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1

Couny, Francois. "Photonic solutions towards optical waveform synthesis." Thesis, University of Bath, 2008. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.478946.

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This thesis presents the development of photonic tools towards the realisation of an optical intensity waveform synthesiser and of an attosecond pulse synthesiser based on the generation and Fourier synthesis of a continuous-wave coherent spectral comb spanning more than 3 octaves (UV to mid-IR) by use of a gas-filled hollow core photonic crystal fibre (HC-PCF).
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2

Atallah, Jad G. "Integrated frequency synthesis for convergent wireless solutions /." Stockholm : Informations- och kommunikationsteknik, Kungliga Tekniska högskolan, 2008. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-9486.

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3

Ranatunga, Lalith Priyadarshi. "Processes synthesis by solving context equations in CCS." Thesis, University of Kent, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.328086.

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4

Kruger, Elna. "Ionic liquids as media for electro-organic synthesis." Thesis, Nelson Mandela Metropolitan University, 2007. http://hdl.handle.net/10948/538.

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The IL’s used in this study were either synthesized or commercially available. Preparation of the IL’s involved 2 step processes: firstly the heating of distilled 1-methylimidazole with distilled 1-chlorobutane under reflux to obtain 1-butyl-3- methylimidazolium chloride; secondly, the metathesis reaction of sodium tetrafluoroborate with 1-butyl-3-methylimidazolium chloride to obtain 1-butyl-3- methylimidazolium tetrafluoroborate. The addition of sodium tetrafluoroborate, sodium hexafluorophosphate and lithium trifluoromethane sulfonamide with 1-butyl-3-methylimidazolium chloride produced good
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5

Parnham, Emily Ruth. "Ionothermal synthesis : a new synthesis methodology using ionic liquids and eutectic mixtures as both solvent and template in zeotype synthesis." Thesis, University of St Andrews, 2006. http://hdl.handle.net/10023/10224.

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The aim of this thesis was to research the new synthesis methodology of ionothermal synthesis, used for the synthesis of zeolite type materials, mainly aluminophosphates. An ionic liquid or eutectic mixture is to act as both the organic template and the solvent, hence eliminating the space filling effects in the reaction from the water. Initial reactions were carried out using the ionic liquid 1-ethyl-3-methylimidazolium bromide which acted as the solvent and template in the production of four three-dimensional structures and one layered structure. The addition of cobalt into the aluminophosph
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6

Yuan, Qiuhua. "Electrochemical Synthesis and Characterization of Inorganic Materials from Aqueous Solutions." Thesis, University of North Texas, 2006. https://digital.library.unt.edu/ark:/67531/metadc5604/.

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The dissertation consists of the following three sections: 1. Hydroxyapatite (HA) coatings. In this work, we deposited HA precursor films from weak basic electrolytic solution (pH= 8-9) via an electrochemical approach; the deposits were changed into crystallite coatings of hydroxyapatite by sintering at specific temperatures (600-800 ºC). The formed coatings were mainly characterized by powder X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM). XRD patterns show well-defined peaks of HA when sintered under vacuum conditions. FTIR mea
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7

Ganguly, Adrish Barsoum M. W. "Synthesis and characterization of solid solutions of M(N+1)AXN phases /." Philadelphia, Pa. : Drexel University, 2006. http://dspace.library.drexel.edu/handle/1860/728.

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8

Nie, Fei. "Synthesis and characterization of poly(ester-imide)s /." Online version of thesis, 1989. http://hdl.handle.net/1850/10685.

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9

Jia, Wenling. "Synthesis and nonlinear optical properties of semiconductor nanoparticles within ionomer solutions." [Gainesville, Fla.] : University of Florida, 2003. http://purl.fcla.edu/fcla/etd/UFE0002379.

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10

Buffinger, Delbert Richard. "The Synthesis and Characterization of Fullerene Salts From Liquid Ammonia Solutions /." The Ohio State University, 1996. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487931993467843.

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11

Zaslavskaya, L. V., E. E. Belousova, S. V. Radio, et al. "Finely Dispersed Powders of Silicon-substituted Hydroxyapatite Obtained from Solutions." Thesis, Sumy State University, 2013. http://essuir.sumdu.edu.ua/handle/123456789/35110.

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Bioactive powders of silicon substituted hydroxyapatites containing 1.4-4.3 wt % Si were synthesized by precipitation from aqueous solutions of calcium nitrate and ammonium (sodium) hydrophospate. Tetra-ethoxysilane and sodium silicate in basic media were used as a source of silicon. Using scanning electron microscopy, surface morphology of the obtained products was studied. It has been found that procedure us-ing sodium silicate allows obtaining of materials with 100-200 nm particle size. Procedure that utilizes tet-raethoxysilane leads to 40-100 nm particles. Chemical, X-ray phase analysis a
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12

Elago, Elago R. T. "The solvent-free approach versus the use of ionic liquids in the synthesis of ferrocenes." Thesis, Nelson Mandela Metropolitan University, 2008. http://hdl.handle.net/10948/853.

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The philosophy of green chemistry has seen much development in the past decade. The use of environmentally benign solvents is amongst the areas of green chemistry that have received the most attention. In this context, imidazolium ionic liquids have been widely reported to offer high product yields, fast reaction rates, excellent selectivity and generally mild working conditions, when used as reaction media. In addition, concerns about costs of solvents and the long-term environmental impact that can potentially result when solvents are discarded after their use have led to focused investigati
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13

Shekunova, T. O., O. S. Ivanova, A. E. Baranchikov, V. K. Ivanov, and A. B. Shcherbakov. "Synthesis of Stable Aqueous Ceria Sols and Study of Their Toxicity." Thesis, Sumy State University, 2012. http://essuir.sumdu.edu.ua/handle/123456789/34954.

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Cerium dioxide is a unique material which is promising for biomedical applications. The properties of ceria are definitely determined by synthesis procedure and further treatment conditions. The vast majority of currently existing methods of synthesis lead to formation of CeO2 in the form of nanopowders, but in some cases (e.g., in biological applications), such powders can not be used because they do not quite satisfy practical requirements. So, in this work we succeed in synthesis of ceria-stable sols with controlled small particle size (2-4 nm) using an inexpensive and facile method an
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14

Wang, Mingsheng. "Thermodynamic modelling of aqueous solutions and applications in some functional materials synthesis /." Stockholm : Tekniska högsk, 1999. http://www.lib.kth.se/abs99/wang0528.pdf.

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15

Shyue, Jing-Jong. "Synthesis of Titanium-Vanadium Oxide Materials from Aqueous Solutions via Co-deposition." Case Western Reserve University School of Graduate Studies / OhioLINK, 2004. http://rave.ohiolink.edu/etdc/view?acc_num=case1089651720.

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16

Wang, Yu. "Synthesis, electrochemical reactivity and electronic structure of 1-R-métallatranes (M=Si,Sn)." Rennes 1, 2012. https://ecm.univ-rennes1.fr/nuxeo/site/esupversions/ee3a66ea-faa0-40e9-86c1-a2e4a88a478e.

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Metallatranes (M = Si, Ge, Sn) have been studied intensively during 50 years and have many applications in various domains namely physics, biology, medicine and so on. However their electrochemical properties were poorly studied up to date. In the present work, new metallatranes have been synthesized and characterized using different approaches and techniques (organic synthesis, cyclic voltammetry, preparative electrolysis, EPR, spectroelectrochemistry, cyclic voltammetry coupled with EPR, NMR, GC-MS). Several novel structures of metallatranes have been obtained and validated by XRD. Electroch
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17

Dean, Jill Barbara. "Development of a novel material for the selective removal of metal ions from dilute solutions." Thesis, University of York, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.336570.

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18

Okello, Maurice O. "Polar ionic media and stabilized charged species in organic synthesis ionic liquids derived from a biorenewable source, d-fructose, as a possible alternative to conventional organic reaction solvents /." Diss., Online access via UMI:, 2004. http://wwwlib.umi.com/dissertations/fullcit/3150493.

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19

Krupko, O. V., Yu B. Khalavka, and L. P. Shcherbak. "Effect of Ph of Synthesis on CdS/L-Cys Colloidal Solutions Optical Properties." Thesis, Міжнародна конференція з фізики і технології тонких плівок і наносистем МКФТТПН-XV-ICPTTFN, 2015. http://dspace.bsmu.edu.ua:8080/xmlui/handle/123456789/9735.

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20

Chae, Mi-Young. "Synthesis and study of conjugate fluorescence probes for analyte detection in aqueous solutions /." The Ohio State University, 1993. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487841548270506.

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21

TADOKORO, SANDRA K. "Sintese de pos de zirconia estabilizada com tamanho nanometrico de particulas." reponame:Repositório Institucional do IPEN, 2000. http://repositorio.ipen.br:8080/xmlui/handle/123456789/9275.

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22

MAGADALENA, CARINA P. "Síntese de zeólitas de cinzas de carvão modificada por surfactante e aplicação na remoção de ácido laranja 8 de solução aquosa: estudo em leito móvel, coluna de leito fixo e avaliação ecotoxicológica." reponame:Repositório Institucional do IPEN, 2015. http://repositorio.ipen.br:8080/xmlui/handle/123456789/23651.

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Submitted by Claudinei Pracidelli (cpracide@ipen.br) on 2015-04-10T14:03:59Z No. of bitstreams: 0<br>Made available in DSpace on 2015-04-10T14:03:59Z (GMT). No. of bitstreams: 0<br>Tese (Doutorado em Tecnologia Nuclear)<br>IPEN/T<br>Instituto de Pesquisas Energeticas e Nucleares - IPEN-CNEN/SP
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23

Bei, Guo-Ping. "Synthesis, microstructural characterization and mechanical properties of nanolaminated Ti3AlxSn(1-x)C2 MAX phases." Poitiers, 2011. http://nuxeo.edel.univ-poitiers.fr/nuxeo/site/esupversions/9a20805b-0e53-47c0-8b16-c1a4ac3c2042.

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Les travaux exposés dans cet ouvrage portent sur l'élaboration, la caractérisation microstructurale et les propriétés mécaniques de solutions solides nanolamellaires de phases dites MAX. Les phases MAX représentent une classe exceptionnellement étendue de céramiques. Elles répondent à une formule générale du type Mn+1AXn (n=1, 2 ou 3) où M est un métal de transition, A est un métal des groupes IIIA ou IVA, et X est un métalloïde (C ou N). Nous avons dans un premier temps réalisé l'optimisation de la synthèse, par métallurgie des poudres, de Ti3AlC2 pur. Une nouvelle phase, Ti3SnC2, ayant été d
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24

Yu, Wenbo. "Synthesis, microstructural characterization, mechanical and transport properties of Ti2Al(CxNy) solid solutions and their relative end-members." Thesis, Poitiers, 2014. http://www.theses.fr/2014POIT2267/document.

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Les travaux exposés dans cet ouvrage décrivent la synthèse, la caractérisation microstructurale et les propriétés physiques de solutions solides nanolamellaires des phases MAX. Les phases Mn+1AXn (M : métal de transition, A : un métal des groupes IlIA ou IV A, et X: carbone ou azote) constituent une famille de nitrures et de carbures ternaires (n = 1 à 3), qui possèdent les meilleures propriétés des métaux et les meilleures propriétés des céramiques.Lors d'une première étape, nous nous concentrons sur la synthèse de solutions solides pures et denses de Ti2AICxNy par compression isostatique à c
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25

Bivigou, Koumba Achille Mayelle. "Design, Synthesis and Characterisation of Amphiphilic Symmetrical triblock copolymers by the RAFT process : their self-organisation in dilute and concentrated aqueous solutions." Phd thesis, Universität Potsdam, 2009. http://opus.kobv.de/ubp/volltexte/2009/3954/.

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This work presents the synthesis and the self-assembly of symmetrical amphiphilic ABA and BAB triblock copolymers in dilute, semi-concentrated and highly concentrated aqueous solution. A series of new bifunctional bistrithiocarbonates as RAFT agents was used to synthesise these triblock copolymers, which are characterised by a long hydrophilic middle block and relatively small, but strongly hydrophobic end blocks. As hydrophilic A blocks, poly(N-isopropylacrylamide) (PNIPAM) and poly(methoxy diethylene glycol acrylate) (PMDEGA) were employed, while as hydrophobic B blocks, poly(4-tert-butyl st
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26

Ezzatahmadi, Naeim. "Synthesis and characterisation of mineral based composite materials for the remediation of contaminated aqueous solutions." Thesis, Queensland University of Technology, 2019. https://eprints.qut.edu.au/131822/1/Naeim%20Ezzatahmadi%20Thesis.pdf.

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Expanding urbanisation and industrialisation have increased aqueous concentrations of organic contaminants which are toxic to human health and the environment. Hence, remediation of these contaminants from aqueous solutions has become an important environmental concern. This research project aims to synthesize novel mineral-based composite materials, namely diatomite/Fe/Ni, palygorskite/Fe/Ni and sepiolite/Fe/Ni and study their applications for the removal of Orange II and 2,4-dichlorophenol from water. Experimental investigations contain material characterization, batch removal experiments, k
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27

Hepburn, James. "An investigation into the enhancement of fluorescence of disazo pigments by their synthesis in micellar solutions." Thesis, University of Strathclyde, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.486456.

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The fluorescence of a series of commercially important yellow disazo pigments have been investigated with a view to enhancing fluorescence in the solid state. Solution absorption and fluorescence measurements in 1,2,4-trichloroben2;ene for some of the pigments was hampered by poor solubility. A comparison of the fluorescence intensities - normalised with respect to the amount of light absorbed - showed PY63 as being the most fluorescent in solution followed by PY12; PY14 and PY13. Fluorescence of the pigments in the solid state (as printed inks and aqueous dispersion~) showed that the relative
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28

Cameron, Christopher Stan. "Synthesis of Amphiphilic Iron-Sulfur Core Dendrimers and Investigations into Their Encapsulation Abilities in Different Solutions." NCSU, 2005. http://www.lib.ncsu.edu/theses/available/etd-07072005-133617/.

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Several novel amphiphilic iron-sulfur core dendrimers were synthesized by modifying the tips of the dendrons to install hydrophilic peripheries. These dendrimers were synthesized via standard convergent and a ?modular? synthetic strategy. The electrochemistry of the dendrimers was investigated in dimethylformamide and dimethylformamide/water solutions. Positive shifts in the redox potential of the iron-sulfur cores corresponding to dendrimer size and periphery type were recorded. Secondary peaks in the anodic wave of cyclic voltammograms of dendrimers in dimethylformamide/water solutions were
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29

Ye, Guozhong. "Synthesis and reactions of cyclic ketene-N,N-acetals." Diss., Mississippi State : Mississippi State University, 2008. http://library.msstate.edu/etd/show.asp?etd=etd-09142008-210135.

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30

Christophe, François. "Semantics and Knowledge Engineering for Requirements and Synthesis in Conceptual Design: Towards the Automation of Requirements Clarification and the Synthesis of Conceptual Design Solutions." Phd thesis, Ecole centrale de nantes - ECN, 2012. http://tel.archives-ouvertes.fr/tel-00977676.

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This thesis suggests the use of tools from the disciplines of Computational Linguistics and Knowledge Representation with the idea that such tools would enable the partial automation of two processes of Conceptual Design: the analysis of Requirements and the synthesis of concepts of solution. The viewpoint on Conceptual Design developed in this research is based on the systematic methodologies developed in the literature. The evolution of these methodologies provided precise description of the tasks to be achieved by the designing team in order to achieve successful design. Therefore, the argu
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31

Kolanka, Varun Kiran. "Cost Effective Synthesis of Ionic Liquids and Their Thermal Properties." TopSCHOLAR®, 2014. http://digitalcommons.wku.edu/theses/1398.

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Ionic liquids (ILs) are liquid organic salts at room temperature which are composed of only ions (cations and anions). Ionic liquids are regarded as “novel solvents” and have been gaining attention as alternatives to volatile molecular organic solvents. Ionic liquids have outstanding properties, such as negligible vapor pressure (no or limited evaporation or volatilization), low melting point, thermal stability, and ionic conductivity. They can be used in efficient and clean energy production and storage. The synthesis of the low-cost and performance-effective ionic liquids using inexpensive r
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32

Li, Wen. "Synthesis and solubility of arsenic tri-sulfide and sodium arsenic oxy-sulfide complexes in alkaline sulfide solutions." Thesis, University of British Columbia, 2013. http://hdl.handle.net/2429/44546.

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Alkaline sulfide leaching (ASL) at approximately 100 ºC has been used to selectively extract arsenic and antimony from enargite and tetrahedrite concentrates. Sodium thio-arsenate has been postulated to crystallize from alkaline sulfide leaching solutions upon cooling. However, literature data on the solubility of sodium thio-arsenate as well as proof of its crystallization from ASL solutions is scant. In this thesis, the solubility of leach-produced and synthetic sodium thio-arsenate is studied. To determine arsenic solubility in ASL solutions, sodium thio-arsenate and sodium arsenic oxide s
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33

Ozawa, Naoshi. "Preparation, micro fabrication and advanced function development of ceramic thin films by using synthesis from aqueous solutions." Kyoto University, 2003. http://hdl.handle.net/2433/148257.

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34

Li, Peng. "Innovative process solutions towards recycling of salt cake from secondary aluminum smelting." Doctoral thesis, KTH, Materialens processvetenskap, 2012. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-101074.

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To offer better solutions for the recycling of salt cake from secondary aluminum melting, several innovative investigations were carried out based on hydrometallurgical and pyrometallurgical views. Thermal diffusivity measurements as a function of temperature on salts-Al composites having various compositions (0, 2, 4, 6, 8, 10, 12wt pct metallic Al) were carried out. Its attempt to derive theoretical relationships between aluminium contents in the salt-Al composites and the thermal conductivities so that these would serve as calibration curves for industrial samples taken out from secondary a
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35

Kas, Onur Y. "Design, synthesis and characterization of bio/electroactive hybrids confining chromophores in dilute solutions using a helical peptide template /." Access to citation, abstract and download form provided by ProQuest Information and Learning Company; downloadable PDF file, 148 p, 2008. http://proquest.umi.com/pqdweb?did=1459918061&sid=4&Fmt=2&clientId=8331&RQT=309&VName=PQD.

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36

Huston, Michael Edward. "Synthesis and study of anthrylmethylpolyamine conjugate fluorescence probes for metal and non-metal ion detection in aqueous solutions /." The Ohio State University, 1990. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487683049375178.

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37

Alby, Delhia. "Matériaux innovants pour la rétention sélective de césium et de strontium à partir de solutions aqueuses multi-composants : synthèse, optimisation et évaluation des performances." Thesis, Montpellier, 2017. http://www.theses.fr/2017MONTT168.

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Ce travail porte sur la synthèse et la caractérisation de nouveaux matériaux afin de proposer une alternative dans le cadre de la dépollution nucléaire. Dans une première partie bibliographique, les principaux matériaux inorganiques utilisés pour ce procédé sont décrits en précisant leurs capacités de sorption. Les matériaux lamellaires apparaissent comme possédant un fort potentiel pour cette application. Deux solides ont retenu notre attention : les nanostructures à base de vanadates et de manganates.Des synthèses solvothermales sous flux micro-ondes de ces composés sont ensuite développées,
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38

Heuvel, Whitney. "Effect of precursor anion in alcohol/water solutions during hydro/solvothermal synthesis on cobalt oxide morphology and catalytic ability." Thesis, Cape Peninsula University of Technology, 2020. http://hdl.handle.net/20.500.11838/3046.

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Thesis (MEng (Chemical Engineering))--Cape Peninsula University of Technology, 2020<br>The textile industry requires water for practically every step during its manufacturing process, and would benefit from water reuse systems. This is challenging, as the reactive dyes used in this industry often escape the conventional wastewater treatment methods used. The use of advanced oxidation processes combats these challenges, as it allows for the conversion of organic toxic waste to harmless H2O and CO2. Potassium peroxymonosulphate (Oxone®) has become popular in these treatment methods, as highly ac
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39

Molina, Julien. "Unsaturated polyesters synthesis for low viscosity and styrene-free resins." Electronic Thesis or Diss., Université de Lille (2018-2021), 2019. http://www.theses.fr/2019LILUR083.

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Les résines polyesters insaturées sont majoritairement utilisées dans le domaine des composites. Etant donnée la viscosité élevée de ces polyesters, il est nécessaire de les diluer avec un solvant réactif pour que la résine puisse être facilement appliquée. Le diluant réactif le plus couramment utilisé est le styrène. Les taux de dilutions sont environ de 35-39%. Cependant le styrène est étiqueté CMR et a fait l’objet d’une valeur limite d’exposition au 1er Janvier 2019. Il est donc nécessaire de réduire ou de changer de diluant réactif afin de respecter les nouvelles normes à venir. A cette f
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40

Rolland, David. "Nanofluidique de solutions polymériques appliquées à la synthèse in situ d'oligosaccharides." Phd thesis, Université de Grenoble, 2012. http://tel.archives-ouvertes.fr/tel-00721738.

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Les biopuces connaissent un grand essor depuis quelques années avec des applicationspossibles pour l'ADN, les protéines et les oligosaccharides. Une puce à oligosaccharidesprésente des difficultés par rapport à une puce à ADN notamment par les contraintes entempérature et il existe moins de travaux dans ce domaine. Ce travail est donc consacré àl'étude d'une puce à oligosaccharide, par synthèse supportée et par masquage avec un film depolymère. Le procédé de fabrications est particulièrement détaillé.Nous étudions tout d'abord expérimentalement la formation d'un film de polymère obtenu parévap
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41

Beija, Mariana. "Synthesis of -dye-labelled thermoresponsive block copolymers by raft polymerization : behaviour at the air-water interface and in aqueous solutions." Thesis, Lyon 1, 2009. http://www.theses.fr/2009LYO10116.

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Les copolymères à blocs di-hydrophiles contenant un bloc thermosensible reçoivent une attention croissante grâce à leur capacité d’auto-organisation en micelles induite par une variation de température. Néanmoins, peu de travaux ont été consacrés à l’étude de leur conformation par fluorescence et de leur dynamique à l’interface air-eau et en solution aqueuse. Dans ce travail, des copolymères à blocs composés d’un bloc thermosensible deN,N-diéthylacrylamide (DEA) et d’un bloc hydrophile de N,N-diméthylacrylamide (DMA) ou d’un bloc réactif [copolymère statistique de DMA et de N-acryloxysuccinimi
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42

Pavelko, Roman G. "Sno2 based oxide systems: synthesis, material science and sensing properties as a function of surface hydroxyls." Doctoral thesis, Universitat Rovira i Virgili, 2010. http://hdl.handle.net/10803/8472.

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The thesis is dedicated to the synthesis, comprehensive material science and some sensing properties of SnO2-MetOx oxide systems (where MetOx are IVB and IIIB metal oxides). The study was performed in comparison with blank SnO2, and SnO2 doped with noble metals (Pd, Pt, Rh and their binary mixtures). Results of 8 ex-situ (TEM, HRTEM, XRD, FTIR, UV-Vis, BET, XPS and element analysis), 5 in-situ (TGA, MS-analysis, DRIFT, TXRD, TPR) techniques and sensing properties characterization (DC measurements as a function of temperature and gas composition) are discussed regarding surface chemistry of SnO
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43

Molina, Julien. "Unsaturated polyesters synthesis for low viscosity and styrene-free resins." Thesis, Lille 1, 2019. http://www.theses.fr/2019LIL1R083.

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Les résines polyesters insaturées sont majoritairement utilisées dans le domaine des composites. Etant donnée la viscosité élevée de ces polyesters, il est nécessaire de les diluer avec un solvant réactif pour que la résine puisse être facilement appliquée. Le diluant réactif le plus couramment utilisé est le styrène. Les taux de dilutions sont environ de 35-39%. Cependant le styrène est étiqueté CMR et a fait l’objet d’une valeur limite d’exposition au 1er Janvier 2019. Il est donc nécessaire de réduire ou de changer de diluant réactif afin de respecter les nouvelles normes à venir. A cette f
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44

Fasol, Silvia. "Exploring the potential of transaminases in aqueous organic solvent solutions through protein engineering: a resource to optimise the synthesis of chiral amines." Thesis, KTH, Skolan för bioteknologi (BIO), 2014. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-163680.

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Garcia-Barron, Javier Enrique. "Synthesis and study of chelating polymers and their application to protein and metal separation from aqueous solutions using novel metal affinity interaction techniques." Diss., The University of Arizona, 1999. http://hdl.handle.net/10150/283931.

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The main objective of this research work was the development, synthesis, and study of polymeric chelating derivatives. These derivatives were characterized in terms of their specific metal affinity interaction with biomolecules and metal ions. These engineered materials were used to test their feasibility as tools for separation of proteins and heavy metal ions from aqueous solutions using different affinity separation techniques. Linear and branched polymers were synthesized to create a variety of materials. Among the linear polymers synthesized was the chelated monomethoxy poly(ethylene) gly
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Gonzaga, de Resende Valdirene. "Synthesis and characterization of Fe-containing oxide powders and carbon nanotube-Fe-oxide nanocomposites." Toulouse 3, 2009. http://thesesups.ups-tlse.fr/493/.

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Les nanotubes de carbone (NTC), très petits, creux et monodimensionnels, sont très étudiés du fait de leurs excellentes propriétés thermiques, électriques et mécaniques. Les buts de cette thèse étaient premièrement de préparer des poudres et mousses de solutions solides Fe/Al2O3 et des poudres Fe/Al6Si2O13, servant comme matériaux catalytiques pour la synthèse de nanocomposites NTC-Fe-oxyde, et deuxièmement de faire une étude approfondie de tous ces matériaux par spectroscopie Mössbauer du 57Fe et de corréler les résultats avec ceux issus d'autres techniques, de manière à obtenir des informati
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He, Man [Verfasser], Björn [Akademischer Betreuer] [Gutachter] Winkler, and Eiken [Gutachter] Haussühl. "Mechanochemical activation assisted solid state synthesis, self-propagating high-temperature synthesis, and characterisation of Ti-containing solid solutions with spinel-, pseudobrookite- and Mn5Si3-type structures / Man He ; Gutachter: Björn Winkler, Eiken Haussühl ; Betreuer: Björn Winkler." Frankfurt am Main : Universitätsbibliothek Johann Christian Senckenberg, 2016. http://d-nb.info/111860721X/34.

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Nicodeme, Marc. "Identifiabilité des signaux parcimonieux structurés et solutions algorithmiques associées : application à la reconstruction tomographique à faible nombre de vues." Thesis, Bordeaux, 2016. http://www.theses.fr/2016BORD0096/document.

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Cette thèse étudie différents problèmes de minimisations avec des fonctions de régularisations qui promeuvent la parcimonie. Plus précisément, on souhaite reconstruire une image, que l'on suppose parcimonieuse et qui a subit une transformation après un opérateur linéaire, à l'aide de problèmes de minimisations. Dans ce manuscrit, on s'intéressera plus particulièrement à la minimisation l1 synthèse, analyse et bloc qui sont très utilisées pour reconstruction une image que l'on sait parcimonieuse. Ces minimisations produisent en pratique des résultats convaincants qui n'ont été compris théorique
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Vijayakrishnan, Balakumar. "Solution and solid phase synthesis of N,N'-diacetyl chitotetraoses." Phd thesis, Universität Potsdam, 2008. http://opus.kobv.de/ubp/volltexte/2008/1883/.

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The three major biopolymers, proteins, nucleic acids and glycoconjugates are mainly responsible for the information transfer, which is a fundamental process of life. The biological importance of proteins and nucleic acids are well explored and oligosaccharides in the form of glycoconjugates have gained importance recently. The β-(1→4) linked N-acetylglucosamine (GlcNAc) moiety is a frequently occurring structural unit in various naturally and biologically important oligosaccharides and related conjugates. Chitin which is the most abundant polymer of GlcNAc is widely distributed in nature where
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Souleiman, Manhal. "Études des solutions solides de type M(1-x)M'xXO4 homéotypes du quartz-alpha et cristallogenèse d’un matériau bi-fonctionnel GaAsO4 à propriétés piézoélectriques et optiques non linéaires." Thesis, Montpellier 2, 2013. http://www.theses.fr/2013MON20182/document.

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Des cristaux de Ga1-xFexPO4 ont été obtenus par voie hydrothermale avec xmax=0.23. La synthèse hydrothermale in-situ par spectroscopie d'absorption des rayons X a permis de mettre en évidence le rôle essentiel des cations Ga3+ lors de la nucléation et la cristallisation de la phase mixte Ga1-xFexPO4 de structure quartz-α. La solution solide a été particulièrement étudiée par spectroscopie Raman et des calculs théoriques par DFT ont permis d'identifier clairement les modes de vibration dont la fréquence dépend de la composition chimique du matériau (modes couplés). Dans la même famille des maté
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