Relevant bibliographies by topics / Synthetic reagents

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  1. Journal articles
  2. Dissertations / Theses
  3. Books
  4. Book chapters
  5. Conference papers
  6. Reports

Academic literature on the topic 'Synthetic reagents'

Author: Grafiati
Published: 3 June 2025
Last updated: 1 August 2025

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Journal articles on the topic "Synthetic reagents"

1

Chen, Ming, and Jiaming Liu. "1,3-Bifunctional Nucleophilic Allylation Reagents: Preparative Methods and Synthetic Applications." Synthesis 53, no. 13 (2021): 2167–82. http://dx.doi.org/10.1055/a-1389-1438.

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Abstract1,3-Bifunctional nucleophilic allylation reagents play an important role in organic synthesis. In this short review, we summarize the methods for the preparation of 1,3-bifunctional reagents and their reactions with various electrophiles. Synthetic applications of these reagents in the context of complex molecule synthesis are also discussed.1 Introduction2 Reagent Synthesis2.1 Symmetrical Reagents2.2 Unsymmetrical Reagents2.2.1 Bis-silane and Silyl-stannane Reagents2.2.2 Bis-boron and Silyl-boron Reagents3 Synthetic Applications3.1 Allylation of Aldehydes3.2 Allylation of Ketones3.3 A
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Hu, Long, and Junfeng Zhao. "Ynamide: A New Coupling Reagent for Amide and Peptide Synthesis." Synlett 28, no. 14 (2017): 1663–70. http://dx.doi.org/10.1055/s-0036-1588860.

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The discovery and application of ynamide coupling reagents is highlighted with a brief summary of the development history of coupling reagents in amide and peptide synthesis. As novel coupling reagents, ynamides are not only effective for simple amide and dipeptide synthesis but also can be used for peptide fragment condensation. More importantly, no racemization was detected during the activation of α-chiral carboxylic acids by employing ynamide coupling reagents.1 Introduction2 Carbodiimide Coupling Reagents3 Uronium/Guanidinium Salt Coupling Reagents4 Phosphonium Salt Coupling Reagents5 Eth
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Narayanaperumal, Senthil, Ricardo S. Schwab, Wystan K. O. Teixeira, and Danilo Yano de Albuquerque. "Recent Advances in the Synthesis of Enantiomerically Enriched Diaryl, Aryl Heteroaryl, and Diheteroaryl Alcohols through Addition of Organometallic Reagents to Carbonyl Compounds." Synthesis 52, no. 13 (2020): 1855–73. http://dx.doi.org/10.1055/s-0039-1690847.

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Enantiomerically enriched diaryl, aryl heteroaryl, and dihetero­aryl alcohols are an important family of compounds known for their biological properties. Moreover, these molecules are highly privileged scaffolds used as building blocks for the synthesis of pharmaceutically relevant products. This short review provides background on the enantioselective arylation and heteroarylation of carbonyl compounds, as well as, the most significant improvements in this field with special emphasis on the application of organometallic reagents.1 Introduction2 Background on the Enantioselective Synthesis of
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Parsons, P. J. "Synthetic reagents." Endeavour 10, no. 1 (1986): 54–55. http://dx.doi.org/10.1016/0160-9327(86)90077-3.

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Sano, Shigeki, Tomoya Matsumoto, Munehisa Toguchi, and Michiyasu Nakao. "Facile Two-Step Synthesis of Methyl Bis(2,2,2-trifluoroethyl)phosphonoacetate by Exploiting Garegg–Samuelsson Reaction Conditions." Synlett 29, no. 11 (2018): 1461–64. http://dx.doi.org/10.1055/s-0036-1591566.

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A facile two-step synthesis of methyl bis(2,2,2-trifluoroethyl)phosphonoacetate (Still–Gennari reagent) has been developed by exploiting Garegg–Samuelsson reaction conditions. Starting from trimethyl phosphonoacetate, Still–Gennari reagent was prepared in 94% yield via methyl 2-{bis[(trimethylsilyl)oxy]phosphoryl}acetate intermediate. This synthetic procedure was also used to prepare some kinds of Horner–Wadsworth–Emmons reagents and related compounds.
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Piccardi, Riccardo, Serge Turcaud, Erica Benedetti, and Laurent Micouin. "Synthesis and Reactivity of Mixed Dimethylalkynylaluminum Reagents." Synthesis 51, no. 01 (2018): 97–106. http://dx.doi.org/10.1055/s-0037-1610392.

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Organoaluminum derivatives are mostly appreciated for their Lewis acidity properties, but generally not considered as reagents of choice in synthetic transformations involving the creation of C–C bonds. Among these species, dimethylalkynylaluminum reagents represent a special class of compounds, with, in many cases, unique reactivity. This review summarizes the preparation and reactivity of these organometallic reagents with a focus on their synthetic potential.1 Introduction2 Preparation of Dimethylalkynylaluminum Reagents3 Reactivity of Dimethylalkynylaluminum Reagents3.1 Reactions with Csp3
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Bhadra, Sanchita, Vylan Nguyen, Jose-Angel Torres, et al. "Producing molecular biology reagents without purification." PLOS ONE 16, no. 6 (2021): e0252507. http://dx.doi.org/10.1371/journal.pone.0252507.

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We recently developed ‘cellular’ reagents–lyophilized bacteria overexpressing proteins of interest–that can replace commercial pure enzymes in typical diagnostic and molecular biology reactions. To make cellular reagent technology widely accessible and amenable to local production with minimal instrumentation, we now report a significantly simplified method for preparing cellular reagents that requires only a common bacterial incubator to grow and subsequently dry enzyme-expressing bacteria at 37°C with the aid of inexpensive chemical desiccants. We demonstrate application of such dried cellul
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Ogawa, Akiya, and Yuki Yamamoto. "Efficacy of radical reactions of isocyanides with heteroatom radicals in organic synthesis." Beilstein Journal of Organic Chemistry 20 (August 26, 2024): 2114–28. http://dx.doi.org/10.3762/bjoc.20.182.

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Isocyanide is a promising synthetic reagent not only as a one-carbon homologation reagent but also as a nitrogen source for nitrogen-containing molecules. Because of their isoelectronic structure with carbon monoxide, isocyanides also react with nucleophiles, electrophiles, carbon radicals, and transition metal reagents, and are widely used in organic synthesis. On the other hand, the use of isocyanides in reactions with heteroatom radicals is limited. However, the reaction of isocyanides with heteroatom radicals is a promising synthetic tool for the construction of nitrogen-containing organic
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Singh, Fateh V., Priyanka B. Kole, Saeesh R. Mangaonkar, and Samata E. Shetgaonkar. "Synthesis of spirocyclic scaffolds using hypervalent iodine reagents." Beilstein Journal of Organic Chemistry 14 (July 17, 2018): 1778–805. http://dx.doi.org/10.3762/bjoc.14.152.

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Hypervalent iodine reagents have been developed as highly valuable reagents in synthetic organic chemistry during the past few decades. These reagents have been identified as key replacements of various toxic heavy metals in organic synthesis. Various synthetically and biologically important scaffolds have been developed using hypervalent iodine reagents either in stoichiometric or catalytic amounts. In addition, hypervalent iodine reagents have been employed for the synthesis of spirocyclic scaffolds via dearomatization processes. In this review, various approaches for the synthesis of spiroc
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Guo, Fenghai, Jayla A. Young, Mina S. Perez, Holden A. Hankerson, and Alex M. Chavez. "Progress on the Cu-Catalyzed 1,4-Conjugate Addition to Thiochromones." Catalysts 13, no. 4 (2023): 713. http://dx.doi.org/10.3390/catal13040713.

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Carbon–carbon bond formation is one of the most important tools in synthetic organic chemists’ toolbox. It is a fundamental transformation that allows synthetic chemists to synthesize the carbon framework of complex molecules from inexpensive simple starting materials. Among the many synthetic methodologies developed for the construction of carbon–carbon bonds, organocopper reagents are one of the most reliable organometallic reagents for this purpose. The versatility of organocuprate reagents or the reactions catalyzed by organocopper reagents were demonstrated by their applications in a vari
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Dissertations / Theses on the topic "Synthetic reagents"

1

Whelligan, Daniel Keith. "Silenes as novel synthetic reagents." Thesis, Durham University, 2003. http://etheses.dur.ac.uk/3135/.

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Several syntheses of aryltris(trimethylsilyl)silanes were investigated and finally a novel route was developed starting from tetrakis(trimethylsilyl)silane, the mechanism for which was investigated. This new robust and reproducible synthesis involved a halogen-metal exchange and exploited a Schlenk equilibrium and was used to produce phenyltris(trimethylsilyl)silane in high yield (-70 %) on scales of up to 20 g. Phenyltris(trimethylsilyl)silane was used as the starting material for the synthesis of silene precursors; 1-hydroxyalkylphenyltrisilanes (silyl alcohols), involving KO'Bu-mediated for
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McLaren, Lee. "Synthetic applications of hypervalent iodine reagents : total synthesis of aranorosin." Thesis, University of East Anglia, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.385890.

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McCall, Matthew D. "Organozinc reagents : structural tailoring for synthetic applications." Thesis, University of Strathclyde, 2012. http://oleg.lib.strath.ac.uk:80/R/?func=dbin-jump-full&object_id=18805.

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Building on recent advances in zincate chemistry, but going beyond the state-of-the-art, this project sought to advance the understanding of the mechanisms involved in alkali metalmediated zincation (AMMZn), as well as design a new type of mixed-metal reagent, magnesium-zinc hybrids, focussing on their applications in nucleophilic additions to ketones and direct zinc-iodine exchange reactions. Unveiling two new applications of the alkali metal TMP-zincates [(THF)Li(TMP)ZntBu₂] (1) and [(TMEDA)Na(TMP)ZntBu₂] (3), reaction with trimethyl(phenoxy)silane (12) allowed the isolation of the first int
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Griffiths, Russell Jon. "Silenes : novel synthetic reagents for olefin functionalisation." Thesis, Durham University, 2000. http://etheses.dur.ac.uk/4331/.

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Silenes, compounds containing silicon-carbon double bonds, have been subject to much theoretical interest over the past 25 years. However, despite their high reactivity, to date there have been no reports of the attempted use of silenes as synthetic reagents. Silenes have been formed by the thermolysis of acyltris(trimethylsilyl)silanes, which have been found to react with dienes to give Diels-Alder cycloadducts in good yield. Further to this, it has been found that silene dimers, formed by the photolysis of acyltris(trimethylsilyl)silanes, have been found to revert to give silenes at much low
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Inoue, Atsushi. "Studies on novel synthetic reactions with organomagnesium reagents." 京都大学 (Kyoto University), 2003. http://hdl.handle.net/2433/148831.

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Kakiya, Hirotada. "Studies on Novel Synthetic Reactions with Organomanganese Reagents." 京都大学 (Kyoto University), 2002. http://hdl.handle.net/2433/149780.

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Fairfull-Smith, Kathryn Elizabeth, and n/a. "Synthetic and Mechanistic Investigations of Some Novel Organophosphorus Reagents." Griffith University. School of Science, 2004. http://www4.gu.edu.au:8080/adt-root/public/adt-QGU20040917.081950.

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The alkoxytriphenylphosphonium ion intermediate of the Mitsunobu reaction for the esterification and inversion of configuration of an alcohol can be generated using the Hendrickson reagent, triphenylphosphonium anhydride trifluoromethanesulfonate, 27. While 27 was used in place of the Mitsunobu reagents (triphenylphosphine and a dialkyl azodicarboxylate) for the esterification of primary alcohols, the reaction failed with secondary alcohols such as (-)-menthol giving predominately elimination rather than the desired SN2 displacement. The difference between the two reactions was shown to be r
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Turner, Jayne Susan. "Molecular recognition of damaged DNA using synthetic affinity reagents." Thesis, Open University, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.418471.

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Potentially carcinogenic DNA damage that may be derived from dietary sources can be quantified using a number of methods. Some of the best of these methods are based on the use of antibodies that have high affinity and specificity for modified DNA bases. However, given the sometimes limited availability of antibodies there is a requirement for novel reagents that mimic the properties of the best antibodies. From a chemical perspective antibodies are `over engineered' and synthetic affinity reagents would recreate the optimal properties of the binding site with respect to selectivity and affini
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Hunter, Christopher. "Investigations and synthetic applications of #beta#-amino zinc reagents." Thesis, University of Newcastle Upon Tyne, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.364835.

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Fairfull-Smith, Kathryn Elizabeth. "Synthetic and Mechanistic Investigations of Some Novel Organophosphorus Reagents." Thesis, Griffith University, 2004. http://hdl.handle.net/10072/367534.

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The alkoxytriphenylphosphonium ion intermediate of the Mitsunobu reaction for the esterification and inversion of configuration of an alcohol can be generated using the Hendrickson reagent, triphenylphosphonium anhydride trifluoromethanesulfonate, 27. While 27 was used in place of the Mitsunobu reagents (triphenylphosphine and a dialkyl azodicarboxylate) for the esterification of primary alcohols, the reaction failed with secondary alcohols such as (-)-menthol giving predominately elimination rather than the desired SN2 displacement. The difference between the two reactions was shown to be r
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Books on the topic "Synthetic reagents"

1

Sundaram, S., and P. S. Raghavan. Chromium -VI Reagents: Synthetic Applications. Springer Berlin Heidelberg, 2011. http://dx.doi.org/10.1007/978-3-642-20817-1.

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Sundaram, S. Chromium -VI Reagents: Synthetic Applications. P.S. Raghavan, 2011.

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Klusener, Peter Anton August. Synthetic applications of strongly basic reagents. [s.n.], 1989.

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McLaren, Lee. Synthetic applications of hypervalent iodine reagents: Total synthesis of aranorosin. Universityof East Anglia, 1994.

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Persson, Eva. Regiocontrol in copper(I)-catalyzed allylic substitution reactions with Grignard reagents: Mechanistic and synthetic aspects. Acta Universitatis Upsaliensis, 1995.

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Coca, Adiel, ed. Boron Reagents in Synthesis. American Chemical Society, 2016. http://dx.doi.org/10.1021/bk-2016-1236.

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Fieser, Mary. Reagents for organic synthesis. Wiley, 1990.

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Fieser, Mary. Reagents for organic synthesis. Wiley, 1989.

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Fieser, Mary. Reagents for organic synthesis. Wiley, 1990.

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Fieser, Mary. Reagents for organic synthesis. Wiley, 1986.

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Book chapters on the topic "Synthetic reagents"

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Ripin, David H. Brown. "Synthesis of “Nucleophilic” Organometallic Reagents." In Practical Synthetic Organic Chemistry. John Wiley & Sons, Inc., 2011. http://dx.doi.org/10.1002/9781118093559.ch12.

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Lipshutz, Bruce H. "Synthetic Procedures Involving Organocopper Reagents." In Organometallics in Synthesis. John Wiley & Sons, Inc., 2013. http://dx.doi.org/10.1002/9781118750407.ch4.

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Arseniyadis, S., R. Rodriguez, R. Brondi, R. Spanevello, J. Ouazzani, and G. Ourisson. "A Comparative Study of Chemical versus Biological Functionalizations of Synthetic Intermediates." In Microbial Reagents in Organic Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-2444-7_25.

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Kanemasa, Shuji. "Effect of External Reagents." In Synthetic Applications of 1,3-Dipolar Cycloaddition Chemistry Toward Heterocycles and Natural Products. John Wiley & Sons, Inc., 2003. http://dx.doi.org/10.1002/0471221902.ch11.

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Zhang, Shaoguang, Wen-Xiong Zhang, and Zhenfeng Xi. "Organo-di-Lithio Reagents: Cooperative Effect and Synthetic Applications." In Organo-di-Metallic Compounds (or Reagents). Springer International Publishing, 2013. http://dx.doi.org/10.1007/3418_2013_71.

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Guanti, Giuseppe, Luca Banfi, and Enrica Narisano. "Asymmetrized Tris (Hydroxymethyl)Methane and Related Synthons as New Highly Versatile Chiral Building Blocks. Chemoenzymatic Preparation and Synthetic Applications." In Microbial Reagents in Organic Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-2444-7_24.

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Uchiyama, Masanobu, and Chao Wang. "New Formulas for Zincate Chemistry: Synergistic Effect and Synthetic Applications of Hetero-bimetal Ate Complexes." In Organo-di-Metallic Compounds (or Reagents). Springer International Publishing, 2014. http://dx.doi.org/10.1007/3418_2013_72.

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Fustero, Santos, José Luis Aceña, and Silvia Catalán. "Synthetic and Biological Applications of Fluorous Reagents as Phase Tags." In Topics in Current Chemistry. Springer Berlin Heidelberg, 2011. http://dx.doi.org/10.1007/128_2011_263.

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Kobayashi, Yuichi, and Miwa Shimoda. "Substitution of Allylic Picolinates with Various Copper Reagents and Synthetic Applications." In Cutting-Edge Organic Synthesis and Chemical Biology of Bioactive Molecules. Springer Singapore, 2019. http://dx.doi.org/10.1007/978-981-13-6244-6_7.

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Gnann, J. W., and M. B. A. Oldstone. "Using Synthetic Peptide Reagents to Distinguish Infections Caused by Different HIV Strains." In Current Topics in Microbiology and Immunology. Springer Berlin Heidelberg, 1990. http://dx.doi.org/10.1007/978-3-642-75267-4_8.

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Conference papers on the topic "Synthetic reagents"

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Kumar, Rishi E., and Katherine Uttley-Stack. "Generative Digital Design of Polymeric Coatings with Advanced Properties." In CONFERENCE 2025. AMPP, 2025. https://doi.org/10.5006/c2025-00601.

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Abstract A materials design pipeline consisting of two machine learning models was used to downselect and validate novel corrosion-resistant polymer structures for use in a high-temperature compatible protective coating. The first model is a generative model that creates polymers as candidates for coating applications. The second model is a graph neural network that predicts a variety of properties for the candidate polymers. Combined, these models create a database of over one million polymers with a variety of predicted properties; these polymers are ranked for their ability to serve as a pr
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Keo, Van Dong, Xuan Tran Hiep, Quoc Nguyen Banh, Tran Anh Son, and Duong Huyen Lynh. "Determination of Geometrical Parameters to Balance the Pressure Drop of Channels on a Microfluidic Chip." In 2024 International Conference on Machining, Materials and Mechanical Technologies. Trans Tech Publications Ltd, 2025. https://doi.org/10.4028/p-me24oh.

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In the past few years, micro-droplets have been widely used in diverse fields of biological and chemical research, spanning from drug delivery and material synthesis to point-of-care diagnostics, digital PCR, and single-cell analysis. Droplet-based microfluidics offers a powerful platform for conducting complex experiments, screening processes, and analyses with enhanced precision, efficiency, and versatility. While creating droplets with uniform sizes is a common objective of microfluidics, it is not limited to producing droplets of a single size per chip. Creating microdroplets with differen
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Santi, Claudio, Loredana Incipini, Elisabetta Rongoni, Luana Bagnoli, and Francesca Marini. "New Chiral Electrophilic Selenium Reagents: Synthesis and Structural Investigation." In The 16th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2012. http://dx.doi.org/10.3390/ecsoc-16-01013.

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Kirschning, Andreas, Silvie Dohmann, Georgia Sourkouni-Argirusi, Nuria Merayo, and Andreas Schonberger. "Cohalogenation of Allyl- and Vinylsilanes using Polymer-bound Haloate(I)-Reagents." In The 4th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2000. http://dx.doi.org/10.3390/ecsoc-4-01881.

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Senge, Mathias, and Xiangdong Feng. "Facile and Efficient Synthesis of Functionalized Asymmetric Porphyrins with Organolithium Reagents." In The 4th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2000. http://dx.doi.org/10.3390/ecsoc-4-01903.

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Ley, Steven, Gloria Brusotti, Marina Caldarelli, Jörg Habermann, and James Scott. "Polymer-Supported Reagents as Versatile Tools in Combinatorial Chemistry and Total Synthesis." In The 4th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2000. http://dx.doi.org/10.3390/ecsoc-4-01885.

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Hodgetts, Kevin, Gerhard Lascober, and Massimo Zorzi. "Studies Towards New Reagents for Asymmetric Hydroboration: Synthesis of Racemic Trans-2,5-diisopropylborolane." In The 4th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2000. http://dx.doi.org/10.3390/ecsoc-4-01875.

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Singhal, Rakshanda, Babita Malik, and Meenakshi Pilania. "Recent advances in synthetic application and functionalization of organohypervalent iodine reagents." In PROCEEDINGS OF THE 11TH INTERNATIONAL ADVANCES IN APPLIED PHYSICS AND MATERIALS SCIENCE CONGRESS & EXHIBITION. AIP Publishing, 2023. http://dx.doi.org/10.1063/5.0139191.

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Gryko, D., Zofia Urbanczyk-Lipkowska, and Janusz Jurczak. "Diastereoselective Addition of Allyl Reagents to N-Monoprotected and N,N-Diprotected L-Alaninals." In The 1st International Electronic Conference on Synthetic Organic Chemistry. MDPI, 1997. http://dx.doi.org/10.3390/ecsoc-1-02048.

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D’Hooghe, Matthias, and Norbert De Kimpe. "Reactivity of 1-arenesulfonyl- and 1-alkyl-2-(bromomethyl)aziridines towards Lithium Cuprate Reagents." In The 9th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2005. http://dx.doi.org/10.3390/ecsoc-9-01474.

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Reports on the topic "Synthetic reagents"

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Prakash, G. K., Markus Etzkorn, George A. Olah, Karl O. Christe, and Stefan Schneider. Triphenylmethyldifluoramine: A Stable Reagent for the Synthesis of gem-Bis(difluoramines). Defense Technical Information Center, 2002. http://dx.doi.org/10.21236/ada409564.

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