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Journal articles on the topic 'Spontaneous crystallization'

Author: Grafiati

Published: 17 May 2025

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1

Kowalak, Stanisł aw, Aldona Jankowska, Ewa Janiszewska, and Emilia Frydrych. "Spontaneous crystallization of zincophosphate sodalite and its modifications." European Journal of Mineralogy 17, no. 6 (January 4, 2006): 853–60. http://dx.doi.org/10.1127/0935-1221/2005/0017-0853.

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2

Karpov, S. V., I. L. Isaev, V. F. Shabanov, A. P. Gavrilyuk, A. S. Grachev, and V. S. Gerasimov. "Spontaneous crystallization of nanocolloids." Doklady Physics 54, no. 2 (February 2009): 51–54. http://dx.doi.org/10.1134/s1028335809020025.

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3

McBride, J. Michael, and Randall L. Carter. "Spontaneous Resolution by Stirred Crystallization." Angewandte Chemie International Edition in English 30, no. 3 (March 1991): 293–95. http://dx.doi.org/10.1002/anie.199102931.

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4

Liu, Shu Jiang, and Yan Fei Zhang. "Spontaneous Crystallization Behavior of Phosphosilicate Glasses." Advanced Materials Research 183-185 (January 2011): 1626–30. http://dx.doi.org/10.4028/www.scientific.net/amr.183-185.1626.

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We studied the spontaneous crystallization behavior for 60.5SiO2-2.5Al2O3-3P2O5- 18Na2O-16RMgO-16(1-R)CaO system glasses during cooling of melts through changing the relative content of alkaline-earth oxides. Such compositional variation leads to the formation of different crystalline phases, as well as different degree of crystallization, with the help of X-ray diffraction (XRD), heat capacity (Cp) and scanning electron microscopy (SEM). It is found that the obtained glasses are opalescent due to formation of orthorhombic NaCaPO4 during cooling when R≤0.5, and the degree of crystallization increases with substituting MgO for CaO. On the other hand, the spontaneous crystallized phases is hexagonal NaCaPO4 for R=0.75 and is Na2MgSiO4 for R=1.0, respectively, and besides, the appearance become transparent.

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5

Karayiannis, Nikos, Katerina Foteinopoulou, and Manuel Laso. "Spontaneous Crystallization in Athermal Polymer Packings." International Journal of Molecular Sciences 14, no. 1 (December 24, 2012): 332–58. http://dx.doi.org/10.3390/ijms14010332.

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6

Sherchenkov, Alexey, Sergey Kozyukhin, Petr Lazarenko, Alexey Babich, Sergey Timoshenkov, Dmitry Gromov, Alexey Yakubov, and Dmitry Terekhov. "Influence of Ti Doping on the Properties of Ge-Sb-Te Thin Films for Phase Change Memory." Solid State Phenomena 247 (March 2016): 30–38. http://dx.doi.org/10.4028/www.scientific.net/ssp.247.30.

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The influence of Ti doping on the resistivity, activation energy of conductivity, energy band gap, Urbach energy, crystallization temperature, heat effect and crystallization kinetic parameters in Ge2Sb2Te5 thin films for phase change memory was investigated. It was shown that introduction of Ti influences on the thermal properties, and kinetics of crystallization process. Results of analyzes showed that Ti doping affects crystallization time, and probability of spontaneous crystallization at room temperature, which must be taken into consideration at designing PCM cells with Ti electrodes.

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7

Ziach, Krzysztof, and Janusz Jurczak. "Mirror symmetry breaking upon spontaneous crystallization from a dynamic combinatorial library of macrocyclic imines." Chemical Communications 51, no. 20 (2015): 4306–9. http://dx.doi.org/10.1039/c4cc10083b.

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8

Castro-Alayo, Efraín M., Llisela Torrejón-Valqui, Marleni Medina-Mendoza, Ilse S. Cayo-Colca, and Fiorella P. Cárdenas-Toro. "Kinetics Crystallization and Polymorphism of Cocoa Butter throughout the Spontaneous Fermentation Process." Foods 11, no. 12 (June 15, 2022): 1769. http://dx.doi.org/10.3390/foods11121769.

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The spontaneous fermentation process of Criollo cocoa is studied for its importance in the development of chocolate aroma precursors. This research supports the importance of spontaneous fermentation, which was studied through the crystallization behavior and polymorphisms of cocoa butter (CB), the most abundant component of chocolate that is responsible for its quality physical properties. The k-means technique was used with the CB crystallization kinetics parameters to observe the division of the process during the first stage (day 0–3). The experimental crystallization time was 15.78 min and the second stage (day 4–7) was 17.88 min. The Avrami index (1.2–2.94) showed that the CB crystallizes in the form of a rod/needle/fiber or plate throughout the process. CB produced metastable crystals of polyforms β1′ and β2′. Three days of fermentation are proposed to generate Criollo cocoa beans with acceptable CB crystallization times.

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9

Bondareva, A. F., M. A. Artemieva, A. B. Kuznetsov, A. A. Ryadun, V. D. Grigorieva, A. D. Fedorenko, V. N. Shlegel, and A. E. Musikhin. "Formation of Na2Mo2xW2(1 − x)O7 solid solutions and derived phase diagram." Журнал структурной химии 65, no. 4 (2024): 124819. http://dx.doi.org/10.26902/jsc_id124819.

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Na2Mo2xW2(1 − x)O7 (x = 0..1 with step 0.1) compositions were obtained by solid-state synthesis and spontaneous crystallization. The sample series were studied by XRD, Raman, DSC and SEM methods. The obtained data indicates formation of solid solutions, with unit cell gradually increasing with increasing tungsten ratio. A refined Na2Mo2O7 - Na2W2O7 phase diagram with unlimited miscibility was constructed. The solidus line was built based on DSC data and the liquidus line was constructed based on spontaneous crystallization experiments data. A luminescence study showed possibility of emission color variation in Na2Mo2xW2(1 − x)O7 solid solutions in dependence from excitation wavelength.

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10

Guillot, Michael, Joséphine de Meester, Laurent Collard, Olivier Riant, and Tom Leyssens. "Co-Crystallization-Induced Spontaneous Deracemization: An Optimization Study." Organic Process Research & Development 25, no. 4 (February 21, 2021): 884–91. http://dx.doi.org/10.1021/acs.oprd.0c00538.

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11

Kryuchkova, L., M. Sinai, and A. Glikin. "Compositional distribution of isomorphic crystals during spontaneous crystallization." Acta Crystallographica Section A Foundations of Crystallography 67, a1 (August 22, 2011): C469. http://dx.doi.org/10.1107/s0108767311088179.

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12

Han, Tae Hee. "Spherulitic Assembly of Peptide Nanowires via Spontaneous Crystallization." Journal of Nanoscience and Nanotechnology 14, no. 11 (November 1, 2014): 8800–8803. http://dx.doi.org/10.1166/jnn.2014.9978.

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13

Porowski, Tadeusz, Jerzy Konstantynowicz, Walentyna Zoch-Zwierz, Jan Krzysztof Kirejczyk, Katarzyna Taranta-Janusz, and Agata Korzeniecka-Kozerska. "Spontaneous urinary calcium oxalate crystallization in hypercalciuric children." Pediatric Nephrology 24, no. 9 (September 2009): 1705–10. http://dx.doi.org/10.1007/s00467-009-1171-4.

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14

Shipilo, V. B., and V. V. Sergeev. "Kinetics of spontaneous crystallization of cubic boron nitride." Soviet Powder Metallurgy and Metal Ceramics 24, no. 4 (April 1985): 301–4. http://dx.doi.org/10.1007/bf00805226.

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15

Yin, Xiuxiu, Yossef Peretz, Pola G. Oppenheimer, Leila Zeiri, Alexandra Masarwa, Natalya Froumin, and Raz Jelinek. "Conductive and SERS-active colloidal gold films spontaneously formed at a liquid/liquid interface." RSC Advances 6, no. 40 (2016): 33326–31. http://dx.doi.org/10.1039/c6ra03403a.

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16

Gangadhararao, G., R. N. Prasad Tulichala, and K. C. Kumara Swamy. "Spontaneous resolution upon crystallization of allenyl-bis-phosphine oxides." Chem. Commun. 51, no. 33 (2015): 7168–71. http://dx.doi.org/10.1039/c5cc00232j.

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17

Спивак, Л. В., and Н. Е. Щепина. "Особенности и закономерности процессов плавления и кристаллизации двухкомпонентных металлических сплавов." Физика твердого тела 61, no. 8 (2019): 1407. http://dx.doi.org/10.21883/ftt.2019.08.47961.436.

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The processes of melting and crystallization in some two-component alloys based on the Ag-Cu model system have been investigated using high resolution differential scanning calorimetry. During crystallization or melting jumps in the heat flow upon reaching the liquidus line were detected. It is assumed that during crystallization, these phenomena are associated with the formation of a large number of local microvolumes (concentration fluctuations) in the liquid, enriched with the component leading to crystallization. Their appearance precedes the beginning of the processes of spontaneous formation and growth of numerous crystals of the new phase. The necessity of correcting the existing ideas about the crystallization and melting of two-component metal alloys is revialed.

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18

Nishigaki, Akari, Mihoko Maruyama, Shun-ichi Tanaka, Hiroshi Y. Yoshikawa, Masayuki Imanishi, Masashi Yoshimura, Yusuke Mori, and Kazufumi Takano. "Metastable Crystallization by Drop Impact." Crystals 12, no. 8 (August 6, 2022): 1104. http://dx.doi.org/10.3390/cryst12081104.

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It has been reported that cavitation bubbles (air–liquid interface) by femtosecond laser and ultrasonic irradiations are effective for metastable phase crystallization in polymorph control. It has also been noted that cavitation bubbles are generated by mechanical shock when dropping a vial. Here we describe the crystallization of acetaminophen by drop impact. In the condition where spontaneous nucleation did not occur, the drop impact produced the metastable form (form II) and trihydrate. This supports the potency of the air–liquid interface in metastable phase formation. Furthermore, crystallization by drop impact is a completely new phenomenon, and new developments are expected in the future.

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19

Xue, Yun-Shan, Xu Tan, Mengjie Zhou, Hua Mei, and Yan Xu. "Synthesis, structures and magnetic properties of two chiral mixed-valence iron(ii,iii) coordination networks." Dalton Transactions 46, no. 47 (2017): 16623–30. http://dx.doi.org/10.1039/c7dt03411c.

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20

Zhang, Qingfu, Mingyuan Lei, Fang Kong, and Yan Yang. "A water-stable homochiral luminescent MOF constructed from an achiral acylamide-containing dicarboxylate ligand for enantioselective sensing of penicillamine." Chemical Communications 54, no. 77 (2018): 10901–4. http://dx.doi.org/10.1039/c8cc06274a.

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21

Elazar, Meyer. "Spontaneous Enantiomeric Enrichment of Chiral 1- (1-Naphthyl) Ethylamine." Technium BioChemMed 6 (October 18, 2023): 27–40. http://dx.doi.org/10.47577/biochemmed.v6i.9740.

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An aqueous solution of the reaction product R-(+)-1-(1-naphthyl)ethylamine hydrochloride, having high enantiomeric excess, was spontaneously resolved into the two enantiomers by simple crystallization to afford the product in nearly 100% ee.

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22

Boquete, A. Costa, G. Baio, G. R. M. Robb, G. L. Oppo, P. Griffin, and T. Ackemann. "Spontaneous atomic crystallization via diffractive dephasing in optical cavities." Journal of Physics: Conference Series 1919, no. 1 (May 1, 2021): 012014. http://dx.doi.org/10.1088/1742-6596/1919/1/012014.

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23

Ribo, J. M., Z. El-Hachemi, J. Crusats, J. M. McBride, and S. Veintemillas-Verdaguer. "Spontaneous mirror symmetry breaking in the crystallization of NaClO3." Acta Crystallographica Section A Foundations of Crystallography 67, a1 (August 22, 2011): C797—C798. http://dx.doi.org/10.1107/s0108767311079797.

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24

Chen, Ling-Yun, Yan-Ping Huang, Shao-Jun Liu, and Pei-Jyu Mao. "A rare case of spontaneous renal cholesterol crystallization embolism." Chinese Medical Journal 132, no. 3 (February 2019): 367–69. http://dx.doi.org/10.1097/cm9.0000000000000078.

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25

Kinuta, Takafumi, Emi Yokoyama, Tomohiro Sato, Nobuo Tajima, Reiko Kuroda, Yoshio Matsubara, and Yoshitane Imai. "Development of novel thioether compound for spontaneous chiral crystallization." CrystEngComm 12, no. 5 (2010): 1394–96. http://dx.doi.org/10.1039/b921416j.

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26

de Graaf, Joost, Jos Zwanikken, Markus Bier, Arjen Baarsma, Yasha Oloumi, Mischa Spelt, and René van Roij. "Spontaneous charging and crystallization of water droplets in oil." Journal of Chemical Physics 129, no. 19 (November 21, 2008): 194701. http://dx.doi.org/10.1063/1.3009762.

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27

He, Xiang, Kang Fang, Xiao-Hai Guo, Jing Han, Xiao-Peng Lu, and Ming-Xing Li. "A homochiral Cu(i) coordination polymer based on achiral precursors and its photocatalytic properties." Dalton Transactions 44, no. 30 (2015): 13545–49. http://dx.doi.org/10.1039/c5dt01328c.

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A homochiral three-dimensional framework material has been successfully synthesized by solvothermal reaction, which is generated through an unusual spontaneous asymmetrical crystallization from achiral precursors without any enantiopure additive.

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28

Jing, Qun, Xiaoyu Dong, Zhihua Yang, and Shilie Pan. "Synthesis and optical properties of the first lead borate bromide with isolated BO3groups: Pb2Ba3(BO3)3Br." Dalton Transactions 44, no. 38 (2015): 16818–23. http://dx.doi.org/10.1039/c5dt02652k.

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29

Tang, Baolei, Huapeng Liu, Feng Li, Yue Wang, and Hongyu Zhang. "Single-benzene solid emitters with lasing properties based on aggregation-induced emissions." Chemical Communications 52, no. 39 (2016): 6577–80. http://dx.doi.org/10.1039/c6cc02616h.

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Highly efficient single-benzene solid emitters exhibiting aggregation-induced emission (AIE), crystallization-enhanced emission (CEE), as well as amplified spontaneous emission (ASE) have been obtained based on structurally simple ESIPT-active organic molecules.

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30

Спивак, Л. В., and Н. Е. Щепина. "Тепловые эффекты при кристаллизации сплавов с неограниченной и ограниченной растворимостью компонентов." Журнал технической физики 89, no. 9 (2019): 1395. http://dx.doi.org/10.21883/jtf.2019.09.48065.95-18.

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The processes of crystallization of two-component alloys with unrestricted and limited solubility of the constituent components were investigated by the method of differential high-resolution scanning calorimetry. It was found that in all cases a jump in the heat evolution of crystallization that is noticeable in magnitude and speed is recorded directly below the liquidus line. Traditional approaches in describing the development of crystallization processes in the intercritical temperature range do not provide an explanation for the observed phenomena. It is assumed that the observed effects are associated with the formation of a large number of local microvolumes (concentration fluctuations) enriched in the leading crystallization component. Their appearance precedes the beginning of processes of spontaneous formation of a large number of crystals in a noticeable volume of the liquid phase.

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31

Slavyanskiy, Anatoliy, Natalia Lebedeva, and Vladimir Voitsekhovsky. "Formation of sucrose crystallization centers and their growth in a vacuum apparatus." BIO Web of Conferences 32 (2021): 03016. http://dx.doi.org/10.1051/bioconf/20213203016.

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The article considers sucrose crystallization as a mass transfer process, which is a phase transition from a liquid phase to a solid phase, and includes two main stages: the formation of crystallization centers and the growth of crystals to the desired size. The scientific novelty of the work lies in the development of existing theoretical and practical ideas about the formation of centers of crystallization of sucrose and their growth in the massecuite mass, the analysis of the main factors affecting this process. On the basis of the studies obtained, a method has been developed to improve the efficiency of the technology for boiling the massecuite of the first crystallization, which refers to the methods of boiling the massecuite I crystallization with intermediate centrifugation of the massecuite. A feature of the method is the formation of crystallization centers in the massecuite by their spontaneous formation. The analysis of the obtained research results showed that the work on the proposed method makes it possible to increase the efficiency of boiling massecuite I crystallization, to ensure an increase in the yield and quality of crystalline white sugar.

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32

Carpenter, John E., and Michael Grünwald. "Heterogeneous Interactions Promote Crystallization and Spontaneous Resolution of Chiral Molecules." Journal of the American Chemical Society 142, no. 24 (May 12, 2020): 10755–68. http://dx.doi.org/10.1021/jacs.0c02097.

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33

Yasuda, H., and H. Mori. "Spontaneous alloying and crystallization in nanometer sized amorphous antimony clusters." Thin Solid Films 298, no. 1-2 (April 1997): 143–46. http://dx.doi.org/10.1016/s0040-6090(96)09154-7.

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34

Nam, Ki Hyun. "Improving the Quality of Spontaneously Growing HviGH11 Crystals by Increasing the Viscosity Using Polyethylene Glycols." Crystals 14, no. 3 (March 21, 2024): 289. http://dx.doi.org/10.3390/cryst14030289.

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Proteins can form crystals spontaneously without crystallization experiments. These crystals can be used to determine three-dimensional structures. However, when X-ray diffraction is poor, crystal optimization is required to obtain a high-resolution crystal structure. Endo-1,4-β-xylanase from the fungus Hypocrea virens (HviGH11) spontaneously formed microcrystals after affinity purification and concentration; however, most HviGH11 microcrystals showed poor diffraction in the synchrotron X-ray and X-ray free-electron laser, so a complete three-dimensional structure could not be obtained. This study presents a method to improve the crystal quality of spontaneously grown HviGH11 microcrystals. The crystallization screening results revealed that temperature, pH, and salt were not crucial factors in increasing the solubility or preventing the spontaneous crystal growth of HviGH11. Conversely, the addition of polyethylene glycols (PEGs) as a precipitant facilitated the growth of larger HviGH11 crystals. The improved large HviGH11 crystal showed a diffraction of up to 1.95 Å when exposed to synchrotron X-rays, providing a complete three-dimensional structural dataset. Based on the nucleation rate equation, it was suggested that PEG increases the viscosity of the protein solution rather than promoting nucleation. This increase in viscosity reduced nucleation and facilitated the growth of larger HviGH11 crystals. These results provide valuable insights for future experiments aimed at increasing the size of spontaneously grown crystals.

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35

Tsiligianni, T., A. Karagiannidis, N. Roubies, P. Saratsis, and P. Brikas. "Concentration of calcium, zinc, magnesium, potassium and sodium in the bovine cervical mucus during normal oestrus and oestrus induced by progesterone and/or PGF2α." Reproduction, Fertility and Development 14, no. 7 (2002): 427. http://dx.doi.org/10.1071/rd02011.

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Ninety-two healthy Friesian cows were used to determine the concentration of calcium (Ca), zinc (Zn), magnesium (Mg), potassium (K) and sodium (Na) in bovine cervical mucus and to compare these concentrations in cervical mucus collected during spontaneous and induced oestrus. Cows were assigned to four groups: (1) no treatment (2) PRID for 12 days plus pregnant mare's serum gonadotrophin (PMSG; 1000 IU, i.m.) at the removal of the PRID (3) PGF2α , two doses (6 mg, i.m.) 11 days apart, and (4) PRID for 7 days plus one dose of PGF2α (6 mg, i.m.) 24 h before removal of the PRID. The cows of the three induced-oestrus groups received two artificial inseminations (AI), whereas those in the spontaneous-oestrus group received only one. Cervical mucus samples were collected from all cows 5 to 30 min before the first AI. The results of this study can be summarized as follows: (1) viscosity was significantly lower (P<0.001) and crystallization was significantly (P<0.001) higher in the cervical mucus of cows in the spontaneous-oestrus group compared with cows in the induced-oestrus groups; (2)�Na concentration was similar in all groups; (3) concentration of all the other elements in the spontaneous-oestrus group was significantly lower (P<0.05) than in the induced-oestrus groups; (4) there was significant positive correlation (P<0.001) between viscosity and all elements, and significant negative correlation (P<0.05–P<0.001) between crystallization and all elements.

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36

Redecke, Lars, Marco Klinge, Robert Schönherr, Dirk Rehders, Dominik Oberthür, Björn Philip Sommer, Jose Martinez-Costas, Michael Duszenko, Rainer Duden, and Christian Betzel. "In vivo protein crystallization in living insect cells." Acta Crystallographica Section A Foundations and Advances 70, a1 (August 5, 2014): C343. http://dx.doi.org/10.1107/s2053273314096569.

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Spontaneous protein crystallization within living cells has been observed several times in nature, e.g. for storage proteins in seeds. In vivo crystal growth can also occur during gene over-expression, as particularly discovered in baculovirus-infected insect cells [1]. We have recently shown that these in vivo crystals represent valuable targets for structural biology after isolation from the cell. Applying serial crystallography techniques at an X-ray free-electron laser (XFEL) as well as using a highly brilliant synchrotron source, single crystal diffraction pattern were collected and combined to yield high-resolution structural information of the associated fully glycosylated protein [2,3]. So far, the cellular mechanisms involved in the in vivo crystallization process remain to be understood, preventing a more successful application of this novel approach. Thus, our study aims at identifying the parameters crucial for optimal crystal growth within baculovirus-infected Sf9 insect cells. Combining confocal microscopy with live-cell imaging techniques and compartment-specific staining methods, we systematically investigated the impact of the intracellular environment on in vivo crystallization by directing recombinant proteins into different cellular compartments using specific signal sequences. Moreover, the impact of cellular transport mechanisms and induced cellular stress on the quality and size of the in vivo crystals was investigated in detail. The presented results provide important insights into the process of protein crystallization within living cells and will therefore significantly contribute to increase the success rate for spontaneous crystal growth of other proteins. Considering that in vivo crystals represent highly suitable targets for structural biology, this approach offers exciting new possibilities for proteins that do not form crystals suitable for conventional X-ray diffraction in vitro.

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37

Yao, Wenjiao, Tao Xu, Xingxing Jiang, Hongwei Huang, Xiaoyang Wang, Zheshuai Lin, and Chuangtian Chen. "Ca3Be6B5O16F: the first alkaline-earth beryllium borate with fluorine anions." Dalton Trans. 43, no. 26 (2014): 9998–10004. http://dx.doi.org/10.1039/c4dt00775a.

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The first all-alkaline-earth beryllium borate with fluorine anions, Ca₃Be₆B₅O₁₆F, was synthesized by a spontaneous crystallization flux method using LiF–B₂O₃as the flux.

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38

Prošek, Zdeněk, Pavla Ryparová, Aleš Jíra, Petr Bílý, and Pavel Tesárek. "Determination of Micromechanical Properties of Cementitious Materials with Self-Healing Agent." Key Engineering Materials 880 (March 2021): 149–54. http://dx.doi.org/10.4028/www.scientific.net/kem.880.149.

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The paper deals with the determination of nano, microstructural, and micromechanical properties of cementitious materials surface with self-healing agent based on calcium carbonate precipitation (calcite). This was done by means of electron microscopy with elemental microanalysis and nanoindentation. These methods can define parameters of individual phases within cementitious materials, which are important for the development of micromechanical models. Bacillus pseudofirmus in combination with culture medium 235 was chosen as a self-healing agent. Our study provides information about micromechanical properties of crystals resulting from spontaneous crystallization from the culture medium and from crystallization caused by bacteria.

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39

Coquerel, Gérard, and Marine Hoquante. "Spontaneous and Controlled Macroscopic Chiral Symmetry Breaking by Means of Crystallization." Symmetry 12, no. 11 (October 30, 2020): 1796. http://dx.doi.org/10.3390/sym12111796.

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In this paper, macroscopic chiral symmetry breaking refers to as the process in which a mixture of enantiomers departs from 50–50 symmetry to favor one chirality, resulting in either a scalemic mixture or a pure enantiomer. In this domain, crystallization offers various possibilities, from the classical Viedma ripening or Temperature Cycle-Induced Deracemization to the famous Kondepudi experiment and then to so-called Preferential Enrichment. These processes, together with some variants, will be depicted in terms of thermodynamic pathways, departure from equilibrium and operating conditions. Influential parameters on the final state will be reviewed as well as the impact of kinetics of the R ⇔ S equilibrium in solution on chiral symmetry breaking. How one can control the outcome of symmetry breaking is examined. Several open questions are detailed and different interpretations are discussed.

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40

Separdar, Leila, José Pedro Rino, and Edgar Dutra Zanotto. "Unveiling nucleation dynamics by seeded and spontaneous crystallization in supercooled liquids." Computational Materials Science 199 (November 2021): 110802. http://dx.doi.org/10.1016/j.commatsci.2021.110802.

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41

Sakamoto, Masami, Mamoru Kato, Yoko Aida, Kazuyuki Fujita, Takashi Mino, and Tsutomu Fujita. "Photosensitized 2 + 2 Cycloaddition Reaction Using Homochirality Generated by Spontaneous Crystallization." Journal of the American Chemical Society 130, no. 4 (January 2008): 1132–33. http://dx.doi.org/10.1021/ja077912m.

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42

Zheng, Wenxu, Yongqin Wei, Xueying Xiao, and Kechen Wu. "Spontaneous asymmetric crystallization of a quartz-type framework from achiral precursors." Dalton Transactions 41, no. 11 (2012): 3138. http://dx.doi.org/10.1039/c2dt12238c.

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43

Linnikov, O. D. "Mechanism of precipitate formation during spontaneous crystallization from supersaturated aqueous solutions." Russian Chemical Reviews 83, no. 4 (April 29, 2014): 343–64. http://dx.doi.org/10.1070/rc2014v083n04abeh004399.

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44

Baidakov, Vladimir G., and Kseniia R. Protsenko. "Spontaneous Crystallization of a Supercooled Lennard-Jones Liquid: Molecular Dynamics Simulation." Journal of Physical Chemistry B 123, no. 38 (September 4, 2019): 8103–12. http://dx.doi.org/10.1021/acs.jpcb.9b06618.

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Huang, Jun, Xiaojuan Liang, Weidong Xiang, Maogao Gong, Guorui Gu, Jiasong Zhong, and Daqin Chen. "Synthesis and luminescence properties of Ce:Y3Al5O12 glass ceramic by spontaneous crystallization." Materials Letters 151 (July 2015): 31–34. http://dx.doi.org/10.1016/j.matlet.2015.03.023.

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Wang, Jingsong, Xinlan Yu, Nengbing Long, Xing Sun, Guoliang Yin, Qing Jiao, Xueyun Liu, Shixun Dai, and Changgui Lin. "Spontaneous crystallization of PbCl2 nanocrystals in GeS2-Sb2S3 based chalcogenide glasses." Journal of Non-Crystalline Solids 521 (October 2019): 119543. http://dx.doi.org/10.1016/j.jnoncrysol.2019.119543.

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Balarew, Christo, Stefka Tepavitcharova, and Stoyan Kamburov. "Study of the spontaneous crystallization of Na2SO4·7H2O and Na2SeO4·7.5H2O." Monatshefte für Chemie - Chemical Monthly 149, no. 2 (December 18, 2017): 289–98. http://dx.doi.org/10.1007/s00706-017-2090-x.

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Kowalak, Stanisław, Aldona Jankowska, and Elżbieta Baran. "Spontaneous crystallization of zincophosphate sodalite by means of dry substrate grinding." Chemical Communications, no. 6 (2001): 575–76. http://dx.doi.org/10.1039/b100434b.

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Calvet, T., M. A. Cuevas-Diarte, H. E. Gallis, and H. A. J. Oonk. "Spontaneous crystallization in undercooled liquid mixtures of l-limonene + l-carvone." Recueil des Travaux Chimiques des Pays-Bas 115, no. 6 (September 2, 2010): 333–35. http://dx.doi.org/10.1002/recl.19961150605.

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Grigorieva, V. D., A. F. Bondareva, M. A. Artemyeva, E. D. Bazanova, A. P. Yelisseyev, A. A. Ryadun, and A. B. Kuznetsov. "Cs2Mo5O16 and Cs2Mo7O22: crystallization, structural and thermal properties." Журнал структурной химии 66, no. 4 (2025): 142914. https://doi.org/10.26902/jsc_id142914.

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Abstract:

Needle-like Cs2Mo7O22 (7*1*1 mm3) and plated Cs2Mo5O16 (4*3*2 mm3) crystals were obtained by spontaneous crystallization method from Cs2Mo5O16 + 2%Cs2O and Cs2Mo7O22 + 2%Cs2O melts. Peritectic nature of Cs2Mo5O16 and Cs2Mo7O22 compounds was confirmed by differential scanning calorimetry and thermogravimetric analysis. Cs2Mo5O16 and Cs2Mo7O22 crystal structures were constructed based on X-ray diffraction data. Unit cell parameters of Cs2Mo5O16 and Cs2Mo7O22 crystal samples were measured in 0-450 °C temperature range and thermal expansion vectors were calculated. Photoluminescence was registered on both Cs2Mo5O16 and Cs2Mo7O22 samples at 80 K.

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