukturen funktioneller Silylamine - M = Si, Ge, Sn; Hal = Cl, Br -." Zeitschrift f�r anorganische und allgemeine Chemie 582, no. 1 (March 1990): 151–61. http://dx.doi.org/10.1002/zaac.19905820119.

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32

Liao, Qian, Anthony Cavaillé, Nathalie Saffon-Merceron, and Nicolas Mézailles. "Direct Synthesis of Silylamine from N2and a Silane: Mediated by a Tridentate Phosphine Molybdenum Fragment." Angewandte Chemie 128, no. 37 (August 4, 2016): 11378–82. http://dx.doi.org/10.1002/ange.201604812.

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33

RHODES, C. J. "ChemInform Abstract: Direct EPR Evidence for Si-N dπ-pπ Bonding in Silylamine Radical Cations." ChemInform 23, no. 18 (August 22, 2010): no. http://dx.doi.org/10.1002/chin.199218104.

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34

Liao, Qian, Anthony Cavaillé, Nathalie Saffon-Merceron, and Nicolas Mézailles. "Direct Synthesis of Silylamine from N2and a Silane: Mediated by a Tridentate Phosphine Molybdenum Fragment." Angewandte Chemie International Edition 55, no. 37 (August 4, 2016): 11212–16. http://dx.doi.org/10.1002/anie.201604812.

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35

Biddinger, E. J., and J. D. Jimenez. "(3-Aminopropyl)triethoxysilane as a Model Silylamine Reversible Ionic Liquid Used as a Reversible Electrolyte." ECS Transactions 64, no. 4 (August 15, 2014): 71–81. http://dx.doi.org/10.1149/06404.0071ecst.

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36

Jung, Sungyup, Showmik Podder, Josephine Chen, and Elizabeth J. Biddinger. "Structure-Property Relationships of Silylamine-Type Reversible Ionic Liquids for Use as a Switchable Electrolyte." Journal of The Electrochemical Society 168, no. 3 (March 1, 2021): 036516. http://dx.doi.org/10.1149/1945-7111/abee5e.

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37

Hirao, Toshikazu, Shinichiro Nagata, Yoshihiro Yamana, and Toshio Agawa. "Nickel enolates in the Ni(CO)4 -induced carbonylation of gem-dibromocyclopropanes with silylamine or silylsulfide." Tetrahedron Letters 26, no. 41 (January 1985): 5061–64. http://dx.doi.org/10.1016/s0040-4039(01)80853-4.

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38

Iyoda, Masahiko, Fatema Sultana, and Mitsuo Komatsu. "Reactions of C60withα-Silylamine Derivatives: Two Types of [3+2] Addition of Azomethine Ylides to C60." Chemistry Letters 24, no. 12 (December 1995): 1133–34. http://dx.doi.org/10.1246/cl.1995.1133.

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39

Bruzaud, S., A. F. Mingotaud, and A. Soum. "Multinucleus NMR characterization of new silylamines and their corresponding lithium silylamides." Journal of Organometallic Chemistry 561, no. 1-2 (June 1998): 77–84. http://dx.doi.org/10.1016/s0022-328x(98)00506-3.

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40

Beach, David B. "Infrared and mass spectroscopic study of the reaction of silyl iodide and ammonia. Infrared spectrum of silylamine." Inorganic Chemistry 31, no. 20 (September 1992): 4174–77. http://dx.doi.org/10.1021/ic00046a035.

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41

Rohan, Amy L., Jackson R. Switzer, Kyle M. Flack, Ryan J. Hart, Swetha Sivaswamy, Elizabeth J. Biddinger, Manish Talreja, et al. "The Synthesis and the Chemical and Physical Properties of Non-Aqueous Silylamine Solvents for Carbon Dioxide Capture." ChemSusChem 5, no. 11 (August 23, 2012): 2181–87. http://dx.doi.org/10.1002/cssc.201200393.

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42

Urgaonkar, Sameer, Joseph F. Cortese, Robert H. Barker, Mandy Cromwell, Adelfa E. Serrano, Dyann F. Wirth, Jon Clardy, and Ralph Mazitschek. "ChemInform Abstract: A Concise Silylamine Approach to 2-Amino-3-hydroxy-indoles with Potent in vivo Antimalaria Activity." ChemInform 42, no. 3 (December 23, 2010): no. http://dx.doi.org/10.1002/chin.201103112.

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43

Wohlthat, Sören, Thomas Kirchner, and Jeffrey R. Reimers. "N-Silylamine Junctions for Molecular Wires to Gold: The Effect of Binding Atom Hybridization on the Electronic Transmission." Journal of Physical Chemistry C 113, no. 47 (November 3, 2009): 20458–62. http://dx.doi.org/10.1021/jp9054457.

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44

Tanaka, Hiromasa, Akira Sasada, Tomohisa Kouno, Masahiro Yuki, Yoshihiro Miyake, Haruyuki Nakanishi, Yoshiaki Nishibayashi, and Kazunari Yoshizawa. "Molybdenum-Catalyzed Transformation of Molecular Dinitrogen into Silylamine: Experimental and DFT Study on the Remarkable Role of Ferrocenyldiphosphine Ligands." Journal of the American Chemical Society 133, no. 10 (March 16, 2011): 3498–506. http://dx.doi.org/10.1021/ja109181n.

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45

BEACH, D. B. "ChemInform Abstract: IR and Mass Spectroscopic Study of the Reaction of Silyl Iodide and Ammonia. IR Spectrum of Silylamine." ChemInform 24, no. 1 (August 21, 2010): no. http://dx.doi.org/10.1002/chin.199301026.

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46

IYODA, M., F. SULTANA, and M. KOMATSU. "ChemInform Abstract: Reactions of C60 with α-Silylamine Derivatives: Two Types of (3 + 2) Addition of Azomethine Ylides to C60." ChemInform 27, no. 16 (August 12, 2010): no. http://dx.doi.org/10.1002/chin.199616136.

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47

WESTERHAUSEN, M., and W. SCHWARZ. "ChemInform Abstract: Tris(trimethylsilyl)silylamine and the Lithiated and Silylated Derivatives. X-Ray Structure of the Dimeric Lithium Trimethylsilyl-( tris(trimethylsilyl)silyl)amide." ChemInform 24, no. 35 (August 31, 2010): no. http://dx.doi.org/10.1002/chin.199335207.

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48

Kim, Harrison Sejoon, Su Min Hwang, Xin Meng, Young-Chul Byun, Yong Chan Jung, Arul Vigneswar Ravichandran, Akshay Sahota, et al. "High growth rate and high wet etch resistance silicon nitride grown by low temperature plasma enhanced atomic layer deposition with a novel silylamine precursor." Journal of Materials Chemistry C 8, no. 37 (2020): 13033–39. http://dx.doi.org/10.1039/d0tc02866e.

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Trisilylamine homolog, tris(disilanyl)amine (TDSA), is introduced as a novel precursor for the deposition of highly etch resistant silicon nitride thin films having a high growth rate at a low temperature (<300 °C) using plasma enhanced ALD process.

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49

Cheng, Fei, Stephen M. Kelly, Frédéric Lefebvre, Adam F. Lee, Karen Wilson, Stephen Clark, and John S. Bradley. "Preparation of a microporous silicon oximide gel from the reaction of tris(dimethylamino)silylamine with formamide and its pyrolytic conversion into a silicon oxynitride based glass." Journal of Materials Chemistry 15, no. 29 (2005): 3039. http://dx.doi.org/10.1039/b504835d.

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50

Jung, Young Shik, William H. Swartz, Wei Xu, Patrick S. Mariano, Neal J. Green, and Arthur G. Schultz. "Exploratory studies of .alpha.-silylamino- and .alpha.-silylamido-2,5-cyclohexadien-1-one SET photochemistry. Methodology for synthesis of functionalized hydroisoquinolines." Journal of Organic Chemistry 57, no. 22 (October 1992): 6037–47. http://dx.doi.org/10.1021/jo00048a046.

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