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Journal articles on the topic 'Stability indicating assay'

Author: Grafiati

Published: 3 June 2025

Last updated: 31 July 2025

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1

Thoppil, Simmy O., and P. D. Amin. "Trimetazidine: stability indicating RPLC assay method." Journal of Pharmaceutical and Biomedical Analysis 25, no. 2 (2001): 191–95. http://dx.doi.org/10.1016/s0731-7085(00)00483-0.

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2

Rajadhyaksha, Namita S., Satish P. Jain, and Purnima D. Amin. "Carbamazepine: Stability Indicating HPLC Assay Method." Analytical Letters 40, no. 13 (2007): 2506–14. http://dx.doi.org/10.1080/00032710701583557.

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3

Al-Masri, R., and M. Al-Mardini. "STABILITY-INDICATING HPLC ASSAY METHOD OF LOVASTATIN." Bulletin of Pharmaceutical Sciences. Assiut 28, no. 2 (2005): 185–89. http://dx.doi.org/10.21608/bfsa.2005.65287.

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4

Jamshidi, Ahmad, Hamid Mobedi, and Farzaneh Ahmad-Khanbeigi. "Stability-indicating HPTLC assay for leuprolide acetate." Journal of Planar Chromatography – Modern TLC 19, no. 109 (2006): 223–27. http://dx.doi.org/10.1556/jpc.19.2006.3.10.

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5

Marwaha, Raj K., Brian F. Johnson, and George E. Wright. "Simple stability-indicating assay for histamine solutions." American Journal of Health-System Pharmacy 42, no. 7 (1985): 1568–71. http://dx.doi.org/10.1093/ajhp/42.7.1568.

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6

Alam, Prawez, Faiyaz Shakeel, Mohammed H. Alqarni, et al. "Development and Validation of A Stability-Indicating Greener HPTLC Method for the Estimation of Flufenamic Acid." Separations 10, no. 1 (2023): 39. http://dx.doi.org/10.3390/separations10010039.

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The literature on ecofriendly/greener high-performance thin-layer chromatographic (HPTLC) methods for quantifying flufenamic acid (FFA) is scant. In order to develop and validate a stability-indicating greener HPTLC densitometry assay for FFA determination in marketed products, this research was conducted. The ecofriendly eluent system was composed of ethanol–water (70:30 v/v). FFA was measured at 290 nm of wavelength. The greenness scale of suggested analytical assay was derived using “Analytical GREENness (AGREE)” methodology. The suggested stability-indicating HPTLC assay was linear for FFA

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7

Garcia, Cássia V. "Stability-Indicating HPLC Method for Posaconazole Bulk Assay." Scientia Pharmaceutica 80, no. 2 (2012): 317–27. http://dx.doi.org/10.3797/scipharm.1111-11.

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8

Sangeetha, M., Tirumala ., and Nagamallika . "STABILITY INDICATING RP-LC ASSAY METHOD FOR CARISOPRODOL." International Journal of Current Pharmaceutical Research 9, no. 6 (2017): 79. http://dx.doi.org/10.22159/ijcpr.2017v9i6.23434.

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Objective: A reverse phase stability-indicating HPLC method was developed for the determination of Carisoprodol in pharmaceutical dosage forms. The chromatographic elution was achieved on C18, 250 mm × 4.6 mm, 5-μm particle size column.Methods: The mobile phase contains a mixture of water and acetonitrile in ratio of 60:40 v/v. The flow rate was 1.0 ml min-1 and was detected by Refractive index detector.Results: The method was proven to be linear over a range of 1 to 4 mg/ml with a mean correlation coefficient of 0.99998. The %mean recovery is in the range of 100.55% to 101.11% and %RSD was le

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9

Stavchansky, S., B. Eghbali, and R. Geary. "Stability Indicating Assay of Lidocaine Hydrochloride in Solution." Analytical Letters 20, no. 5 (1987): 821–27. http://dx.doi.org/10.1080/00032718708062931.

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10

Saravanan, G., B. M. Rao, M. Ravikumar, M. V. Suryanarayana, N. Someswararao, and P. V. R. Acharyulu. "A Stability-Indicating LC Assay Method for Bicalutamide." Chromatographia 66, no. 3-4 (2007): 219–22. http://dx.doi.org/10.1365/s10337-007-0280-0.

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11

Desai, Namita D., Pirthipal P. Singh, Purnima D. Amin, and Satishkumar P. Jain. "Stability-Indicating LC Method for Assay of Cholecalciferol." Chromatographia 69, no. 3-4 (2008): 385–88. http://dx.doi.org/10.1365/s10337-008-0914-x.

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12

Bempong, Daniel K., Ronald G. Manning, Tahseen Mirza, and Lokesh Bhattacharyya. "A stability-indicating HPLC assay for metronidazole benzoate." Journal of Pharmaceutical and Biomedical Analysis 38, no. 4 (2005): 776–80. http://dx.doi.org/10.1016/j.jpba.2005.02.019.

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13

Rao, B. Mallikarjuna, Arpita Chakraborty, M. K. Srinivasu, et al. "A stability-indicating HPLC assay method for docetaxel." Journal of Pharmaceutical and Biomedical Analysis 41, no. 2 (2006): 676–81. http://dx.doi.org/10.1016/j.jpba.2006.01.011.

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14

Hou, Shuguang, Michael Hindle, and Peter R. Byron. "A stability-indicating HPLC assay method for budesonide." Journal of Pharmaceutical and Biomedical Analysis 24, no. 3 (2001): 371–80. http://dx.doi.org/10.1016/s0731-7085(00)00424-6.

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15

Prabhu, Chitra, Ganesa Subramanian, Arumugam Karthik, Suvarna Kini, Mallayasamy Rajan, and Nayanabhirama Udupa. "Determination of telmisartan by HPTLC — A stability indicating assay." Journal of Planar Chromatography – Modern TLC 20, no. 6 (2007): 477–81. http://dx.doi.org/10.1556/jpc.20.2007.6.14.

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16

Hoyer, G. L., J. Ledoux, and P. E. Nolan. "A Sensitive Stability Indicating Assay for the H2Blocker Ranitidine." Journal of Liquid Chromatography 18, no. 6 (1995): 1239–49. http://dx.doi.org/10.1080/10826079508009288.

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17

Radwan, Mahasen A. "Stability - Indicating Hplc Assay of Zidovudine in Extemporaneous Syrup." Analytical Letters 27, no. 6 (1994): 1159–64. http://dx.doi.org/10.1080/00032719408000286.

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18

Saravanan, G., M. V. Suryanarayana, M. J. Jadhav, M. Ravikumar, N. Someswararao, and P. V. R. Acharyulu. "A Stability-Indicating LC Assay Method for Pemetrexed Disodium." Chromatographia 66, no. 5-6 (2007): 431–34. http://dx.doi.org/10.1365/s10337-007-0309-4.

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19

Bakshi, Monika, and Saranjit Singh. "Development of validated stability-indicating assay methods—critical review." Journal of Pharmaceutical and Biomedical Analysis 28, no. 6 (2002): 1011–40. http://dx.doi.org/10.1016/s0731-7085(02)00047-x.

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20

Naik, CN Prathyusha, and KB Chandra Sekhar. "Reliable and Sensitive Stability Indicating Assay Method of Armodafinil." Journal of Young Pharmacists 10, no. 1 (2018): 52–56. http://dx.doi.org/10.5530/jyp.2018.10.13.

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21

Shahjahan, M., and R. P. Enever. "A stability-indicating assay for nitrofurazone by paper chromatography." International Journal of Pharmaceutics 82, no. 3 (1992): 215–21. http://dx.doi.org/10.1016/0378-5173(92)90177-4.

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22

Kaushal, Gagan, Million Woldemariam, Brian E. Sayre, and Terrence Prettyman. "STABILITY OF FAMOTIDINE IN POLYPROPYLENE SYRINGES USING A STABILITY-INDICATING HPLC ASSAY." Journal of Liquid Chromatography & Related Technologies 34, no. 14 (2011): 1283–94. http://dx.doi.org/10.1080/10826076.2011.565538.

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23

Cheung, Andrew P., Elaine Struble, Namphuong Nguyen, and Paul Liu. "Stability-indicating HPLC assay and solution stability of a new diaziridinyl benzoquinone." Journal of Pharmaceutical and Biomedical Analysis 24, no. 5-6 (2001): 957–66. http://dx.doi.org/10.1016/s0731-7085(00)00566-5.

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24

Jaya, P. Ambhore, S. Adhao Vaibhav, S. Cheke Rameshwar, R. Popat Ritesh, and J. Gandhi Shital. "Futuristic review on progress in force degradation studies and stability indicating assay method for some antiviral drugs." GSC Biological and Pharmaceutical Sciences 16, no. 1 (2021): 133–49. https://doi.org/10.5281/zenodo.5168617.

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Force degradation studies of drug substance give perceptive knowledge about the intrinsic stability of the molecule as well as possible degradants which formed during the shelf life of drug and thus, aid within the successive development of its stable formulation. A number of analytical methods with hyphenated techniques are required for the identification, determination and characterization of degraded product and impurities produce during different conditions of stress studies; Chromatographic methodology play a vital role in the field of impurity and degradation profiling .This review summa

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25

Alam, Prawez, Faiyaz Shakeel, Wael A. Mahdi, et al. "Determination of Gefitinib Using Routine and Greener Stability-Indicating HPTLC Methods: A Comparative Evaluation of Validation Parameters." Processes 10, no. 4 (2022): 762. http://dx.doi.org/10.3390/pr10040762.

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“High-performance thin-layer chromatography (HPTLC)” methods for gefitinib (GFT) estimation are scarce in the literature. In addition, greener analytical techniques for GFT estimation are also lacking in the literature. Accordingly, an attempt was undertaken to invent and validate a sensitive and greener normal-phase HPTLC method for GFT analysis in commercial tablets in comparison to the routine normal-phase HPTLC method. The greenness index for both methods was assessed using “Analytical GREENness (AGREE)” methodology. GFT detection was carried out using both methods at 332.0 nm. In the 30–7

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26

Sinha, VR, RV Kumar, and JR Bhinge. "A stability-indicating RP-HPLC assay method for 5-fluorouracil." Indian Journal of Pharmaceutical Sciences 71, no. 6 (2009): 630. http://dx.doi.org/10.4103/0250-474x.59544.

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27

Tenjarla, S. N., and D. S.-L. Chow. "Stability Indicating HPLC Assay of Propranolol for Transdermal Permeation Study." Journal of Liquid Chromatography 16, no. 13 (1993): 2899–913. http://dx.doi.org/10.1080/10826079308019622.

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28

Barrett, David A., and P. Nicholas Shaw. "A Stability Indicating HPLC Assay for Diamorphine in Aqueous Solution." Journal of Liquid Chromatography 17, no. 17 (1994): 3727–33. http://dx.doi.org/10.1080/10826079408013988.

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29

Junnarkar, G., and S. Stavchansky. "Thermal Degradation of Famotidine in Aqueous Solution Stability Indicating Assay." Analytical Letters 25, no. 10 (1992): 1907–13. http://dx.doi.org/10.1080/00032719208018261.

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30

Srinivasan, V., H. Sivaramakrishnan, and B. Karthikeyan. "Stability-Indicating RP-HPLC Method for Assay of Silver Lactate." E-Journal of Chemistry 8, no. 2 (2011): 483–90. http://dx.doi.org/10.1155/2011/234640.

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A simple, economic and time-efficient stability-indicating, reverse-phase high-performance liquid chromatographic (RP-HPLC) method has been developed for analysis of silver lactate in the presence of degradation products generated by decomposition. When silver lactate was subjected to acid hydrolysis, base hydrolysis, oxidative, photolytic, humidity and thermal stress, degradation was observed during base hydrolysis, oxidation, humidity and thermal stress. The drug was found to be stable to other stress conditions. Successful chromatographic condition of the drug from the degradation products

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31

Saravanan, G., M. V. Suryanarayana, N. Balaji, N. Someswararao, and N. M. Sekhar. "A Stability-Indicating LC Method for Assay of Topotecan Hydrochloride." Chromatographia 67, no. 1-2 (2007): 179–82. http://dx.doi.org/10.1365/s10337-007-0468-3.

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32

Raju, T. Satyanarayana, K. S. V. Raghavachary, A. Raghupathi Reddy, M. Satish Varma, M. Ravikumar, and P. Yadagiri Swamy. "A Validated and Stability-Indicating LC Assay Method for Valdecoxib." Chromatographia 69, no. 5-6 (2009): 507–11. http://dx.doi.org/10.1365/s10337-008-0933-7.

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33

Khedr, A., and A. Sakr. "Stability-Indicating High-Performance Liquid Chromatographic Assay of Buspirone HCI." Journal of Chromatographic Science 37, no. 12 (1999): 462–68. http://dx.doi.org/10.1093/chromsci/37.12.462.

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34

Vaucher, Lauren C., Clésio S. Paim, Alini D. Lange, and Elfrides E. S. Schapoval. "LC method for telithromycin in tablets: A stability-indicating assay." International Journal of Pharmaceutics 366, no. 1-2 (2009): 82–87. http://dx.doi.org/10.1016/j.ijpharm.2008.09.010.

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35

Basavaiah, K., and N. Swamy. "Stability-Indicating UV-Spectrophotometric Assay of Diethylcarbamazine Citrate in Pharmaceuticals." Pharmaceutical Chemistry Journal 52, no. 3 (2018): 271–77. http://dx.doi.org/10.1007/s11094-018-1805-6.

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36

Khanvilkar, Vineeta. "Stability indicating assay method for estimation of Empagliflozin using HPTLC." Journal of Medical Pharmaceutical and Allied Sciences 14, no. 1 (2025): 7017–23. https://doi.org/10.55522/jmpas.v14i1.6782.

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A planer chromatographic method capable of indicating the stability of the empagliflozin was developed and validated. Separations were achieved on the silica gel 60F254 as the planar stationary phase and a solvent mixture comprising of Chloroform, Toluene, Methyl alcohol, and Methanolic acid mixed in a proportion of 8:4:2:0.1 v/v/v/v. Examination of the band developed for empagliflozin indicated a densito metric value with an retardation factor of 0.33±0.02. The calibration data analysis through linear regression showed a statistically significant correlation (R2 > 0.990) between peak area

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37

Kombath, Sonoube, Issa-Bella Balde, Sandra Carret, et al. "Stability-Indicating HPLC Assay for Determination of Idebenone in Pharmaceutical Forms." Journal of Analytical Methods in Chemistry 2015 (2015): 1–5. http://dx.doi.org/10.1155/2015/835986.

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A stability-indicating method was validated for the determination in pharmaceutical forms of idebenone a coenzyme Q10-like compound. The assay was achieved by liquid chromatography analysis using a reversed-phase C18 column and a detector set at 480 nm. The optimized mobile phase consisted of isocratic flow rate at 1.0 mL/min for 3 min with methanol. The linearity of the assay was demonstrated in the range of 3.0 to 8.0 mg/mL with a correlation coefficientr2>0.998. The limits of detection and quantification were 0.03 and 0.05 mg/mL, respectively. The intraday and interday precisions were le

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38

Alam, Prawez, Faiyaz Shakeel, Mohammed H. Alqarni, et al. "Determination of Cordycepin Using a Stability-Indicating Greener HPTLC Method." Separations 10, no. 1 (2023): 38. http://dx.doi.org/10.3390/separations10010038.

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A wide range of analytical techniques have been reported to determine cordycepin (CDN) in various sample matrices. Nevertheless, greener analytical approaches for CDN estimation are scarce in the literature. As a result, this study was designed to develop and validate a stability-indicating greener “high-performance thin-layer chromatography (HPTLC)” technique for CDN determination in a laboratory-developed formulation. The greener eluent system for CDN detection was ethanol–water (75:25 v/v). At a wavelength of 262 nm, CDN was measured. The greenness scale of the proposed analytical technolog

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39

R., Sairam Aditya, Tengli Anandkumar, Ramesha, S. Chandan R., Anupama K., and M. Gurupadayya B. "Development and Validation of Stability Indicating UFLC Method for the Estimation of Anti-spasmodic Drug - Valethamate Bromide." Journal of Advances in Medical and Pharmaceutical Sciences 13, no. 3 (2017): 1–12. https://doi.org/10.9734/JAMPS/2017/26825.

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A stability indicating Ultra-Fast Liquid Chromatography (UFLC) method has been developed to estimate valethamate bromide (V&B) in tablet dosage forms and to separate analyte from other degradants and to carryout forced degradation studies. The chromatographic separation was achieved by using phenomenex kinetex 5 μ C<sub>18</sub> 100A (250x 4.6 mm) column with a flow rate of 1 mL/min in an isocratic mode with the mobile phase consisting of 0.05 M potassium dihydrogen phosphate buffer pH 7.5 (adjusted with potassium hydroxide) and acetonitrile in the ratio of 50:50. The eluents were monitore

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40

Ahmad, Iqbal, Syed Haider Abbas, Zubair Anwar, et al. "Stability-Indicating Photochemical Method for the Assay of Riboflavin: Lumichrome Method." Journal of Chemistry 2015 (2015): 1–8. http://dx.doi.org/10.1155/2015/256087.

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A stability-indicating photochemical method for the assay of riboflavin (RF) in photodegraded samples and aged vitamin preparations has been developed. It is based on photochemical conversion of RF to lumichrome (LC) in alkaline solution under controlled conditions of light intensity, temperature, pH, time of exposure, and distance. Under these conditions about two-thirds of RF is converted to LC and on the basis of the RF : LC ratio the concentration of RF can be determined in degraded solutions. The method involves the extraction of photolyzed solutions of RF (pH 2.0) with chloroform and det

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41

Khedr, A., and I. Darwish. "A validated stability-indicating high performance liquid chromatographic assay of amoxicillin." Bulletin of Pharmaceutical Sciences. Assiut 23, no. 1 (2000): 11–21. http://dx.doi.org/10.21608/bfsa.2000.65971.

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42

Jain, Hemant K., and Vishal K. Nikam. "FORMULATION DEVELOPMENT AND STABILITY INDICATING HPLC ASSAY OF TABLETS OF APIXABAN." International Journal of Pharmacy and Pharmaceutical Sciences 9, no. 10 (2017): 24. http://dx.doi.org/10.22159/ijpps.2017v9i10.20343.

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Objective: Cost effective formulation development and stability indicating HPLC method for estimation of apixaban in bulk and tablets dosage form.Methods: 32 factorial design was applied to formulate the immediate release tablets of apixaban by using direct compression method. The chromatographic separation was performed on Purospher Star RP-18e (5 µm, 250x4, 6 mm) column and a stability indicating assay method was developed by using HPLC. The mobile phase consists of water: acetonitrile (60:40 v/v) was delivered at a flow rate of 1 ml/min and UV detection at 280 nm. The method was validated w

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43

Musharraf, Syed Ghulam, Qamar ul Arfeen, Faraz Ul Haq, Aliya Khatoon, and Rahat Azher Ali. "Stability-Indicating TLC-Densitometric Assay for Methyltestosterone and Quantum Chemical Calculations." Journal of Chromatographic Science 55, no. 9 (2017): 954–60. http://dx.doi.org/10.1093/chromsci/bmx055.

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44

Diksha, Vibhute, Deshpande Anant, Komal Shinde, and Priyanka Wankhede. "Stability Indicating RP-HPLC Method for Posaconazole Assay Using QbD Approach." INTERNATIONAL JOURNAL OF PHARMACEUTICAL QUALITY ASSURANCE 15, no. 03 (2024): 1401–7. http://dx.doi.org/10.25258/ijpqa.15.3.48.

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The development and optimization of analytical techniques utilizing the quality by design methodology is essential in the pharmaceutical industry. This approach helps in the direction of identifying and optimizing critical parameters during drug development and assesses their impact on key quality attributes. A stability-indicating RP-HPLC method was developed for quantifying posaconazole in bulk and tablet forms utilizing the quality-by-design approach. The Box-Behnken design optimized buffer flow rate, organic modifier percentage, and temperature, affecting retention time, theoretical plate

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45

Deore, Sharada L., Minal A. Mohod, Bhushan A. Baviskar, and Somshekhar S. Khadabadi. "HPTLC validated stability indicating assay method for marketed herbal antihypertensive formulations." Pharmaceutical Methods 4, no. 1 (2013): 11–15. http://dx.doi.org/10.1016/j.phme.2013.06.001.

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46

He, Jingyi, Andrew P. Cheung, Euphemia Wang, et al. "Stability-indicating LC assay of and impurity identification in homoharringtonine samples." Journal of Pharmaceutical and Biomedical Analysis 22, no. 3 (2000): 541–54. http://dx.doi.org/10.1016/s0731-7085(99)00314-3.

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47

Walash, Mohamed I., Fathalla Belal, Nahed El-Enany, Manal Eid, and Rania N. El-Shaheny. "Stability-Indicating Spectrofluorimetric Method for the Assay of Ziprasidone in Capsules." Journal of Fluorescence 21, no. 4 (2011): 1659–67. http://dx.doi.org/10.1007/s10895-011-0855-x.

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48

Driouich, R., H. Trabelsi, and K. A. Bouzouita. "Stability—Indicating assay for haloperidol syrup by high-performance liquid chromatography." Chromatographia 53, no. 11-12 (2001): 629–34. http://dx.doi.org/10.1007/bf02493010.

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49

Vinay, K., H. Revanasiddappa, M. Cijo, P. Ramesh, N. Swamy, and N. Rajendraprasad. "Stability indicating ultra performance liquid chromatographic assay of lomotrigine in pharmaceuticals." Trakia Journal of Science 13, no. 1 (2015): 1–11. http://dx.doi.org/10.15547/tjs.2015.01.001.

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50

Ezhava, Sindhu, Shaival Shah, Arpit Patwari, and Mahesh Chhabria. "Development and validation of a stability-indicating assay method for naftopidil." JPC - Journal of Planar Chromatography - Modern TLC 29, no. 3 (2016): 195–202. http://dx.doi.org/10.1556/1006.2016.29.3.5.

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