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1

Sutijan, S., Arief Budiman, and Arie Yohanes. "Pengaruh perlakuan daun dan suhu terhadap waktu distilasi pada isolasi minyak cengkeh menggunakan super-steam distillation." Jurnal Teknik Kimia Indonesia 8, no. 2 (2018): 69. http://dx.doi.org/10.5614/jtki.2009.8.2.6.

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The effects of leaves treatment and temperature to distillation times in clove oil isolation using super steam distillation Clove oil was generally obtained from clove leaves by using steam distillation. Distillation time was the most important factors in steam distillation as it was proportional to energy cost. In this work, the use of high boiling compound to accelerate steam distillation was studied in which steam distillation was conducted using temperature greater than 100oC. High temperature saturated steam could be obtained by boiling glycerol–water mixture. Glycerol was selected due to
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Soekarno, Siswoyo, Setyawan Dwi Hernanto, Dian Purbasari, and Dewi Melani. "Study of Distillation Method and Time on the Quality of Basil (Ocimum sanctum L.) Essential Oil." Jurnal Teknik Pertanian Lampung (Journal of Agricultural Engineering) 13, no. 2 (2024): 606. http://dx.doi.org/10.23960/jtep-l.v13i2.606-614.

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"Basil" or basil has economic value both in fresh form, simplicia and essential oil. This research aims to evaluate the method and duration of distillation in making essential oil from basil. Two distillation methods, namely steam and boil distillation, are carried out with different distillation times (1 hour, 2 hours, and 3 hours). The parameters observed were physical characteristics which included oil volume, yield, pH, distillation rate, color, aroma and spots. The results show that the best distillation process time is 2 h for both distillation methods. Steam distillation for 2 hours pro
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3

Padilla-de la Rosa, José Daniel, Magaly Dyanira Manzano-Alfaro, Jaime Rosalío Gómez-Huerta, et al. "Innovation in a Continuous System of Distillation by Steam to Obtain Essential Oil from Persian Lime Juice (Citrus latifolia Tanaka)." Molecules 26, no. 14 (2021): 4172. http://dx.doi.org/10.3390/molecules26144172.

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The citrus industry is one of the most important economic areas within the global agricultural sector. Persian lime is commonly used to produce lime juice and essential oil, which are usually obtained by batch distillation. The aim of this work was to validate a patented continuous steam distillation process and to both physically and chemically characterize the volatile fractions of essential Persian lime oil. Prior to distillation, lime juice was obtained by pressing the lime fruit. Afterwards, the juice was subjected to a continuous steam distillation process by varying the ratio of distill
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Ayub, Muhammad Adnan, Gulden Goksen, Ambreen Fatima, Muhammad Zubair, Muhammad Amin Abid, and Małgorzata Starowicz. "Comparison of Conventional Extraction Techniques with Superheated Steam Distillation on Chemical Characterization and Biological Activities of Syzygium aromaticum L. Essential Oil." Separations 10, no. 1 (2023): 27. http://dx.doi.org/10.3390/separations10010027.

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Syzygium aromaticum L. is an aromatic plant with a significant amount of essential oil (EO), which is used in food, medicine, for flavoring, and in the fragrance industry. The purpose of this study was to comparatively evaluate the chemical composition, yield, and antioxidant and antifungal activities of Syzygium aromaticum essential oils extracted by the conventional hydro-distillation, steam distillation, and the emerging superheated steam distillation methods. It was noticed that the extraction methods significantly influenced the yield, chemical composition, and antioxidant and antimicrobi
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5

Paluch, Justyna, Joanna Kozak, Karolina Mermer, et al. "Novel Integrated Flow-Based Steam Distillation and Titration System for Determination of Volatile Acidity in Wines." Molecules 26, no. 24 (2021): 7673. http://dx.doi.org/10.3390/molecules26247673.

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Novel integrated flow-based steam distillation and titration system with spectrophotometric detection was developed for determination of volatile acidity in wines. Using the system, the distillation procedure was carried out in an automatic manner, starting with introducing into a heated steam distillation module a sample and subjecting it to steam distillation. Under selected conditions, all the analyte was transferred to the distillate; therefore, the system did not require calibration. The collected distillate and titrant were introduced into the next monosegments in varying proportions, in
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6

Arliani, R., I. Machdar, N. S. Kurnia, A. Bakar, and Husni. "Extraction of patchouli essential oil using multi-injection steam distillation." IOP Conference Series: Earth and Environmental Science 1356, no. 1 (2024): 012013. http://dx.doi.org/10.1088/1755-1315/1356/1/012013.

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Abstract Patchouli essential oil is typically obtained through traditional batch distillation, a process involving the introduction of a sole stream of steam at the base of the tank or column, followed by the condensation of the resulting vapor at the top of the tank. In a quest to explore the impact of the multiple injection steam method on both the yield and quality of the oil product, a comparison with the conventional single injection steam approach was conducted. The research variables encompassed different steam valve openings. The findings revealed that the steam valve openings indeed p
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7

Charles, Denys J., and James E. Simon. "Comparison of Extraction Methods for the Rapid Determination of Essential Oil Content and Composition of Basil." Journal of the American Society for Horticultural Science 115, no. 3 (1990): 458–62. http://dx.doi.org/10.21273/jashs.115.3.458.

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Essential oils were extracted from leaves, flowers, and stems of Ocimum basilicurn, O. kilimandscharicum, and O. micranthum by solvent extraction, hydrodistillation, and steam distillation for essential oil content and the oil analyzed by GC and GC/MS for composition. While the yield of essential oil was consistently higher from steam distillation than hydrodistillation, a similar number of compounds was recovered from both hydrodistillation and steam distillation. Though the relative concentration of the major constituents was similar by both methods, the absolute amounts were higher with ste
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8

Lubis, F. I., G. I. S. Putra, I. Mailisa, et al. "Comparative study of maceration and steam distilation extraction methods of volatile organic compounds composition from female oil palm inflorescences." IOP Conference Series: Earth and Environmental Science 1208, no. 1 (2023): 012035. http://dx.doi.org/10.1088/1755-1315/1208/1/012035.

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Abstract Secondary metabolites of oil palm have various potentials. Research on the secondary metabolite of oil palms inflorescences very limited. The purpose of this research is to compare the extraction method between maceration and steam distillation of oil palm female inflorescence’s volatile organic compounds (VOCs). The maceration used ethanolic for 5 × 24 hours, then concentrated with a rotary evaporator. Steam distillation was carried out at a temperature of >80 °C for 4 hours. The extraction results were analyzed by Gas Chromatography-Mas Spectrometry (GC-MS). VOCs found from macer
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9

Rocha-Uribe, J. A., V. M. Sandoval-Peraza, M. A. Flores Córdova, and Laura Catalina Soto Armenta. "Comparison of the composition and cost estimation of steam distillation and supercritical fluid extraction from leaves of Lippia graveolens." Latin American Applied Research - An international journal 54, no. 2 (2024): 271–76. http://dx.doi.org/10.52292/j.laar.2024.3107.

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Lippia graveolens, mostly known as Mexican oregano, is an aromatic plant with great economic im-portance. However, very little is known about the reasons that could explain the variation observed with respect to the yield and composition of the essential oil obtained. The effect of steam distillation and supercritical fluid extraction processes on composition, yield and economic viability were evaluated. The essential oil was obtained by steam distillation, with a laboratory scale equipment and supercritical extraction equipment with a 1L capacity cell. The extracts were analyzed by GC–MS. whe
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10

Lane, R. K., P. D. Provence, M. W. Adkins, and E. J. Eisenbraun. "Laboratory steam distillation using electrically generated superheated steam." Journal of Chemical Education 64, no. 4 (1987): 373. http://dx.doi.org/10.1021/ed064p373.

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11

Chilev, Chavdar, and Dimitar Peshev. "HYDRO-DISTILLATION VERSUS STEAM DISTILLATION FOR CLOVE OIL PRODUCTION." Journal of Chemical Technology and Metallurgy 60, no. 2 (2025): 311–18. https://doi.org/10.59957/jctm.v60.i2.2025.13.

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The production of clove essential oil by hydro distillation and steam distillation has been experimentally investigated. The density of the oil was determined to be ρ ≈ 1.0648 g cm-3. By means of hydro-distillation, a higher yield of 9.714 mass % was obtained compared to the steam distillation - 4.986 mass %. This is due to the formation of a hard-to-break emulsion in the distillate when using the steam distillation technique. Liquid-liquid extraction and gravity sedimentation were independently applied for the aim of separating the essential oil from the obtained distillate. The obtained yiel
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12

Widayat, Widayat, Ayu Sofiati Dita, Cahyono Bambang, and Satriadi Hantoro. "Study of Rendement of Red Ginger Essential Oil from Red Ginger Waste by Using Steam Distillation Process." E3S Web of Conferences 73 (2018): 07002. http://dx.doi.org/10.1051/e3sconf/20187307002.

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This study aims to determine the value of rendement of red ginger essential oil from red ginger waste that has been dried through the steam distillation process. Red ginger waste from fresh red ginger that has been taken the juice then dried with the help of sunlight for 1,2,3 and 4 days. The dried red ginger waste then subjected to steam distillation for 3 and 7 hours to determine the rendement of the red ginger essential oil produced. Based on the study, the rendement of each essential oil on 3 hours distillation time were 0.2%; 0.6%; 1%; and 0.8%, while at 7 hours distillation time the rend
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13

Herdhiansyah, Dhian, Subhan, La Rianda, and Asriani. "Kajian Pengolahan Nilam (Patchouli) Menggunakan Metode Penyulingan Uap di Kecamatan Poleang Utara Kabupaten Bombana." JURNAL AGROINDUSTRI HALAL 9, no. 3 (2023): 355–64. http://dx.doi.org/10.30997/jah.v9i3.6404.

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This study examines the processing of patchouli oil using the steam distillation method in North Poleang District, Bombana Regency. Data collection methods: (a) observation; (b) interviews); (c) questionnaires; and (d) documentation. The method in this study is to describe the processing of patchouli oil using the steam distillation method. The results showed the processing of patchouli oil using the steam distillation method in North Poleang District, Bombana Regency. Distilleries are used with water and steam distillation systems. Distil water and steam through a kettle filled with water to
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14

Sumalyani, Aisyah, Sholeh Ma'mun, and Riyanto Riyanto. "Zodia (Evodia suaveolens) Leaves as Natural Mosquito Repellent Material: Effectiveness Test of Distillation Methods." BERKALA SAINSTEK 12, no. 4 (2024): 149. https://doi.org/10.19184/bst.v12i4.53351.

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Indonesia has around 40 types of plants with essential oil content from a total of around 150 types of essential oils traded in the international market. Essential oils are produced from various parts of aromatic plants such as fruits, seeds, leaves, flowers, roots, stems, bark, and even the entire tree. One of the plants that contains and has the potential to produce essential oils is the zodia (Evodia suaveolens), especially the leaves. Evodone is one of the active compounds contained in the essential oil of zodia leaves which has the ability as a mosquito repellent. This study aims to deter
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15

Bouxin, Florent P., James H. Clark, Jiajun Fan, and Vitaliy Budarin. "Combining steam distillation with microwave-assisted pyrolysis to maximise direct production of levoglucosenone from agricultural wastes." Green Chemistry 21, no. 6 (2019): 1282–91. http://dx.doi.org/10.1039/c8gc02994f.

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The favourable impact of using a wet waste stream of agricultural residues in a biorefinery was studied through a combination of pyrolysis and self-induced steam distillation of hemicellulose depleted barley straw.
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16

Richardson, W. C., M. K. Beladi, and C. H. Wu. "Steam Distillation Studies for the Kern River Field." SPE Reservoir Evaluation & Engineering 3, no. 01 (2000): 13–22. http://dx.doi.org/10.2118/60909-pa.

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Summary The interactions of heavy oil and injected steam in the mature steamflood at the Kern River Field have been extensively studied to gain insight into the effect of steam on compositional changes of oil during the recovery process and to provide input for compositional thermal simulation. Steam distillation behavior of this 13°API California oil between 300 and 467°F under a variety of process conditions, along with extensive analysis of distilled hydrocarbons were incorporated to give a more in-depth description of what is happening to the oil and what changes are occurring in the disti
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17

Dewi, Luthfi Kurnia, Dwi Lerian Friatnasary, Windhi Herawati, Vivi Nurhadianty, and Chandrawati Cahyani. "Comparative Study of Isolation Methods of Solvent Extraction and Steam Distillation of Basil Essential Oil on the Composition of Active Compounds." Rekayasa Bahan Alam dan Energi Berkelanjutan 2, no. 1 (2018): 13–19. http://dx.doi.org/10.21776/ub.rbaet.2018.002.01.03.

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Basil plants has potential as one source of essential oil applied in the flavor and fragrance industries. The isolation can be carried out by two methods, steam distillation and solvent extraction. This study analyzes the comparison of steam distillation and solvent extraction methods on the result of compound composition. The steam distillation process was performed for 4 hours, 6 hours, and 8 hours. Distillate was separated between the crude essential oil and water layer. The extraction process was performed for 6 cycles using n-hexane and ethanol as the solvent. The extract was separated be
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18

Ali, Imran. "A Compact Steam Distillation Apparatus." Journal of Chemical Education 73, no. 3 (1996): 285. http://dx.doi.org/10.1021/ed073p285.

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19

Nino, Jefrianus, Maria Magdalena Endah Mulat Satmalawati, Marsianus Fallo, and Faustinus Kadha. "Guidance for Increases Production Capacity of Citronella Oil Gema Industri Farmers Group." SERVIRE: Jurnal Pengabdian Kepada Masyarakat 5, no. 1 (2025): 15–29. https://doi.org/10.46362/servire.v5i1.278.

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Lemongrass (Cymbopogon nardus. L) is a type of essential oil plant whose essential oil is obtained from the leaves and stems of lemongrass. Lemongrass is classified as a medicinal plant with active compounds that can be used as medicine. The lemongrass oil distillation technique carried out by the Gema Industri farmer group uses the water distillation method. The water distillation method carried out by the Gema Industri farmer group using iron drums can affect the quality of the lemongrass oil produced. An inefficient cooling system (condenser) causes product loss because the components of le
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20

MAK, William Chi Keung. "Comparisons between Hydro and Steam Distillation Processes to Extract Prunella Vulgaris Volatile Compounds, and their Anti-oxidative Activities." Journal of Drug Delivery and Therapeutics 13, no. 3 (2023): 51–57. http://dx.doi.org/10.22270/jddt.v13i3.5955.

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Objective The aim is to verify our earlier suggestion which accounted for the dynamics of volatile compounds extraction from the herb Prunella vulgaris (PV) using steam distillation. Then, the anti-oxidative property of PV is explored.
 Methods Because we suggested earlier that the inefficient extraction using steam distillation was due to the obstruction of a mass of herb in the steam flow path, we used hydro distillation which tried to eliminate this obstacle. We used GC-MS to characterize the volatile compounds extracted, and thus compare the extraction efficiency. Then, treating the c
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Gujarathi, D. B., and N. T. Ilay. "Continuous Water Circulation Distillation: A Modification of Steam Distillation." Journal of Chemical Education 70, no. 1 (1993): 86. http://dx.doi.org/10.1021/ed070p86.

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22

Sani, Inuwa Lamido, Aliyu Abba Bashir, and Ibrahim Muazu. "Essential oil extraction from lemongrass using steam and hydro distillation from a locally fabricated extractor." Global Journal of Engineering and Technology Advances 21, no. 1 (2024): 190–96. https://doi.org/10.5281/zenodo.14922611.

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This study compares the chemical composition of lemongrass essential oil extracted through two distillation methods: steam distillation and hydrodistillation, using Gas Chromatography-Mass Spectrometry (GC-MS) analysis. The results reveal significant differences in the relative abundance and types of compounds present in the oils obtained by each method. Hydrodistillation yielded a higher concentration of Geranial Citral (43.50%), the primary lemon-scented component, compared to steam distillation (20.24%), making it more suitable for applications in perfumery and aromatherapy where a natural
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Sani Inuwa Lamido, Bashir Aliyu Abba, and Muazu Ibrahim. "Essential oil extraction from lemongrass using steam and hydro distillation from a locally fabricated extractor." Global Journal of Engineering and Technology Advances 21, no. 1 (2024): 190–96. http://dx.doi.org/10.30574/gjeta.2024.21.1.0198.

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This study compares the chemical composition of lemongrass essential oil extracted through two distillation methods: steam distillation and hydrodistillation, using Gas Chromatography-Mass Spectrometry (GC-MS) analysis. The results reveal significant differences in the relative abundance and types of compounds present in the oils obtained by each method. Hydrodistillation yielded a higher concentration of Geranial Citral (43.50%), the primary lemon-scented component, compared to steam distillation (20.24%), making it more suitable for applications in perfumery and aromatherapy where a natural
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Zekovic, Zoran, Dusan Adamovic, Gordana Cetkovic, Marija Radojkovic, and Senka Vidovic. "Essential oil and extract of coriander (Coriandrum sativum L.)." Acta Periodica Technologica, no. 42 (2011): 281–88. http://dx.doi.org/10.2298/apt1142281z.

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Two different methods of coriander (Coriandrum sativum L.) essential oil isolation, steam distillation and extraction by methylene chloride (Soxhlet extraction) were investigated. After the determination of essential oil content in the investigated drug and in dry extract (using steam distillation), qualitative and quantitative composition of obtained essential oils, determined by TLC and GC-MS methods, were compared. The content of linalool was higher (52.4%) in essential oil obtained by coriander steam distillation than that in essential oil separeted from dry extract (42.8%), and, on the ot
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Alkire, Ben H., and James E. Simon. "CONSTRUCTION AND DESIGN OF A PORTABLE STEAM DISTILLATION UNIT FOR ESSENTIAL OIL CROPS." HortScience 25, no. 9 (1990): 1165b—1165. http://dx.doi.org/10.21273/hortsci.25.9.1165b.

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A 500 liter (130 gallon) stainless steel steam distillation unit has been built to extract volatile essential oils from aromatic plants. A 1.5 m × 0.75 m dia. steam vessel (hydrostatically tested @ 125 psi) serves as the distillation tank. Low pressure or high pressure steam is supplied by a diesel fuel fired boiler of 10 horsepower. The steam vessel can hold peppermint from plots of 25 m2 and extract approximately 100 ml of essential oil per distillation. The size of the tub was designed to provide oil in sufficient quantity for industrial evacuation or for pesticide residue analysis. Followi
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Daryasafar, Amin, Arash Ahadi, and Riyaz Kharrat. "Modeling of Steam Distillation Mechanism during Steam Injection Process Using Artificial Intelligence." Scientific World Journal 2014 (2014): 1–8. http://dx.doi.org/10.1155/2014/246589.

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Steam distillation as one of the important mechanisms has a great role in oil recovery in thermal methods and so it is important to simulate this process experimentally and theoretically. In this work, the simulation of steam distillation is performed on sixteen sets of crude oil data found in the literature. Artificial intelligence (AI) tools such as artificial neural network (ANN) and also adaptive neurofuzzy interference system (ANFIS) are used in this study as effective methods to simulate the distillate recoveries of these sets of data. Thirteen sets of data were used to train the models
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Putra, Sandy Buana, Muhammad Rifqy Zamzami, Caecilia Pujiastuti, Nove Kartika Erliyanti, and Renova Panjaitan. "The Comparison between Microwave Steam Distillation and Microwave Steam Diffusion in Extraction of Citronella Oil." Rekayasa Bahan Alam dan Energi Berkelanjutan 8, no. 1 (2024): 30–37. http://dx.doi.org/10.21776/ub.rbaet.2024.008.01.05.

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Citronella essential oil extraction can be settled through various methods. The extraction method used can affect the quantity of the essential oil obtained. The advanced extraction method provides good efficiency and effectiveness. One of the advanced extraction methods is Microwave Assisted Extraction (MAE). The MAE method has many developments, including Microwave Steam Distillation (MSD) and Microwave Steam Diffusion (MSDf). In this research, the MSD and MSDf methods were studied by comparing the products of citronella oil obtained. In addition, the general techniques of MSD and MSDf were
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Gavahian, Mohsen, and Yan-Hwa Chu. "Ohmic accelerated steam distillation of essential oil from lavender in comparison with conventional steam distillation." Innovative Food Science & Emerging Technologies 50 (December 2018): 34–41. http://dx.doi.org/10.1016/j.ifset.2018.10.006.

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Galiga, Henley. "Development of an improvised convertible distillation apparatus for teaching and learning chemistry." Palawan Scientist 11 (July 2019): 65–84. http://dx.doi.org/10.69721/tps.j.2019.11.1.06.

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Distillation is an important concept in chemistry as it involves separation techniques which are widely used in various industries. However, despite its significance, it is hardly understood and appreciated because it is rarely performed in laboratory experiments. Distillation requires expensive apparatus to conduct which most schools cannot afford. Hence, an improvised convertible distillation apparatus for simple, fractional and steam distillation was developed using common household and recyclable materials. Improvised measuring devices were also fabricated to determine the purity of the di
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Yang, Guo En, Gui Wu Wang, Zhi Ping Wu, and Xiang Zhou Li. "Study on Steam Extraction Technology Assisted by Microwave of Anise Star Oil from the Fruit of Illicium verum Hook. f." Advanced Materials Research 201-203 (February 2011): 2935–38. http://dx.doi.org/10.4028/www.scientific.net/amr.201-203.2935.

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Evaluated with the yield of anise star oil, steam extraction method assisted by microwave is studied for the extraction of anise star oil from Illicium verum Hook. f. in contrast with the traditional steam distillation (SD) method in this paper. The new optimal steam extraction technology assisted by microwave of anise star oil is obtained as: extracting time 80 minutes, solid-liquid ratio(g/mL) 1:7, size of material 80~100 mesh and extracting temperature 80°C. Average yield of anise star oil is up to 11.6% (g/g) under the above technology. Size of material is the most important influencing fa
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Aayush, Parab, Salgaonkar Kashmira, Padwekar Omkar, and S.J. Purohit Dr. "Extraction and Formulation of Perfume from Lemongrass." International Journal of Environmental & Agriculture Research 6, no. 12 (2020): 26–30. https://doi.org/10.5281/zenodo.4405058.

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<strong>Abstract</strong><strong>&mdash;</strong> Perfume extraction is the extraction of aromatic compounds from raw materials, using methods such as distillation, solvent extraction etc. The extracts are essential oils, absolutes, butters, depending on the amount of waxes in the extracted product. Here, in this work solvent extraction, Enfleurage method, hydrodistillation and steam distillation methods were used to extract essential oil from lemongrass leaves. Distillation based recovery processes such as steam and vacuum distillation are preferred for the extraction of essential oils from p
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Lachenmeier, Dirk W., Leander Plato, Manuela Suessmann, et al. "Improved automatic steam distillation combined with oscillation-type densimetry for determining alcoholic strength in spirits and liqueurs." SpringerPlus 4 (December 18, 2015): 783. https://doi.org/10.1186/s40064-015-1574-6.

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The determination of the alcoholic strength in spirits and liqueurs is required to control the labelling of alcoholic beverages. The reference methodology prescribes a distillation step followed by densimetric measurement. The classic distillation using a Vigreux rectifying column and a West condenser is time consuming and error-prone, especially for liqueurs that may have problems with entrainment and charring. For this reason, this methodology suggests the use of an automated steam distillation device as alternative. The novel instrument comprises an increased steam power, a redesigned geome
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Kurnia, Dewi Luthfi, Vivi Nurhadianty, Chandrawati Cahyani, Riza Ayu Permatasari, and Rizka Amelia Situmorang. "Effect of Steam Distillation Time on Antimicrobial Activity of Kaffir Lime Hydrosol to Gram-Positive and Gram-Negative Bacteria." Research Journal of Chemistry and Environment 27, no. 1 (2022): 60–64. http://dx.doi.org/10.25303/2701rjce060064.

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This study was conducted in order to investigate the antimicrobial activity of kaffir lime hydrosol produced from steam distillation at different times to gram-positive and gram-negative bacteria. The study measured the antimicrobial activity of kaffir lime hydrosol produced from steam distillation at different times against S. aureus (gram-positive) and E. coli (gram-negative) bacteria. Hydrosols were obtained from steam distillation time of 4, 6 and 8 hours. Antimicrobial activity was represented by the clear zone in the disk-diffusion method. The clear zone on the paper disk indicates the d
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Ibrahim, M., G. E. Ankwai, J. R. Gungshik, and P. Taave. "Comparative extraction of essential oils of Mentha piperita (mint) by steam distillation and enfleurage." Nigerian Journal of Chemical Research 26, no. 2 (2022): 56–62. http://dx.doi.org/10.4314/njcr.v26i2.2.

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The extraction of essential oils is generally carried out by two main techniques: azeotropic distillation (hydrodistillation, hydrodiffusion, and steam distillation) and extraction with solvents. This work consists in studying the two methods of extraction of the essential oils of Mentha piperita: Steam distillation (azeotropic) and Enfleurage (solvent extraction). The optimum yield for the extraction of essential oil via steam distillation from Mentha piperita was obtained at 540 minutes with production coming to an end at 1080 minutes yielding 1.36 % of essential oil at 80 0C per 240 g of sa
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Pahua-Angel, Tania, Mirna Estarrón-Espinosa, Eduardo Castaño-Tostado, Edmundo Mateo Mercado-Silva, Silvia Lorena Amaya-Llano, and José Daniel Padilla-de la Rosa. "Innovative Technology of Continuous-Steam Distillation with Packed Column to Obtain Essential Oil-Differentiated Fractions from Mexican Lime (Citrus aurantifolia)." ChemEngineering 8, no. 5 (2024): 88. http://dx.doi.org/10.3390/chemengineering8050088.

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Continuous distillation (CD) by steam is a patented emerging technology that allows us to obtain essential-oil fractions from citrus juices. It presents benefits such as reducing steam consumption by 50%, lowering environmental impact, and, by its design, obtaining fractions enriched in terpenic and oxygenated compounds that can be further processed. The CD of essential oils from Mexican lime juice (Citrus aurantifolia) was studied and the results were compared with conventional steam distillation (batch) in terms of steam consumption, extraction yield, chemical composition, and quality of the
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Carlos Alberto Tosta Machado, Herman Augusto Lepikson, Matheus Antônio Nogueira de Andrade, and Paulo Renato Câmera da Silva. "Essential Oil Steam Distillation: Manufacturing 4.0." JOURNAL OF BIOENGINEERING AND TECHNOLOGY APPLIED TO HEALTH 4, no. 3 (2021): 95–99. http://dx.doi.org/10.34178/jbth.v4i3.170.

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Smart sensors, self-configuration, operational flexibility, and automatic learning, among others, are technological attributes from industry 4.0 appliable to the essential oil extraction by the steam distillation process. These operations are recognized by their simplicity. Nevertheless, lack of automatic controls, process monitoring, and self-adjustment lead to uncontrolled extraction, poor yields, low quality of products. It occurs because of overexposure to high temperatures and overspending resources like energy and water. As far as capacity utilization is concerned, the optimized process
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37

Taber, Douglass F., and Andrew J. Weiss. "Cinnamaldehyde by Steam Distillation of Cinnamon." Journal of Chemical Education 75, no. 5 (1998): 633. http://dx.doi.org/10.1021/ed075p633.

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38

Castrillon, Jose. "Cinnamaldehyde by Steam Distillation of Cinnamon." Journal of Chemical Education 76, no. 3 (1999): 318. http://dx.doi.org/10.1021/ed076p318.1.

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39

Anwar, Zainuri, Ahmad Imam Rifa'i, and Almas Nurzain. "EFFECT OF STEAM PRESSURE AND TEMPERATURE ON THE AMOUNT OF OIL PRODUCED IN A CITRONELLA OIL DISTILLATION MACHINE." T R A K SI 23, no. 2 (2024): 247. https://doi.org/10.26714/traksi.23.2.2023.247-253.

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One of the parameters that affect the citronella oil distillation process is the pressure and temperature of the steam. The aim of this research was to determine the optimal working pressure and temperature for the distillation process. The distillation method uses the direct steam type, by varying the pressure in the boiler, namely 2 bar, 2.5 bar and 3 bar. Steam temperature increases with increasing working pressure, namely 100 - 110ºC. The raw material for citronella used 5 kg with a long distillation process of 4 hours. The test results showed that the highest amount of oil and yield occur
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40

Li, Jian, Shuai Di Song, Ruo Nan Zhang, Ning Liu, and Chen Chen Li. "Chemical Components and Nitrite Cleaning Activity of Essential Oil from Tagetes erecta L. Leaf." Advanced Materials Research 183-185 (January 2011): 1168–72. http://dx.doi.org/10.4028/www.scientific.net/amr.183-185.1168.

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Steam distillation oil (SDO) and simultaneous distillation oil (SDEO) were obtained from Tagetes Erecta L. leaf of Heilongjiang province by steam distillation method and simultaneous distillation method, respectively. The yields were 0.0943% and 1.005%. Compared the differentiation of essential oil through the GC-MS analysis, the result indicated that there were twenty-nine kinds of compounds can be confirmed from SDO and fifty-one kinds can be confirmed from SDEO. The two kinds of essential oil were assayed for affinity to scavenge sodium nitrite for the purpose of characterizing mechanisms o
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Caballero, P., S. F. Villanueva, and B. O. Juliano. "Comparison of Steam and Molecular Distillation Methods in Rice." International Rice Research Newsletter 13, no. 6 (1988): 17–18. https://doi.org/10.5281/zenodo.7146254.

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This article 'Comparison of Steam and Molecular Distillation Methods in Rice' appeared in the International Rice Research Newsletter series, created by the International Rice Research Institute (IRRI). The primary objective of this publication was to expedite communication among scientists concerned with the development of improved technology for rice and for rice based cropping systems. This publication will report what scientists are doing to increase the production of rice in as much as this crop feeds the most densely populated and land scarce nations in the world.
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42

Campbell, Duncan C. "Micro-Kjeldahl Analysis Using 40-Tube Block Digestor and Steam Distillation." Journal of AOAC INTERNATIONAL 69, no. 6 (1986): 1013–16. http://dx.doi.org/10.1093/jaoac/69.6.1013.

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Abstract A steam distillation unit was developed for use with a 40-tube block digestor (25 x 290 mm tubes). Initial digestion for 10 min with sufficient H2SO4 alone avoids frothing. A K2SO4/HgO mixture is then added and the digestion is continued. Use of condenser tubes and a fan to cool condensers and the tops of digestion tubes allows the use of high block temperatures (450°C) and long digestion times (1.5 h) with little loss of acid. The steam distillation unit incorporates a large head which contains the steam/sample solution mixture during distillation. The large distillation head allows
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43

Rzepa, Józef, Mieczysław Sajewicz, Tomasz Baj, et al. "A Comparison of Methodical Approaches to Fingerprinting of the Volatile Fraction from Winter Savory (Satureja montana)." Chromatography Research International 2012 (January 12, 2012): 1–8. http://dx.doi.org/10.1155/2012/596807.

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It was the aim of this study to compare the efficiency of the different essential oil extraction methods upon the two winter savory (Satureja montana) samples of different origin. The compared techniques were the headspace gas chromatography with mass spectrometric detection (HS-GC/MS) run at the two different headspace temperatures (i.e., at 80 and 100°C) and the three different steam distillation techniques preceding the GC/MS analysis. HS-GC/MS is considered as the technique of the first choice, and the compared steam distillation techniques are recommended, respectively, by Polish Pharmaco
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Zheng, Qiang, Hui Qing Liu, Zhan Xi Pang, and Fang Li. "A Study on Effect Evaluating and Parameters Sensitivity Analyzing of Superheated Steam Soak in Heavy Oil Reservoirs." Advanced Materials Research 239-242 (May 2011): 3069–73. http://dx.doi.org/10.4028/www.scientific.net/amr.239-242.3069.

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By using the technology of numerical reservoir simulation, we have compared superheated steam soak with saturated steam soak in area of heating, effect of distillation, capability of increasing oil production, volume of steam in need to evaluate the effect of superheated steam soak in heavy oil reservoirs. Analyzed the sensitivity of parameters like steam injection intensity, steam injection rate, soak time, degree of superheat to conclude the rule that they affect on recovery percentage. The research shows that, heating radius of superheated steam is greater than that of saturated steam, dist
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Petrovic, Lidija, Zika Lepojevic, Verica Sovilj, Dusan Adamovic, and Vele Tesevic. "An investigation of CO2 extraction of marigold (Calendula officinalis L.)." Journal of the Serbian Chemical Society 72, no. 4 (2007): 407–13. http://dx.doi.org/10.2298/jsc0704407p.

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Essential oil content (0.05 %) of marigold (Calendula officinalis L.) was determined using the official steam distillation procedure. High-pressure CO2 extraction of plant material under supercritial (100, 200 and 300 bar and 40?C) and subcritical (60, 90 and 120 bar and 15?C) conditions for 3 h was investigated. It was found that the increase in the pressure promoted an increase in the yield. The essential oil contents obtained from the investigated CO2 extracts by steam distillation were significantly higher (1.52-2.70 times) and increased with pressure. Major constituents of the oil, identi
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Rienoviar, T. Irawadi, D. Setyaningsih, and A. Ismayana. "Distillation Delayed Time on The Characteristics of Lemon Peel Oil and Activity against Staphylococcus aureus." IOP Conference Series: Earth and Environmental Science 950, no. 1 (2022): 012033. http://dx.doi.org/10.1088/1755-1315/950/1/012033.

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Abstract Delay time effect (curing) in lemon peel essential oil extraction often occurs in factories when the number of distillers does not match the amount of available lemon peel. This delay time can reduce the quantity and the lemon peel oil quality due to degradation. This study aimed to determine the delay time period before distillation process that affected changes in the lemon peel oil aromatic compound quantity and quality based on the yield, limonene percentage, and the inhibitory effect of lemon peel oil on Staphylococcus aureus bacterial growth. The distillation method used the coh
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47

Arnau, Pedro, Naeria Navarro, Javier Soraluce, Jose Martínez-Iglesias, Jorge Illas, and Eugenio Oñate. "Cool Steam Method for Desalinating Seawater." Water 11, no. 11 (2019): 2385. http://dx.doi.org/10.3390/w11112385.

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Cool steam is an innovative distillation technology based on low-temperature thermal distillation (LTTD), which allows obtaining fresh water from non-safe water sources with substantially low energy consumption. LTTD consists of distilling at low temperatures by lowering the working pressure and making the most of low-grade heat sources (either natural or artificial) to evaporate water and then condensate it at a cooler heat sink. To perform the process, an external heat source is needed that provides the latent heat of evaporation and a temperature gradient to maintain the distillation cycle.
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Tăbărașu, Ana-Maria, Dragoș-Nicolae Anghelache, Iuliana Găgeanu, Sorin-Ștefan Biriș, and Nicolae-Valentin Vlăduț. "Considerations on the Use of Active Compounds Obtained from Lavender." Sustainability 15, no. 11 (2023): 8879. http://dx.doi.org/10.3390/su15118879.

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Lavender is among the medicinal and aromatic plants with high economic value in the food, pharmaceutical, cosmetic and aromatherapeutic industries, and in its composition has numerous compounds, such as tannins, anthocyanins, minerals, saponins, flavonoids, polyphenols, essential oil and others. The qualitative and quantitative characteristics of lavender are best highlighted by extraction techniques such as hydrodistillation, steam distillation and supercritical CO2 extraction. In the water distillation extraction method, the plants are soaked in water until boiling and steam is released, car
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Katsanidis, Eugenios, and Konstantina Zampouni. "Development of a Novel Steam Distillation TBA Test for the Determination of Lipid Oxidation in Meat Products." Foods 12, no. 2 (2023): 359. http://dx.doi.org/10.3390/foods12020359.

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The 2-thiobarbituric acid (TBA) method has been used for the spectrophotometric determination of secondary lipid oxidation products, such as malonaldehyde (MA), due to its good correlation with sensorial perception of lipid oxidation. Other approaches have been proposed over time. Direct distillation can result in artificially increased MA concentrations due to intense heating. Extraction is a milder and faster method, but it suffers from false color development in the presence of sugars or other compounds. A novel approach using steam distillation for the recovery of MA was developed. Validat
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Hsu, Sheng-Yen, Chan-Chiung Liu, Chia-En Yang, and Lung-Ming Fu. "Multifunctional microchip-based distillation apparatus I - Steam distillation for formaldehyde detection." Analytica Chimica Acta 1062 (July 2019): 94–101. http://dx.doi.org/10.1016/j.aca.2019.02.016.

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