Relevant bibliographies by topics / Synthesis of Thioureas

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  1. Journal articles
  2. Dissertations / Theses
  3. Books
  4. Book chapters
  5. Conference papers

Academic literature on the topic 'Synthesis of Thioureas'

Author: Grafiati
Published: 5 June 2025
Last updated: 1 August 2025

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Journal articles on the topic "Synthesis of Thioureas"

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Ngaini, Zainab, Wan Sharifatun Handayani Wan Zulkiplee, and Ainaa Nadiah Abd Halim. "One-Pot Multicomponent Synthesis of Thiourea Derivatives in Cyclotriphosphazenes Moieties." Journal of Chemistry 2017 (2017): 1–7. http://dx.doi.org/10.1155/2017/1509129.

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In this study, hexasubstituted thiourea was carried out via reaction of isothiocyanato cyclophosphazene intermediates with a series of aromatics amines and amino acids in a one-pot reaction system. The reaction was not as straightforward as typical thiourea synthesis. Six unexpected thiourea derivatives3a–fwere formed in the presence of cyclotriphosphazene moieties in good yields (53–82%). The structures of3a–fwere characterized by elemental analysis and FTIR,1H,13C, and31P NMR spectroscopies. The occurrence of reverse thioureas formation in a one-pot reaction system is discussed. The possible
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Milosavljevic, Milutin, Ivan Vukicevic, Veis Serifi, et al. "Optimization of the synthesis of N-alkyl and N,N-dialkyl thioureas from waste water containing ammonium thiocyanate." Chemical Industry and Chemical Engineering Quarterly 21, no. 4 (2015): 501–10. http://dx.doi.org/10.2298/ciceq141221006m.

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The optimized methods for N-alkyl and N,N-dialkyl substituted thioureas synthesis starting from ammonium thiocyanates, waste water constituent from the production of tetramethylthiuram monosulfide (TMTS), and alkyl amine, are presented in this work. Therefore, thioureas synthesis was developed in two ways: Method I - reaction of the thiocyanate and alkylamine in the presence of hydrochloric acid; Method II - reaction of the thiocyanate with benzoyl chloride following by amine addition in the first step, and base hydrolysis in the second step. The structure of the synthesized compounds was conf
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Siddharth A. Waghmare and Swapnil B. Sarkate. "Design, synthesis and characterization of some novel Thiocarbamidopyrimidines." International Journal of Science and Research Archive 10, no. 2 (2023): 895–99. http://dx.doi.org/10.30574/ijsra.2023.10.2.1034.

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Interaction of 2 chloro pyrimidines with various substituted thioureas such as thiourea, N- phenylthiourea, 1,3 Dimethylthiourea, N- allylthiourea and ethyl thiourea were carried in presence of isopropanol as a medium. The product isolated in these reactions were characterized on the basis of elemental analysis, chemical characteristics and spectral studies.
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Elshaier, Yaseen A. M. M., Ashraf A. Aly, Mohamed Abdel-Aziz, et al. "Synthesis and Identification of New N,N-Disubstituted Thiourea, and Thiazolidinone Scaffolds Based on Quinolone Moiety as Urease Inhibitor." Molecules 27, no. 20 (2022): 7126. http://dx.doi.org/10.3390/molecules27207126.

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Synthesis of thiazolidinone based on quinolone moiety was established starting from 4-hydroxyquinol-2-ones. The strategy started with the reaction of ethyl bromoacetate with 4-hydroxyquinoline to give the corresponding ethyl oxoquinolinyl acetates, which reacted with hydrazine hydrate to afford the hydrazide derivatives. Subsequently, hydrazides reacted with isothiocyanate derivatives to give the corresponding N,N-disubstituted thioureas. Finally, on subjecting the N,N-disubstituted thioureas with dialkyl acetylenedicarboxylates, cyclization occurred, and thiazolidinone derivatives were obtain
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Erol Günal, Şule, and Engin Kaplan. "SYNTHESIS, EVALUATION OF ANTIFUNGAL ACTIVITY AND DRUG-LIKENESS OF BENZOYL THIOUREA DERIVATIVES." İstanbul Ticaret Üniversitesi Fen Bilimleri Dergisi 24, no. 47 (2025): 217–28. https://doi.org/10.55071/ticaretfbd.1588118.

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Herein, we report the synthesis of a series of 2-bromobenzoyl-substituted thiourea derivatives. The structures of the synthesized thioureas were characterized by spectroscopic methods. These derivatives, together with 2-fluorobenzoyl thioureas synthesized previously, have been evaluated for their potential antifungal activity. Compounds 2d and 2f showed antifungal activity against Candida albicans. Compound 2f also demonstrated activity against C. parapsilosis. Drug-likeness properties of the compounds were also estimated, and it was found that all compounds showed good drug-likeness propertie
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Chrzanowski, Jacek, Luca Sancineto, Malgorzata Deska, Michal Rachwalski, and Jozef Drabowicz. "Thioureas Derived from (S)-1-(2-pyridyl)ethylamine Enantiomer: Synthesis and Selected Applications as an Organocatalyst." Symmetry 17, no. 2 (2025): 216. https://doi.org/10.3390/sym17020216.

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In order to expand the group of chiral thiourea structures, several optically active thioureas derived from the (S)-1-(2-pyridyl)ethylamine enantiomer were prepared via its reaction with achiral or optically active isothiocyanates. To show their synthetic potential as chiral auxiliaries the isolated thioureas were tested as an optically active organocatalyst in the asymmetric version of the selected aldol condensation and addition of diethylzinc to benzaldehyde. The observation of asymmetric induction in these model reactions encourages further research on the use of this group of thioureas in
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Chayah, Mariem, M. Encarnación Camacho, M. Dora Carrión, Miguel A. Gallo, Miguel Romero, and Juan Duarte. "N,N′-Disubstituted thiourea and urea derivatives: design, synthesis, docking studies and biological evaluation against nitric oxide synthase." MedChemComm 7, no. 4 (2016): 667–78. http://dx.doi.org/10.1039/c5md00477b.

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Mojtahedi, Mohammad M., Mohammad R. Saidi, and Mohammad Bolourtchian. "A Novel Method for the Synthesis of Disubstituted Ureas and Thioureas under Microwave Irradiaton." Journal of Chemical Research 23, no. 12 (1999): 710–11. http://dx.doi.org/10.1177/174751989902301213.

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Several symmetrically disubstituted ureas and thioureas are synthesized by heating of urea or thiourea with aromatic amines or phenylhydrazine under environmentally benign conditions without any solvent in a conventional microwave oven.
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Dhaene, Evert, Isabel Van Driessche, Klaartje De Buysser, and Kristof Van Hecke. "Crystal structures of three N,N,N′-trisubstituted thioureas for reactivity-controlled nanocrystal synthesis." Acta Crystallographica Section E Crystallographic Communications 78, no. 2 (2022): 184–90. http://dx.doi.org/10.1107/s2056989022000147.

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The synthesis and single-crystal X-ray structures of three N,N,N′-trisubstituted thioureas are reported, namely N,N,N′-tribenzylthiourea, C22H22N2S (1), N-methyl-N,N′-diphenylthiourea, C14H14N2S (2), and N,N-di-n-butyl-N′-phenylthiourea, C15H24N2S (3). The influence of the different substituents on the thioureas is clear from the delocalization of the thiourea C—N and C=S bonds, while the crystal structures show infinite chains of N,N,N′-tribenzylthiourea (1), hydrogen-bonded pairs of N-methyl-N,N′-diphenylthiourea (2) and hexamer ring assemblies of N,N-di-n-butyl-N′-phenylthiourea (3) molecul
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Al-Riyahee, Ali A. A. "First Row Transition Metal Complexes Derived from N, Nʹ-Substituted Thiourea: Synthesis, Geometrical Structures and Cyclic Voltammetry Probe: A Review". BASRA JOURNAL OF SCIENCE 39, № 1 (2021): 96–118. http://dx.doi.org/10.29072/basjs.202117.

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Thioureas or thiourea derivatives as organosulfur compounds are one of the most widely used ligands in different applications as we are going to discuss it extensively such as in coordination chemistry by involving them to rich sources of N, O and S atoms coordinating through S atom, S and O atoms in benzoyl derivatives or S, O and N atoms in pyridyl hetrocylic benzoyl derivatives. These hard and soft donor sites facilitate the bonding between thiourea free ligand and metal ion through one or more to make ligands behave as mono, bi or multidentate ligands to form huge and stable series of the
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Dissertations / Theses on the topic "Synthesis of Thioureas"

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Ngo, Thi Thuy Duong. "Chiral thioureas, thiourea-phosphines and amines derived from biomass : synthesis and applications in asymmetric organocatalysis." Thesis, Université Paris-Saclay (ComUE), 2016. http://www.theses.fr/2016SACLS476.

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Cette thèse porte sur la préparation de nouveaux catalyseurs chiraux à partir de composés naturels issus de la biomasse, et leurs applications en organocatalyse asymétrique. La première partie décrit la synthèse de thiourées énantiomériquement pures dérivées de l'isosorbide et l’isommanide. Ces thiourées ont été évaluées comme catalyseurs organiques dans des réactions asymétriques de Friedel-Crafts, d’alkylation, d’addition de type aza-Michael, d’hydroamination et de type Morita-Baylis-Hillman (MBH). Les meilleurs résultats en termes de réactivité et d’induction asymétrique, ont été obtenus da
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Wongkhan, Kittiya. "Synthesis and applications of palladium complexes : Part I. The synthesis, single crystal structures and liquid crystalline phase behavior of alkoxy substituted Tolans; Part II. Palladium-complexes of thioureas and phosphine sulfides." Thesis, Durham University, 2008. http://etheses.dur.ac.uk/2139/.

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Three series of alkoxy substituted tolans p-X-C(_6)H(_4)-C≡C-C(_6)H(_4)-p-OC(_n)H(_2n+1) [X = H (series 1), CH(_3) (series 2), OCH(_3) (series 3)] with varying chain length were synthesized by Pd/Cu-catalysed Sonogashira cross-coupling reactions of terminal alkynes and iodoarenes, crystal structures and phase behavior of three series of tolans. Twenty-eight of the tolans were structurally characterised by single-crystal X-ray diffraction. Their phase behavior was characterised by tplm; only the tolans in series 3 show liquid crystalline phases. The melting points of the tolans decrease with in
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Rampalakos, Konstantinos. "Asymmetric synthesis with vapol derivatives and novel chiral thiourea organocatalysts." Diss., Connect to online resource - MSU authorized users, 2008.

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Apps, James Frederick Shuan-Liang. "Synthesis and application of thiourea-S,S-dioxide derivatives." Thesis, University of Warwick, 2008. http://wrap.warwick.ac.uk/53126/.

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The structure and synthesis of N,N'-disubstituted thiourea-S,S-dioxides were investigated experimentally and computationally. Hydrogen peroxide oxidation of acyclic and cyclic N,N'-dialkylthioureas furnished S,S-dioxides in agreement with computational predictions. Some s,S,S-trioxides were also isolated. An X-ray crystallographic study of N,N'-diisopropylthiourea dioxide, fIrst synthesised in this work, verilled computational models. The prediction of a stable N,N'-diarylthiourea dioxide derivative was supported by successful isolation of the dioxide. The application of N,N'-diisopropylthiour
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Kyne, Graham M. "Rational design and synthesis of receptors for carboxylates." Thesis, University of Southampton, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.326397.

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Ghebregziabiher, Berhe Haile. "Synthesis of chiral thiourea ligands and their transition metal complexes." Thesis, Stellenbosch : Stellenbosch University, 2003. http://hdl.handle.net/10019.1/53610.

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Thesis (MSc)--Stellenbosch University, 2003.<br>ENGLISH ABSTRACT: Modification of chitosan with benzoylisothiocyanate was attempted, however due to solvent problem the study was left incomplete till appropriate solvent is designed. N,N-diethyl-N -camphanoylthiourea (HL8), N-piperidyl-N '-camphanoylthiourea (HL9), N-pyrrolidyl-N -camphanoylthiourea (HL10) and N,N-diethyl-N -adamantylcarbonyl thiourea (HL11)have been synthesised and characterised for the first time. Two of these ligands HL8 and HL11, were used to form a number of transition metal complexes, namely H30+{fae-[Co(L8-S,Obn, c
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Jones, Charlotte E. S. "Enantioselective homogeneous catalysts for the synthesis of fluorinated organic compounds." Thesis, University of St Andrews, 2011. http://hdl.handle.net/10023/2611.

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This thesis is divided into three main results chapters that reflect the path my research took. In the first results chapter, the first organocatalyst for the carbonyl-ene reaction was discovered and found to give high conversion using 1,3-bis(3,5-bis(trifluoromethyl)phenyl)thiourea. Various carbonyl and alkene precursors were examined in the ene reaction in both catalysed and uncatalysed reactions. It was found that ene reactions using fluoral and ethyl trifluoropyruvate give higher rates of reaction when compared to other carbonyl compounds. A novel enantiopure thiourea was synthesised and t
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Franklin, Constance D. "A Novel Synthesis and Subsequent Decyclization of Iminothiozolidinones: Expansion of Thiourea Chemistry for Biological Applications." VCU Scholars Compass, 2017. http://scholarscompass.vcu.edu/etd/4853.

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Small molecule synthesis has become a valuable tool in the study of biological systems. Biologically active compounds can be designed based on well-characterized endogenous systems or they can be found through the screening of large libraries of small molecules. This work involves the development of a small library of cyclic thiourea-based small molecules by use of an unreported synthetic pathway. Briefly, parent thioureas were cyclized by reaction with bromoacetyl bromide, and one or two isomeric heterocycles were found to form. Further studies indicated that the reaction could be easily mani
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Saglam, Guluzar. "Synthesis Of Novel Chiral Thiourea Derivatives And Their Applications, Synthesis Of Some Hdac Inhibitors, Addition Of Acyl Phosphonates To Ethylcyanoformate." Master's thesis, METU, 2008. http://etd.lib.metu.edu.tr/upload/3/12609265/index.pdf.

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The thiourea derivatives have become a main focus of research in asymmetric synthesis as an organocatalyst in recent years. In the first part, the thiourea catalysts are synthesized starting from easily available L-tartaric acid and application of the catalysts to some addition reactions showed no significant asymmetric induction. A number of HDAC inhibitors have been developed as anti-cancer agent at the present time.In the second part, some aryl butenoic acid derivatives are synthesized as HDAC inhibitors starting from substituted benzaldehyde and pyruvic acid. The HDAC activity studies sho
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Chandanshive, Jay Zumbar <1983&gt. "Regiocontrolled Synthesis of Pyrazole Derivatives Through 1,3-Dipolar Cycloaddition Reaction And Synthesis of Helicene-Thiourea based and Polymer Supported Soos's Catalyst for Asymmetric Synthesis." Doctoral thesis, Alma Mater Studiorum - Università di Bologna, 2013. http://amsdottorato.unibo.it/5826/1/Chandanshive_JAY_ZUMBAR_Thesis.pdf.

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In first part we have developed a simple regiocontrolled protocol of 1,3-DC to get ring fused pyrazole derivatives. These pyrazole derivatives were synthesized using 1,3-DC between nitrile imine and various dipolarophiles such as alkynes, cyclic α,β-ketones, lactones, thiocatones and lactums. The reactions were found to be highly regiospecific. In second part we have discussed about helicene, its properties, synthesis and applications as asymmetric catalyst.Due to inherent chirality, herein we have made an attempt to synthesize the helicene-thiourea based catalyst for asymmetric catalysi
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Books on the topic "Synthesis of Thioureas"

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Saenz, Natalie. Synthesis and Characterization of Nanoplatelets and Nanoplatelet Heterostructures made with Thiourea and Selone Precursors. [publisher not identified], 2022.

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Lalonde, Mathieu Pascal. Chiral thioureas in asymmetric catalysis: From simple to bifunctional. 2009.

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Raheem, Izzat Tiedje. I. Enantioselective total synthesis of quinine and quinidine: II. Thiourea-catalyzed enantioselective C-C bond-forming reactions : a. catalytic asymmetric N-Acyliminium ion cyclizations : b. catalytic asymmetric aza-Baylis-Hillman reactions. 2008.

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Book chapters on the topic "Synthesis of Thioureas"

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Tjarks, Werner, Hartmut Ketz, and Detlef Gabel. "Synthesis and Biological Properties of Boronated Thioureas as Highly Selective Tumor Seekers for Melanoma." In Progress in Neutron Capture Therapy for Cancer. Springer US, 1992. http://dx.doi.org/10.1007/978-1-4615-3384-9_51.

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Takemoto, Yoshiji, and Tsubasa Inokuma. "Bifunctional Thiourea Catalysts." In Asymmetric Synthesis II. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527652235.ch29.

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Costamagna, J. A., J. Granifo, Marcetta Y. Darensbourg, and Patricia A. Tooley. "(Substituted Thiourea)Pentacarbonylchromium(0) Complexes." In Inorganic Syntheses. John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132548.ch1.

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Aucken, I., and Russell S. Drago. "Mercury(II) Chloride Thiourea Complexes." In Inorganic Syntheses. John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132371.ch9.

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Tsukano, Chihiro, Motohiro Yasui, and Yoshiji Takemoto. "Total Synthesis of Avenaol." In Modern Natural Product Synthesis. Springer Nature Singapore, 2024. http://dx.doi.org/10.1007/978-981-97-1619-7_18.

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AbstractAvenaol is a terpene with a unique all-cis cyclopropane in which all bulky substituents are oriented in the same direction. It is categorized into a non-canonical strigolactone. We have synthesized alkylidenecyclopropanes by Rh-catalyzed intramolecular cyclopropanation of allenes, followed by iridium-catalyzed diastereoselective double bond isomerization to construct all-cis cyclopropanes. Subsequently, distinction of the two hydroxymethyl groups of 1,3-diol by an intramolecular SN1-type reaction, followed by cleavage of the tetrahydropyranyl ring by regioselective C–H oxidation, led t
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Song, Baoan, Linhong Jin, Song Yang, and Pinaki S. Bhadury. "Synthesis and Antiviral Activity of Chiral Thiourea Derivatives." In Environment-Friendly Antiviral Agents for Plants. Springer Berlin Heidelberg, 2010. http://dx.doi.org/10.1007/978-3-642-03692-7_4.

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Swain, Sharada Prasanna, Kankanala Naveen Kumar, and V. Ravichandiran. "Thiourea Catalysts for Synthesis of Active Pharmaceutical Ingredients." In Recent Advances in Pharmaceutical Innovation and Research. Springer Nature Singapore, 2023. http://dx.doi.org/10.1007/978-981-99-2302-1_11.

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Cui, Shengchao, Guangzheng Wang, Shu Liu, Xintong Yan, and Ming Fan. "Synthesis and Property Analysis of a Novel Epoxy Composite Curing Agent Based on Soft Soil Curing." In Lecture Notes in Civil Engineering. Springer Nature Singapore, 2024. https://doi.org/10.1007/978-981-97-6238-5_46.

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AbstractTo meet the demand for shore-based engineering, engineering rescue and traffic emergency support in different complex conditions, a new low-temperature fast solidifier for epoxy resin was synthesized by Mannich reaction using thiourea, polyamine, formaldehyde, phenol and benzyl alcohol. The performance of the curing agent was investigated based on raw material ratio, reaction temperature and reaction time. Moreover, the curing time, amine value, viscosity and infrared spectrum were tested. It was compounded with other highly active curing agents and resins. The compressive strength of
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Kassim, Karimah, Noor Khadijah Mustafa Kamal, Siti Noriah Mohd Shotor, and Adibatul Husna Fadzil. "New Cyclic Thiourea for Corrosion Inhibition: Synthesis, Characterization and Corrosion Inhibition Studies of 1,3-BIS(N’-2,3,4-Methyl Benzoylthioureido)-1,3-Methylbenzene." In Engineering and Technical Development for a Sustainable Environment. Apple Academic Press, 2017. http://dx.doi.org/10.1201/9781315207322-11.

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Unger, Thomas A. "Thioureas." In Pesticide Synthesis Handbook. Elsevier, 1996. http://dx.doi.org/10.1016/b978-081551401-5.50162-3.

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Conference papers on the topic "Synthesis of Thioureas"

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Queiroz, Carlos H. B., Chiara Z. Mazzari, Luis G. R. Sá, et al. "Synthesis and Investigation of Sulfur/Nitrogen Doped Carbon Dots as Corrosion Inhibitors for Mild Steel in CO2 Saturated Saline Medium." In LatinCORR 2023. AMPP, 2023. https://doi.org/10.5006/lac23-20445.

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The oil and gas industry can be considered one of the main industrial fields in corrosion inhibitor usage. In this aggressive environment, dissolved CO2poses as an intensifying component. The study and synthesis of new materials that can mitigate corrosion rates in such an aggressive environment is a constant scientific effort. Nanomaterials research can be considered a fast-growing field with many applications [1]. Specifically for corrosion inhibitor studies, materials that present a 2D or 0D structure, such as graphene oxide and carbon dots, respectively, may offer excellent inhibition capa
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Chen, Guang-You, Xiang-Rong Tian, Chong-Lin Cai, Yi-Wan Zhou, and Xing Zhang. "Synthesis and Mosquito Larvicidal Activities of Benzoyl Thioureas." In 2015 International Conference on Medicine and Biopharmaceutical. WORLD SCIENTIFIC, 2016. http://dx.doi.org/10.1142/9789814719810_0128.

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Edrah, Salem. "SYNTHESIS, CHARATERIZATION AND BIOLOGICAL ACTIVITIES OF UREAS AND THIOUREAS DERIVATIVES." In The 14th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2010. http://dx.doi.org/10.3390/ecsoc-14-00479.

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Dinh Thanh, Nguyen, Do Son Hai та Pham Hong Lan. "SYNTHESIS OF PER‐O‐ACETYL‐β‐D‐GLUCOPYRANOSYL THIOUREAS CONTAINING THIAZOLE RING". У The 13th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2009. http://dx.doi.org/10.3390/ecsoc-13-00155.

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Shutalev, Anatoly. "A New Route for the Synthesis of Cyclic Thioureas and Related Compounds." In The 3rd International Electronic Conference on Synthetic Organic Chemistry. MDPI, 1999. http://dx.doi.org/10.3390/ecsoc-3-01751.

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Thi Ha Thu, Tran, Nguyen Phuong Nhan, Nguyen Thi Thanh Mai та Nguyen Dinh Thanh. "Microwave-Assisted Synthesis of N-Tetra-O-Acetyl-β-DGlucopyranosyl- N'-(4',6'-Diarylpyrimidine-2'-yl)thioureas". У The 13th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2009. http://dx.doi.org/10.3390/ecsoc-13-00152.

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Silva, Tiago Lima da, and Paulo Henrique Schneider. "Multicomponent Synthesis of Bifunctional Thiourea Organocatalysts for the Enantioselective Aldol Reaction." In 14th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-14bmos-r0012-1.

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Saitz, Claudio, Eduardo Bastidas, Horacio Gómez, et al. "Synthesis of new artificial receptors for anion recognition: calix[4]arenes thiourea derivative." In 14th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-14bmos-r0118-1.

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Silva*, Claudia Brito da, and Fabiano Severo Rodembusch. "Synthesis and spectroscopic characterization of urea/thiourea derivatives for potential optical sensors application." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_201310114206.

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Vo-Thanh, Giang, and Huong Nguyen Thi Thu. "Synthesis of Chiral Thiourea-Phosphine Organocatalysts derived from L-Proline." In The 19th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2015. http://dx.doi.org/10.3390/ecsoc-19-a058.

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