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Dissertations / Theses on the topic 'Synthesis of metal dithiocarbamates'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Thangwane, Selaelo Christabel. "Synthesis and characterization of substituted dithiocarbamates ligands and complexes as a source of metal (Pb, Ni & Co) sulphide nanoparticles." Thesis, Vaal University of Technology, 2017. http://hdl.handle.net/10352/396.

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M. Tech. (Department of Chemistry, Faculty of Applied and Computer Sciences), Vaal University of Technology.<br>Lead, nickel and cobalt dithiocarbamates complexes were synthesized using methanol and water as solvents. All complexes were refluxed at 60 °C, cooled at room temperature, washed with methanol to remove the impurities and dried under the fume hood. A combination of Fourier transformer infrared (FTIR), elemental analysis (EA) and thermogravimetric analysis (TGA) were used to characterize these complexes. There was shifting of bands from low to high frequencies of the dithiocarbamates

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2

Exarchos, George. "Reactions between metal sulfur chelate complexes and class B metal centres." Thesis, King's College London (University of London), 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.312991.

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3

Ahmed, Mohammed A. K. "Synthesis and physical investigation of tellurium dithiocarbamates." Thesis, Aston University, 1985. http://publications.aston.ac.uk/11726/.

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4

Roe, Stephen Mark. "Structural studies of main group metal carboxylates and dithiocarbamates." Thesis, University of Warwick, 1989. http://wrap.warwick.ac.uk/56212/.

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The work contained in this thesis describes the crystal structures of a number of tin(IV) and tellurium(IV) carboxylates and dithiocarbamates. The results show the regularity at which these types of compounds form secondary bonds (weak interactions), and the effect of the lone pair of tellurium(IV) on the geometries formed. The area has been studied through the determination of the following crystal structures: i) monocarboxylates: Ph3SnOCOCH2Cl, Ph3SnOCOCHCh, Ph3SnOCOCCh.MeOH. Ph3SnOCOCCh and Ph3TeOCOCCh. ii) dicarboxulates : Ph2Sn(OCOCH3)2, Ph2Sn(OCOCH2CI)2 and Ph2Te(OCOCCI3)2 iii) dithiocar

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5

Fiddy, J. M. "A Moessbauer effect study of iron(III) dithiocarbamates." Thesis, University of Liverpool, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.233819.

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6

Coxall, Robert Andrew. "Structural studies of some mononuclear and polynuclear metal complexes." Thesis, University of Newcastle Upon Tyne, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.299640.

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7

Garcia, Con Luis Miguel. "Dormant radical technology synthesis of materials and potential applications." Thesis, Cranfield University, 2011. http://dspace.lib.cranfield.ac.uk/handle/1826/7247.

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This research was focused on the study of the polymer dormant radical systems, species containing free radical structures that have longer lifetimes and greater stability than radicals in general. In order to understand the nature and reactivity of the dormant radicals, polymeric systems capable of producing dormant free radicals were synthesised. In addition, the use of these novel polymeric materials in a range of applications were studied. Those applications exploited the nature of the dormant radical groups and included controlled modifications in the polymeric structure, heterogeneous cat

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8

Nqombolo, Azile. "Synthesis and structural studies of NiS and PdS nanoparticles/nanocomposites from dithiocarbamates single source precursors." Thesis, University of Fort Hare, 2016. http://hdl.handle.net/10353/d1021326.

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The main aim of this research is to synthesize Ni(II) and Pd(II) dithiocarbamate complexes and use them as single source precursors for the synthesis of NiS and PdS nanoparticles and metal sulphides potato starch nanocomposites. Four dithiocarbamate ligands were synthesized and characterized using elemental analysis and spectroscopic techniques. The ligands were used to prepared homoleptic Ni(II) and Pd(II) complexes of the dithiocarbamate ligands. The metal complexes were characterized with elemental analysis, UV-Vis, FTIR and 1H-NMR spectroscopic techniques. Conductivity measurements indicat

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9

Rodriguez-Garcia, Valerie. "Efficient methodology for the synthesis of 2,4-benzodiazepin-1-ones, sulfonylbenzotriazoles, sulfonamides, ethylene sulfonamides, thiocarbamates, dithiocarbamates and thioamides." [Gainesville, Fla.] : University of Florida, 2004. http://purl.fcla.edu/fcla/etd/UFE0006303.

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10

Carkner, Andrew. "Green metal nanoparticle synthesis." Thesis, McGill University, 2008. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=22037.

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Title: Green Metal Nanoparticle Synthesis Silver and nickel nanoparticles have diverse applications in catalysis, composite materials, and electronics. Current production methods rely on high-energy processes or harsh chemicals; thus it is preferable to use environmentally benign compounds for their synthesis. This project studied the aqueous synthesis of nickel nanoparticles from nickel acetate using glucose, formate, and hydrazine as reducing agents. It was found that although the reactions are thermodynamically favourable, nickel nanoparticles could not be produced using glucose or formate

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11

Salvarese, Nicola. "Synthesis and biological evaluation of Technetium(III)-based radiopharmaceuticals." Doctoral thesis, Università degli studi di Padova, 2012. http://hdl.handle.net/11577/3422151.

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Development of new 99mTc and 186/188Re radiopharmaceuticals still remain an interesting research topic because of their almost ideal nuclear properties. 99mTc is the radioisotope of election for SPECT‐imaging (Eγ=140 keV, t1/2=6.02 h), while 186/188Re are radionuclides with an important therapeutic potential (186Re: Eβ‐=1.07 MeV, Eγ=137 keV, t1/2=90.6 h; 188Re: Eβ‐ =2.12 MeV, Eγ=155 keV, t1/2=17 h). Compounds of both Tc and Re in the 3+ oxidation state are well known, however, the chemistry of Tc(III) and Re(III) applied to Nuclear Medicine is still relatively unexplored. This study reports t

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12

Bharde, A. "Microbial synthesis of metal oxide and metal nanoparticles." Thesis(Ph.D.), CSIR-National Chemical Laboratory, Pune, 2007. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/2553.

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13

Imbault, Alexander Luis. "Alcohol synthesis using metal phosphides." Thesis, University of British Columbia, 2015. http://hdl.handle.net/2429/53655.

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Biofuels make up to 10wt% of gasoline sold in the United States of America and Canada, the largest portion of these biofuel additives is ethanol. Past research working with MoP/SiO₂ using syn gas (H₂:CO 1:1) as a feed have shown how an effective oxygenate catalyst can be promoted with K to become more selective towards ethanol. In this thesis, various metal phosphide catalysts including CoP, Co₂P, RuP and Fe₂P (all supported on SiO₂) are investigated using molecular modelling and activity tests with syn gas to find an effective oxygenate catalyst which can be understood and ultimately converte

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14

Tovey, R. C. "Studies in metal vapour synthesis." Thesis, University of Oxford, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.375325.

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15

Hasell, Tom. "Synthesis of metal-polymer nanocomposites." Thesis, University of Nottingham, 2008. http://eprints.nottingham.ac.uk/10495/.

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This thesis details the synthesis and characterisation of novel nanocomposite materials. The unifying theme of all the projects investigated, is the aim to combine metal or metal oxide nanoparticles with polymer systems. In order to investigate the structure of the materials produced, the extensive use of advanced electron microscopy techniques is essential throughout. Chapter 1: This introductory chapter outlines key themes that are relevant to all the areas of research in this thesis. Theory, background and applications are provided for the fields of nanoparticles, polymers, and supercritica

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16

Musa, Mazlina. "Ionothermal synthesis of metal aluminophosphates." Thesis, University of St Andrews, 2014. http://hdl.handle.net/10023/4483.

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The aim of this thesis was to synthesise CoAPO-34 and FeAPO-34 using ionothermal synthesis in the presence of organic amines. Using this method provides an alternative route to prepare such materials under low pressure instead of the higher pressure associated with hydrothermal or solvothermal synthesis. Both materials have chabazite (CHA) topology and they are known to act as catalysts. CoAPO-34 was ionothermally prepared using 1-ethyl-3-methylimidazolium bromide (EMIMBr) in presence of 1, 6-hexadiamine (HDA). This study has found that when the synthesis was carried out without HDA, AlPO-11 w

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17

Bahadory, Mozhgan Solomon Sally. "Synthesis of noble metal nanoparticles /." Philadelphia, Pa. : Drexel University, 2008. http://hdl.handle.net/1860/2901.

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18

Barry, Brian Michael. "Synthesis of transition-metal polyphosphides." Diss., University of Iowa, 2010. https://ir.uiowa.edu/etd/460.

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This dissertation describes the synthesis of several transition-metal polyphosphides including orthorhombic FePc2, cubic CoP3, cubic NiP2, monoclinic PdP2 and monoclinic CuP2. The investigation of these materials was initiated by the discovery of MPx formation upon reacting a metal halide with yellow P4 in superheated toluene. When these MPx products were annealed at moderate temperatures (350-500 °C), crystalline phosphorus-rich phases were afforded. Upon further investigation, we found that these phases have been primarily synthesized from high-temperature elemental reactions and that low te

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19

Chan, Lai-fung, and 陳麗鳳. "Synthesis, structures and properties of metal-metal bonded transition metal with organothiolate ligands." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2008. http://hub.hku.hk/bib/B40687703.

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20

Chan, Lai-fung. "Synthesis, structures and properties of metal-metal bonded transition metal with organothiolate ligands." Click to view the E-thesis via HKUTO, 2008. http://sunzi.lib.hku.hk/hkuto/record/B40687703.

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21

Aksomaityte, Gabriele. "Synthesis of metal and metal oxide nanoparticles in supercritical fluids." Thesis, University of Nottingham, 2010. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.523001.

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22

Skinner, Stephen John. "Synthesis and characterisation of metal oxides and metal doped variants." Thesis, Open University, 1997. http://oro.open.ac.uk/57713/.

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23

Chen, Jingyi. "Synthesis and utilization of metal nanostructures /." Thesis, Connect to this title online; UW restricted, 2006. http://hdl.handle.net/1773/11547.

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24

Coteron, Almudena. "Methanol synthesis by amorphous metal catalysts." Thesis, University of Cambridge, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.240079.

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25

Bah, Juho. "Metal-Free Catalysis for Efficient Synthesis." Doctoral thesis, KTH, Organisk kemi, 2014. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-144577.

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The strength of efficient metal-free catalysis will be examined in this thesis. Efforts towards more sustainable processes will be demonstrated through implementation of strategies that meet several of the 12 principles of Green Chemistry.In the first part, a stereoselective total synthesis of multiple alkaloids from the Corynantheine and Ipecac families together with their non-natural analogues will be disclosed. A highly efficient, common synthetic strategy is applied leading to high overall yields starting from easily available starting material. Overall operational simplicity and sustainab

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26

Mobbs, B. E. "Arene transition metal complexes in synthesis." Thesis, University of Oxford, 1985. http://ora.ox.ac.uk/objects/uuid:4c7030d4-297e-4af8-a622-d5b4963fc0a3.

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This thesis deals with the applications of organopalladium and organochromium chemistry to the functionalisation of the benzopyran ring system, at a variety of oxidation levels. Section I demonstrates the functionalisation of 3-, 6-, and 8-bromochromones via palladium (0) insertion into the C-Br bond. The resultant arylpalladium species are shown to undergo addition to the least substituted end of a variety of olefins including methyl acrylate, acrylonitrile and styrene. Subsequent palladium-hydride elimination leads to overall palladium catalysed vinylation of the chromone and the synthesis o

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27

Shaw, Graham Andrew. "Solvent mediated synthesis of metal chalcogenides." Thesis, University College London (University of London), 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.326065.

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28

Hinks, Jeremy David. "Metal carbenes in natural product synthesis." Thesis, University of Southampton, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.393940.

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29

Hunter, Rupert Alexander. "Transition metal mediated synthesis of heterocycles." Thesis, University of Southampton, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.402426.

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30

Abser, Mohammed Nurul. "Synthesis of metal containing liquid crystals." Thesis, University of Central Lancashire, 1991. http://clok.uclan.ac.uk/20372/.

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The primary objective of the present study was to develop mesogenic metal complexes. Part of this work was concerned with the synthesis of structural analogues of existing mesogenic bis-1,2-dithiolatonickel(II) complexes to explore the impact of structural variations on the mesophase behaviour of these complexes and to develop complexes with novel mesophase behaviour. The study was successfully continued to develop new mesogenic systems. The work has shown that replacement of the hydrogen atom at the 2-position of the metallodithiolato ring by a phenyl or alkyl group diminishes the tendency of

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31

Reneker, Joseph (Joseph William). "Sonoelectrochemical synthesis of submicron metal powders." Thesis, Massachusetts Institute of Technology, 2012. http://hdl.handle.net/1721.1/70439.

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Thesis (S.M.)--Massachusetts Institute of Technology, Dept. of Mechanical Engineering, 2012.<br>Cataloged from PDF version of thesis.<br>Includes bibliographical references (p. 46-48).<br>Pulsed sonoelectrochemical synthesis is a widely used technique for producing nanoparticles. In this technique, alternating pulses of electric current and power ultrasound are applied to an electrochemical cell to create and suspend particles in the electrolyte. The pulsed technique largely separates the particle morphology defining physical action of electrochemistry and ultrasound. Despite the large body of

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32

Steven, Christopher R. "Plasmonic metal nanoparticles : synthesis and applications." Thesis, University of Strathclyde, 2017. http://digitool.lib.strath.ac.uk:80/R/?func=dbin-jump-full&object_id=27939.

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Plasmonic metal nanoparticles are widely exploited in academia and industry for use in various assay types. In collaboration with an industrial partner, BBI Solutions, the work here details investigations into the production and use of the plasmonic nanoparticles. The work was split into two themes. The first of these was flow chemistry of nanoparticles, covering a microfluidic assay platform and continuous colloid production. In chapter one, a novel microfluidic assay platform was developed which facilitated the transfer of multiple, sequential bench-top procedures into a single device. This

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33

Tang, Yongan. "SYNTHESIS AND ELECTROCATALYSIS OF METAL NANOMATERIALS." Miami University / OhioLINK, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=miami1402313477.

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34

Howie, Rowena Anne. "Metal-organic frameworks : towards greener synthesis." Thesis, University of Nottingham, 2017. http://eprints.nottingham.ac.uk/41707/.

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Metal Organic Frameworks (MOFs) are an interesting class of porous materials, for potential commercial applications such as storage and separation of gases. However, the industrial use of MOFs would require their synthesis on a much larger scale, necessitating the development of scalable synthesis techniques that are both greener and faster than those currently employed. This Thesis describes the recent progress towards the clean and scalable synthesis of MOF materials via the use of high temperature water (HTW) and related solvents. Supercritical ethanol extraction is also presented as a gree

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35

BRAMBILLA, ELISA. "METAL-CATALYZED SYNTHESIS OF POLYCYCLIC INDOLES." Doctoral thesis, Università degli Studi di Milano, 2021. http://hdl.handle.net/2434/819484.

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The indole core is ubiquitous in bioactive natural products and pharmaceutical compounds and the chemistry of the indole nucleus is the subject of intense investigations both for the synthesis of the indole core and the functionalization at both pyrrole and benzene moieties. One of the most employed building blocks is 2-vinylindole that pertains to the class of heterocyclic internal-external ring dienes, a useful class of molecules able to take part in cycloadditions with various dienophiles providing an easy access to poly(hetero)cycles. Another interesting compound, is 4H-furo[3,2-b]indoles

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36

Maity, B. C. "Transition metal templates for stereoselective synthesis." Thesis(Ph.D.), CSIR-National Chemical Laboratory, Pune, 2001. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/2309.

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37

Bray, A. C. "The synthesis of metal cluster species for unsaturated dinuclear metal compounds." Thesis, University of Bristol, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.373734.

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38

Mundell, V. J. "Synthesis and functionalisation of metal and metal oxide nanoparticles for theranostics." Thesis, Nottingham Trent University, 2013. http://irep.ntu.ac.uk/id/eprint/315/.

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Metal and metal oxide nanoparticles including calcium oxide, gold, and superparamagnetic iron oxide nanoparticles (SPIOs) were synthesised using a range of techniques including reduction, co-precipitation and spinning disc technology. SPIOs were primarily synthesised via a co-precipitation method using iron (II) chloride, iron (III) chloride and ammonia; a spinning disc reactor and gaseous ammonia were trialled successfully for scale up, producing spherical particles of 10-40 nm in diameter as analysed by TEM. Nanoparticles were coated via a novel solvent-free grinding process which was succes

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39

Singh, S. K. "Bio-inspired metal and metal-oxide nanoparticles: synthesis, characterization and applications." Thesis(Ph.D.), CSIR-National Chemical Laboratory, Pune, 2008. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/2670.

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40

Maisuradze, Mariam. "Synthesis and Characterization of Double Metal Hexacyanoferrates." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2020. http://amslaurea.unibo.it/21014/.

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Manganese Hexacyanoferrate (MnHCF) and nickel doped manganese hexacyanoferrate were synthesized by simple co-precipitation method. The water content and chemical formula was obtained by TGA and MP-AES measurements, functional groups by FT-IR analysis, the crystal structure by PXRD and a local geometry by XAS. Elemental species of cycled samples were further investigated by TXM and 2D XRF. Electrochemical tests were performed in the glass cell. With addition of nickel, vacancies and water content increased in the sample. Crystal structure changed from monoclinic to cubic. Ni disturbed the local

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41

Landman, Marile. "Synthesis of metal complexes with thiophene ligands." Thesis, Access to E-Thesis, 2000. http://upetd.up.ac.za/thesis/available/etd-12042006-143722/.

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42

Black, Cameron. "Synthesis and characterisation of transition metal fluorides." Thesis, University of St Andrews, 2015. http://hdl.handle.net/10023/9652.

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This thesis reports exploratory studies on the synthesis of new vanadium and copper-containing compounds, with a particular emphasis on preparing new magnetically-active materials with S = ½ spin configurations. Eighteen crystal structures are reported, sixteen of which represent new compounds. These materials were studied for magnetic behaviour where appropriate. The sixteen vanadium-containing compounds were prepared using either the hydrothermal, Solvothermal or ionothermal synthesis methods at temperatures ranging from 60 °C to 200 °C. Inorganic cations and organic moieties were used as te

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43

Ballisai, Antonio. "Synthesis of rigid-rod metal-alkynyl complexes." Thesis, Imperial College London, 2006. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.433302.

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44

Guillo, Nathalie Christine Monique Marie. "Aspects of transition metal-mediated organic synthesis." Thesis, Imperial College London, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.267885.

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45

Warner, P. "Asymmetric synthesis via transition metal acyl complexes." Thesis, University of Oxford, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.355823.

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46

Buffet, Jean-Charles. "Homochiral metal complexes for biodegradable polymer synthesis." Thesis, University of Edinburgh, 2010. http://hdl.handle.net/1842/4618.

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Chapter One introduces the principle of alkoxide and phosphine oxide as ligands for lanthanides and electropositive metals, ligand self-recognition, stereoselective polymerisation of lactide, fixation of CO2 and finally copolymerisation of CO2 and epoxide. Chapter Two shows the synthesis of the proligands rac-HLR (a racemic phosphine oxide-alkoxide, A, where R = tBu, Ph or C6H3-Me-3,5) and explores the resolution into diastereomeric RRR- and SSS-M(LR)3 to afford C3–symmetric M(LR)3 complexes, B (where M = Sc, Lu, Y, In, Bi or La). It also demonstrates that the process is under thermodynamic co

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47

Lazuen-Garay, A. "Solvent-free synthesis of metal-organic frameworks." Thesis, Queen's University Belfast, 2012. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.546378.

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48

Dutton, Sian E. "Synthesis and characterisation of mixed-metal oxides." Thesis, University of Oxford, 2008. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.496850.

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49

Rees, David Alan. "Synthesis of alkaline earth transition metal sulfides." Thesis, University of Nottingham, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.311775.

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50

Hunt, Paul. "Polynuclear metal carboxylates : synthesis, structures and reactivities." Thesis, University of Newcastle Upon Tyne, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.304566.

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