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Dissertations / Theses on the topic 'Synthetic ketone'

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Published: 5 June 2025

Last updated: 1 August 2025

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1

Jiao, Guansheng. "Ketone catalyzed diastereoselective and enantioselective epoxidation of olefins : catalyst design and synthetic application /." Hong Kong : University of Hong Kong, 2000. http://sunzi.lib.hku.hk/hkuto/record.jsp?B21981772.

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2

Waymouth, Robert M. Grubbs Robert H. "Synthesis and reactivity of alkylaluminum adducts of zirconium ketene and ketone complexes /." Diss., Pasadena, Calif. : California Institute of Technology, 1987. http://resolver.caltech.edu/CaltechETD:etd-10142008-080353.

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3

Cerone, Matthew. "Synthesis of Alkyl Substituted Phenylated Poly(Ether Ether Ketone Ketone)s." Wright State University / OhioLINK, 2017. http://rave.ohiolink.edu/etdc/view?acc_num=wright1496856789109456.

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4

Dziadulewicz, E. K. "Ketene dithioacetals in synthesis." Thesis, University of Bath, 1987. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.375640.

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5

Lynam, Jason Martin. "Vinyl ketone and vinyl aldehyde complexes of ruthenium." Thesis, University of York, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.265558.

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6

Walker, Louise F. "Synthetic applications of alkylidene carbenes." Thesis, University of Warwick, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.343952.

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7

Howard-Jones, Andrew Glyn. "A synthetic approach to Câ†2 symmetric guanidine bases and the synthesis of model compounds of ptilomycalin A." Thesis, Bangor University, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.340956.

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8

Silvanus, Andrew. "Exploring the synthetic utility of divinyl ketones." Thesis, University of Bath, 2010. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.535271.

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Divided into three distinct research areas, this thesis investigates the synthetic utility of divinyl ketones as versatile substrates in the construction of novel cyclic structures. The first volume of work (Chapter 2) examines the one-pot Brønsted acid-catalysed tandem double alkylation of indole with non-symmetrical divinyl ketones. The [6,5,7] tricyclic indole products are often furnished in excellent yield, with complete regioselectivity and high levels of syn-diastereoselectivity. Optimisation, a thorough substrate investigation and initial results are all discussed within. An in-depth me

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9

Ko, Jinren. "Synthetic Applications of Ketene Cycloadditions: Natural and Novel Pyrethroid Insecticides." Thesis, North Texas State University, 1985. https://digital.library.unt.edu/ark:/67531/metadc331031/.

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A new synthetic route to natural and novel pyrethroid acids was developed utilizing ketene cycloaddition which is a significant improvement over existing syntheses. The newly synthesized pyrethroid acids were converted to pyrethroid esters and used to study structure-activity relationships. The cycloaddition of dichloroketene with 2,5-dimethyl-2,4-hexadiene yields (2+2) cycloaddition products, 2,2-dichlorocyclobutanones. The reductive removal of one chlorine atom from these cycloaddition products gave monochlorocyclobutanones which underwent a Favorskii-type ring contraction to yield cis- and

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10

Salter, D. P. "The synthesis and chemistry of ketene-o,o-acetal and ketene-o,s,acetals." Thesis, Lancaster University, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.381786.

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11

Yoshida, Suguru. "Studies on Synthetic Reactions of Ketene Dithioacetal Derivatives." 京都大学 (Kyoto University), 2009. http://hdl.handle.net/2433/77960.

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Kyoto University (京都大学)<br>0048<br>新制・課程博士<br>博士(工学)<br>甲第14581号<br>工博第3049号<br>新制||工||1454(附属図書館)<br>26933<br>UT51-2009-D293<br>京都大学大学院工学研究科材料化学専攻<br>(主査)教授大嶌幸一郎, 教授檜山爲次郎, 教授松原誠二郎<br>学位規則第4条第1項該当

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12

Bena, Luvuyo Clifford. "Investigations into the asymmetric reduction of ketones." Thesis, University of Port Elizabeth, 2003. http://hdl.handle.net/10948/323.

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A six-step synthesis of salbutamol from methyl salicylate with an overall yield of 17% has been completed, although the yield was not optimised. In the process, Zn(BH4)2 was found to selectively reduce a ketone carbonyl group in the presence of an ester unit. In contrast, borane was found to reduce both the ketone and ester carbonyl groups. Reduction of phenacyl bromide with borane in the presence of chiral catalysts based on (R)-alaninol and (R,S)-ephidrine resulted a measure of enantioselectivity in the product. However, the configuration of the alcohol obtained in the case of (R)-alaninol w

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13

Palmer, Matthew Jon. "The stereoselective synthesis of alcohols." Thesis, University of Warwick, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.263813.

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14

Kitagawa, Kristen. "Studies in the asymmetric reduction of (3s)-3-amino-1-chloro-4-phenyl-2-butanone derivatives." Diss., Georgia Institute of Technology, 2010. http://hdl.handle.net/1853/39464.

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This thesis focuses on the asymmetric reduction of N-protected derivatives of (3S)-3-amino-1-chloro-4-phenyl-2-butanone to their corresponding diastereomeric alcohol products, which are key intermediates in the synthesis of HIV protease inhibitors. Although the stereoselective synthesis of the (S,S) alcohol product is easily achieved, preparing the (R,S) diastereomer is much more challenging. I investigated three diastereoselective reduction processes: 1) Meerwein-Ponndorf-Verley (MPV) reduction, 2) asymmetric transfer hydrogenation, and 3) boron reducing agents. The diastereoselectivity of

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15

Wu, An-hsiang. "Syntheses of Highly Strained Energetic Molecules and Development of New Synthetic Methodology." Thesis, North Texas State University, 1987. https://digital.library.unt.edu/ark:/67531/metadc331132/.

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The objective of this study was to synthesize new energetic, strained, saturated polycyclic compounds. For this purpose, new methodology has been developed, as follows: (i) Ketenes have been generated in situ via treatment of aldo-, keto- or alkenoic acid with either toluenesulfonyl chloride or 2-chloro-1-methylpyridfniurn iodide (Mulkaiyama's reagent). The reactive intermediates thereby generated have been found to undergo intramolecular [2+2] cycloaddition reactions in these systems.

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16

Turner, R. L. "Novel approaches to the synthesis of Wieland-Miescher ketone analogues." Thesis, University College London (University of London), 2014. http://discovery.ucl.ac.uk/1443288/.

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Important for the regulation of bodily glucose levels and within the fight-or-flight response, the glucocorticoid receptor has become an interesting pharmaceutical target, with the discovery that both natural and synthetic glucocorticoids induce a significant anti-inflammatory effect. Current research focuses on the synthesis and identification of novel selective glucocorticoid receptor modulators, which lack the debilitating side effects associated with these drugs. Building upon the work of previously successful glucocorticoid modulators, pyrazole 2 is the target for this work. The first par

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17

Gao, Ming. "Ketone synthesis via rhodium-catalyzed traceless chelation-controlled hydroacylation reactions." Thesis, University of Oxford, 2018. http://ora.ox.ac.uk/objects/uuid:487b65f9-d1f7-4fee-b2bb-358837866ca2.

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This thesis documents the development of rhodium-catalyzed traceless chelation-controlled hydroacylation reactions for the synthesis of a variety of ketone products. <strong>Chapter 1</strong> provides an overview of rhodium-catalyzed hydroacylation chemistry, focusing on the origin of chelation-controlled strategies and the benefits thereof. <strong>Chapter 2</strong> describes a sequential reaction involving alkene hydroacylation, sulfide elimination and boronic acid conjugate addition, which affords products with the initial sulfide coordinating group replaced by a stereochemically defined

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18

Fang, Zhijia. "Asymmetric reduction of functionalized ketones and their synthetic applications." Thesis, University of Warwick, 2013. http://wrap.warwick.ac.uk/59696/.

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Asymmetric transfer hydrogenation (ATH) represents a powerful methodology for the synthesis of chiral secondary alcohols. The synthesis of chiral propargylic alcohols by asymmetric transfer hydrogenation of acetylenic ketones has been applied to a number of applications including target oriented synthesis. In this thesis, the asymmetric transfer hydrogenation of a large number of functionalized alkyones and dialkyones has been fully investigated. Basic principles as well as detailed reaction conditions for the ATH of acetylenic ketones have been established. Chiral propargylic alcohols have be

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19

Lively, Sarah Elizabeth. "Catalytic asymmetric synthesis of #alpha#-hydroxy ketones." Thesis, University of Sheffield, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.388709.

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20

Wu, Luis Eduardo. "Synthesis of unnatural sugars from unsaturated ketones." Thesis, University of Liverpool, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.368669.

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21

Wommack, Andrew Joseph. "A Modular Synthesis of Ketones and Gem-diborylalkanes by Catalytic Carbon Insertion with Non-stabilized Diazoalkanes." Thesis, Boston College, 2011. http://hdl.handle.net/2345/2225.

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Thesis advisor: Jason S. Kingsbury<br>Chapter 1: The reaction of diazomethane with simple aldehydes to deliver methyl ketones has a long studied history in the art of organic synthesis. Formyl electrophiles have also been homologated with trimethylsilyldiazomethane, diazoacetates, and aryl-diazomethanes that very rarely proceed with catalytic activation. Due to the stigma of handling non-stabilized diazoalkanes this history is limited to examples utilizing αdiazoesters and entirely missing are examples of tertiary αsubstituted ketone synthesis beginning with disubstituted (internal

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22

Masters, Susannah Jane. "Studies towards the synthesis of the squalestatins." Thesis, University of Sheffield, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.298950.

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23

Math, Shivanand Kumarswamy, and Shivanand Kumarswamy Math. "Diastereoselective cyclopropanation of medium and large ring alpha, beta-unsaturated homochiral ketals and enantioselective synthesis of (-)-modhephene." Diss., The University of Arizona, 1989. http://hdl.handle.net/10150/184664.

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A general straightforward synthetic approach for the enantioselective construction of medium and large ring cyclopropyl ketones via diastereoselective Simmons-Smith cyclopropanation is discussed. Medium and large 2-cycloalkenone 1,4Di-O-benzyl-L-threitol ketals undergo efficient and diastereoselective cyclopropanation when treated with an excess of the Simmons-Smith reagent. The cyclopropyl ketals are obtained in 80-94% with >23:1-8:1 diastereoselectivity. The first enantioselective synthesis of (-)-modhephene, a natural product possessing the carbocyclic (3.3.3) propellane skeleton, by the us

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24

Qin, Wenling <1985&gt. "Synthesis and applications of N-Metallo ketene imines." Doctoral thesis, Alma Mater Studiorum - Università di Bologna, 2014. http://amsdottorato.unibo.it/6381/1/Qin_Wenling_Tesi.pdf.

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N-metallo ketene imines are attractive for the preparation of a wide range of organic compounds. Our research group has been engaged in the preparation and application of the N-metallo imines (SKIs). In this frame we have studied the uncatalyzed reaction of SKIs with isocyanates to give the corresponding malonamides with good yields. It has been demonstrated that the use of SKIs, instead of simple lithium anion of nitriles, is essential for the success of the reaction. A possible explanation assumes that this new reaction proceeds via a silatropism. In the course of our studies, reported in th

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25

Qin, Wenling <1985&gt. "Synthesis and applications of N-Metallo ketene imines." Doctoral thesis, Alma Mater Studiorum - Università di Bologna, 2014. http://amsdottorato.unibo.it/6381/.

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N-metallo ketene imines are attractive for the preparation of a wide range of organic compounds. Our research group has been engaged in the preparation and application of the N-metallo imines (SKIs). In this frame we have studied the uncatalyzed reaction of SKIs with isocyanates to give the corresponding malonamides with good yields. It has been demonstrated that the use of SKIs, instead of simple lithium anion of nitriles, is essential for the success of the reaction. A possible explanation assumes that this new reaction proceeds via a silatropism. In the course of our studies, reported in th

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26

Tavasli, Mustafa. "Synthesis of a new class of homochiral amines and novel bio-active tropanes." Thesis, Durham University, 1999. http://etheses.dur.ac.uk/4552/.

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This thesis describes two main programmes: the synthesis of a new class of homochiral amines and the synthesis of ketone analogues of 3a-esterified tropane alkaloids. In chapter one, a scaled-up synthesis of (5)-a-(diphenylmethyl)pyrrolidine 1 is described. The key hydrogenation step of the oxazolidinone intermediate 2 was extended to the synthesis of the other chiral amines 70, 73, 76, 79 and 82. Hydrogenation of the oxazolidinones proceeded in good yields (71 - 87 %) and was not susceptible to racemisation. Thus, a convenient route from amino acid ester hydrochlorides (S)-valine 65, (S)-phen

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27

Le, Guen Anne Carleton University Dissertation Chemistry. "Synthesis, properties and transformation of naphthalene-based poly(arylene ether ketone)s." Ottawa, 1994.

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28

Broughton, Peter William Carleton University Dissertation Chemistry. "The synthesis and properties of naphthalene-based poly(arylene ether ketone)s." Ottawa, 1995.

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29

Swain, Simon A. "The enzymatic resolution of racemic enol acetates derived from prochiral oxabicyclic ketones." Thesis, University of Liverpool, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.367792.

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30

Milsom, Greig. "Synthetic approaches to the asymmetric synthesis of #alpha#-keto and #beta#-hydroxy esters." Thesis, Kingston University, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.285949.

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31

Kennedy, Isaac Ato. "Taxoid synthesis: Ketene cycloadditions as a radical cyclization approach." Thesis, University of Ottawa (Canada), 1993. http://hdl.handle.net/10393/6815.

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Studies directed towards the synthesis of the taxane skeleton is described. The synthesis and cyclopropanation of 170 was attempted, and the preparation and base induced cyclization of gamma,delta-epoxyketone 187 and gamma,delta-epoxyester 198 examined. An unusual cycloaddition of ethyl vinyl ether to ketene carbonyls to form oxetanes was uncovered. The ketenes were generated from the cyclic diazoketones 210, 211 and 213 and the acyclic system 215. In all cases, with either Rh2(OAc)4, Pd(OAc) 2 or CuCl as catalyst, the oxetanes were the major products. Irradiation afforded the cyclobutanone

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32

Ye, Guozhong. "Synthesis and reactions of cyclic ketene-N,N-acetals." Diss., Mississippi State : Mississippi State University, 2008. http://library.msstate.edu/etd/show.asp?etd=etd-09142008-210135.

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33

Wong, Man-kin. "Design and synthesis of chiral ketones for catalytic asymmetric epoxidation of unfunctionalized olefins /." Hong Kong : University of Hong Kong, 1996. http://sunzi.lib.hku.hk/hkuto/record.jsp?B1815623X.

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34

Lauret, Christelle. "Approaches towards the total asymmetric synthesis of puetuberosanol and marshrin." Thesis, University of Liverpool, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.272738.

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35

Winders, J. A. "Synthesis of natural products via intramolecular trapping of photogenerated ketenes." Thesis, University of Salford, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.381729.

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36

Martins, Jose Alberto Ribeiro. "Studies on solution and solid phase biotransformations." Thesis, University of Warwick, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.341560.

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37

Bi, Feng Jr. "The Asymmetric Synthesis Of The C1'-C10' Portion of Pamamycin-621A." Thesis, Virginia Tech, 1998. http://hdl.handle.net/10919/36903.

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This thesis describes the synthesis of the C1'-C10' portion 72 of the pamamycin-621A using a cuprate conjugate addition to join enone fragment 52 and organostannane fragment 64a. Fragments 52 and 64a were both synthesized from (S)-methylketene dimer 51.<br>Master of Science

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38

Keita, Ousainou Ansumana. "The synthesis of new phenylhydroxyiodonium phosphates from (diacetoxyiodobenzene) and dialkyl phosphates and their use in the α-phosphorylation of ketones to mono-ketol phosphates". University of Akron / OhioLINK, 2008. http://rave.ohiolink.edu/etdc/view?acc_num=akron1197558427.

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39

Catterick, David. "The parallel synthesis of natural product families." Thesis, University of Oxford, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.299756.

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40

Hayter, Barry R. "Synthesis of chiral ketones for use in asymmetric epoxidation reactions." Thesis, University of Nottingham, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.285722.

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41

Cox, B. "The synthesis of #Beta#-amino ketones as potential antifungal agents." Thesis, University of Manchester, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.375078.

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42

Hussaini, Ayman S. al. "Synthesis and characterization of novel poly(imino ketone)s via palladium-catalyzed aryl amination." [S.l.] : [s.n.], 2005. http://deposit.ddb.de/cgi-bin/dokserv?idn=975953389.

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43

黃文健 and Man-kin Wong. "Design and synthesis of chiral ketones for catalytic asymmetric epoxidation of unfunctionalized olefins." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1996. http://hub.hku.hk/bib/B31236285.

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44

Klein, Solange. "Design and synthesis of catalysts for the asymmetric epoxidation of alkenes with Oxone." Thesis, University of Liverpool, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.250699.

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45

Rajapaksa, Naomi Samadara. "I. Stereoselective Construction of Polycyclic Architectures: Enantioselective Catalytic Transannular Ketone-Ene Reactions and an Enantioselective Total Synthesis of (+)-Reserpine II. Synthesis of Chiral Bisthioureas for Anion-Abstraction Catalysis." Thesis, Harvard University, 2013. http://dissertations.umi.com/gsas.harvard:11127.

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The research presented herein explores three aspects of asymmetric catalysis: (1) the development of new catalytic enantioselective reactions, (2) the application of stereoselective catalysis to natural product total synthesis, and (3) the design and synthesis of new chiral catalysts.<br>Chemistry and Chemical Biology

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46

Roseblade, Stephen. "Intramolecular asymmetric nitrone cycloadditions in the synthesis of Î² amino acids." Thesis, University of Bristol, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.251146.

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47

Mathis, Tiffaney M. "Synthesis and characterization of o-Acylnaphthols a thesis presented to the faculty of the Graduate School, Tennessee Technological University /." Click to access online, 2008. http://proquest.umi.com/pqdweb?index=0&did=1679676631&SrchMode=1&sid=2&Fmt=6&VInst=PROD&VType=PQD&RQT=309&VName=PQD&TS=1268416679&clientId=28564.

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48

Nguyen, René-Viet 1981. "Catalytic tandem nucleophilic addition for the synthesis of heterocycles." Thesis, McGill University, 2008. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=115708.

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Classical methodologies for carbon-carbon bond formation often require stoichiometric amount of reagent to prefunctionalize a C-H bond. Such methods generate a lot of waste and are therefore not atom-efficient. On the other hand, the use of catalysts for the direct use of C-H bond without prior functionalization is a more desirable approach for carbon-carbon formation. For example, an overall addition reaction is 100% atom economical. This thesis focuses on the catalytic addition of the three types of C-H bonds (Csp-H, Csp2-H and Csp3-H) to unsaturated molecules such as conjugated dienes, imin

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49

Canbolat, Eylem. "Organocatalytic Resolution Of Racemic Alpha Azido Ketones." Master's thesis, METU, 2012. http://etd.lib.metu.edu.tr/upload/12614602/index.pdf.

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Chiral cyclic alpha azido ketones are very important compounds in organic chemistry. Because, the reduced forms of them are amino alcohols and these amino alcohols are interesting compounds for their biological activities. They have some pharmaceutical activities such as: potassium channel open up properties, treatment of central nervous system, antihypertensive properties, the agent of dopamin receptor activator, hypolipemic agent and dopamine agonist. These types of compounds have highly acidic alpha-protons, and many kinds of reactions can be performed with them. In this study, mainly, sel

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50

Hernandez, Maria Luisa Escudero. "Enzymatic desymmetrization of prochiral cyclohexanones : synthesis of a non-peptidic NK2 antagonist." Thesis, University of Liverpool, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.343757.

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