Relevant bibliographies by topics / SPE-HPLC-MS/MS

Contents

  1. Journal articles
  2. Dissertations / Theses
  3. Conference papers
  4. Reports

Academic literature on the topic 'SPE-HPLC-MS/MS'

Author: Grafiati
Published: 25 January 2025

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Journal articles on the topic "SPE-HPLC-MS/MS"

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Chen, Kun-Ming, Ana Calcagnotto, Junjia Zhu, Yuan-Wan Sun, Karam El-Bayoumy, and John P. Richie Jr. "Comparison of an HPLC-MS/MS Method with Multiple Commercial ELISA Kits on the Determination of Levels of 8-oxo-7,8-Dihydro-2'-Deoxyguanosine in Human Urine." Journal of New Developments in Chemistry 2, no. 2 (2018): 1–13. http://dx.doi.org/10.14302/issn.2377-2549.jndc-18-2430.

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Introduction: Analysis of 8-oxodG is usually conducted by either chromatography-based methods or by immunochemical methods commonly used based upon their low cost and high-throughput. However, concern regarding the accuracy of ELISA methods has complicated their use. We directly compare the levels of urinary 8-oxodG obtained by HPLC-MS/MS with three commercially available ELISA kits in this report. Methods: In the current study, a total of 9 human urine samples were analyzed by LC-MS/MS and three commonly used commercial available ELISA kits. Results: We found that urinary 8-oxodG levels analy
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Pang, Guo-Fang, Chun-Lin Fan, Feng Zhang, et al. "High-Throughput GC/MS and HPLC/MS/MS Techniques for the Multiclass, Multiresidue Determination of 653 Pesticides and Chemical Pollutants in Tea." Journal of AOAC INTERNATIONAL 94, no. 4 (2011): 1253–96. http://dx.doi.org/10.1093/jaoac/94.4.1253.

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Abstract An effcient and sensitive method has been established for simultaneous determination of 653 pesticides in teas by GC/MS and HPLC/MS/MS. The method involved extraction with acetonitrile followed by cleanup using Cleanert-TPT SPE and subsequent identifcation and quantitation of 490 pesticides by GC/MS and 448 pesticides by HPLC/MS/MS. The LODs for pesticides determined by GC/MS were between 1.0 and 500 µg/kg, and those determined by HPLC/MS/MS were between 0.03 and 4820 µg/kg. At the low fortifcation levels of 0.01–100 µg/kg, the average recoveries of 94% of the pesticides determined by
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Miao, Hong-Hao, Yi-Nan Wang, Ru-Song Zhao, et al. "Determination of triclocarban in aquatic plants by using SPE combined with HPLC-ESI-MS/MS." Anal. Methods 6, no. 7 (2014): 2227–32. http://dx.doi.org/10.1039/c3ay42304b.

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A convenient and reliable analytical method was developed for determination of antibacterial triclocarban in aquatic plants based on homogenate extraction, SPE clean-up, and HPLC-ESI-MS/MS determination.
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Kovalczuk, T., J. Poustka, and J. Hajšlová. "HPLC-MS/MS method for analysis of isoproturon in difficult matrix: poppy seeds." Czech Journal of Food Sciences 26, No. 2 (2008): 146–52. http://dx.doi.org/10.17221/2469-cjfs.

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While several validated methods have been developed for analysis of phenylurea herbicides in staple food plants, analytical procedures suitable for their quantification in minor crops such as poppy seeds are not available. For the registration of isoproturon use in this crop, the documentation of dynamics of its residues following treatment was requested. To accomplish this task, HPLC-MS/MS method was developed. Extraction of residues was realised by methanol-water mixture, Supelclean LC-18 SPE cartridges were used for purification of crude extracts. For HPLC separation of isoproturon SPE frac
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Sturm, Sonja, Christina Högner, Christoph Seger, and Hermann Stuppner. "Combining HPLC-DAD-QTOF-MS and HPLC-SPE-NMR to Monitor In Vitro Vitetrifolin D Phase I and II Metabolism." Metabolites 11, no. 8 (2021): 529. http://dx.doi.org/10.3390/metabo11080529.

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By combining HPLC-DAD-QTOF-MS and HPLC-SPE-NMR, the in vitro metabolism of vitetrifolin D, a pharmacologically active key molecule from Vitex agnus-castus in liver cell fractions, was investigated. Twenty-seven phase I and phase II metabolites were tentatively identified from the culture broth by HPLC-DAD-QTOF-MS. The subsequent HPLC-SPE-NMR analysis allowed for the unequivocal structural characterization of nine phase I metabolites. Since the preparative isolation of the metabolites was avoided, the substance input was much lower than in conventional strategies. The study did prove that the u
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Liu, Lei, Yabin Wen, Kangning Liu, Liang Sun, Yaxin Lu, and Zheng Yin. "Simultaneous determination of a broad range of cardiovascular drugs in plasma with a simple and efficient extraction/clean up procedure and chromatography-mass spectrometry analysis." RSC Adv. 4, no. 38 (2014): 19629–39. http://dx.doi.org/10.1039/c4ra01045k.

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A simple, easy to use and efficient method was described for simultaneous determination of ten cardiovascular drugs with a broad range of physicochemical properties in rat plasma via online SPE and HPLC-MS/MS.
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Sun, Xiaojie, Yuanhao Yang, Qiangbing Tian, Derong Shang, Jun Xing, and Yuxiu Zhai. "Determination of gentamicin C components in fish tissues through SPE-Hypercarb-HPLC-MS/MS." Journal of Chromatography B 1093-1094 (September 2018): 167–73. http://dx.doi.org/10.1016/j.jchromb.2018.07.011.

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Wang, Bo, Jianyu Liu, Xia Zhao, et al. "Determination of Eight Coccidiostats in Eggs by Liquid–Liquid Extraction–Solid-Phase Extraction and Liquid Chromatography–Tandem Mass Spectrometry." Molecules 25, no. 4 (2020): 987. http://dx.doi.org/10.3390/molecules25040987.

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A method for the simultaneous determination of robenidine, halofuginone, lasalocid, monensin, nigericin, salinomycin, narasin, and maduramicin residues in eggs by liquid chromatography–tandem mass spectrometry (LC–MS/MS) was developed. The sample preparation method used a combination of liquid–liquid extraction (LLE) and solid-phase extraction (SPE) technology to extract and purify these target compounds from eggs. The target compounds were separated by gradient elution using high-performance liquid chromatography (HPLC) and ultra-performance liquid chromatography (UPLC). Tandem mass spectrome
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Nurfadhila, Lina, Marsah Rahmawati, Nur Komala Fitri, Salsabila Granadha Nibullah, and Welly Windari. "Analisis senyawa acetaminophen dalam sampel biologis dengan berbagai macam metode." Journal of Pharmaceutical and Sciences 6, no. 3 (2023): 1221–37. http://dx.doi.org/10.36490/journal-jps.com.v6i3.197.

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Acetaminophen atau Paracetamol merupakan senyawa yang memiliki efek farmakologi sebagai analgesik dan antipiretik. Tujuan dari review jurnal ini yaitu guna mengetahui serta memahami berbagai macam metode yang bisa digunakan untuk menganalisis sampel biologis pasien ketika mengkonsumsi paracetamol melalui sampel biologisnya. Proses awal untuk melakukan analisis yaitu dengan melakukan preparasi sampel, sampel-sampel dipreparasi dengan berbagai macam metode yang sesuai seperti, metode ekstraksi cair-cair, ekstraksi fase padat (solid phase extraction (SPE) dan metode presipitasi protein, selanjutn
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Wang, Xiaoli, Tao Guo, Yunbo Wei, et al. "Determination of Quinolone Antibiotic Residues in Human Serum and Urine Using High-Performance Liquid Chromatography/Tandem Mass Spectrometry." Journal of Analytical Toxicology 43, no. 7 (2019): 579–86. http://dx.doi.org/10.1093/jat/bkz034.

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Abstract Quinolone antibiotic residues may pose potential threat to human health. A rapid and sensitive method was developed for the determination of quinolone residues in human serum and urine. After solid phase extraction (SPE) process, eight quinolone residues were analyzed by high-performance liquid chromatography/tandem mass spectrometry (HPLC-MS/MS) using ciprofloxacin-d8 as the internal standard. The relative standard deviation of intra-day and inter-day precision for the eight quinolones were less than 7.52% and the accuracies ranged from 95.8% to 103% in human serum, and from 94.1% to
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Dissertations / Theses on the topic "SPE-HPLC-MS/MS"

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Brown, Stacy D., Fessou Lawson-Hellu, Derek Murrell, and Sam Harirforoosh. "Simultaneous Determination of Five Antiretroviral Drugs Plus Cobicistat in Human Plasma Using Strong Cation Mixed-Mode SPE and HPLC-MS/MS." Digital Commons @ East Tennessee State University, 2017. https://dc.etsu.edu/etsu-works/5268.

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Figueiredo, Natália Guimarães de. "Avaliação da remoção de interferentes endócrinos, ativos farmacêuticos e cafeína em água para abastecimento público do estado de São Paulo." Universidade de São Paulo, 2014. http://www.teses.usp.br/teses/disponiveis/9/9141/tde-02102014-140733/.

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Alguns compostos orgânicos como interferentes endócrinos e ativos farmacêuticos estão sendo encontrados em águas superficiais e vêm chamando a atenção de orgãos públicos e da comunidade científica. Dentre esses compostos, foram enfatizados nesse trabalho, o hormônio sintético 17α-etinilestradiol, o surfactante (4-nonilfenol), bisfenol A, o antibiótico β-lactâmico amoxicilina e a cafeína como traçador de atividade antrópica. Estes compostos são continuamente introduzidos em corpos d\'água pelo lançamento de esgoto in natura o que afeta a qualidade da água, a saúde dos ecossistemas e i
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Gru, Yvan. "Couplage avancé de type HPLC avec préconcentration en ligne et spectrométrie de masse (SPE-LC/MS/MS) : identification et quantification de micropolluants organiques dans les eaux : effets de la matrice." Rennes 1, 2010. http://www.theses.fr/2010REN1S020.

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De nombreux composés d’origine anthropique sont détectés dans l’environnement, particulièrement dans les eaux de surface utilisées comme ressource. Parmi ces molécules, les pesticides, bien qu’ils soient parfois présents à de très faibles concentrations, peuvent causer des dommages sanitaires ou environnementaux. La préparation de l’échantillon et la méthode de détection sont les deux points critiques de la qualité du dosage de tels substances dans les eaux. L’extraction demeure notamment une étape fastidieuse qui génère des problèmes de récupération. Pour les réduire, une technique de chromat
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Čáková, Veronika. "Contribution à l'étude phytochimique d'orchidées tropicales : identification des constituants d'Aerides rosea et d'Acampe rigida : techniques analytiques et préparatives appliquées à Vanda coerulea et Vanda teres." Phd thesis, Université de Strasbourg, 2013. http://tel.archives-ouvertes.fr/tel-00997451.

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L'analyse de la composition chimique de deux orchidées de la sous-tribu des Aeridinae, Aerides rosea Lodd. ex. Lindl. & Paxton et Acampe rigida (Buch.-Ham. ex Sm.) P. F. Hunt, a été menée en ayant recours à des techniques de couplages et grâce à une stratégie de déréplication. Dix dérivés phénanthréniques ont ainsi été identifiés dans les tiges d'A. rosea, dont deux nouvellement décrits. Quatre stilbénoïdes, trois dérivés d'acides phénoliques et quatre esters d'acide cinnamique ont été identifiés dans les tiges d'A. rigida. Nous avons également effectué des dosages de traceurs dans différents
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Alves, Filho Elenilson de Godoy. "Análises de compostos orgânicos não específicos no esgoto sanitário doméstico através das técnicas RMNq e HPLC-(UV/MS)-SPE-ASS-NMR." Universidade Federal de São Carlos, 2014. https://repositorio.ufscar.br/handle/ufscar/6338.

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Made available in DSpace on 2016-06-02T20:35:01Z (GMT). No. of bitstreams: 1 6559.pdf: 9613917 bytes, checksum: 67420e43ad6fad43e2f813af1d7fb65b (MD5) Previous issue date: 2014-10-10<br>Universidade Federal de Sao Carlos<br>The growth of industrial deployment and urbanization play a major role in the degradation of global environmental and resource depletion mainly in countries in development such as Brazil. The problems regarding water pollution in Latin America have been well-documented, and there is no evidence of substantive effort to change the situation. There are a large number of org
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Schwalbe-Herrmann, Miriam [Verfasser], Dieter [Akademischer Betreuer] Leibfritz, and Herbert [Akademischer Betreuer] Thiele. "Lipidanalyse von Bioflüssigkeiten durch kombinierte SPE/HPLC-, MS- und NMR-Techniken / Miriam Schwalbe-Herrmann. Gutachter: Dieter Leibfritz ; Herbert Thiele. Betreuer: Dieter Leibfritz." Bremen : Staats- und Universitätsbibliothek Bremen, 2013. http://d-nb.info/107208306X/34.

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Benešová, Markéta. "Stanovení léčiv pomocí HPLC s různými typy detektorů." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2011. http://www.nusl.cz/ntk/nusl-216704.

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This diploma thesis deals with the determination of macrolide antibiotics in wastewater, especially with erythromycin, clarithromycin and roxithromycin. In this time are these pharmaceuticals prescribed quite frequently. Solid phase extraction (SPE) was used for the isolation and the purification of selected analytes from an aqueous matrix; as the suitable procedure was found the using Oasis HLB cartridges. High performance liquid chromatography with mass spectrometry detection (HPLC-MS) was optimized for its analysis of selected pharmaceuticals. The optimized method was used for the determina
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Rolisola, Ana Marta Cavinato Marchini [UNESP]. "Análise de especiação e fracionamento de biocidas de zinco (Piritionato de zinco, Zineb e Ziram) utilizando SPE, DGT, HPLC e ICP-MS em água estuarina." Universidade Estadual Paulista (UNESP), 2018. http://hdl.handle.net/11449/154339.

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Submitted by ANA MARTA CAVINATO MARCHINI ROLISOLA (anamartarolisola@hotmail.com) on 2018-06-21T22:43:46Z No. of bitstreams: 1 Ana Marta C M Rolisola_Tese de Doutorado.pdf: 4492180 bytes, checksum: d1fdb4a15ef3fdf8d398b1f8be14c005 (MD5)<br>Rejected by Ana Paula Santulo Custódio de Medeiros null (asantulo@rc.unesp.br), reason: - Falta o número do processo FAPESP nos agradecimentos: se você recebeu financiamento da FAPESP, ela exige que nos agradecimentos apareça o número do processo. on 2018-06-22T17:15:12Z (GMT)<br>Submitted by ANA MARTA CAVINATO MARCHINI ROLISOLA (anamartarolisola@hotmail.co
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Rolisola, Ana Marta Cavinato Marchini. "Análise de especiação e fracionamento de biocidas de zinco (Piritionato de zinco, Zineb e Ziram) utilizando SPE, DGT, HPLC e ICP-MS em água estuarina /." Rio Claro, 2018. http://hdl.handle.net/11449/154339.

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Orientador: Amauri Antonio Menegário<br>Banca: Didier Gastmans<br>Banca: Lauren Nozomi Marques Yabuki<br>Banca: Luciana Polese<br>Banca: Anne Hélène Fostier<br>Resumo: Atualmente, cerca de 18 compostos são utilizados como biocidas de reforço (metálicos) em tintas anti-incrustantes, como por exemplo Piritionato de Zinco (Zn(PT)2), Zineb e Ziram. É relevante o desenvolvimento de um método analítico para determinação das concentrações ambientais de biocidas metálicos. O presente estudo teve como objetivos i)desenvolver uma metodologia de extração em fase sólida (SPE) e cromatografia líquida de al
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Bettioui, Terkia. "Lipidomique du globule rouge par des techniques de spectrométrie de masse et d'imagerie infrarouge : Application à l'étude de la maladie de Gaucher." Electronic Thesis or Diss., université Paris-Saclay, 2024. http://www.theses.fr/2024UPASF085.

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Les globules rouges suscitent un intéret clinique particulier en raison de leur importance biologique. Il a été récemment démontré que certaines pathologies érythrocytaires pouvaient être associées à une composition lipidique anormale. Parmi ces pathologies figure la maladie de Gaucher, un trouble lysosomal rare causé par une déficience en β-glucocérébrosidase, enzyme dont l'absence entraîne une accumulation excessive de certains sphingolipides dans l'organisme. Cette surcharge lipidique altère les propriétés morphologiques et rhéologiques des globules rouges, provoquant des anomalies hématolo
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Conference papers on the topic "SPE-HPLC-MS/MS"

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Sun, Jing, Xi-Kui Wang, Ru-Yi Xu, Xia Wang, and Ru-Song Zhao. "Notice of Retraction: Sensitive Determination of Triclosan in Water Using SPE Packed with Bamboo Carbon Combined with HPLC-ESI-MS." In 2011 5th International Conference on Bioinformatics and Biomedical Engineering. IEEE, 2011. http://dx.doi.org/10.1109/icbbe.2011.5780744.

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Weissenberger, Markus Christian, and Sukhmeet Dhillon. "Interrelationship of Weak Organic Acids, Bases, pH and HPLC Analysis Method in Produced Waters." In SPE/CSUR Unconventional Resources Conference – Canada. Society of Petroleum Engineers, 2014. http://dx.doi.org/10.2118/171650-ms.

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Tumewu, Putranda Yeremia, and Ester Tio Minar E. Silalahi. "Chemical Tracer Application to Compare Napthalene Sulfonic Acid and Sodium Fluorobenzoic Acid as Part of Polymer Field Trial Project." In SPE Improved Oil Recovery Conference. SPE, 2024. http://dx.doi.org/10.2118/218180-ms.

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Abstract Tracer testing is the effective method to characterize subsurface, especially to investigate well connectivity or fluid pathways, estimate traveling velocity of injected fluid, assess the breakthrough times of the tracers between injectors and producers, and evaluate swept pore volume and sweep efficiency particularly in Enhanced Oil Recovery (EOR) operation. Fluoro-benzoic acid (FBA) remains the primary and most common liquid phase tracer in oil industry, but recent laboratory and geothermal field test using Naphthalene Sulfonic Acid (NSA) also looks very promising. The NSAs are ther
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Liu, Ya, Dong Lee, Haiping Lu, and Jeffrey Russek. "Development of Fluorescence Tagged Scale Inhibitors for Squeeze Applications in Gulf of Mexico." In SPE International Conference on Oilfield Chemistry. SPE, 2021. http://dx.doi.org/10.2118/204349-ms.

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Abstract Fluorescence tagged (F-tagged) scale inhibitors are drawing more interest in the oil industry and are being applied in the field. One main reason is being easily detectable and differentiable from other scale inhibitors. However, when applied to a new oilfield, it is necessary to evaluate their thermal stability, limit of detection (LOD), and fluorescence measurement interference from other chemicals. Two F-tagged scale inhibitors were tested in this study. They are the same polymeric inhibitors with different and differentiable fluorescent tags. Both F-tagged inhibitors were able to
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Ow, Hooisweng, Sehoon Chang, Gawain Thomas, Wei Wang, Afnan A. Mashat, and Hussein Shateeb. "Automatable High Sensitivity Tracer Detection: Toward Tracer Data Enriched Production Management of Hydrocarbon Reservoirs." In SPE Annual Technical Conference and Exhibition. SPE, 2021. http://dx.doi.org/10.2118/206338-ms.

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Abstract The development of automatable high sensitivity analytical methods for tracer detection has been one of the most central challenges to realize ubiquitous full-field tracer deployment to study reservoirs with many cross-communicating injector and producer wells. Herein we report a tracer analysis approach, inspired by strategies commonly utilized in the biotechnology industry, that directly addresses key limitations in process throughput, detection sensitivity and automation potential of state-of-the-art technologies. A two-dimensional high performance liquid chromatography (2D-HPLC) m
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Taylor, Grahame, Jonathan Wylde, and Bridgette Allan. "Novel H2S Scavenger Testing Methodology to Meet the Ever-Present Challenge of Simulating Scavenger Application Methods with Laboratory Testing Protocols." In SPE International Conference on Oilfield Chemistry. SPE, 2021. http://dx.doi.org/10.2118/204356-ms.

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Abstract The design methodology for H2S scavengers relies heavily on developing a test protocol that most closely simulates field applications. These include gas contact towers, direct gas production injection and multiphase treatments, such as subsea umbilical delivery lines to sea floor well heads, hydrocarbon flow lines and sour storage tank treatments. There are very few testing standards and while there are industry accepted methods, the novel methods presented fill the gaps that exist. A thorough review is made of existing test methodologies such as the static gas breakthrough test and t
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Chen, Hsieh, Sehoon Chang, Gawain Thomas, Wei Wang, Afnan Mashat, and Hussain Shateeb. "Comparison of Water and Gas Tracers Field Breakthrough." In SPE Annual Technical Conference and Exhibition. SPE, 2021. http://dx.doi.org/10.2118/205863-ms.

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Abstract We are developing new classes of barcoded advanced tracers, which, compared to present commercial offerings, can be optically detected in an automated fashion. The eventual goal for the advanced tracers is to deploy cost-effective, ubiquitous, long-term, and full-field tracer tests in supporting large-scale waterflooding optimization for improved oil recovery. In this paper, we compare model predictions to breakthrough data from two field tests of advanced tracers in a pilot during water alternating gas (WAG) cycles, where gas tracer tests have recently been performed as well. Two adv
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Reports on the topic "SPE-HPLC-MS/MS"

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Crouch, Rebecca, Jared Smith, Bobbi Stromer, et al. Preparative, extraction, and analytical methods for simultaneous determination of legacy and insensitive munition (IM) constituents in aqueous, soil or sediment, and tissue matrices. Engineer Research and Development Center (U.S.), 2021. http://dx.doi.org/10.21079/11681/41480.

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No standard method exists for determining levels of insensitive munition (IM) compounds in environmental matrices. This project resulted in new methods of extraction, analytical separation and quantitation of 17 legacy and 7 IM compounds, daughter products of IM, and other munition compounds absent from USEPA Method 8330B. Extraction methods were developed for aqueous (direct-injection and solid-phase extraction [SPE]), soil, sediment, and tissue samples using laboratory-spiked samples. Aqueous methods were tested on 5 water sources, with 23 of 24 compounds recovered within DoD QSM Ver5.2 limi
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Crouch, Rebecca, Jared Smith, Bobbi Stromer, et al. Methods for simultaneous determination of legacy and insensitive munition (IM) constituents in aqueous, soil/sediment, and tissue matrices. Engineer Research and Development Center (U.S.), 2021. http://dx.doi.org/10.21079/11681/41720.

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Currently, no standard method exists for analyzing insensitive munition (IM) compounds in environmental matrices, with or without concurrent legacy munition compounds, resulting in potentially inaccurate determinations. The primary objective of this work was to develop new methods of extraction, pre-concentration, and analytical separation/quantitation of 17 legacy munition compounds along with several additional IM compounds, IM breakdown products, and other munition compounds that are not currently included in U.S. Environmental Protection Agency (EPA) Method 8330B. Analytical methods were d
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