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Dissertations / Theses on the topic 'Synthesis of organometallics'

Author: Grafiati

Published: 4 June 2021

Last updated: 15 February 2022

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1

Bott, Adrian William. "Clusters : synthesis and topology." Thesis, University of Cambridge, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.316027.

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2

Abdelsalam, Mansour. "Synthesis of piperidines using organometallic chemistry." Thesis, University of Sheffield, 2013. http://etheses.whiterose.ac.uk/4069/.

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3

Stern, James Andrew. "The synthesis and manipulation of organoiron complexes." Thesis, Imperial College London, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.321665.

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4

Dennehy, Robert Daniel. "The synthesis and reactivity of titanium metallacycles." Thesis, University of Southampton, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.359239.

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5

Amoroso, Angelo James. "The synthesis and reactivity of osmium carbonyl clusters." Thesis, University of Cambridge, 1993. https://www.repository.cam.ac.uk/handle/1810/272544.

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6

Loveridge, Tracey. "Chiral chromium complexes in synthesis." Thesis, University of Oxford, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.296868.

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7

Ward, Mark Frederick. "The synthesis and reactivity of (vinylketene) iron(0) complexes." Thesis, Imperial College London, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.294843.

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8

Charlton, Adam. "Synthesis, characterisation, and evaluation of novel nonlinear optical materials." Thesis, Bangor University, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.359051.

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9

De, Lima Geraldo Magela. "The synthesis, characterization and reactivity of some tin(II) compounds." Thesis, University of Sussex, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.360500.

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10

Wong, D. M. "Synthesis, structure and reactivity of chiral cyclopentadienyl ruthenium (II) complexes." Thesis, University of Salford, 1996. http://usir.salford.ac.uk/43028/.

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This thesis concerns the preparation, structural, and reactivity studies of new chiral monometallic cyclopentadienyl ruthenium(II) complexes exhibiting a combination of metal-centred and ligand-derived chirality.

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11

McCormick, Gillian J. "Synthesis and reactivity of naphthyne complexes of ruthenium." Thesis, Brunel University, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.389113.

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12

Lawrence, Heather Bunting Elizabeth. "Organometallic compounds with non-linear optical properties." Thesis, University of Oxford, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.276835.

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13

Martinelli, Marcia. "The synthesis and properties of some organo-ruthenium and organo-osmium clusters." Thesis, University of Cambridge, 1991. https://www.repository.cam.ac.uk/handle/1810/271906.

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14

Collier, Philip Edward. "Synthesis and reactivity of titanium imido complexes." Thesis, University of Nottingham, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.243752.

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15

Nichols, Lorna Susan. "The synthesis and structural characterisation of novel main group organometallics." Thesis, University of Southampton, 2006. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.438681.

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16

Barozzino, Consiglio Gabriella. "Organometallics in regio- and enantio-selective synthesis : structures and reactivity." Rouen, 2010. http://www.theses.fr/2010ROUES022.

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Ce travail présente deux études en chimie organométallique (organolithiens). Dans le premier chapitre, des réactions d'isomérisation réalisées en présence de superbases bimétalliques sont impliquées, et la transformation d'aziridines fonctionnalisées est examinée. Deux voies sont possibles : la β-élimination ou la cyclisation 4-exo intracyclique. Le processus réactionnel étant accompagné de la formation de centre(s) stéréogène(s), une approche asymétrique est explorée avec 3-APLi's. Le deuxième chapitre s'intéresse à l'étude structurale de phosphines (boranes) lithiées dans le but d'aborder la

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17

Palin, Michael G. "Synthesis and structure of diene-iron and arene-chromium complexes containing phosphine ligands." Thesis, Keele University, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.357157.

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18

Probert, Gareth David. "The zirconocene-mediated synthesis of amines." Thesis, University of Southampton, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.242623.

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19

Muldoon, David James. "Synthesis, structural and catalytic studies of some new complexes of molybdenum(II) and tungsten(II)." Thesis, Bangor University, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.385795.

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20

Moore, Rebecca J. "Novel approaches to natural product synthesis using organozinc intermediates." Thesis, University of Newcastle Upon Tyne, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.362516.

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21

Qi, Miao. "Developing an Electrochemically Redox Switchable System for Polymer Synthesis:." Thesis, Boston College, 2020. http://hdl.handle.net/2345/bc-ir:108945.

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Thesis advisor: Jeffery A. Byers<br>This dissertation discusses the development of an electrochemically switchable system for copolymer synthesis as well as surface modifications. In Chapter one, the usage of electrochemistry to control polymerization reactivities is introduced. In Chapter two, an electrochemically redox switchable polymerization for lactide and cyclohexene oxide will be presented. In Chapter three, a surface modification method based on the electrochemically redox switchable catalysis is discussed. The surface-anchored catalyst responds to applied electrochemical potentials t

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22

El-Assiery, Saied Abdullah. "Synthesis of compounds containing phenolic or boronic acid residues by reaction of boron hydrides with metallated systems." Thesis, Lancaster University, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.317402.

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23

Matthews, Jennifer Louise. "The synthesis and potential applications of asymmetric silacycles." Thesis, Durham University, 1994. http://etheses.dur.ac.uk/5504/.

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Although the use of silicon-based reagents has undergone rapid development during the last twenty years, the application of organosilicon chemistry to asymmetric synthesis has been somewhat slower to develop. The many problems associated with the use of 'Si-centred' chiral organosilicon compounds has led to the application of 'C-centred' chiral organosilicon compounds. This work has been aimed at the synthesis and application of cyclic silicon species. Routes towards the synthesis of medium-sized rings have been investigated as a potential application of enantiomerically pure silacycles. This

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24

Hewlett, Dudley Francis. "The use of the [eta]Â²-aldehyde, ketone and benzyne complexes of Ti and Zr in organic synthesis." Thesis, University of Southampton, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.359225.

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25

Lian, Yiqian. "Chromium and iron organometallics in organic synthesis synthetic studies toward total synthesis of taxol and chromium to iron transfer processes /." Diss., Connect to online resource - MSU authorized users, 2006.

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26

Barbey, Sabine. "A novel approach to the ergot alkaloid skeleton." Thesis, University of Reading, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.294855.

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27

Yu, Yongfei. "Synthesis, structure and properties of some chiral-at-metal transition metal organometallics." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1998. http://www.collectionscanada.ca/obj/s4/f2/dsk1/tape10/PQDD_0015/NQ42488.pdf.

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28

Murphy, Don M. "Synthesis and properties of novel carboranes and organometallics for second harmonic generation." Thesis, University of Oxford, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.303617.

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29

Arbit, Ruslan Mikhaylovich. "I. Homologation of alpha-diketones. II. Synthesis of epiafricanol and advances toward longithorone a and paclitaxel." The Ohio State University, 2003. http://rave.ohiolink.edu/etdc/view?acc_num=osu1070356064.

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30

Joy, Jonathan Stuart. "Synthesis and charaterisation of mixed s-/p-block organometallics and p-block ligand systems." Thesis, University of Southampton, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.402058.

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31

Cardona, Laia Davin. "Exploiting cooperative effects in s-Block organometallics for new applications in synthesis and catalysis." Thesis, University of Strathclyde, 2017. http://digitool.lib.strath.ac.uk:80/R/?func=dbin-jump-full&object_id=28408.

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Focussing on group 1 and group 2 metals, this thesis advances the use of polar organometallics in catalysis, in particular intermolecular hydroamination processes; as well as other key stoichiometric transformations, namely deprotonative metallation and C-F bond activation. Group 1 alkyl compounds MCH2SiMe3 (M = Li, Na or K) have proved to be efficient catalysts for intermolecular hydroamination of a wide range of substituted vinylarenes and alkynes at room temperature and with short timescales. Similarly,advancing in the concept of s-block cooperative bimetallic catalysis, alkali-metal magnes

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32

Li, Chunmei. "Designing phase selective soluble polymers for applications in organic chemistry." Diss., Texas A&M University, 2003. http://hdl.handle.net/1969/105.

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33

Schofield, Daniel. "The synthesis and reactivity of Group 4 metal hydrazides." Thesis, University of Oxford, 2012. http://ora.ox.ac.uk/objects/uuid:8eb27904-237b-4065-ad37-6008166731e9.

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This thesis describes the synthesis, characterisation and reactivity of diamide-amine and bis(cyclopentadienyl) supported Group 4 hydrazido(2-) compounds towards unsaturated molecules. The mechanisms of these transformations are probed using a range of structural, kinetic and computational methods.

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34

Campbell, Michael Glenn. "Synthesis, Structure, and Reactivity of New Palladium(III) Complexes." Thesis, Harvard University, 2014. http://dissertations.umi.com/gsas.harvard:11289.

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Palladium is one of the most common and versatile transition metals used in modern organometallic chemistry. The chemistry of palladium in its 0, +II, and +IV oxidation states is well-known; by comparison, the chemistry of palladium in its +III oxidation state is in its infancy. The work in this thesis involves the study of previously unknown Pd(III) complexes, including applications in materials chemistry and catalysis.<br>Chemistry and Chemical Biology

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35

Orchard, Katherine Lorraine. "The mild synthesis of zinc oxide nanoparticles and nanocomposites via hydrolysis of well-characterised zinc organometallics." Thesis, Imperial College London, 2011. http://hdl.handle.net/10044/1/17786.

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This thesis centres on the development of a clean, one step method for generating surface-functionalised zinc oxide (ZnO) nanoparticles for application in the synthesis of well-dispersed inorganic-organic nanocomposites. The nanoparticle synthesis method utilises the controlled hydrolysis of organometallic zinc compounds, employing diethylzinc as a bulk precursor and an alkylzinc carboxylate as a substoichiometric, secondary precursor to deliver the capping ligands. A series of ethylzinc carboxylate species were synthesised and studied by NMR spectroscopy (EtZn(OOCR); R = H, CH3, and (CH2)nCH3

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36

Charette, Bronte J. "Synthesis, coordination chemistry and reactivity of new diarylamido and disilylamido SeNSe pincer ligands." Canadian Science Publishing, 2015. http://hdl.handle.net/1993/31830.

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This thesis presents advancements in the chemistry of selenium-bearing pincer ligands with respect to their synthesis, metal association and reactivity in addition to the overall nature of selenium as a donor atom. The synthesis of a new disilylamido ligand HN(SiMe2CH2SePh)2 2.1 and its potassium salt 2.2 is reported. The attempted metal association of these species was unsuccessful with various transition metals. Multinuclear NMR data suggests coordination to silver(I), 2.3 and copper(I), 2.4 with dπ-dπ back donation from the metal to the selenium donors. It is suggested from this data that

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37

Kaplan, Hilan. "A General Approach to Cis-Fused Sesquiterpene Quinones and Synthesis, Characterization, and Catalytic Applications of Bis(Imino)-N-Heterocyclic Carbene Complexes of Iron." Thesis, Boston College, 2014. http://hdl.handle.net/2345/3862.

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Thesis advisor: James P. Morken<br>Sesquiterpene quinones are a prolific class of marine natural products that are particularly interesting due to their antibacterial, antiviral, and anti-inhibitory properties. Hundreds of these biologically active molecules are based on decalin frameworks, both cis- as well as trans-fused, however, significantly less synthetic work has focused on targeting the cis-fused series of compounds. In this chapter, progress towards an asymmetric, general route to various sesquiterpene quinones in the cleordane family of natural products will be described. The key ste

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38

Hlavinka, Mark Louis. "Dizinc organometallics based on pre-organized binucleating bis(amidoamine) ligands; synthesis, structure, and reactivity of zinc enolates." Diss., Connect to online resource, 2006. http://gateway.proquest.com/openurl?url_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:dissertation&res_dat=xri:pqdiss&rft_dat=xri:pqdiss:3207756.

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39

Mayberry, Darrell D. "Synthesis, Characterization, and Reactivity of Prochiral Ruthenium Clusters and Bimetallic Rhenium Complexes with an Unsymmetrical Diphosphine and Hard-Soft Donor Ligands." Thesis, University of North Texas, 2019. https://digital.library.unt.edu/ark:/67531/metadc1538707/.

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The reaction of [BrRe(CO)₄]₂ with 2-(diphenylphosphino)pyridine (PN) and 6-(diphenylphosphino)-2-formylpyridine (PON) was investigated. The reactions were regiospecific and exclusively produced the phosphorus-coordinated products, BrRe(CO)₄(κᵖ-PN) and BrRe(CO)₄(κᴾ-PON). The kinetics for the chelate ring closure (κᴾ→ κᴾᴺ) in BrRe(CO)₄(κᴾ-PN) were confirmed to occur by dissociative CO loss. The reaction of [BrRe(CO)₄]₂ with 2-(diphenylphosphino)pyridine (PN) was modeled computationally by DFT calculations. The preferred reaction pathway for the substitution reaction was determined to occur by di

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40

Thomas, Jaron Michael. "On Metal synthesis of Some Substituted Rhenium and Manganese Complexes." TopSCHOLAR®, 2012. http://digitalcommons.wku.edu/theses/1225.

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Heterocyclic organic and organometallic compounds (i.e. polypyrrole), and their derivatives, have been of great interest for conductive polymers due to their novel properties and environmental stability as compared to their non-aromatic analogs (i.e. polyacetylene). Our current interest focus upon the potential role of metal ligand bound pyridazines as the next generation of electronic devices that utilize the metal ligands bound to organics as the semiconducting material. Pyridazine is a 6-membered aromatic ring with two adjacent nitrogen atoms. These are promising candidates for a variety of

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41

Clevenger, Margo. "Synthetic Routes to 3-Fold Symmetric Tridentate Oxygen Donor Ligands." Thesis, Virginia Tech, 1997. http://hdl.handle.net/10919/36964.

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The class of ligands represented by [CpCo(P(O)(OR)2)3]-, L- , were first synthesized by W. KlÃ¤ui in 1977. These ligands have been found to coordinate to a variety of low and high oxidation state metals through the use of its three P=O oxygen atoms as donors. The ligands act as mono-anionic six electron donors which make them similar to the more widely known cyclopentadienyl ligands, (C5H5-xRx)-, but have electronic properties like those of fluoride or oxide. Also, it has been found that the coordination chemistry of L- resembles the unsubstituted tris(pryrazolyl)hydroborato six electron

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42

Palmer, Erick J. "Synthesis, characterization and density functional theory investigations of tris-cyclopentadienyl compounds of zirconium and hafnium." The Ohio State University, 2005. http://rave.ohiolink.edu/etdc/view?acc_num=osu1109969235.

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43

Smith, Charlene Amanda. "The synthesis and magnetochemistry of transition and lanthanide metal compounds." Thesis, University of Manchester, 2013. https://www.research.manchester.ac.uk/portal/en/theses/the-synthesis-and-magnetochemistry-of-transition-and-lanthanide-metal-compounds(1f50bd6e-19e2-4cf6-9211-e22fcef578f9).html.

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The introductory Chapter to this thesis outlines fundamental aspects of 4f lanthanide(III) coordination chemistry, in particular compounds that possess the intriguing properties of slow relaxation of magnetisation, (or the ability to behave as single-molecule magnets, SMMs). The recent renaissance into the study of the magnetic behaviour of 4f-coordination complexes has led to the consideration of utilising organometallic precursors for the development of novel lanthanide containing compounds, which may possess interesting magnetic properties, subsequently forming the basis of Chapter Two. In

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44

Stokes, Francesca Alice. "Synthetic applications of polar transition metal metallocenes." Thesis, University of Cambridge, 2013. https://www.repository.cam.ac.uk/handle/1810/264975.

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Since the sandwich structure of ferrocene was elucidated in 1952, metallocenes have generated a vast amount of interest. Transition metal metallocenes have previously been shown to be suitable precursors in the syntheses of novel organometallic and metallo-organic complexes, although the use of metal halide starting materials for organometallic synthesis is much more common due to their being readily commercially available and generally easier to handle than the extremely air- and moisture-sensitive metallocene alternatives. In this project, the polar transition metal metallocenes Cp2V, Cp2Cr,

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45

Poulten, Rebecca. "Synthesis and reactivity of low coordinate nickel(I) complexes bearing ring expanded N-heterocyclic carbene ligands." Thesis, University of Bath, 2015. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.669038.

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This thesis describes the development of nickel(I) complexes incorporating ring expanded N-heterocyclic carbene (RE NHC) ligands and examines their electronic characterisation, activation of O2, reactivity and catalytic applications. A series of three coordinate, paramagnetic Ni(I) complexes of the form Ni(RE NHC)(PPh3)Br (1 – 10) were prepared by comproportionation of Ni(COD)2 and Ni(PPh3)2Br2 in the presence of RE NHCs. The RE NHCs employed varied in the degree of ring expansion (6-, 7- and 8-membered), extent of N-substituent steric bulk (Mes, oTol, oAnis) and the donor/acceptor properties

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46

Bertrand, Benoit. "Gold-based complexes : synthesis and evaluation as anticancer agents." Thesis, Dijon, 2015. http://www.theses.fr/2015DIJOS013.

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Depuis sa mise sur le marché à la fin des années 70, le Cisplatin est devenu l’un des pricipaux agents de chimiothérapie anticancéreuse. Actuellement, les composés à base de platine sont présents dans la majorité des coktails de chimiothérapie. Cependant, malgré leur succès clinique, ces composés présentent de nombreux inconvenients comme par exemple de nombreux et graves effets secondaires. Une des stratégies envisagées pour parer à ces défauts a été de remplacer le platine par d’autres métaux de transition. Parmi les différents métaux possibles, l’or est apparu comme particulièrement promett

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47

Qin, J. "Studies in organometallic solid state chemistry." Thesis, University of Oxford, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.379942.

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48

Zini, Simone. "Synthesis of manganese organometallic complexes." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2021. http://amslaurea.unibo.it/22235/.

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Il presente lavoro di tesi si inserisce in un progetto di ricerca volto alla sintesi di nuovi complessi di metalli di transizione per lo sviluppo di catalizzatori da impiegare in reazioni di catalisi omogenea. In particolare il mio progetto si è concentrato sulla sintesi di complessi organometallici di manganese con leganti carbenici N-eterociclici (NHC). La scelta dei leganti è stata effettuata in modo tale da poter avere leganti chelanti NHC di tipo MIC (mesoionic carbene) sintetizzati tramite cicloaddizione tra un alchino ed un azide catalizzata da rame (CuAAC) e N-alchilazione. Lo studio d

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49

Lee, Peter D. "Organometallic synthesis in supercritical fluids." Thesis, University of Nottingham, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.336862.

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50

Stewart, A. S. J. "Organometallic derivatives of amino acids and peptides." Thesis, Robert Gordon University, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.376684.

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