Academic literature on the topic 'Solid state Sn NMR'

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Journal articles on the topic "Solid state Sn NMR"

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Wrackmeyer, Bernd, Oleg L. Tok, and Amin Badshah. "NMR Spectroscopy of Tetra(propyn- 1-yl)silane in the Solid State and in Solution." Zeitschrift für Naturforschung B 58, no. 8 (2003): 809–12. http://dx.doi.org/10.1515/znb-2003-0815.

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The crystal structure of tetra(propyn-1-yl)silane, Si(C≡CMe)4 1, has revealed a completely asymmetric molecule (point group C1). Since this finding concerns a single crystal, the bulk material of 1 was studied by solid-state 29Si and 13C MAS NMR. This confirmed the result of the X-ray analysis, and by comparison with previous NMR measurements of the tin analogue 1(Sn) it is concluded that 1 and 1(Sn) must have very similar solid-state structures which are in contrast to those known for other tetra(alkyn-1-yl)silicon and -tin compounds. The NMR data set of 1 in solution was completed by determi
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Hampden-Smith, Mark J., Teresa A. Wark, Arnold Rheingold, and John C. Huffman. "Solid state and solution structural investigation of homoleptic tin(IV) alkoxide compounds. Part I. Sn(O—t-Bu)4 and [Sn(O—i-Pr)4•HO—i-Pr]2." Canadian Journal of Chemistry 69, no. 1 (1991): 121–29. http://dx.doi.org/10.1139/v91-020.

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The crystal and molecular structures of Sn(O—t-Bu)4• and [Sn(O—i-Pr)4•HO—i-Pr]2 have been determined by single-crystal X-ray diffraction. Sn(O—t-Bu)4 crystallizes in the monoclinic crystal system with space group C2/c, where a = 17.382(6) Å, b = 8.742(2) Å, c = 15.518(5) Å, β = 116.44(1)°, Z = 4, and R = 2.5%. Sn(O—t-Bu)4 is monomeric in the solid state, with a distorted tetrahedral tin coordination environment. [Sn(O—i-Pr)4•HO—i-Pr]2 crystallizes in the monoclinic crystal system with space group P21/n, where a = 11.808(3) Å, b = 14.356(3) Å, c = 12.380(2) Å, β = 95.27(2)°, Z = 2, and R = 4.9%
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Schappacher, Falko M., Panchanana Khuntia, Anakot K. Rajarajan, et al. "Solid-state 119Sn NMR and M¨ossbauer Spectroscopic Studies of the Intermediate-valent Stannide CeRuSn." Zeitschrift für Naturforschung B 67, no. 5 (2012): 473–78. http://dx.doi.org/10.5560/znb.2012-0072.

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The ternary stannide CeRuSn is a static mixed-valent cerium compound with an ordering of trivalent and intermediate-valent cerium on two distinct crystallographic sites. 119Sn Mössbauer spectra showed two electronically almost identical tin atoms at 323 K, while at 298 K and below (77 and 4:2 K) two tin sites can clearly be distinguished. Solid-state 119Sn NMR experiments were performed to probe the local hyperfine fields at the two different Sn sites. Powder 119Sn NMR spectra are nicely fitted with two Sn sites with nearly the same magnetic anisotropy, but with different absolute shift values
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Huber, Friedo, Anil K. Saxena, Robin K. Harris, and Angelika Sebald. "Solid state 119-Sn NMR studies on some organotin compounds." Journal of Organometallic Chemistry 368, no. 1 (1989): 31–33. http://dx.doi.org/10.1016/0022-328x(89)80115-9.

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Jędryka, E., P. Panissod, P. Guilmin, and G. Marchal. "NMR study of solid state reaction in Co-Sn multilayers." Hyperfine Interactions 51, no. 1-4 (1989): 1103–10. http://dx.doi.org/10.1007/bf02407835.

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Lee, Carolyn W. B., John S. Waugh, and Robert G. Griffin. "Solid-state NMR study of trehalose/1,2-dipalmitoyl-sn-phosphatidylcholine interactions." Biochemistry 25, no. 13 (1986): 3737–42. http://dx.doi.org/10.1021/bi00361a001.

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Bakhmutov, Vladimir I., Douglas W. Elliott, Gregory P. Wylie, Abraham Clearfield, Aida Contreras-Ramirez, and Hong-Cai Zhou. "Pyridine-d5 as a 2H NMR probe for investigation of macrostructure and pore shapes in a layered Sn(iv) phosphonate–phosphate material." Chemical Communications 56, no. 25 (2020): 3653–56. http://dx.doi.org/10.1039/c9cc09254d.

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Isotropic and anisotropic motions and molecular states of pyridine-d<sub>5</sub>, adsorbed on the surface within the pores of a layered Sn(iv) phosphonate–phosphate material (1) have been characterized thermodynamically and kinetically by solid-state NMR.
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Jaworski, Aleksander, Jędrzej Piątek, Liuda Mereacre, Cordula Braun, and Adam Slabon. "14N, 13C, and 119Sn solid-state NMR characterization of tin(II) carbodiimide Sn(NCN)." Zeitschrift für Naturforschung B 76, no. 10-12 (2021): 745–50. http://dx.doi.org/10.1515/znb-2021-0122.

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Abstract We report the first magic-angle spinning (MAS) nuclear magnetic resonance (NMR) study on Sn(NCN). In this compound the spatially elongated (NCN)2− ion is assumed to develop two distinct forms: either cyanamide (N≡C–N2−) or carbodiimide (−N=C=N−). Our 14N MAS NMR results reveal that in Sn(NCN) the (NCN)2− groups exist exclusively in the form of symmetric carbodiimide ions with two equivalent nitrogen sites, which is in agreement with the X-ray diffraction data. The 14N quadrupolar coupling constant | C Q | $\vert {C}_{\text{Q}}\vert $ ≈ 1.1 MHz for the −N=C=N− ion in Sn(NCN) is low whe
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Robinson, Loleth E., Jonah Wang, Harrison Asare, et al. "Development of Fluoride-Ion Primary Batteries." ECS Meeting Abstracts MA2024-02, no. 9 (2024): 1270. https://doi.org/10.1149/ma2024-0291270mtgabs.

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The primary lithium-carbon monofluoride (Li-CFx) cell offers the highest specific energy of any commercial lithium metal battery chemistry known. However, the practical discharge voltage even at low current densities (ca. 2.5-2.7 V) is significantly lower relative to the theoretical value (4.57 V), causing a significant penalty in specific energy. To reduce the overpotential at the CFx electrode, we altered the electrochemical reaction mechanism to defluorinating the CFx electrode upon discharge, without concomitant lithiation. Here, using a room temperature fluoride-ion (F-ion) conducting ele
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Möller, Julia. "Solid-State NMR Revealing the Impact of Polymer Additives on Li-Ion Motions in Plastic-Crystalline Succinonitrile Electrolytes." ECS Meeting Abstracts MA2023-02, no. 56 (2023): 2726. http://dx.doi.org/10.1149/ma2023-02562726mtgabs.

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To enhance the safety of lithium-ion batteries (LIBs), alternatives to liquid electrolytes are widely studied. One of them is the plastic-crystal succinonitrile (SN) which can solvate various Li salts.[1] This system can be further extended by inserting polymers, bringing additional advantages such as higher melting points and the possibility of adjusting thermo-mechanical and electrochemical properties.[2] The plastic-crystalline electrolyte consisting of the Li salt lithium bis(trifluoro-methanesulfonyl)imide (LiTFSI) dissolved in SN was extended by adding various thermoplastic polymers, nam
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Dissertations / Theses on the topic "Solid state Sn NMR"

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Sneddon, Scott. "Characterisation of inorganic materials using solid-state NMR spectroscopy." Thesis, University of St Andrews, 2016. http://hdl.handle.net/10023/8239.

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This thesis uses solid-state nuclear magnetic resonance (NMR) spectroscopy and density functional theory (DFT) calculations to study local structure and disorder in inorganic materials. Initial work concerns microporous aluminophosphate frameworks, where the importance of semi-empirical dispersion correction (SEDC) schemes in structural optimisation using DFT is evaluated. These schemes provide structures in better agreement with experimental diffraction measurements, but very similar NMR parameters are obtained for any structures where the atomic coordinates are optimised, owing to the simila
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Tarhouchi, Ilyas. "Etude des phases Li10MP2S12 (M=Sn, Si) comme électrolyte pour batteries tout-solide massives." Thesis, Bordeaux, 2015. http://www.theses.fr/2015BORD0220/document.

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En remplaçant l’électrolyte liquide par un solide, les batteries tout-solide massivessont souvent considérées comme une solution aux problèmes de sécurité desbatteries Li-ion actuelles. La récente découverte du matériau Li10GeP2S12 destructure dite LGPS présentant une conductivité ionique équivalente à celles desélectrolytes liquides a réactivé ce domaine de recherche.Dans cette optique, nous avons étudié les matériaux Li10MP2S12 (M=Sn, Si) destructure LGPS, au moyen de diverses caractérisations structurales (DRX,RMN du 31P, spectroscopie Mössbauer …), de propriétés de mobilité/conductionioniq
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Heitjans, Paul, Sylvio Indris, and Martin Wilkening. "Solid-state diffusion and NMR." Universitätsbibliothek Leipzig, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-195770.

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Diffusion in solids, which requires the presence of crystal defects or disorder, has both microscopic and macroscopic aspects. Nuclear magnetic resonance techniques provide access to microscopic diffusion parameters like atomic jump rates and activation energies as well as to the tracer diffusion coefficient for macroscopic transport. Microscopic NMR methods include spin-lattice relaxation spectroscopy of stable and beta-radioactive nuclei, spin-spin relaxation or linewidth and spin alignment decay measurements, whereas macroscopic NMR methods are represented by the techniques of static and pu
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Heitjans, Paul, Sylvio Indris, and Martin Wilkening. "Solid-state diffusion and NMR." Diffusion fundamentals 2 (2005) 45, S. 1-20, 2005. https://ul.qucosa.de/id/qucosa%3A14378.

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Diffusion in solids, which requires the presence of crystal defects or disorder, has both microscopic and macroscopic aspects. Nuclear magnetic resonance techniques provide access to microscopic diffusion parameters like atomic jump rates and activation energies as well as to the tracer diffusion coefficient for macroscopic transport. Microscopic NMR methods include spin-lattice relaxation spectroscopy of stable and beta-radioactive nuclei, spin-spin relaxation or linewidth and spin alignment decay measurements, whereas macroscopic NMR methods are represented by the techniques of static and pu
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Kirby, Christopher William. "Solid-state NMR studies of cobalamins." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2001. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp04/NQ60546.pdf.

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Jackson, P. "Dipolar coupling in solid-state NMR." Thesis, Durham University, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.379058.

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Heindrichs, Axel Stefan Dirk. "New methodologies in solid state NMR." Thesis, University of Nottingham, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.342111.

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Crockford, Charles. "New methodologies in solid state NMR." Thesis, University of Nottingham, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.289481.

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Stein, Robin Stephanie. "Structural studies using solid-state NMR." Thesis, University of Cambridge, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.612912.

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Portieri, Alessia. "Solid state NMR of sulfa-drugs." Thesis, Durham University, 2001. http://etheses.dur.ac.uk/3781/.

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This work has been a study of systems, mostly of sulfa-drugs, showing polymorphic behaviour. Using different means as solid state NMR, X-ray analysis, and theoretical calculations, we have seen how it is possible to understand results obtained from the different techniques, proving how the study of polymorphic systems needs cooperative advice from the different techniques that are able to detect polymorphic differences. Within the sulfa-drugs I have been mostly concentrating on sulfanilamide, studying (^13)C and (^15)N solid state NMR spectra of the different polymorphs. The NMR parameters tha
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Books on the topic "Solid state Sn NMR"

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Chan, Jerry C. C., ed. Solid State NMR. Springer Berlin Heidelberg, 2012. http://dx.doi.org/10.1007/978-3-642-24803-0.

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Bernhard, Blümich, and Bennett A. E, eds. Solid-state NMR. Springer-Verlag, 1994.

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Chan, Jerry C. C. Solid State NMR. Springer-Verlag Berlin Heidelberg, 2012.

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Bernhard, Blümich, and Brinkmann D, eds. Solid-state NMR. Springer-Verlag, 1994.

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Bernhard, Blümich, Born R, and Spiess Hans Wolfgang 1942-, eds. Solid state NMR. Springer-Verlag, 1994.

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Blümich, Bernhard, ed. Solid-State NMR II. Springer Berlin Heidelberg, 1994. http://dx.doi.org/10.1007/978-3-642-50049-7.

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Blümich, Bernhard, ed. Solid-State NMR IV Methods and Applications of Solid-State NMR. Springer Berlin Heidelberg, 1994. http://dx.doi.org/10.1007/978-3-642-79127-7.

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Blümich, Bernhard, ed. Solid-State NMR I Methods. Springer Berlin Heidelberg, 1994. http://dx.doi.org/10.1007/978-3-642-78483-5.

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Mathias, Lon J., ed. Solid State NMR of Polymers. Springer US, 1991. http://dx.doi.org/10.1007/978-1-4899-2474-2.

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Mathias, Lon J. Solid State NMR of Polymers. Springer US, 1991.

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Book chapters on the topic "Solid state Sn NMR"

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Brown, Steven P., and Lyndon Emsley. "Solid-State NMR." In Handbook of Spectroscopy. Wiley-VCH Verlag GmbH & Co. KGaA, 2005. http://dx.doi.org/10.1002/3527602305.ch9.

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Brown, Steven P., and Lyndon Emsley. "Solid-State NMR." In Handbook of Spectroscopy. Wiley-VCH Verlag GmbH & Co. KGaA, 2014. http://dx.doi.org/10.1002/9783527654703.ch10.

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Lubach, Joseph W., and Eric J. Munson. "Solid-state NMR Spectroscopy." In Polymorphism. Wiley-VCH Verlag GmbH & Co. KGaA, 2006. http://dx.doi.org/10.1002/3527607889.ch4.

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Aliev, Abil E. "Solid state NMR spectroscopy." In Nuclear Magnetic Resonance. Royal Society of Chemistry, 2022. http://dx.doi.org/10.1039/9781839167690-00120.

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Aliev, A. E., and R. V. Law. "Solid state NMR spectroscopy." In Nuclear Magnetic Resonance. Royal Society of Chemistry, 2015. http://dx.doi.org/10.1039/9781782622758-00294.

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Hunger, Michael. "Solid-State NMR Spectroscopy." In Zeolite Chemistry and Catalysis. Springer Netherlands, 2009. http://dx.doi.org/10.1007/978-1-4020-9678-5_2.

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Aliev, Abil E. "Solid state NMR spectroscopy." In Nuclear Magnetic Resonance. Royal Society of Chemistry, 2020. http://dx.doi.org/10.1039/9781788010665-00139.

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Aliev, Abil E. "Solid state NMR spectroscopy." In Nuclear Magnetic Resonance. Royal Society of Chemistry, 2021. http://dx.doi.org/10.1039/9781839164965-00098.

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Pfeifer, Harry. "NMR of Solid Surfaces." In Solid-State NMR II. Springer Berlin Heidelberg, 1994. http://dx.doi.org/10.1007/978-3-642-50049-7_2.

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Barbet-Massin, Emeline, and Guido Pintacuda. "Biomolecular Solid-State NMR/Basics." In NMR of Biomolecules. Wiley-VCH Verlag GmbH & Co. KGaA, 2012. http://dx.doi.org/10.1002/9783527644506.ch20.

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Conference papers on the topic "Solid state Sn NMR"

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Aydin, Eren, Amirhossein Jouyaeian, Zhong Tang, and Kofi Makinwa. "A Direct Conversion Transceiver for Portable Microfluidic NMR Flowmeters." In 2024 IEEE European Solid-State Electronics Research Conference (ESSERC). IEEE, 2024. http://dx.doi.org/10.1109/esserc62670.2024.10719403.

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Sun, Nan, Tae-Jong Yoon, Hakho Lee, et al. "Palm NMR and one-chip NMR." In 2010 IEEE International Solid- State Circuits Conference - (ISSCC). IEEE, 2010. http://dx.doi.org/10.1109/isscc.2010.5433836.

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Ghoshray, Amitabha, Mayukh Majumder, Asok Poddar, Chandan Mazumdar, Kajal Ghoshray, and David Berardan. "Magnetization and NMR studies in SmFeAsO0.86F0.14." In SOLID STATE PHYSICS: Proceedings of the 56th DAE Solid State Physics Symposium 2011. AIP, 2012. http://dx.doi.org/10.1063/1.4710282.

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Tsukanov, A. V., A. A. Larionov, and K. A. Valiev. "Resonant-tunneling solid state NMR quantum computer." In SPIE Proceedings, edited by Yuri I. Ozhigov. SPIE, 2003. http://dx.doi.org/10.1117/12.517897.

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Ghoshray, Kajal. "3d spin dynamics in co-oxypnictides: NMR investigation." In SOLID STATE PHYSICS: Proceedings of the 56th DAE Solid State Physics Symposium 2011. AIP, 2012. http://dx.doi.org/10.1063/1.4709876.

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Majumder, M., K. Ghoshray, A. Ghoshray, A. Pal, and V. P. S. Awana. "Anisotropic spin-fluctuations in SmCoPO: 31P NMR study." In SOLID STATE PHYSICS: Proceedings of the 56th DAE Solid State Physics Symposium 2011. AIP, 2012. http://dx.doi.org/10.1063/1.4710426.

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Prajapati, A. V., Y. A. Sonvane, H. P. Patel, and P. B. Thakor. "Temperature dependent electrical resistivity of liquid Sn." In DAE SOLID STATE PHYSICS SYMPOSIUM 2015. Author(s), 2016. http://dx.doi.org/10.1063/1.4948088.

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Böhme, Ute, Karsten Gelfert, and Ulrich Scheler. "Solid-State NMR on Polymers under Mechanical Stress." In MAGNETIC RESONANCE IN POROUS MEDIA: Proceedings of the 10th International Bologna Conference on Magnetic Resonance in Porous Media (MRPM10), including the 10th Colloquium on Mobile Magnetic Resonance (CMMR10). AIP, 2011. http://dx.doi.org/10.1063/1.3562245.

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Marchessault, R. H., M. G. Taylor, G. Hamer, and Y. Deslandes. "Solid State NMR of Cellulose, Wood, and Pulp." In Papermaking Raw Materials, edited by V. Punton. Fundamental Research Committee (FRC), Manchester, 1985. http://dx.doi.org/10.15376/frc.1985.1.37.

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High resolution ¹³C NMR of crystalline celluloses is both complementary and supplementary to x-ray diffraction analysis because it is effective both for crystalline an non-crystalline materials. Good spectral quality has been achieved for a range of cellulose samples and spectral elements related to lateral order are observed but some interpretational details are still evolving. The spectrum of a complex material such as wood, shows morphological and conformational features for each chemical component. The resolution achieved is sufficient to allow identification of carbohydrate resonances, me
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Ansari, Mohd Azaj, and K. Sreenivas. "Light up-conversion and structural properties of Sn and Er3+ doped Ba.995 Er.005 (Sn.06Ti.94)O3 ceramics." In DAE SOLID STATE PHYSICS SYMPOSIUM 2018. AIP Publishing, 2019. http://dx.doi.org/10.1063/1.5112840.

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Reports on the topic "Solid state Sn NMR"

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Yamamoto, Yoshihisa. Solid-State NMR Quantum Computer. Defense Technical Information Center, 2005. http://dx.doi.org/10.21236/ada442582.

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T. STEPHENS and A. LABOURIAU. SOLID-STATE NMR - PROGRESS REPORT. Office of Scientific and Technical Information (OSTI), 2000. http://dx.doi.org/10.2172/768913.

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Sun, Boqin. Scalar operators in solid-state NMR. Office of Scientific and Technical Information (OSTI), 1991. http://dx.doi.org/10.2172/10114719.

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Rice, David M. DURIP Advanced Polymer Solid State NMR Instrumentation. Defense Technical Information Center, 1990. http://dx.doi.org/10.21236/ada221401.

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Miknis, F. P. Solid-state NMR characterization of Mowry Formation shales. Office of Scientific and Technical Information (OSTI), 1992. http://dx.doi.org/10.2172/7095074.

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Miknis, F. P. Solid-state NMR characterization of Mowry Formation shales. Office of Scientific and Technical Information (OSTI), 1992. http://dx.doi.org/10.2172/10131870.

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Axelson, D. E., and Y. Theriault. Carbon-13 solid state NMR of pitch. part 2. Natural Resources Canada/ESS/Scientific and Technical Publishing Services, 1987. http://dx.doi.org/10.4095/304995.

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Nissan, R. A., and T. A. Vanderah. 31P Solid State NMR Studies of ZrP, Mg3P2, and CdPS3. Defense Technical Information Center, 1988. http://dx.doi.org/10.21236/ada199981.

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Gann, Sheryl Lee. High-Resolution NMR of Quadrupolar Nuclei in the Solid State. Office of Scientific and Technical Information (OSTI), 1995. http://dx.doi.org/10.2172/6371.

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Haw, James F. Solid State NMR Studies of Morphology and Orientation in Polymers. Defense Technical Information Center, 1995. http://dx.doi.org/10.21236/ada302354.

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