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Journal articles on the topic 'Strecker reaction; Trimethylsilyl cyanide'

Author: Grafiati

Published: 4 June 2021

Last updated: 11 February 2022

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1

Najar, Asef H., Zinatossadat Hossaini, Shahrzad Abdolmohammadi та Daryoush Zareyee. "ZnO-nanorods Promoted Synthesis of α-amino Nitrile Benzofuran Derivatives using One-pot Multicomponent Reaction of Isocyanides". Combinatorial Chemistry & High Throughput Screening 23, № 4 (2020): 345–55. http://dx.doi.org/10.2174/1386207323666200219124625.

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Aims & Objective: In this work ZnO-nanorod (ZnO-NR) as reusable catalyst promoted Strecker-type reaction of 2,4-dihydroxyacetophenone, isopropenylacetylene, trimethylsilyl cyanide (TMSCN), primary amines and isocyanides at ambient temperature under solvent-free conditions and produced α-amino nitriles benzofuran derivatives in high yields. These synthesized compounds may have antioxidant ability. Materials and Methods: ZnO-NRs in these reactions were prepared according to reported article. 2,4-dihydroxyacetophenone 1 (2 mmol) and isopropenylacetylene 2 (2 mmol) were mixed and stirred for 3

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2

Madadi, Elaheh. "Strecker Synthesis of α-aminonitriles Facilitated by N-methyl Imidazolium Acetate". Alinteri Journal of Agriculture Sciences 36, № 1 (2021): 323–27. http://dx.doi.org/10.47059/alinteri/v36i1/ajas21048.

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N-Methyl imidazolium acetate [HMIm]OAc was simply prepared through reaction of N-methyl imidazole with acetic acid and it was applied as a media and promoter for Strecker synthesis of α-aminonitriles. The three component reaction of a variety of structurally different aldehydes and amines with trimethylsilyl cyanide (TMSCN) in the presence of [HMIm]OAc were evaluated. Reaction of aromatic aldehydes and cinnamaldehyde with either aromatic and aliphatic amines provided the corresponding α-aminonitriles in high to excellent isolated yields after short period of time at room temperature.

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3

Zhang, Guang-Wu, Dong-Hua Zheng, Jing Nie, Teng Wang, and Jun-An Ma. "Brønsted acid-catalyzed efficient Strecker reaction of ketones, amines and trimethylsilyl cyanide." Organic & Biomolecular Chemistry 8, no. 6 (2010): 1399. http://dx.doi.org/10.1039/b924272d.

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4

Takahashi, Eiki, Hidehiko Fujisawa, Toshiharu Yanai, and Teruaki Mukaiyama. "Lewis Base-catalyzed Diastereoselective Strecker-type Reaction between Trimethylsilyl Cyanide and Chiral Sulfinimines." Chemistry Letters 34, no. 4 (2005): 604–5. http://dx.doi.org/10.1246/cl.2005.604.

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5

Zhang, Guang-Wu, Dong-Hua Zheng, Jing Nie, Teng Wang, and Jun-An Ma. "ChemInform Abstract: Broensted Acid-Catalyzed Efficient Strecker Reaction of Ketones, Amines and Trimethylsilyl Cyanide." ChemInform 41, no. 31 (2010): no. http://dx.doi.org/10.1002/chin.201031082.

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6

Takahashi, Eiki, Hidehiko Fujisawa, Toshiharu Yanai, and Teruaki Mukaiyama. "Lewis Base-catalyzed Strecker-type Reaction between Trimethylsilyl Cyanide andN-Tosylimines in Water-containing DMF." Chemistry Letters 34, no. 3 (2005): 318–19. http://dx.doi.org/10.1246/cl.2005.318.

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7

Jiao, Zhigang, Xiaoming Feng, Bo Liu, Fuxue Chen, Guolin Zhang, and Yaozhong Jiang. "Enantioselective Strecker Reactions between Aldimines and Trimethylsilyl Cyanide Promoted by ChiralN,N′-Dioxides." European Journal of Organic Chemistry 2003, no. 19 (2003): 3818–26. http://dx.doi.org/10.1002/ejoc.200300319.

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8

Gal, Emese, Luiza Gaina, Hermina Petkes, et al. "Ultrasound-assisted Strecker synthesis of novel 2-(hetero)aryl-2-(arylamino)acetonitrile derivatives." Beilstein Journal of Organic Chemistry 16 (November 30, 2020): 2929–36. http://dx.doi.org/10.3762/bjoc.16.242.

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This work describes an efficient, simple, and ecofriendly sonochemical procedure for the preparation of new α-(arylamino)acetonitrile derivatives C-substituted with phenothiazine or ferrocene units. The synthetic protocol is based on the Strecker reaction of a (hetero)aryl aldimine substrate with trimethylsilyl cyanide (TMSCN) in poly(ethylene glycol) (PEG) solution. The advantages of the sonochemical versus the conventional α-(arylamino)acetonitrile synthesis are the significantly shorter reaction time (30 min instead of 72 hours), the higher purity and the easier separation of the product th

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9

Lu, Yongping, Yanping Wang та Xingxian Zhang. "MgI2 Etherate-Catalysed Strecker Reaction: A Facile and Efficient Synthesis of α-Aminonitriles from Aldimines and Trimethylsilyl Cyanide". Journal of Chemical Research 37, № 11 (2013): 709–11. http://dx.doi.org/10.3184/174751913x13817705381783.

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10

Mojtahedi, Mohammad M., M. Saeed Abaee та Hassan Abbasi. "One-pot, solvent-free synthesis of α-aminonitriles under catalysis by magnesium bromide ethyl etherate". Canadian Journal of Chemistry 84, № 3 (2006): 429–32. http://dx.doi.org/10.1139/v06-024.

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A three-component, efficient, and facile procedure has been developed for the synthesis of α-aminonitriles from aldehydes, amines, and trimethylsilyl cyanide using a catalytic amount of magnesium bromide ethyl etherate in the absence of solvent. Rapid formation of products is observed at room temperature in a one-pot procedure under very mild conditions giving excellent yields of the title compounds.Key words: catalyzed Strecker's reaction, α-aminonitriles, magnesium bromide, solvent-free.

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11

Lu, Yongping, Yanping Wang та Xingxian Zhang. "ChemInform Abstract: MgI2Etherate-Catalyzed Strecker Reaction: A Facile and Efficient Synthesis of α-Aminonitriles from Aldimines and Trimethylsilyl Cyanide." ChemInform 45, № 24 (2014): no. http://dx.doi.org/10.1002/chin.201424083.

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12

Yuan, Xiao-Ming, Jian Xu, Zhen-Jiang Liu та ін. "The Regio-specific solvent controlled asymmetric Strecker reaction of trifluoromethyl α,β-unsaturated N-tert-butanesulfinyl ketimines with trimethylsilyl cyanide". Journal of Fluorine Chemistry 144 (грудень 2012): 102–7. http://dx.doi.org/10.1016/j.jfluchem.2012.07.017.

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13

Li, Nai-Kai, Zhao-Min Liu, Xiao-Fei Huang, et al. "Enantioselective Strecker-type reaction between azomethine imines and trimethylsilyl cyanide catalyzed by a cinchona alkaloid-derived thiourea bearing multiple hydrogen-bonding donors." RSC Advances 3, no. 24 (2013): 9154. http://dx.doi.org/10.1039/c3ra41640b.

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14

Yuan, Xiao-Ming, Jian Xu, Zhen-Jiang Liu та ін. "ChemInform Abstract: The Regio-Specific Solvent Controlled Asymmetric Strecker Reaction of Trifluoromethyl α,β-Unsaturated N-tert-Butanesulfinyl Ketimines with Trimethylsilyl Cyanide." ChemInform 44, № 14 (2013): no. http://dx.doi.org/10.1002/chin.201314030.

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15

Das, Biswanath, Kongara Damodar, Boddu Shashikanth, Yallamalla Srinivas та Itikala Kalavathi. "A Mild and Efficient Catalytic Strecker Reaction of N-Alkoxycarbonylamino Sulfones with Trimethylsilyl Cyanide Using Indium(III) Chloride: A Facile Synthesis of α-Aminonitriles". Synlett 2008, № 20 (2008): 3133–36. http://dx.doi.org/10.1055/s-0028-1087277.

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16

Enders, Dieter, and Michael Moser. "Asymmetric Strecker synthesis by addition of trimethylsilyl cyanide to aldehyde SAMP-hydrazones." Tetrahedron Letters 44, no. 46 (2003): 8479–81. http://dx.doi.org/10.1016/j.tetlet.2003.09.098.

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17

Grundke, Caroline, and Till Opatz. "Strecker reactions with hexacyanoferrates as non-toxic cyanide sources." Green Chemistry 21, no. 9 (2019): 2362–66. http://dx.doi.org/10.1039/c9gc00720b.

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18

Guthrie, J. Peter, and Goonisetty Bhaskar. "The Strecker reaction — an examination in terms of no-barrier theory." Canadian Journal of Chemistry 86, no. 4 (2008): 285–89. http://dx.doi.org/10.1139/v08-014.

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For those examples of the Strecker reaction where information about both rate and equilibrium is available, we have been able to calculate rate constants for the addition of cyanide ion to the iminium ion by the no-barrier theory (NBT) approach. Both experimental and calculated values are for reaction in aqueous solution. Only for the reactions of benzaldehyde with benzyl or allyl amines and HCN are the equilibrium constants and rate constants for the final, rate-determining, step directly available from the literature. For the reactions of acetone with ammonia, methylamine, or dimethylamine a

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19

Carr, Steve A., and William P. Weber. "Zinc Iodide Catalyzed Reaction of Oxetanes With Trimethylsilyl Cyanide." Synthetic Communications 15, no. 9 (1985): 775–81. http://dx.doi.org/10.1080/00397918508063872.

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20

Sander, Michael, and Wolfgang Sundermeyer. "Zur Synthese fluororganischer O-(Trimethylsilyl)-cyanhydrine / Synthesis of Fluoroorganic O-(Trimethylsilyl)Cyanhydrines." Zeitschrift für Naturforschung B 53, no. 3 (1998): 296–306. http://dx.doi.org/10.1515/znb-1998-0308.

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Abstract Fluororganic and/or sterically hindered cyanohydrines are useful synthetic reagents, not readily available directly from e.g. aldehydes or ketones and hydrogen cyanide. By using trimethylsilyl cyanide (TMSCN), the obtained O-Silyl-cyanohydrines can be applied successfully for the same purpose. Selected examples of the type R1R2C-CN(OSiMe3) 1 -12 are presented which prove the extensive applicability of this reaction [R = (fluoro)alkyl, (fluoro)aryl, anthryl, cyclopropyl, CCl3, CBr3 etc.]. Malodinitrile derivatives RC(CN)2OSiMe3 14 were obtained from carboxylic acid chlorides, α-, β- an

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21

Matsumoto, Kiyoshi, Jong Chul Kim, Naoto Hayashi та Gérard Jenner. "High pressure mediated three component Strecker synthesis of α-aminonitriles from ketones, aromatic amines and trimethylsilyl cyanide". Tetrahedron Letters 43, № 50 (2002): 9167–69. http://dx.doi.org/10.1016/s0040-4039(02)02270-0.

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22

Still, Ian W. J., та Wang Daoquan. "THE REACTION OF O-SILYLATED α-KETOLS WITH TRIMETHYLSILYL CYANIDE". Phosphorus, Sulfur, and Silicon and the Related Elements 62, № 1-4 (1991): 83–89. http://dx.doi.org/10.1080/10426509108034462.

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23

Chen, H. G., O. P. Goel, S. Kesten, and J. Knobelsdorf. "A novel modification of the Ritter reaction using trimethylsilyl cyanide." Tetrahedron Letters 37, no. 45 (1996): 8129–32. http://dx.doi.org/10.1016/0040-4039(96)01890-4.

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24

Chatani, Naoto, Takumi Takeyasu, Nobuhiko Horiuchi, and Terukiyo Hanafusa. "Palladium- and nickel-catalyzed reaction of trimethylsilyl cyanide with acetylenes. Addition of trimethylsilyl cyanide to the carbon-carbon triple bonds." Journal of Organic Chemistry 53, no. 15 (1988): 3539–48. http://dx.doi.org/10.1021/jo00250a023.

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25

Ramalingam, Balamurugan, Abdul Majeed Seayad, Li Chuanzhao, et al. "A Remarkable Titanium-Catalyzed Asymmetric Strecker Reaction using Hydrogen Cyanide at Room Temperature." Advanced Synthesis & Catalysis 352, no. 13 (2010): 2153–58. http://dx.doi.org/10.1002/adsc.201000462.

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26

Saravanan, S., Noor-ul H. Khan, Ajay Jakhar, et al. "Enantioselective Strecker reaction of aldimines using potassium cyanide catalyzed by a recyclable macrocyclic V(v) salen complex." RSC Advances 5, no. 121 (2015): 99951–58. http://dx.doi.org/10.1039/c5ra18914d.

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Chiral dimeric V(v) salen complexes have been synthesized and used as catalysts for asymmetric Strecker reaction of N-benzylimines using both KCN to produce chiral α-amino nitrile. The catalyst was recycled upto five times without loss in its activity.

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27

Ruan, Sai, Xia Zhong, Quangang Chen, Xiaoming Feng та Xiaohua Liu. "An asymmetric hydrocyanation/Michael reaction of α-diazoacetates via Cu(i)/chiral guanidine catalysis". Chemical Communications 56, № 14 (2020): 2155–58. http://dx.doi.org/10.1039/c9cc09521g.

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An asymmetric one-pot hydrocyanation/Michael reaction of α-aryl diazoacetates with trimethylsilyl cyanide, tert-butanol, and N-phenylmaleimides has been realized using a chiral guanidinium salt/CuBr catalyst.

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28

Zang, Yong, Shaowei Zhang, Xinliang Fu, Xiaolian Hu, Demin Ren, and Xiaofang Li. "Synthesis of 2-Cyano-3-Nitroporphyrin Derivatives with Silyl Cyanide." Journal of Chemical Research 41, no. 10 (2017): 614–16. http://dx.doi.org/10.3184/174751917x15071160940473.

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2-Cyano-3-nitroporphyrin derivatives were synthesised by the reaction of 2-nitroporphyrin with trimethylsilyl cyanide in the presence of tetrabutylammonium fluoride with moderate yields. The reaction took place regioselectively on the 3-position carbon of the porphyrins, which was confirmed by X-ray analysis.

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29

Fu, Xinliang, Demin Ren, Xiaofang Li, and Xiaolian Hu. "Synthesis of 3-cyano-N-confused porphyrin derivatives by silyl cyanide." Journal of Chemical Research 41, no. 7 (2017): 420–22. http://dx.doi.org/10.3184/174751917x14967701767076.

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3-Cyano- N-confused porphyrin derivatives were synthesised by the reaction of N-confused porphyrin with trimethylsilyl cyanide in the presence of tetrabutylammonium fluoride in moderate yield. The reaction took placed regioselectively in the 3-position carbon of the inverted pyrrole of N-confused porphyrins.

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30

Xue, Hansong, Choon-Hong Tan, and Ming Wah Wong. "Guanidine-catalyzed asymmetric Strecker reaction: modes of activation and origin of stereoselectivity." Canadian Journal of Chemistry 94, no. 12 (2016): 1099–108. http://dx.doi.org/10.1139/cjc-2016-0307.

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Density functional theory calculations were employed to study the catalytic mechanism, modes of activation, and origin of enantioselectivity of guanidine-catalyzed asymmetric Strecker reaction of N-benzhydryl imine with hydrogen cyanide. Two types of bifunctional activation mode were identified, namely conventional bifunctional Brønsted acid activation and unconventional bifunctional Brønsted–Lewis acid activation. The lowest-energy transition states correspond to the conventional bifunctional mode of activation. The calculated enantiomeric excess, based on eight lowest-energy C–C bond forming

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31

Satoh, Yasushi, and Yasushi Obora. "Synthesis of arylacetonitrile derivatives: Ni-catalyzed reaction of benzyl chlorides with trimethylsilyl cyanide under base-free conditions." RSC Adv. 4, no. 30 (2014): 15736–39. http://dx.doi.org/10.1039/c4ra01153h.

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32

CHEN, H. G., O. P. GOEL, S. KESTEN, and J. KNOBELSDORF. "ChemInform Abstract: A Novel Modification of the Ritter Reaction Using Trimethylsilyl Cyanide." ChemInform 28, no. 8 (2010): no. http://dx.doi.org/10.1002/chin.199708088.

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33

STILL, I. W. J., та D. WANG. "ChemInform Abstract: The Reaction of O-Silylated α-Ketols with Trimethylsilyl Cyanide." ChemInform 23, № 1 (2010): no. http://dx.doi.org/10.1002/chin.199201220.

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34

Matveyev, Yu I., S. V. Sereda, and V. I. Gorbatenko. "Reaction of perchloro-3, 5-diazahepta-2, 4-diene with trimethylsilyl cyanide." Tetrahedron Letters 33, no. 15 (1992): 2035–38. http://dx.doi.org/10.1016/0040-4039(92)88134-q.

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35

MATVEYEV, YU I., S. V. SEREDA, and V. I. GORBATENKO. "ChemInform Abstract: Reaction of Perchloro-3,5-diazahepta-2,4-diene with Trimethylsilyl Cyanide." ChemInform 23, no. 42 (2010): no. http://dx.doi.org/10.1002/chin.199242163.

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36

Ramalingam, Balamurugan, Abdul Majeed Seayad, Li Chuanzhao, et al. "ChemInform Abstract: A Remarkable Titanium-Catalyzed Asymmetric Strecker Reaction Using Hydrogen Cyanide at Room Temperature." ChemInform 42, no. 7 (2011): no. http://dx.doi.org/10.1002/chin.201107023.

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37

Yurino, Taiga, Yuji Tange, Ryutaro Tani, and Takeshi Ohkuma. "Ag2O-catalysed nucleophilic isocyanation: selective formation of less-stable benzylic isonitriles." Organic Chemistry Frontiers 7, no. 11 (2020): 1308–13. http://dx.doi.org/10.1039/d0qo00336k.

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Both primary and secondary benzylic isonitriles were exclusively produced by the Ag<sub>2</sub>O-catalysed reaction of benzylic phosphates and trimethylsilyl cyanide without formation of the thermodynamically favoured regioisomers, benzylic nitriles.

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38

Mahmoud, Abdallah G., Kamran T. Mahmudov, M. Fátima C. Guedes da Silva, and Armando J. L. Pombeiro. "Reaction of sodium 2-(2-(2,4-dioxopentan-3-ylidene)hydrazinyl) benzenesulfonate with ethylenediamine on Cu(ii) and Ni(ii) centres: efficient Cu(ii) homogeneous catalysts for cyanosilylation of aldehydes." RSC Advances 6, no. 59 (2016): 54263–69. http://dx.doi.org/10.1039/c6ra12274d.

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Reaction of sodium 2-(2-(2,4-dioxopentan-3-ylidene)hydrazinyl)benzenesulfonate with ethylenediamine on Cu(ii) and Ni(ii) centres lead to variety of metal complexes which effectively catalyse the cyanosilylation of aldehydes with trimethylsilyl cyanide.

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39

ODINETS, I. L., E. A. ANTONOV, P. V. PETROVSKII, et al. "ChemInform Abstract: Reaction of 2-Methyl-2,5-dioxo-1,2-oxaphospholane with Trimethylsilyl Cyanide." ChemInform 25, no. 15 (2010): no. http://dx.doi.org/10.1002/chin.199415225.

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40

Kobayashi, Shu, Yoshikazu Tsuchiya, and Teruaki Mukaiyama. "A Facile Synthesis of Cyanohydrin Trimethylsilyl Ethers by the Addition Reaction of Trimethylsilyl Cyanide with Aldehydes under Basic Condition." Chemistry Letters 20, no. 4 (1991): 537–40. http://dx.doi.org/10.1246/cl.1991.537.

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41

Yurino, Taiga, Takeshi Ohkuma, Hamdiye Ece, and Yuji Tange. "Silyl Cyanopalladate-Catalyzed Friedel–Crafts-Type Cyclization Affording 3-Aryloxindole Derivatives." Synlett 32, no. 09 (2021): 935–39. http://dx.doi.org/10.1055/a-1373-7017.

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Abstract3-Aryloxindole derivatives were synthesized through a Friedel–Crafts-type cyclization. The reaction was catalyzed by a trimethylsilyl tricyanopalladate complex generated in situ from trimethylsilyl cyanide and Pd(OAc)2. Wide varieties of diethyl phosphates derived from N-arylmandelamides were converted almost quantitatively into oxindoles. When N,N-dibenzylamide was used instead of an anilide substrate, a benzo-fused δ-lactam was obtained. An oxindole product was subjected to substitution reactions to afford 3,3-diaryloxindoles with two different aryl groups.

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42

Abdollahi-Alibeik, Mohammad, and Ali Rezaeipoor-Anari. "BF3/MCM-41 as nano structured solid acid catalyst for the synthesis of 3-iminoaryl-imidazo[1,2-a]pyridines." Catal. Sci. Technol. 4, no. 4 (2014): 1151–59. http://dx.doi.org/10.1039/c3cy00947e.

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Multi-component reaction of various types of aldehydes, 2-aminopyridines and trimethylsilyl cyanide was carried out in the presence of MCM-41 supported boron trifluoride (BF<sub>3</sub>/MCM-41) as a nanostructured solid acid catalyst for the synthesis of 3-iminoaryl-imidazo[1,2-a]pyridine derivatives.

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43

Galletti, Paola, Matteo Pori, and Daria Giacomini. "Catalyst-Free Strecker Reaction in Water: A Simple and Efficient Protocol Using Acetone Cyanohydrin as Cyanide Source." European Journal of Organic Chemistry 2011, no. 20-21 (2011): 3896–903. http://dx.doi.org/10.1002/ejoc.201100089.

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44

Kudelska, Wieslawa. "Synthesis of Glycosyl Cyanides by the Reaction of 1-S-Phosphorothioates of Carbohydrates with Trimethylsilyl Cyanide." Zeitschrift für Naturforschung B 53, no. 11 (1998): 1277–80. http://dx.doi.org/10.1515/znb-1998-1107.

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A new procedure is described for the synthesis of α,β-glycosyl cyanides by the reaction of per-O-benzylated S-α-ᴅ-glycopyranosyl phosphorothioates with trimethylsilyl cyanide in the presence of Lewis acid. Starting S-glycosyl phosphorothioates are prepared, directly, from O-benzyl protected reducing D-hexopyranoses (gluco-, galacto-, manno-) and alkylammonium salt of phosphorothioic acid under Lewis acid catalysis.

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45

CHATANI, N., S. MURAI, and T. HANAFUSA. "ChemInform Abstract: Cobalt-Catalyzed Reaction of Acetylenes with Trimethylsilyl Cyanide and tert.-Butyl Isocyanide." ChemInform 22, no. 32 (2010): no. http://dx.doi.org/10.1002/chin.199132150.

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46

Kumar, A. Sanjeev, Samir Ghosh, Kale Bhima, and G. N. Mehta. "Convenient synthesis of amaryllidaceae alkaloid, (+/-) latifine dimethyl ether." Journal of Chemical Research 2009, no. 10 (2009): 635–37. http://dx.doi.org/10.3184/030823409x12523442871697.

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A short route for the synthesis of (+/-) latifine dimethyl ether is reported. The key steps involved are Grignard reaction, conversion of alcohol to nitrile using trimethylsilyl cyanide, reduction of the nitrile intermediate followed by Pictet–Spengler cyclisation and reductive N-methylation in a single step to provide latifine dimethyl ether as a racemate.

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47

Shen, Hang, Liangzhen Hu, Qing Liu та ін. "Iron-catalysed sequential reaction towards α-aminonitriles from secondary amines, primary alcohols and trimethylsilyl cyanide". Chemical Communications 52, № 13 (2016): 2776–79. http://dx.doi.org/10.1039/c5cc10346k.

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48

Mendoza, Jose H. Quintana, J. A. Henao, Aurora L. Carreño Otero, and Vladimir V. Kouznetsov. "Synthesis and X-ray diffraction data of 2-morpholino-2-(3,4,5-trimethoxyphenyl)acetonitrile, (C15H20N2O4)." Powder Diffraction 31, no. 2 (2016): 149–52. http://dx.doi.org/10.1017/s0885715616000075.

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The α-aminonitrile, 2-morpholino-2-(3,4,5-trimethoxyphenyl)acetonitrile (C15H20N2O4), was prepared through a silica sulfuric acid-catalyzed Strecker reaction between 3,4,5-trimethoxybenzaldehyde, morpholine, and two different cyanide sources. Molecular characterization was performed by Fourier transform infrared spectroscopy, gas chromatography–mass spectrometry, (1H, 13C – mono and bidimensional) nuclear magnetic resonance; crystallographic characterization was completed by X-ray powder diffraction of polycrystalline samples. The title compounds crystallized in a monoclinic system and unit-ce

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49

Gurbanov, Atash V., Abel M. Maharramov, Fedor I. Zubkov, Alexander M. Saifutdinov та Firudin I. Guseinov. "Cyanosilylation of Aldehydes Catalyzed by Iron(III) Arylhydrazone-β-Diketone Complexes". Australian Journal of Chemistry 71, № 3 (2018): 190. http://dx.doi.org/10.1071/ch17595.

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Two known iron(iii) complexes, [Fe(H2O)3(L1)]·xH2O (x = 4 (1), 5 (2)) and [Fe(H2O)3(L2)]·3H2O (3), bearing the basic forms of 5-chloro-3-(2-(4,4-dimethyl-2,6-dioxocyclohexylidene)hydrazinyl)-2-hydroxybenzenesulfonic acid (H3L1) and 3-(2-(2,4-dioxopentan-3-ylidene)hydrazinyl)-2-hydroxy-5-nitrobenzenesulfonic acid (H3L2), were prepared and used as homogeneous catalysts for cyanosilylation of a variety of aldehydes with trimethylsilyl cyanide leading to the corresponding cyanohydrin trimethylsilyl ethers. High yield (up to 98 %) was observed in the reaction catalyzed by 3 at room temperature in m

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KOBAYASHI, S., Y. TSUCHIYA, and T. MUKAIYAMA. "ChemInform Abstract: A Facile Synthesis of Cyanohydrin Trimethylsilyl Ethers by the Addition Reaction of Trimethylsilyl Cyanide with Aldehydes Under Basic Condition." ChemInform 22, no. 45 (2010): no. http://dx.doi.org/10.1002/chin.199145126.

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