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Relevant bibliographies by topics / Synthesis of metal phosphates

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Academic literature on the topic 'Synthesis of metal phosphates'

Author: Grafiati

Published: 4 June 2021

Last updated: 2 February 2022

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Journal articles on the topic "Synthesis of metal phosphates"

1

Szirtes, László, László Riess, János Megyeri, and Ernõ Kuzmann. "Comparative study of layered tetravalent metal phosphates containing various first-row divalent metals. Synthesis, crystalline structure." Open Chemistry 5, no. 2 (June 1, 2007): 516–35. http://dx.doi.org/10.2478/s11532-007-0003-2.

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AbstractThe transition metal forms of α-zirconium-. titanium-, and hafnium phosphates were prepared by ion exchange method. Their structure was investigated by X-ray powder diffraction (XRPD) method. It was found that the transition metal containing phosphates have the same layered structure as the pristine tetravalent metal phosphates, except for the increase of interlayer distance from 7.6 Å to ∼9.5 Å. As a result of the incorporation of transition metals in the layers, the c-axis is increased from ∼15 Å to ∼20 Å (in the case of titanium phosphate to ∼25 Å). All other parameters (a, b and β °) are practically unchanged.

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Qrareya, Hisham, Lorenzo Meazza, Stefano Protti, and Maurizio Fagnoni. "Metal-free synthesis of biarenes via photoextrusion in di(tri)aryl phosphates." Beilstein Journal of Organic Chemistry 16 (December 8, 2020): 3008–14. http://dx.doi.org/10.3762/bjoc.16.250.

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A metal-free route for the synthesis of biarenes has been developed. The approach is based on the photoextrusion of a phosphate moiety occurring upon irradiation of biaryl- and triaryl phosphates. The reaction involves an exciplex as the intermediate and it is especially suitable for the preparation of electron-rich biarenes.

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Dinamani, M., and P. Vishnu Kamath. "Electrochemical synthesis of metal phosphates by cathodic reduction." Materials Research Bulletin 36, no. 11 (September 2001): 2043–50. http://dx.doi.org/10.1016/s0025-5408(01)00682-1.

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Yakubovich, Olga, Nellie Khasanova, and Evgeny Antipov. "Mineral-Inspired Materials: Synthetic Phosphate Analogues for Battery Applications." Minerals 10, no. 6 (June 7, 2020): 524. http://dx.doi.org/10.3390/min10060524.

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For successful development of novel rechargeable batteries, considerable efforts should be devoted to identifying suitable cathode materials that will ensure a proper level of energy output, structural stability, and affordable cost. Among various compounds explored as electrode materials, structural analogues of minerals–natural stable inorganic solids–occupy a prominent place. The largest number of varieties of phosphate minerals occurs in rare metal granite pegmatites, and many of which contain transition metals as essential components. Transition metal phosphates are promising candidates for exploration as cathode materials due to a perfect combination of easily scalable synthesis, moderate-to-high voltage operation, thermal/chemical stability, and environmental safety. However, impurities usually presented in natural objects, and often inappropriate sample morphologies, do not permit the use of minerals as battery electrode materials. Nevertheless, the minerals of different classes, especially phosphates, are considered as prototypes for developing novel materials for battery applications. The crystal chemical peculiarities of the phosphate representatives that are most relevant in this aspect and the electrochemical characteristics of their synthetic analogues are discussed here.

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Lanfranco, A. M., P. F. Schofield, P. J. Murphy, M. E. Hodson, J. F. W. Mosselmans, and E. Valsami-Jones. "Characterization and identification of mixed-metal phosphates in soils: the application of Raman spectroscopy." Mineralogical Magazine 67, no. 6 (December 2003): 1299–316. http://dx.doi.org/10.1180/0026461036760166.

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AbstractThe development of protocols for the identification of metal phosphates in phosphate-treated, metalcontaminated soils is a necessary yet problematical step in the validation of remediation schemes involving immobilization of metals as phosphate phases. The potential for Raman spectroscopy to be applied to the identification of these phosphates in soils has yet to be fully explored. With this in mind, a range of synthetic mixed-metal hydroxylapatites has been characterized and added to soils at known concentrations for analysis using both bulk X-ray powder diffraction (XRD) and Raman spectroscopy.Mixed-metal hydroxylapatites in the binary series Ca –Cd, Ca –Pb, Ca –Sr and Cd –Pb synthesized in the presence of acetate and carbonate ions, were characterized using a range of analytical techniques including XRD, analytical scanning electron microscopy (SEM), infrared spectroscopy (IR), inductively coupled plasma-atomic emission spectrometry (ICP-AES) and Raman spectroscopy. Only the Ca –Cd series displays complete solid solution, although under the synthesis conditions of this study the Cd5(PO4)3OH end member could not be synthesized as a pure phase. Within the Ca –Cd series the cell parameters, IR active modes and Raman active bands vary linearly as a function of Cd content. X-ray diffraction and extended X-ray absorption fine structure spectroscopy (EXAFS) suggest that the Cd is distributed across both the Ca(1) and Ca(2) sites, even at low Cd concentrations.In order to explore the likely detection limits for mixed-metal phosphates in soils for XRD and Raman spectroscopy, soils doped with mixed-metal hydroxylapatites at concentrations of 5, 1 and 0.5 wt.% were then studied. X-ray diffraction could not confirm unambiguously the presence or identity of mixed-metal phosphates in soils at concentrations below 5 wt.%. Raman spectroscopy proved a far more sensitive method for the identification of mixed-metal hydroxylapatites in soils, which could positively identify the presence of such phases in soils at all the dopant concentrations used in this study. Moreover, Raman spectroscopy could also provide an accurate assessment of the degree of chemical substitution in the hydroxylapatites even when present in soils at concentrations as low as 0.1%.

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Pet’kov, V. I., M. V. Sukhanov, A. S. Shipilov, V. S. Kurazhkovskaya, E. Yu Borovikova, N. V. Sakharov, M. M. Ermilova, and N. V. Orekhova. "Synthesis and structure of alkali metal zirconium vanadate phosphates." Russian Journal of Inorganic Chemistry 58, no. 9 (September 2013): 1015–21. http://dx.doi.org/10.1134/s0036023613090167.

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Haushalter, R. "Synthesis and structure of new alkali metal molybdenum phosphates." Solid State Ionics 26, no. 2 (March 1988): 158. http://dx.doi.org/10.1016/0167-2738(88)90102-6.

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Zatovsky, Igor V., Nikolay S. Slobodyanik, Denis A. Stratiychuk, Konstantin V. Domasevitch, Joachim Sieler, and Eduard B. Rusanov. "A Novel Convenient Synthesis of Mixed-Valence TiIII/TiIV Double Phosphates Starting with Titanium Nitride TiN." Zeitschrift für Naturforschung B 55, no. 3-4 (April 1, 2000): 291–98. http://dx.doi.org/10.1515/znb-2000-3-411.

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Abstract A new synthetic approach for the low- and mixed-valence double titanium phosphates starting with titanium nitride, TiN, and based on the controlled oxidation of a low-valent metal in the phosphate melt is presented. The reaction of the system MI2O - P2O5 - TiN (MI = Na, K) in air (800-1050 °C) leads to loss of nitrogen, N2, and results in the formation of a number of double phosphates: KTiP2O7, K2TiniTiIV(PO4)3, KTiOPO4, NaTiP2O7, NaTi2(PO4)3 and a new mixed-valent diphosphate, NaTiIIITiIV(P2O7)2. The mixed-valent species K2TiIIITiIV(PO4)3 and NaTiIIITiIV(P2O7)2 were characterized by single crystal X-ray diffraction. The described synthetic procedure is proposed as a simple and convenient method for the preparation of lowand mixed-valent phosphate materials

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Rao, C. N. R., Srinivasan Natarajan, Amitava Choudhury, S. Neeraj, and R. Vaidhyanathan. "Synthons and design in metal phosphates and oxalates with open architectures." Acta Crystallographica Section B Structural Science 57, no. 1 (February 1, 2001): 1–12. http://dx.doi.org/10.1107/s0108768100017638.

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We briefly describe the structures of open-framework metal phosphates with different dimensionalities, such as the one-dimensional linear-chain and ladder structures, two-dimensional layer structures and three-dimensional structures with channels. We demonstrate the role of the zero-dimensional four-membered ring monomer and of the one-dimensional ladder structure as the starting building units or synthons involved in the formation of the complex architectures. Thus, we show how the one-dimensional ladder structure transforms to two- and three-dimensional structures under mild conditions. The two-dimensional layer structures also transform to three-dimensional structures, while the zero-dimensional monomer transforms to layered and three-dimensional structures under ordinary reaction conditions. These transformations provide an insight into the possible pathways involved in the building up of the complex structures of metal phosphates. The isolation of amine phosphates during the hydrothermal synthesis of metal phosphates and also the facile reactions between amine phosphates and metal ions to yield a variety of open-framework materials have thrown light on the mechanism of formation and design of these structures. The existence of a hierarchy of open-framework metal oxalates and their ready formation by employing amine oxalates as intermediates provides additional support to the observations made earlier with regard to the phosphates.

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Dong, Angang, Nan Ren, Yi Tang, Yajun Wang, Yahong Zhang, Weiming Hua, and Zi Gao. "General Synthesis of Mesoporous Spheres of Metal Oxides and Phosphates." Journal of the American Chemical Society 125, no. 17 (April 2003): 4976–77. http://dx.doi.org/10.1021/ja029964b.

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Dissertations / Theses on the topic "Synthesis of metal phosphates"

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Lightfoot, P. "Synthesis and characterisation of some transition metal phosphates." Thesis, University of Oxford, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.382771.

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Gaslain, Fabrice O. M. "Synthesis and characterisation of new microporous metal phosphates." Thesis, University of Reading, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.402611.

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Liu, Jun-Yao. "Synthesis and catalytic activity of metal phosphates, phosphites and phosphonates." Thesis, University of Liverpool, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.366368.

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Musa, Mazlina. "Ionothermal synthesis of metal aluminophosphates." Thesis, University of St Andrews, 2014. http://hdl.handle.net/10023/4483.

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The aim of this thesis was to synthesise CoAPO-34 and FeAPO-34 using ionothermal synthesis in the presence of organic amines. Using this method provides an alternative route to prepare such materials under low pressure instead of the higher pressure associated with hydrothermal or solvothermal synthesis. Both materials have chabazite (CHA) topology and they are known to act as catalysts. CoAPO-34 was ionothermally prepared using 1-ethyl-3-methylimidazolium bromide (EMIMBr) in presence of 1, 6-hexadiamine (HDA). This study has found that when the synthesis was carried out without HDA, AlPO-11 was preferentially obtained instead of CoAPO-34. Broad line signals which appear between 2000 to 5000 ppm in both spin-echo ³¹P NMR spectra of as-synthesised and calcined CoAPO-34 confirm that the Co²⁺ ions have been successfully incorporated within the framework of the material. FeAPO-34 was synthesised under ionothermal conditions using 1-ethyl-3-methylimidazolium chloride in the presence of ethylenediamine (EDA). In the absence of EDA, the synthesis has produced AlPO-34 instead of FeAPO-34. Broad line signals that appear between 1000 to 14000 ppm in spin-echo ³¹P NMR spectra of both as-synthesised and calcined FeAPO-34 are direct evidence of isomorphous substitution of framework aluminum by Fe(II) or Fe(III). Another aim of this study was to explore the ionothermal synthesis of copper containing aluminophoshate of DNL-1 (Cu/DNL-1). This material was attractive to explore because it contains 20 ring extra-large pores and Cu(I) species in the channels of the framework, potentially giving material the ability to simultaneous store NO and to generate NO from NO₂⁻ anions. Cu/DNL-1 was successfully prepared under ionothermal conditions using EMIMBr and HDA. Without HDA in the synthesis, AlPO-11 was obtained. In this material, copper ions were not incorporated in the Cu/DNL-1 skeleton framework. This was confirmed by absence of broadline signal at >500 ppm in spin-echo ³¹P NMR spectrum of the sample. The copper ions are expected to be present as extra-framework cations. Extra-framework Cu(I) species that were formed by high temperature calcination of Cu/DNL-1 are active to produce NO from NO₂⁻. Therefore, the calcined Cu/DNL-1 can be used to simultaneously store and produce NO from nitrite. This has the potential to signiﬁcantly extend the lifetime of gas delivery in the material to prevent thrombus formation.

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Warner, Joanne K. "The synthesis and structural characterisation of some transition metal phosphates." Thesis, University of Oxford, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.306026.

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Burnell, Victoria Anne. "The synthesis, characterisation and ion exchange of mixed metal phosphates." Thesis, University of Birmingham, 2011. http://etheses.bham.ac.uk//id/eprint/3161/.

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This thesis presents work investigating the synthesis and characterisation of a range of mixed metal phosphates. The main aim of the project was to develop materials for the remediation of nuclear waste. In light of this, the materials developed were subject to ion exchange studies and leach testing. The thermal behaviour of the phosphates and nature of the decomposition products were also investigated. This study demonstrates that the true solid solution cannot be formed in any of the mixed metal series investigated, which included zirconium-titanium, germanium-titanium, germanium-zirconium, tin-titanium and tin-zirconium. In all cases a miscibility gap was observed and the reasons for these were established. The co-precipitates that formed were characterised by a variety of analytical techniques which included powder X-ray diffraction (PXRD), thermogravimetric analysis (TGA), pair distribution function (PDF) analysis and X-ray fluorescence (XRF). Structural characterisation was undertaken using both traditional Rietveld analysis of synchrotron X-ray powder diffraction data and PDF analysis of high energy synchrotron total scattering data. The results of the ion exchange studies yielded four exchanged products: strontium exchanged zirconium phosphate, a strontium exchanged zirconium-titanium phosphate and two sodium exchanged titanium phosphate products. Although it was not possible to solve the structures of these phases, they were further characterised by a number of methods and their use as potential stores were investigated by leach testing. The strontium exchanged zirconium phosphate product demonstrated good strontium retention and is recommended for further investigation as a possible strontium waste form.

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Eral, Leyla Eanes Mehtap. "Hydrothermal synthesis and characterization of transition metal (Mn and V) oxides containing phosphates/." [s.l.]: [s.n.], 2006. http://library.iyte.edu.tr/tezler/master/kimya/T000562.pdf.

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Stark, Michael Andreas [Verfasser]. "Synthesis of nanosized, electrochemically active lithium transition metal phosphates / Michael Andreas Stark." Ulm : Universität Ulm. Fakultät für Naturwissenschaften, 2011. http://d-nb.info/1017543364/34.

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Stalder, Sloane Marie. "The synthesis and characterization of some gallophosphates using transition metal complexes as templates." Thesis, Georgia Institute of Technology, 1997. http://hdl.handle.net/1853/27992.

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Lu, Ling. "Synthesis and properties of pillared and non-pillared metal organo-phosphates and phosphonates." Thesis, University of Liverpool, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.385318.

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Books on the topic "Synthesis of metal phosphates"

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Gshalaev, Valeri S., and Aleksandra C. Demirchan. Hydroxyapatite: Synthesis, properties, and applications. Hauppauge, N.Y: Nova Science Publishers, 2012.

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Billington, David C. Inositol phosphates: Chemical synthesis and biological significance. Weinheim: VCH Verlagsgeselschaft, 1993.

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Spencer, Peter C. Synthesis and reactions of protected aminoacyl ethyl phosphates. Ottawa: National Library of Canada, 1998.

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Matear, W. A. The synthesis of metal alkoxides. Manchester: UMIST, 1992.

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Metal carbenes in organic synthesis. Weinheim: Wiley-VCH, 1999.

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Spiers, Ian David. Synthesis, crystallography and biological activity of myo-inositol phosphates. Birmingham: Aston University.Department of Pharmaceutical and Biological Sciences, 1996.

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Dreef, Cornelis Erik. Chemical synthesis of myo-inositol phospholipids, phosphates, and analogues thereof. [The Hague]: C.E. Dreef, 1991.

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8

Jasem, Abdul Kadem J. Synthesis, characterization and ion exchange properties of cerium(iv) phosphates. Salford: University ofSalford, 1987.

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Noels, A. F., M. Graziani, and A. J. Hubert, eds. Metal Promoted Selectivity in Organic Synthesis. Dordrecht: Springer Netherlands, 1991. http://dx.doi.org/10.1007/978-94-011-3408-8.

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Graedel, T. E. Metal stocks in society: Scientific synthesis. Nairobi: UNEP, 2010.

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Book chapters on the topic "Synthesis of metal phosphates"

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Tas, A. Cuneyt. "Biomimetic Calcium Phosphate Synthesis by using Calcium Metal." In Advances in Bioceramics and Porous Ceramics VI, 93–106. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2013. http://dx.doi.org/10.1002/9781118807811.ch8.

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Boatner, Lynn A. "4. Synthesis, Structure, and Properties of Monazite, Pretulite, and Xenotime." In Phosphates, edited by Matthew J. Kohn, John Rakovan, and John M. Hughes, 87–122. Berlin, Boston: De Gruyter, 2002. http://dx.doi.org/10.1515/9781501509636-007.

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Malisch, Wolfgang, Klaus Grün, Heinrich Jehle, Joachim Reising, Stephan Möller, Oliver Fey, and Christa Abdelbaky. "Metal Mediated Synthesis of Chiral Secondary Phosphane Ligands via the Organophosphenium Complexes Cp(OC)(L)M=P(H)R (M = Mo, W; L = OC, Me3P; R = t-Bu, Mes). Regiospecific Functionalization of Iron and Ruthenium Substituted Disilanes." In Selective Reactions of Metal-Activated Molecules, 257–63. Berlin, Heidelberg: Springer Berlin Heidelberg, 1998. http://dx.doi.org/10.1007/978-3-662-00975-8_39.

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Greenblatt, M., and B. Raveau. "Other Reduced Transition Metal Phosphates." In Inorganic Reactions and Methods, 239. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470145203.ch148.

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Codée, Jeroen D. C., and Peter H. Seeberger. "Oligosaccharide Synthesis with Glycosyl Phosphates." In ACS Symposium Series, 150–64. Washington, DC: American Chemical Society, 2007. http://dx.doi.org/10.1021/bk-2007-0960.ch010.

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Fang, Zhen. "Metal Oxides Synthesis." In Rapid Production of Micro- and Nano-particles Using Supercritical Water, 29–55. Berlin, Heidelberg: Springer Berlin Heidelberg, 2010. http://dx.doi.org/10.1007/978-3-642-12987-2_3.

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Patwardhan, Siddharth V., and Stephen J. Clarson. "Bioinspired Silica Synthesis." In Macromolecules Containing Metal and Metal-Like Elements, 203–23. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2005. http://dx.doi.org/10.1002/0471712566.ch8.

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Brunner, Henri. "Optically Active Transition Metal Compounds Containing Chiral Transition Metal Atoms." In Chemical Synthesis, 91–111. Dordrecht: Springer Netherlands, 1996. http://dx.doi.org/10.1007/978-94-009-0255-8_4.

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Czaja, Alexander, Emi Leung, Natalia Trukhan, and Ulrich Müller. "Industrial MOF Synthesis." In Metal-Organic Frameworks, 337–52. Weinheim, Germany: Wiley-VCH Verlag GmbH & Co. KGaA, 2011. http://dx.doi.org/10.1002/9783527635856.ch14.

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Shvets, V. I., A. E. Stepanov, L. Schmitt, B. Spiess, and G. Schlewer. "Synthesis and Complexation Properties of Inositol—Phosphates." In ACS Symposium Series, 155–71. Washington, DC: American Chemical Society, 1991. http://dx.doi.org/10.1021/bk-1991-0463.ch012.

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Conference papers on the topic "Synthesis of metal phosphates"

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WEN, F. S., X. ZHAO, C. Y. XI, and J. S. CHEN. "HYDROTHERMAL SYNTHESIS AND PHOTOLUMINESCENCE OF METAL PHOSPHATE-BASED MATERIALS." In Proceedings of the Seventh International Symposium on Hydrothermal Reactions. WORLD SCIENTIFIC, 2003. http://dx.doi.org/10.1142/9789812705228_0007.

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Sulistyani, Susila Kristianingrum, Annisa Fillaeli, Risca Febyan, and Isma P. Loka. "Synthesis and Utilization of Composite Beads of Activated Carbon-Phosphate-Chitosan as Adsorbent of Mg2+ and Pb2+ Metal Ions." In 7th International Conference on Research, Implementation, and Education of Mathematics and Sciences (ICRIEMS 2020). Paris, France: Atlantis Press, 2021. http://dx.doi.org/10.2991/assehr.k.210305.026.

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Terebilenko, A., K. Terebilenko, N. Slobodyanik, and E. Zubar. "Synthesis and luminescence properties of calcium phosphates." In 2014 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE). IEEE, 2014. http://dx.doi.org/10.1109/omee.2014.6912394.

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Kim, J. K., D. Y. Kim, H. N. Cho, and C. Y. Kim. "Characteristics of a complex of ethylene oxide-phosphate copolymer with LiCLO/sub 4/ as a polymer electrolyte." In International Conference on Science and Technology of Synthetic Metals. IEEE, 1994. http://dx.doi.org/10.1109/stsm.1994.835288.

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Chy Hyung Kim and Hyun Suk Kim. "Ag(I) and Cu(II) ion exchange on α-zirconium phosphate using molten nitrate salts and thier electric properties." In International Conference on Science and Technology of Synthetic Metals. IEEE, 1994. http://dx.doi.org/10.1109/stsm.1994.835750.

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WANG, D., R. B. YU, N. KUMADA, N. KINOMURA, K. YANAGISAWA, D. WANG, Y. MATHMURA, and T. YASHIMA. "NON-AQUEOUS SYNTHESIS OF NOVEL LOW-DIMENSIONAL ZIRCONIUM PHOSPHATES." In Proceedings of the International Symposium on Solid State Chemistry in China. WORLD SCIENTIFIC, 2002. http://dx.doi.org/10.1142/9789812776846_0030.

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Kannan, Thanukrishnan, Subramaniam Vinodhkumar, and Duraikkannu Loganathan. "Synthesis of Glycosyl Phosphoramidates: Novel Isosteric Analogs of Glycosyl Phosphates." In The 3rd International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 1999. http://dx.doi.org/10.3390/ecsoc-3-01768.

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Asadi-Eydivand, Mitra, Amir Hossein Hakami Vala, Arghavan Farzadi, Soheila Ali Akbari Ghavimi, and Mehran Solati-Hashjin. "Using an artificial intelligence technique to optimize calcium phosphates synthesis conditions." In 2012 IEEE EMBS Conference on Biomedical Engineering and Sciences (IECBES 2012). IEEE, 2012. http://dx.doi.org/10.1109/iecbes.2012.6498107.

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Tbib, B., M. Eddya, and K. El-Hami. "Phosphates based pigments for new anti-corrosion application: Synthesis and characterization." In INTERNATIONAL CONFERENCE ON STRUCTURAL ANALYSIS OF ADVANCED MATERIALS: ICSAAM 2017. Author(s), 2018. http://dx.doi.org/10.1063/1.5024192.

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Voropaeva, O. V., Tripti Tripti, A. Kumar, K. A. Panikovskaya, M. G. Maleva, and G. G. Borisova. "Screening of metal tolerant plant growth-promoting endophytic (PGPE) bacteria for the preparation of bioformulation." In 2nd International Scientific Conference "Plants and Microbes: the Future of Biotechnology". PLAMIC2020 Organizing committee, 2020. http://dx.doi.org/10.28983/plamic2020.277.

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Metal tolerant plant growth-promoting bacteria capable of synthesizing IAA from tryptophan, solubilizing phosphates and converting protein nitrogen into ammonia were isolated from plants growing on contaminated soils.

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Reports on the topic "Synthesis of metal phosphates"

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X. Shari Li, W. Yantasee A.R. Courtney, and S.V. Mattigod. TEMPLATED SYNTHESIS OF MESOPOROUS TITANIUM PHOSPHATES FOR THE SEQUESTRATION OF RADIONUCLIDES. Office of Scientific and Technical Information (OSTI), October 2005. http://dx.doi.org/10.2172/884953.

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Baker, R. T. Tandem metal-mediated synthesis. Office of Scientific and Technical Information (OSTI), December 1998. http://dx.doi.org/10.2172/350837.

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Serne, R. J., W. J. Martin, V. L. LeGore, C. W. Lindenmeier, S. B. McLaurine, P. F. C. Martin, and R. O. Lokken. Leach tests on grouts made with actual and trace metal-spiked synthetic phosphate/sulfate waste. Office of Scientific and Technical Information (OSTI), October 1989. http://dx.doi.org/10.2172/5391748.

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Brumlik, Charles J., and Charles R. Martin. Template Synthesis of Metal Microtubules. Fort Belvoir, VA: Defense Technical Information Center, March 1991. http://dx.doi.org/10.21236/ada232827.

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Speyer, Robert F. Synthesis and Processing of Ultra-High Temperature Metal Carbide and Metal Diboride Nanocomposite Materials. Fort Belvoir, VA: Defense Technical Information Center, April 2008. http://dx.doi.org/10.21236/ada483547.

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West, M. H., M. M. Martinez, J. B. Nielsen, D. C. Court, and Q. D. Appert. Synthesis of uranium metal using laser-initiated reduction of uranium tetrafluoride by calcium metal. Office of Scientific and Technical Information (OSTI), September 1995. http://dx.doi.org/10.2172/106523.

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Loehman, R. E., K. G. Ewsuk, and A. P. Tomsia. Synthesis and processing of composites by reactive metal penetration. Office of Scientific and Technical Information (OSTI), April 1997. http://dx.doi.org/10.2172/494120.

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Rubin, Yves F. Total Synthesis of Buckminsterfullerene (C60) and Endohedral Metal Complexes. Fort Belvoir, VA: Defense Technical Information Center, August 1997. http://dx.doi.org/10.21236/ada328578.

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Chapman, Robert D., Richard A. Hollins, Thomas J. Groshens, and David A. Nissan. Benzylamine-Free, Heavy-Metal-Free Synthesis of CL-20. Fort Belvoir, VA: Defense Technical Information Center, December 2006. http://dx.doi.org/10.21236/ada608401.

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McBreen, J., and J. J. Reilly. Synthesis and characterization of metal hydride electrodes. Interim report. Office of Scientific and Technical Information (OSTI), October 1995. http://dx.doi.org/10.2172/150915.

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