Relevant bibliographies by topics / Solid-state hydrogen/deuterium exchange

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  1. Journal articles
  2. Dissertations / Theses
  3. Conference papers

Academic literature on the topic 'Solid-state hydrogen/deuterium exchange'

Author: Grafiati
Published: 4 June 2021
Last updated: 1 February 2022

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Journal articles on the topic "Solid-state hydrogen/deuterium exchange"

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Dadayan, A. K., Yu A. Borisov, Yu A. Zolotarev, E. V. Bocharov, I. Yu Nagaev, and N. F. Myasoedov. "Solid-State Catalytic Hydrogen/Deuterium Exchange in Mexidol." Russian Journal of Physical Chemistry A 95, no. 2 (2021): 273–78. http://dx.doi.org/10.1134/s0036024421020096.

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Dadayan, A. K., Yu A. Borisov, E. V. Bocharov, Yu A. Zolotarev, I. Yu Nagaev, and N. F. Myasoedov. "Solid state catalytic hydrogen exchange for deuterium in cycloprolylglycine." Доклады Академии наук 484, no. 3 (2019): 307–11. http://dx.doi.org/10.31857/s0869-56524843307-311.

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The reaction of spillover hydrogen (SH) with cyclopropylglycine (cPG) in high-temperature solid-state catalytic hydrogen isotope exchange (HTCIE) has been studied experimentally and using density functional theory (DFT). NMR spectroscopy and mass spectrometry have shown a high regioselectivity and stereoselectivity for the reaction of spillover hydrogen with cPG fragments. The Gly fragment has been shown to be the most reactive in HTCIE, for which high stereoselectivity of substitution of hydrogen by deuterium has been demonstrated.
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3

Kammari, Rajashekar, and Elizabeth M. Topp. "Prehydration and the Reversibility of Solid-State Hydrogen–Deuterium Exchange." Molecular Pharmaceutics 17, no. 9 (2020): 3541–52. http://dx.doi.org/10.1021/acs.molpharmaceut.0c00571.

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4

Kita, Akiko, and Yukio Morimoto. "Hydrogen/deuterium exchange behavior in tetragonal hen egg-white lysozyme crystals affected by solution state." Journal of Applied Crystallography 53, no. 3 (2020): 837–40. http://dx.doi.org/10.1107/s1600576720005488.

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Neutron diffraction studies of hydrogen/deuterium-exchanged hen egg-white lysozyme were performed by a joint X-ray and neutron refinement to elucidate the hydrogen/deuterium exchange behavior. Large crystals for neutron work, consisting of molecules that were exchanged before crystallization, were obtained by repeatedly adding protein solution to the crystal batch using deuterated precipitant reagent. There are differences in hydrogen/deuterium exchange behavior compared with previous crystallographic or NMR studies, which could be due to intermolecular interactions in the crystal or to differ
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Dadayan, A. K., Yu A. Borisov, E. V. Bocharov, Yu A. Zolotarev, I. Yu Nagaev, and N. F. Myasoedov. "Solid-State Catalytic Isotope Exchange of Hydrogen for Deuterium in Cyclopropylglycine." Doklady Physical Chemistry 484, no. 1 (2019): 15–19. http://dx.doi.org/10.1134/s0012501619010056.

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Hagemann, Hans, Vincenza D’Anna, Jean-Philippe Rapin, and Klaus Yvon. "Deuterium−Hydrogen Exchange in Solid Mg(BH4)2." Journal of Physical Chemistry C 114, no. 21 (2010): 10045–47. http://dx.doi.org/10.1021/jp101484f.

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del Amo, Juan-Miguel Lopez, Uwe Fink, and Bernd Reif. "Quantification of protein backbone hydrogen-deuterium exchange rates by solid state NMR spectroscopy." Journal of Biomolecular NMR 48, no. 4 (2010): 203–12. http://dx.doi.org/10.1007/s10858-010-9450-8.

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8

Kammari, Rajashekar, and Elizabeth M. Topp. "Solid-State Hydrogen–Deuterium Exchange Mass Spectrometry (ssHDX-MS) of Lyophilized Poly-d,l-Alanine." Molecular Pharmaceutics 16, no. 7 (2019): 2935–46. http://dx.doi.org/10.1021/acs.molpharmaceut.9b00162.

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9

Moorthy, Balakrishnan S., Isidro E. Zarraga, Lokesh Kumar, et al. "Solid-State Hydrogen–Deuterium Exchange Mass Spectrometry: Correlation of Deuterium Uptake and Long-Term Stability of Lyophilized Monoclonal Antibody Formulations." Molecular Pharmaceutics 15, no. 1 (2017): 1–11. http://dx.doi.org/10.1021/acs.molpharmaceut.7b00504.

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10

Cotten, M., R. Fu, and T. A. Cross. "Solid-State NMR and Hydrogen-Deuterium Exchange in a Bilayer-Solubilized Peptide: Structural and Mechanistic Implications." Biophysical Journal 76, no. 3 (1999): 1179–89. http://dx.doi.org/10.1016/s0006-3495(99)77282-6.

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Dissertations / Theses on the topic "Solid-state hydrogen/deuterium exchange"

1

Owens, Simon. "Kinetics and mechanisms of hydrogen isotope exchange over solid storage media." Thesis, University of Bath, 2015. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.687343.

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Hydrogen isotope separation systems using palladium (Pd) are currently being designed for both reactor designs with the aim of separating and purifying the reactor exhaust products which contain valuable unspent hydrogen isotopes. Hydrogen isotope exchange in Pd offers an efficient, ambient condition process that can produce pure isotopic species in a process far simpler and less costly than the current state of the art cryogenic distillation processes. The method is applicable whether separating hydrogen (protium), deuterium or tritium and any combination of these. If practical fusion devices
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Rashid, Shaan. "Dual-spray Synthesis and Reactions." Thesis, Université d'Ottawa / University of Ottawa, 2017. http://hdl.handle.net/10393/35726.

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By using two electrospray emitters containing different solutions (“dual-spray”) we have recently conducted in-source hydrogen/deuterium exchange (HDX) reactions and synthesized organometallic species. For dual-spray HDX reactions, peptide and protein solutions were electrosprayed through one emitter and the deuterating agent D2O through the secondary electrospray emitter. Clear shifts in isotope distributions indicated hydrogen-deuterium exchange occurring within the ion source. By ion mobility, simultaneous deuterium exchange for two isobaric species, the oxytocin monomer and dimer, was obse
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Stefanopoulos, Konstantinos Leonidas. "Small Angle Neutron Scattering studies of hydrogen (deuterium) trapping on dislocations in metals." Thesis, University of Salford, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.261990.

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Cornish, Simon Lee. "A solid state laser system for high resolution spectroscopy of the 1S-2S transition in muonium." Thesis, University of Oxford, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.297937.

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Ntsendwana, Bulelwa. "Advanced low temperature metal hydride materials for low temperature proton exchange membrane fuel cell application." Thesis, University of the Western Cape, 2010. http://etd.uwc.ac.za/index.php?module=etd&action=viewtitle&id=gen8Srv25Nme4_8494_1307431585.

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<p>Energy is one of the basic needs of human beings and is extremely crucial for continued development of human life. Our work, leisure and our economic, social and physical welfare all depend on the sufficient, uninterrupted supply of energy. Therefore, it is essential to provide adequate and affordable energy for improving human welfare and raising living standards. Global concern over environmental climate change linked to fossil fuel consumption has increased pressure to generate power from renewable sources [1]. Although substantial advances in renewable energy technologies have been made
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(10900263), Rishabh Tukra. "MECHANISMS AND APPLICATIONS OF SOLID-STATE HYDROGEN DEUTERIUM EXCHANGE." Thesis, 2021.

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<div><div><div><p>To prolong their long-term stability, protein molecules are commonly dispensed as lyophilized powders to be reconstituted before use. Evaluating the stability of these biomolecules in the solid state is routinely done by using various analytical techniques such as glass transition temperature, residual moisture content and other spectroscopic techniques. However, these techniques often show poor correlation with long term storage stability studies. As a result, time intensive long term storage stability studies are still the golden standard for evaluating protein formulations
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(9095855), Rajashekar Kammari. "SOLID-STATE HYDROGEN-DEUTERIUM EXCHANGE MASS SPECTROMETRY OF LYOPHILIZED PEPTIDES." Thesis, 2020.

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<div>Proteins are susceptible to physical and chemical degradation in solution, which can lead to the loss of therapeutic activity and increase the potential for immunogenic responses when administered. Many degradation reactions are mediated by water, and therefore the proteins are often formulated as solids in which degradation rates are slowed significantly. Lyophilization is the most common method for producing solid protein formulations, which removes the water by sublimation and desorption under vacuum from the frozen protein solutions. Lyophilization requires excipients to protect the p
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(11192397), Eunbi Cho. "Solid-state Stability of Antibody-drug Conjugates." Thesis, 2021.

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<p>Antibody-drug conjugates (ADCs) combine the cytotoxicity of traditional chemotherapy with the site-specificity of antibodies by conjugating payloads to antibodies with immunoaffinity. However, the conjugation alters the physicochemical properties of antibodies, increasing the risks of various types of degradation. The effects of common risk factors such as pH, temperature, and light on the stability of ADCs differ from their effects on monoclonal antibodies (mAb) due to these altered physicochemical properties. </p> <p>To date, ADC researchers have developed linkers with improved <i>in viv
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(7827434), Nathan E. Wilson. "Effects of Formulation and Manufacturing Conditions on Protein Structure and Physical Stability." Thesis, 2019.

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This work focuses on the effects of formulation and manufacturing as it effects protein structure and physical stability. Using common physical characterization techniques, X-ray photoelectron spectroscopy, and solid-state hydrogen/deuterium exchange with mass spectrometry, correlations are identified between these results and accelerated stability studies.
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Murphy, Owen James. "Structural changes between signaling states of bacterial chemoreceptors probed by solid -state NMR and hydrogen exchange." 2001. https://scholarworks.umass.edu/dissertations/AAI3000324.

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The limitations of structural studies of membrane proteins imposed by the lipid environment has made it difficult to determine the molecular mechanism of transmembrane signaling. For the bacterial chemoreceptor family there are crystal structures of the internal and external domains, structural models of the transmembrane domain, and evidence for subtle ligand-induced conformational changes, but the signaling mechanism remains controversial. We have used a novel site-directed solid-state NMR distance measurement approach, using 13C19F REDOR, to measure a ligand-induced change of 1.0 ± 0.3 Å in
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Conference papers on the topic "Solid-state hydrogen/deuterium exchange"

1

Ahn, C. G., J. H. Kim, Y. K. Kim, Y. H. Lee, and B. K. Kang. "Effects of Hydrogen and Deuterium Annealing on Plasma Process-Induced Damages." In 1999 International Conference on Solid State Devices and Materials. The Japan Society of Applied Physics, 1999. http://dx.doi.org/10.7567/ssdm.1999.a-11-1.

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2

Park, Hokyung, Byounghun Lee, Mark Gardner, and Hyunsang Hwang. "Effects of high pressure hydrogen and deuterium annealing on nMOSFET with Hf-base gate dielectrics." In 2004 International Conference on Solid State Devices and Materials. The Japan Society of Applied Physics, 2004. http://dx.doi.org/10.7567/ssdm.2004.b-8-2.

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Journal articles
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