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Journal articles on the topic 'Substituted Phenylthiourea'

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Published: 5 June 2025

Last updated: 1 August 2025

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1

Kaválek, Jaromír, Josef Jirman, and Vojeslav Štěrba. "Kinetics and mechanism of rearrangement and methanolysis of acylphenylthioureas." Collection of Czechoslovak Chemical Communications 50, no. 3 (1985): 766–78. http://dx.doi.org/10.1135/cccc19850766.

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S-Acyl-1-phenylthioureas and their 3-methyl derivatives are rearranged to 1-acyl derivatives of thiourea in methanolic solution. The rearrangement of the 1-acyl-1-phenyl derivative to the thermodynamically more stable 3-acyl derivative is subject to specific base catalysis. The rearrangement of acetyl group is about 2 orders of magnitude slower than that of benzoyl group. 1-Acetyl-l-phenylthiourea undergoes base-catalyzed methanolysis (giving phenylthiourea and methyl acetate) instead of the rearrangement. The methanolysis rates of l-acyl-3-phenylthioureas and their N-methyl derivatives have b

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2

B., H. Zaware, A. Mane R., and B. Ingle D. "Kinetics of reaction of chloroacetone with thioureas." Journal of Indian Chemical Society Vol. 77, Apr 2000 (2000): 213–14. https://doi.org/10.5281/zenodo.5867060.

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Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad-431 004, India <em>Manuscript received 20 July 1998, revised 16 August 1999, accepted 26 November 1999</em> The second order rate constants for the reactions of chloroacetone with thiourea, phenylthiourea and p-substituted phenylthioureas have been evaluated in ethanol medium. The rate of reaction is first order with respect to chloroacetone and first order with respect to thioureas. The effect of substituents on the rate of reaction is also studied. Thermodynamic parameters are used to explain the nature of reac

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3

Khawar Rauf, M., Amin Badshah, Michael Bolte, and Imtiaz Ahmad. "1-(2,4-Dichlorobenzoyl)-3-phenylthiourea." Acta Crystallographica Section E Structure Reports Online 63, no. 3 (2007): o1155—o1157. http://dx.doi.org/10.1107/s1600536807004527.

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The title compound, C14H10Cl2N2OS, crystallizes with two molecules in the asymmetric unit. The two molecules, differing only in the conformation of the dichlorophenyl ring, show the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

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4

Roecker, Lee, Mohammed Aiyegbo, Aladdin Al-Haddad, et al. "Synthesis and Characterisation of [(en)2Co]3+ Complexes Coordinated by Substituted Thiourea Ligands." Australian Journal of Chemistry 66, no. 8 (2013): 944. http://dx.doi.org/10.1071/ch13150.

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Substituted thiourea ligands bind in a bidentate manner forming a four-membered ring through the sulfur atom and a deprotonated thiourea nitrogen atom when reacted with [(en)2Co(OSO2CF3)2]+ in tetramethylene sulfone. Reaction of unsymmetrical ligands results in the formation of coordination isomers, some of which can be separated by column chromatography using Sephadex SPC-25. Coordination isomers are easily distinguishable based on visible and 1H NMR spectroscopy . Twelve para-substituted and one meta-substituted ligands were studied: N,N′-dibenzylthiourea (1a); N-(R)phenyl-N′-benzylthiourea

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5

Siddharth A. Waghmare and Swapnil B. Sarkate. "Design, synthesis and characterization of some novel Thiocarbamidopyrimidines." International Journal of Science and Research Archive 10, no. 2 (2023): 895–99. http://dx.doi.org/10.30574/ijsra.2023.10.2.1034.

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Interaction of 2 chloro pyrimidines with various substituted thioureas such as thiourea, N- phenylthiourea, 1,3 Dimethylthiourea, N- allylthiourea and ethyl thiourea were carried in presence of isopropanol as a medium. The product isolated in these reactions were characterized on the basis of elemental analysis, chemical characteristics and spectral studies.

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6

Y., D. KULKARNI, RASHMI SHARMA (Miss), L. SHARMA V, and R. DUA P. "2-Substituted-5-chloro/nitrobenzophenones as Possible Anticonvulsants." Journal of Indian Chemical Society Vol. 64, Jan 1987 (1987): 46–48. https://doi.org/10.5281/zenodo.6196157.

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Department of Chemistry, Lucknow University, Lucknow.-226 007 Pharmacology Division, Central Drug Research Institute, Lucknow-226 001 <em>Manuscript received 8 July 1985, revised 22 May 1986, accepted 26 November 1986</em> Twenty one new 2-(<em>N</em><sup>1</sup>-substituted-phenylthiourea-<em>N<sup>2</sup></em> -y1)/(substituted-phenyl thiocarham ato)/[2-(substituted-phen)limino)thiazolid-4-one-3 yl]/[ (3-merca p to-4-su bstitutedphenyl-1, 2, 4(1)-triazol-5-yl)methylaminolmethyleneoxy]-5-chloro / nitrobenzophenones were synthesised and screened for their acute toxicit

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7

Neha, Mathur, Bargotya Sonlata, and Saxena Pooja. "Novel complexes of metal surfactants with substituted phenylthiourea and their thermogravimetric properties." Journal of Indian Chemical Society Vol. 92, Jul 2015 (2015): 1137–41. https://doi.org/10.5281/zenodo.5607248.

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Department of Chemistry Govt. P.G. College, Dausa-303 303, Rajasthan, India <em>E-mail</em> : nehavmathur@yahoo.co.in, b.sonlata@gmail.com <em>Manuscript received online 05 October 2014, revised 20 October 2014, accepted 27 October 2014</em> Binuclear macrocyclic metal complexes represent an important and integral class of organic compounds which are well recognised for their multifaceted biological properties and medicinal relevance. They are no doubt the transition metal complexes which have opened new vistas of research in present era of chemistry. Related studies to them would be of immens

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8

Alharbi, Abdulrahman Salim, and Nawaa Ali Alshammari. "Synthesis of some new 5-amino-3-(substituted-amino)-6-(fluoro/ nitro)aryl-1,2,4-triazine derivatives as lamotrigine analogs and their evaluation in vitro as antibacterial agents." Mediterranean Journal of Chemistry 8, no. 6 (2019): 486–93. http://dx.doi.org/10.13171/mjc861907296asa.

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Some new fluorine-substituted 3,5-disubstituted amino-1,2,4-triazines have been obtained from aryl-amination of 2,2,2-trifluoro-N-[2-(5-hydroxy-3-thioxo-2,3-dihydro-1,2,4-triazin-6-yl)-4-nitrophenyl] acetamide followed by ammonolysis to produce N-(2-(5-amino-3-(arylamino)-1,2,4-triazin-6-yl)-4-nitrophenyl)-2,2,2-trifluoroacetamides which reacted with N-phenylthiourea. The structures of products were deduced from their elemental analysis and spectral measurements. The new lamotrigine analogs were evaluated in vitro as antibacterial. Interestingly, some compounds showed interesting activity agai

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9

Pytela, Oldřich, Josef Jirman, and Antonín Lyčka. "Chemometrical analysis of substituent effects on 13C and 15N NMR chemical shifts in 1-aroyl-3-substituted thioureas." Collection of Czechoslovak Chemical Communications 54, no. 9 (1989): 2399–407. http://dx.doi.org/10.1135/cccc19892399.

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The methods of conjugated deviations and regression analysis have been used to study the substituent effects on 13C and 15N NMR chemical shifts of 12 derivatives of 1-aroyl-3-phenylthiourea and 1-aroyl-3-methylthiourea. The 13C NMR chemical shifts can be described by two latent variables, one univocally correlated with the Hammett substituent constants (r = 0.993) and the other reflecting the increased shielding of the nuclei due to overlap of the adjacent bond electrons as a consequence of electron-donor or electron-acceptor character of the substituents.This effect is less pronounced with th

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10

Park, Kyung-Lae. "Emergence of hydrogen bonds from molecular dynamics simulation of substituted N-phenylthiourea–catechol oxidase complex." Archives of Pharmacal Research 40, no. 1 (2016): 57–68. http://dx.doi.org/10.1007/s12272-016-0866-x.

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11

Abouzied, Amr S., Jehan Y. Al-Humaidi, Abdulrahman S. Bazaid, et al. "Synthesis, Molecular Docking Study, and Cytotoxicity Evaluation of Some Novel 1,3,4-Thiadiazole as Well as 1,3-Thiazole Derivatives Bearing a Pyridine Moiety." Molecules 27, no. 19 (2022): 6368. http://dx.doi.org/10.3390/molecules27196368.

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Pyridine, 1,3,4-thiadiazole, and 1,3-thiazole derivatives have various biological activities, such as antimicrobial, analgesic, anticonvulsant, and antitubercular, as well as other anticipated biological properties, including anticancer activity. The starting 1-(3-cyano-4,6-dimethyl-2-oxopyridin-1(2H)-yl)-3-phenylthiourea (2) was prepared and reacted with various hydrazonoyl halides 3a–h, α-haloketones 5a–d, 3-chloropentane-2,4-dione 7a and ethyl 2-chloro-3-oxobutanoate 7b, which afforded the 3-aryl-5-substituted 1,3,4-thiadiazoles 4a–h, 3-phenyl-4-arylthiazoles 6a–d and the 4-methyl-3- phenyl

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12

Sabaa, Magdy W., Riham R. Mohamed, and Ahmady A. Yassin. "Organic thermal stabilizers for rigid poly(vinyl chloride) IX. N-Benzoyl-N′-p-substituted phenylthiourea derivatives." Polymer Degradation and Stability 81, no. 3 (2003): 431–40. http://dx.doi.org/10.1016/s0141-3910(03)00128-9.

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13

Maharramova, Gunel, Parham Taslimi, Afsun Sujayev, Vagif Farzaliyev, Lokman Durmaz, and İlhami Gulçin. "Synthesis, characterization, antioxidant, antidiabetic, anticholinergic, and antiepileptic properties of novel N‐substituted tetrahydropyrimidines based on phenylthiourea." Journal of Biochemical and Molecular Toxicology 32, no. 12 (2018): e22221. http://dx.doi.org/10.1002/jbt.22221.

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14

Sabaa, Magdy W., Riham R. Mohamed, and Ahmady A. Yassin. "Organic thermal stabilizers for rigid poly(vinyl chloride).Part X: N-acryloyl-N′-p-substituted phenylthiourea derivatives." Polymer Degradation and Stability 82, no. 3 (2003): 387–93. http://dx.doi.org/10.1016/s0141-3910(03)00175-7.

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15

Hritzová, Ol'ga, Juraj Černák, Peter Šafař, Zdenka Frőhlichová, and Ingeborg Csőregh. "Furan derivatives of substituted phenylthiourea: spectral studies, semi-empirical quantum-chemical calculations and X-ray structure analyses." Journal of Molecular Structure 743, no. 1-3 (2005): 29–48. http://dx.doi.org/10.1016/j.molstruc.2005.02.014.

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16

Koshchii, I., Yu. Klimko та T. Shamota. "CF3-β-DIKETONES AND TRIMETHYLHALOSILANES AS SYNTHONS FOR TETRAHYDROPYRIMIDINES". Znanstvena misel journal, № 91 (26 червня 2024): 10–22. https://doi.org/10.5281/zenodo.12541088.

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Trimethylchlorosilane, which is an effective promoter and water-condensing agent, was used for the first time in cyclocondensation reactions with substituted ureas and thioureas. By varying the solvent, ratio of reagents, temperature and reaction time, 100% conversion was achieved for the model compounds. The optimal conditions for the reaction were: reaction temperature 20°C, dimethylformamide solvent, reaction time 48 hours, presence of 4 equivalents of Me<sub>3</sub>SiCl. The use of Me<sub>3</sub>SiCl made it possible to introduce a wide range of aromatic and heterocyclic aldehydes, mon

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17

Ren, Peng, Tao Liu, Jingui Qin, and Chuangtian Chen. "Syntheses, Spectroscopy and Calculated Second-Order Nonlinear Optical Properties of a New Series of Square-Pyramidal Substituted Phenylthiourea Zinc(II) Complexes." Journal of Coordination Chemistry 56, no. 10 (2003): 885–93. http://dx.doi.org/10.1080/0095897031000135270.

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18

Strzyga-Łach, Paulina, Alicja Chrzanowska, Katarzyna Podsadni, and Anna Bielenica. "Investigation of the Mechanisms of Cytotoxic Activity of 1,3-Disubstituted Thiourea Derivatives." Pharmaceuticals 14, no. 11 (2021): 1097. http://dx.doi.org/10.3390/ph14111097.

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Substituted thiourea derivatives possess confirmed cytotoxic activity towards cancer but also normal cells. To develop new selective antitumor agents, a series of 3-(trifluoromethyl)phenylthiourea analogs were synthesized, and their cytotoxicity was evaluated in vitro against the cell line panel. Compounds 1–5, 8, and 9 were highly cytotoxic against human colon (SW480, SW620) and prostate (PC3) cancer cells, and leukemia K-562 cell lines (IC50 ≤ 10 µM), with favorable selectivity over normal HaCaT cells. The derivatives exerted better growth inhibitory profiles towards selected tumor cells tha

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19

(MRS.), M. J. KULKARNI, and MADHA VA RAO B. "Stoichiometry and Kinetic Studies of Oxidation of structurally related Organic Substrates, viz. Thiourea, N-Phenylthiourea and N,N'-Diphenyl- thiourea with Ammonium Hexanitrato- cerate(IV) in Perchloric Acid Medium." Journal of Indian Chemical Society Vol. 72, Apr 1995 (1995): 235–44. https://doi.org/10.5281/zenodo.5902183.

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Department of Chemistry, Visvesvaraya Regional College of Engineering, Nagpur-440 011 <em>Manuscript received 27 August 1993, revised 16 November 1993, accepted 2 December 1993</em> In planning optimal analytical conditions through stoichiometry as well as in the study of structure-reactivity correlations of oxidation of thiourea (TU), <em>N</em>-phenylthiourea (<em>N</em>-PTU), N,N'-diphenylthiourea (<em>N</em>,<em>N'</em>-DPTU) with cerium(IV) in perchloric acid medium, systematic spectrophotometric kinetic studies at 295 nm are of paramount importance. Second order rate constants (<

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20

Spooner, Michael J., and Philip A. Gale. "Anion transport across varying lipid membranes – the effect of lipophilicity." Chemical Communications 51, no. 23 (2015): 4883–86. http://dx.doi.org/10.1039/c5cc00823a.

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21

Qian, Xuhong, Zhibin Li, Gonghua Song, and Zhong Li. "Yellow HgO as an efficient Cyclodesulfurising agent in the Synthesis of 2-substituted Aminobenzoxazoles from N-(2-hydroxyphenyl)-N′-phenylthioureas." Journal of Chemical Research 2001, no. 4 (2001): 138–39. http://dx.doi.org/10.3184/030823401103169441.

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22

Brown, Ainka T., and Nadale K. Downer-Riley. "A Green Approach to 2-Substituted Benzo- and Naphthothiazoles via N-bromosuccinimide/Bromide-Mediated C(aryl)-S Bond Formation." Molecules 27, no. 22 (2022): 7876. http://dx.doi.org/10.3390/molecules27227876.

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2-Substituted benzo- and naphthothiazoles have been conveniently prepared from the intramolecular cyclization of phenylthioureas and activated thiobenzanilides or the coupling of isothiocyanates with amines under mild conditions using N-bromosuccinimide/tetrabutylammonium bromide in 1,2-dimethoxyethane (DME) under ambient conditions. The reactions produce moderate to excellent yields with good functional group tolerance and avoid the use of harsh thermal conditions, corrosive reagents, halogenated solvents, toxic metal salts, and expensive metal catalysts, and are amenable to preparations on a

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23

Glotova, Tatýana, Nadezhda Protsuk, Alexander Albanov, Valentin Lopyrev, and Gennadii Dolgushin. "Dithiobiuretes in reactions with electrophilic acetylenes. New derivatives of 1,3,5-dithiazines,-thiadiazines and-triazines as the products of competing reactions of nucleophilic cycloaddition." Open Chemistry 1, no. 3 (2003): 222–32. http://dx.doi.org/10.2478/bf02476225.

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AbstractThe nucleophilic addition of 2,4-dithiobiurete, 1- and 1,4-substituted 2,4-dithiobiuretes (2 a-e) with benzoylacetylene (1) has been studied. 2-(Benzoylmethyl)-4-(R1-imino)-6-(R2-imino)dihydro-4H-1,3,5-dithiazinium perchlorates (3 a-e) are obtained in glacial acetic acid (AcOH) in the presence of equimolar quantities of HClO4. The reaction of benzoylacetylene with 1,5-diphenyl-2,4-dithiobiurete in either of MeOH, C6H6, or MeCN solvents proceeds non-selectively to give a mixture of products such as 2-(benzoylmethyl)-4,6-di(phenylimino)dihydro-4H-1,3,5-dithiazine (5), 2-(benzoylmethyl)-4

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24

Unkovskii, B. V., I. P. Boiko, Yu F. Malina, T. D. Sokolova, V. F. Shchegel'skii, and L. N. Knyaz'kova. "Synthesis of 5,6-dihydro-4h-1,3-thiazines based on substituted n-phenylthioureas." Chemistry of Heterocyclic Compounds 28, no. 10 (1992): 1225–28. http://dx.doi.org/10.1007/bf00529593.

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25

Valdés-Martı́nez, Jesús, Simón Hernández-Ortega, Georgina Espinosa-Pérez, et al. "Structural, spectral and thermal studies of substituted N-(2-pyridyl)-N′-phenylthioureas." Journal of Molecular Structure 608, no. 1 (2002): 77–87. http://dx.doi.org/10.1016/s0022-2860(01)00934-6.

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26

UNKOVSKII, B. V., I. P. BOIKO, YU F. MALINA, T. D. SOKOLOVA, V. F. SHCHEGEL'SKII, and L. N. KNYAZ'KOVA. "ChemInform Abstract: Synthesis of 5,6-Dihydro-4H-1,3-thiazines from Substituted N- Phenylthioureas." ChemInform 24, no. 46 (2010): no. http://dx.doi.org/10.1002/chin.199346186.

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27

Avetisyan, K. S., and L. Kh Galstyan. "Alkylation of 5,5-Substituted N-[4-Methyl-3-phenylfuran-2(5H)-ylidene]-N′-phenylthioureas." Russian Journal of Organic Chemistry 55, no. 7 (2019): 974–77. http://dx.doi.org/10.1134/s1070428019070091.

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28

Kononchuk, Anastasia G., Vyacheslav V. Martemyanov, Anastasia N. Ignatieva, Irina A. Belousova, Maki N. Inoue, and Yuri S. Tokarev. "Susceptibility of the Gypsy Moth Lymantria dispar (Lepidoptera: Erebidae) to Nosema pyrausta (Microsporidia: Nosematidae)." Insects 12, no. 5 (2021): 447. http://dx.doi.org/10.3390/insects12050447.

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The gypsy moth, Lymantria dispar, is a notorious forest defoliator, and various pathogens are known to act as natural regulators of its population density. As a widespread herbivore with a broad range of inhabited areas and host plants, it is potentially exposed to parasitic microorganisms from other insect hosts. In the present paper, we determined the susceptibility of gypsy moth larvae to the microsporidium Nosema pyrausta from the European corn borer, Ostrinia nubilalis. Gypsy moth samples from two localities of Western Siberia were used. N. pyrausta developed infections in the salivary gl

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29

Chang, Hae Sung, Gyu Hwan Yon, and Yong Hae Kim. "Facile Synthesis of 2-Substituted Aminobenzoxazole. One Pot Cyclodesulfurization ofN-(2-Hydroxyphenyl)-N′-phenylthioureas with Superoxide Radical Anion." Chemistry Letters 15, no. 8 (1986): 1291–94. http://dx.doi.org/10.1246/cl.1986.1291.

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30

Qian, Xuhong, Zhibin Li, Gonghua Song, and Zhong Li. "ChemInform Abstract: Yellow HgO as an Efficient Cyclodesulfurizing Agent in the Synthesis of 2-Substituted Aminobenzoxazoles (II) from N-(2-Hydroxyphenyl)-N′-phenylthioureas (I)." ChemInform 32, no. 38 (2010): no. http://dx.doi.org/10.1002/chin.200138122.

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31

Dr., C. J. Patil. "Studies on Aminobenzothiazole and Derivatives: Part-2. Synthesis of Intermediates -Substituted Phenylthiourea using Ammonium Thiocyanate." February 4, 2021. https://doi.org/10.5281/zenodo.4500935.

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The substituted phenylthiourea is used as intermediate in different reactions because they play an important role in synthesizing the heterocyclic compounds. These reactions involve the synthesis of an intermediate phenylammonium chloride which is converted to substituted thiourea using ammonium thiocyanate. The final product formed, substituted phenylthiourea has potential to use as an intermediate in the synthesis of a building block for the heterocyclic compound, 2-aminobenzothiazole.

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32

Lunge, M. S., K. M. Ingole, N. B. Jadhav, and D. A. Pund. "A NOVEL SYNTHESIS OF [(4-AMINO)-PHENYL] SUBSTITUTED THIOCARBAMIDES." Gurukul International Multidisciplinary Research Journal, May 31, 2025. https://doi.org/10.69758/gimrj/2505i5vxiiip0077.

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Abstract- Recently in this laboratory the synthesis of [(4-amino)-phenyl]substituted thiocarbamides (3a-b) were carried out by the interactions of 4-chloroaniline(1) with various thiourea (2a-b) in 1:1 proportions in isopropanol medium for 4 hours. The synthesized compounds were characterized on the basis of elemental analysis, chemical characteristics and spectral data. Keywords-4-chloroaniline, thiourea, phenylthiourea, isopropanol.

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33

"A Comparative Antibacterial Analysis of Substituted Benzothiazole and Substituted Phenylthiourea Complexes with Copper Metal." international journal of green and herbal chemistry 7, no. 1 (2018). http://dx.doi.org/10.24214/ijghc/gc/7/1/17384.

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34

Oliaie, Samira Sooreni, Mahdieh Safakish, Rouhollah Vahabpour Roudsari, Mohammad Mahboubi-Rabbani, Zahra Hajimahdi, and Afshin Zarghi. "Design, Synthesis, Docking Studies, and Biological Evaluation of Novel 2- Hydroxyacetophenone Derivatives as Anti-HIV-1 Agents." Current HIV Research 21 (November 16, 2023). http://dx.doi.org/10.2174/011570162x261377231107110447.

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Background: The persistence of HIV mutations and the existence of multidrug resistance have produced an opportunity for an array of innovative anti-HIV medicines with a variety of structures that target HIV key enzymes. Objective: The goal of this work was to find a new class of anti-HIV drugs founded on HIV integrase inhibitor pharmacophores. Method: A novel class of 2-hydroxy acetophenone analogs featuring substituted benzamide or N-phenylthiourea groups was designed and synthesized based on the general pharmacophore of HIV-1 integrase inhibitors (INs). Results: Most of the synthesized analo

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35

Sujayev, Afsun, Nastaran Sadeghian, Parham Taslimi та ін. "Functionally substituted derivatives of novel thiourea and phenylthiourea as potent aldose reductase, α-amylase, and α-glycosidase inhibitors: in vitro and in silico studies". Macromolecular Research, 19 лютого 2024. http://dx.doi.org/10.1007/s13233-024-00247-9.

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36

CHANG, H. S., G. H. YON, and Y. H. KIM. "ChemInform Abstract: Facile Synthesis of 2-Substituted Aminobenzoxazole (II). One-Pot Cyclodesulfurization of N-(2-Hydroxyphenyl)-N′-phenylthioureas (I) with Superoxide Radical Anion." ChemInform 18, no. 9 (1987). http://dx.doi.org/10.1002/chin.198709170.

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