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Dissertations / Theses on the topic 'Synthetic reagents'

Author: Grafiati

Published: 3 June 2025

Last updated: 1 August 2025

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1

Whelligan, Daniel Keith. "Silenes as novel synthetic reagents." Thesis, Durham University, 2003. http://etheses.dur.ac.uk/3135/.

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Several syntheses of aryltris(trimethylsilyl)silanes were investigated and finally a novel route was developed starting from tetrakis(trimethylsilyl)silane, the mechanism for which was investigated. This new robust and reproducible synthesis involved a halogen-metal exchange and exploited a Schlenk equilibrium and was used to produce phenyltris(trimethylsilyl)silane in high yield (-70 %) on scales of up to 20 g. Phenyltris(trimethylsilyl)silane was used as the starting material for the synthesis of silene precursors; 1-hydroxyalkylphenyltrisilanes (silyl alcohols), involving KO'Bu-mediated for

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2

McLaren, Lee. "Synthetic applications of hypervalent iodine reagents : total synthesis of aranorosin." Thesis, University of East Anglia, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.385890.

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3

McCall, Matthew D. "Organozinc reagents : structural tailoring for synthetic applications." Thesis, University of Strathclyde, 2012. http://oleg.lib.strath.ac.uk:80/R/?func=dbin-jump-full&object_id=18805.

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Building on recent advances in zincate chemistry, but going beyond the state-of-the-art, this project sought to advance the understanding of the mechanisms involved in alkali metalmediated zincation (AMMZn), as well as design a new type of mixed-metal reagent, magnesium-zinc hybrids, focussing on their applications in nucleophilic additions to ketones and direct zinc-iodine exchange reactions. Unveiling two new applications of the alkali metal TMP-zincates [(THF)Li(TMP)ZntBu₂] (1) and [(TMEDA)Na(TMP)ZntBu₂] (3), reaction with trimethyl(phenoxy)silane (12) allowed the isolation of the first int

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4

Griffiths, Russell Jon. "Silenes : novel synthetic reagents for olefin functionalisation." Thesis, Durham University, 2000. http://etheses.dur.ac.uk/4331/.

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Silenes, compounds containing silicon-carbon double bonds, have been subject to much theoretical interest over the past 25 years. However, despite their high reactivity, to date there have been no reports of the attempted use of silenes as synthetic reagents. Silenes have been formed by the thermolysis of acyltris(trimethylsilyl)silanes, which have been found to react with dienes to give Diels-Alder cycloadducts in good yield. Further to this, it has been found that silene dimers, formed by the photolysis of acyltris(trimethylsilyl)silanes, have been found to revert to give silenes at much low

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5

Inoue, Atsushi. "Studies on novel synthetic reactions with organomagnesium reagents." 京都大学 (Kyoto University), 2003. http://hdl.handle.net/2433/148831.

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6

Kakiya, Hirotada. "Studies on Novel Synthetic Reactions with Organomanganese Reagents." 京都大学 (Kyoto University), 2002. http://hdl.handle.net/2433/149780.

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7

Fairfull-Smith, Kathryn Elizabeth, and n/a. "Synthetic and Mechanistic Investigations of Some Novel Organophosphorus Reagents." Griffith University. School of Science, 2004. http://www4.gu.edu.au:8080/adt-root/public/adt-QGU20040917.081950.

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The alkoxytriphenylphosphonium ion intermediate of the Mitsunobu reaction for the esterification and inversion of configuration of an alcohol can be generated using the Hendrickson reagent, triphenylphosphonium anhydride trifluoromethanesulfonate, 27. While 27 was used in place of the Mitsunobu reagents (triphenylphosphine and a dialkyl azodicarboxylate) for the esterification of primary alcohols, the reaction failed with secondary alcohols such as (-)-menthol giving predominately elimination rather than the desired SN2 displacement. The difference between the two reactions was shown to be r

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8

Turner, Jayne Susan. "Molecular recognition of damaged DNA using synthetic affinity reagents." Thesis, Open University, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.418471.

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Potentially carcinogenic DNA damage that may be derived from dietary sources can be quantified using a number of methods. Some of the best of these methods are based on the use of antibodies that have high affinity and specificity for modified DNA bases. However, given the sometimes limited availability of antibodies there is a requirement for novel reagents that mimic the properties of the best antibodies. From a chemical perspective antibodies are `over engineered' and synthetic affinity reagents would recreate the optimal properties of the binding site with respect to selectivity and affini

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9

Hunter, Christopher. "Investigations and synthetic applications of #beta#-amino zinc reagents." Thesis, University of Newcastle Upon Tyne, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.364835.

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10

Fairfull-Smith, Kathryn Elizabeth. "Synthetic and Mechanistic Investigations of Some Novel Organophosphorus Reagents." Thesis, Griffith University, 2004. http://hdl.handle.net/10072/367534.

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The alkoxytriphenylphosphonium ion intermediate of the Mitsunobu reaction for the esterification and inversion of configuration of an alcohol can be generated using the Hendrickson reagent, triphenylphosphonium anhydride trifluoromethanesulfonate, 27. While 27 was used in place of the Mitsunobu reagents (triphenylphosphine and a dialkyl azodicarboxylate) for the esterification of primary alcohols, the reaction failed with secondary alcohols such as (-)-menthol giving predominately elimination rather than the desired SN2 displacement. The difference between the two reactions was shown to be r

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11

Nishikawa, Toshihiro. "Studies on Novel Synthetic Reactions with Organomanganate and Organochromate Reagents." 京都大学 (Kyoto University), 2004. http://hdl.handle.net/2433/147626.

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12

Brahmbhatt, Shweta. "Development of synthetic peptide reagents as a diagnostic tool for leprosy." Thesis, London School of Hygiene and Tropical Medicine (University of London), 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.251991.

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13

Hata, Takeshi. "Studies on the Synthetic Aspects of Fluoromethylmetal Reagents Derived from Tribromofluoromethane." Kyoto University, 2000. http://hdl.handle.net/2433/157077.

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本文データは平成22年度国立国会図書館の学位論文(博士)のデジタル化実施により作成された画像ファイルを基にpdf変換したものである<br>Kyoto University (京都大学)<br>0048<br>新制・課程博士<br>博士(工学)<br>甲第8330号<br>工博第1895号<br>新制||工||1166(附属図書館)<br>UT51-2000-F234<br>京都大学大学院工学研究科材料化学専攻<br>(主査)教授檜山爲次郎, 教授大嶌幸一郎, 教授吉田潤一<br>学位規則第4条第1項該当

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14

Precht, Thea-Luise. "Preparing main group metal clusters from organoaluminium reagents : new possibilities in alkali-activated polymer crosslinking." Thesis, University of Cambridge, 2018. https://www.repository.cam.ac.uk/handle/1810/285495.

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The reactions of carboxylic acids with organoaluminium reagents were studied, which led to the formation of novel aluminium compounds. The reactions of orthofunctionalised derivatives of benzoic acid with trivalent aluminium organyls AlR3, led to the formation of different Al-based molecular clusters, depending on the nature of R, the reaction stoichiometry and the character of the benzoic acid derivative. The obtained compounds were characterised in the solid state by X-ray diffraction methods and two main motifs were observed. When the acid and AlR3 reacted in a one-to-two stoichiometry the

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15

Wang, Zhongren. "New reagents for radical allylations, and the synthetic use of 5-endo trigonal radical cyclization." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1997. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp04/mq22689.pdf.

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16

Goddard-Borger, Ethan D. "Some synthetic carbohydrate chemistry : natural product synthesis, rational inhibitor design and the development of a new reagent." University of Western Australia. School of Biomedical, Biomolecular and Chemical Sciences, 2008. http://theses.library.uwa.edu.au/adt-WU2009.0043.

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Earnest carbohydrate research was initiated in the nineteenth century by several talented organic chemists. Carbohydrates, now known to play essential roles in a range of fundamental biological processes, are presently studied by a throng of scientists from many fields, including: biochemistry, molecular biology, immunology, structural biology, medicine, agriculture, pharmacology and, of course, chemistry. Organic chemistry remains as relevant to carbohydrate research as it has ever been; its practitioners, with their skills in synthesis and fundamental understanding of molecules, are truly in

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17

Matloka, Kornelia K. "Synthetic development of C₃-symmetric triphenoxymethane based reagents for the selective recognition and sequestration of lanthanides and actinides." [Gainesville, Fla.] : University of Florida, 2006. http://purl.fcla.edu/fcla/etd/UFE0013811.

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18

Ramaya, Sharn. "Synthetic studies towards C-glycosyl amino acids : Part I, The synthesis of C-glycosyl amino acids using zinc reagents; Part II, Approaches towards the synthesis of C-glycosyl amino acids using an imino ene reaction." Thesis, University of Bristol, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.390646.

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19

Petersson, Maria Jenni. "Development of Phosphonium Anhydrides for the Synthesis of Heterocycles; Synthesis of Potential Inhibitors of Glycogen Phosphorylase." Thesis, Griffith University, 2009. http://hdl.handle.net/10072/367001.

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The use of several phosphonium anhydride reagents for the synthesis of a range of heterocyclic compounds has been investigated. The structure of a polymer-supported version of the Hendrickson ‘POP’ reagent, prepared by the reaction of polymer-supported triphenylphosphine oxide (57) with triflic anhydride, was established as an equilibrium mixture of polymer-supported triphenylphosphine ditriflate 54 (δ 79.4 ppm) and polymer-supported phosphonium anhydride 76 (δ 73.3 ppm). The 31P NMR chemical shift reported previously for 54 was shown to be incorrect. β-Hydroxy amides 96 and 103 were treated w

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20

Reeve, K. M. "Selenium reagents in organic synthesis." Thesis, Imperial College London, 1985. http://hdl.handle.net/10044/1/37829.

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21

Marques, Carolina Silva. "Synthesis and evaluation of chiral phosphine and NHC-Ligands or heterogeneous asymmetric catalysis." Doctoral thesis, Universidade de Évora, 2013. http://hdl.handle.net/10174/15896.

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No âmbito deste trabalho, foram estudadas as reacções de arilação catalítica assimétrica em vários substratos, utilizando novos e já conhecidos catalisadores quirais, possuindo metais de transição. Esta metodologia levou à formação de novas ligações C-C, fornecendo uma panóplia de interessantes compostos, podendo-se revelar intermediários extremamente úteis na síntese de compostos biologicamente activos. Deve-se salientar a síntese de aminas quirais, α-hidroxiésteres, α-amino-ácidos e α-aminoésteres e também bi-arildiarilaminas, utilizando catalisadores de metais de transição, baseados em Pd,

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22

Holt, Jay. "1,8-Diarylanthracenes as reagents for asymmetric synthesis." Diss., Georgia Institute of Technology, 1992. http://hdl.handle.net/1853/29902.

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23

Wu, An-hsiang. "Syntheses of Highly Strained Energetic Molecules and Development of New Synthetic Methodology." Thesis, North Texas State University, 1987. https://digital.library.unt.edu/ark:/67531/metadc331132/.

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The objective of this study was to synthesize new energetic, strained, saturated polycyclic compounds. For this purpose, new methodology has been developed, as follows: (i) Ketenes have been generated in situ via treatment of aldo-, keto- or alkenoic acid with either toluenesulfonyl chloride or 2-chloro-1-methylpyridfniurn iodide (Mulkaiyama's reagent). The reactive intermediates thereby generated have been found to undergo intramolecular [2+2] cycloaddition reactions in these systems.

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24

Topping, Chris Mark. "Design and synthesis of chiral ligands for copper catalysed asymmetric synthesis." Thesis, University of Hull, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.301496.

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25

Dent, Phillip Damian. "Asymmetric ligands for lanthanide(II) reagents." Thesis, Durham University, 1999. http://etheses.dur.ac.uk/4583/.

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Although the use of Ln(^2+) species as one electron reducing agents has recently become popular, relatively few processes have focused on the control of stereochemistry by the incorporation of chiral auxiliaries at the metal centre. This thesis discusses work aimed at the synthesis of chiral bis(pentaalkylcyclopentadienyl) and polyaza/oxo ligands for Ln(II) ions, and their subsequent application in asymmetric organic synthesis. Synthesis of enantiomerically pure bis(pentaalkylcyclopentadienyl) ligands was attempted via a novel double Nazarov cyclisation of 5,6-di-(methyl)-decane-3,8-dione. A c

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26

Smithies, Helen Kirsty. "Lead(IV) reagents in organic synthesis." Thesis, University of Oxford, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.413211.

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27

Czyzewski, Michal. "Silenes : novel reagents for organic synthesis." Thesis, Durham University, 2010. http://etheses.dur.ac.uk/476/.

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Whilst silenes have long been studied for their unique chemistry there has been little attempt to exploit this in other synthetic strategies. As part of a programme to explore this aspect the reactions of readily accessible silenes with alkenes and dienes were studied. Silenes, generated by the thermolysis of acylpolysilanes, add to α,β-unsaturated esters to form silacyclobutanes and silyl-substituted cyclopropanes in moderate yields. Upon silicon-carbon bond oxidation the cyclopropanes were converted directly to 1,4-dicarbonyl compounds, thus demonstrating the formal acyl anion chemistry of a

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28

Orton, Darren. "Nitroacrylates : versatile reagents in organic synthesis." Thesis, Durham University, 2001. http://etheses.dur.ac.uk/3782/.

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Nitroacrylates are stable, crystalline solids and have frequently been used in synthesis as reactive dienophiles in the Diels-Alder reaction. The regio- and diastereoselectivity of the Diels-Alder reaction is controlled by the electronic properties of the nitro group. This thesis describes work to utilise the nitro group to provide control of stereochemistry in the synthesis of natural products. The thesis begins by discussing the synthesis of nitroacrylates using both a nitro-aldol and radical based route. An investigation into their selectivity in the Diels-Alder reaction with a diverse arra

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29

Low, C. M. R. "Organoiron complexes as reagents for synthesis." Thesis, Imperial College London, 1987. http://hdl.handle.net/10044/1/47137.

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30

Douglas, Craig. "Silacycles : novel reagents in asymmetric synthesis." Thesis, Durham University, 1998. http://etheses.dur.ac.uk/4785/.

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Silicon based organic reagents have enjoyed a wealth of applications in the last thirty year. However, the development of organosilanes for asymmetric synthesis has been less prolific. The drawbacks of using 'Si-centred' chiral organosilanes has led to 'C- centred' organosilicon compounds being the substrate of choice. This research has been directed at the synthesis and application of C(_2) symmetric 'C-centred' cyclic organosilicon species and their potential applications in asymmetric synthesis. A variety of synthetic methods have been considered, the most successful of which has been the d

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31

Schuster, Christopher Henry. "Synthesis and Utility of Organoboron Reagents for Enantioselective Synthesis." Thesis, Boston College, 2014. http://hdl.handle.net/2345/bc-ir:103558.

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Thesis advisor: James P. Morken<br>Described herein are three distinct projects centered on the formation and use of carbon-boron bonds. In the first, the enantioselective platinum-catalyzed 1,4-diboration of trans-1,3-dienes is advanced in both selectivity and scope through the development of a novel class of electron rich chiral monodentate phosphines. Under the action of the new ligands, highly selective diboration is maintained at reduced loadings of catalyst. Secondly, enantioenriched 1,2-bis(pinacol boronates) are engaged in regioselective Suzuki-Miyaura cross-coupling with aryl and viny

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32

Desai, Bimbisar. "Microwave assisted organic synthesis." Thesis, University of Surrey, 2002. http://epubs.surrey.ac.uk/842821/.

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The area of chemical research and synthesis increasingly recognises the need for improved technologies and methods, which involves chemical processes with less energy consumption, time savings, reduction and/or minimisation of waste, simple processes and an overall clean production. Microwave heating has been exploited in a variety of disciplines for many useful applications and organic synthesis is an area, which has benefited significantly over the past decade. The present study investigates organic reactions accelerated under microwave irradiations. In particular, the study involves use of

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33

Pearson, Mark. "Organometallic reagents for catalytic cross-coupling." Thesis, University of Oxford, 1992. http://ora.ox.ac.uk/objects/uuid:c5eea9a0-8f0c-46bf-a1ea-28a40b79546d.

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Phosphine complexes of nickel and palladium provide the best catalysts for the homogeneous catalysed carbon-carbon bond forming reaction between an organometallic nucleophile and an organic electrophile. Use of a homochiral ligand on the catalyst can lead to stereoselectivity in the cross-coupling reaction, with high ee's of coupled product being obtained. The processes of selectivity in the transmetalation step of the catalytic cycle have not been elucidated and the initial aim of the project was to study these processes. Initial experiments using organotin derivatives as the organometallic n

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34

Richardson, Nigel. "Studies on fluorescent triazoline-3,5-diones." Thesis, University of Exeter, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.279752.

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35

Steele, Rebecca Mary. "Chiral sulfur-based reagents in asymmetric synthesis." Thesis, University of Bristol, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.288453.

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36

Hemming, David. "Applications of copper-boryl reagents in synthesis." Thesis, Durham University, 2017. http://etheses.dur.ac.uk/12232/.

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Previous work into the copper catalysed borylation of alkenyl halides has resulted in the synthesis of cyclic Bpin esters. To date however, the reaction has not been applied to the synthesis of saturated heterocycles nor substituted carbocycles. An overview of the literature precedent for reactions involving copper-boryl complexes is provided in the introduction (chapter 1). Investigations into the reaction were undertaken in an attempt to further expand its scope, and the second chapter outlines preliminary results and investigations into the formation of carbocyclic boronate esters. Applicat

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37

Kim, Shang-U. "Synthesis of diene ceramides with organozirconium reagents." Thesis, The University of Arizona, 2004. http://hdl.handle.net/10150/292081.

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Ceramide serves as a precursor to sphingomyelins and glycosphingolipids, and as an important intermediate in the de novo biosynthesis. Ceramide will act as second messenger in cell systems to induce programmed cell death (apoptosis). Ceramide is composed of a sphingosine backbone and fatty acid linked in an amide bond, and its structural variations have been modified and synthesized by many research group. The diene ceramide, unusual analogues of ceramide with a conjugated diene may have higher reactivity than other novel ceramide in mitochondria by facilitated oxidation at C3. One of the most

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38

Pearce, Alan James. "The synthesis of c-glycopeptides and hydroxylamine reagents." Thesis, University of Bristol, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.262833.

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39

Skinner, Christopher John. "Elemental fluorine as a valid synthetic reagent." Thesis, Durham University, 1994. http://etheses.dur.ac.uk/5141/.

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Chapter I Chapter I reviews the uses of elemental fluorine in selective organic synthesis and its use in the generation of selective electrophilic fluorinating agents. Chapter II Chapter II describes a systematic investigation into suitable solvents for the direct fluorination of deactivated aromatic systems. After highlighting 98% formic acid and 98 % sulphuric acid as excellent media for fluorinations, a number of other protonic acids were investigated. The work confirms the power of the resulting in situ fluorinating species is dependent on the pKa of the protonic acid. Chapter III Chapter

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40

He, Song Helen, and 何松. "Synthesis and applications of polystyrene-supported phosphine and arsine reagents." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2006. http://hub.hku.hk/bib/B38646122.

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41

Houghton, Mark Phillip. "Polymer-supported reactions using ion-exchange resins." Thesis, Lancaster University, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.255343.

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42

Cragg-Hine, Ian. "Early main group metal complexes of multi-functional organic molecules." Thesis, University of Cambridge, 1995. https://www.repository.cam.ac.uk/handle/1810/271932.

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43

Wright, Emma. "The development of organolead reagents in organic synthesis." Thesis, University of Oxford, 1995. http://ora.ox.ac.uk/objects/uuid:3cf2abd7-79f8-4963-82ad-ea3bb6eb98db.

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This thesis describes the synthesis of novel lead(IV) tetracarboxylates and the development of their use in carbon-carbon bond formation processes, with a particular emphasis on the construction of chiral, quaternary centres. Organolead(IV) tricarboxylates have been widely used in the functionalisation of a range of β-dicarbonyl compounds, and the available evidence suggests that these reactions occur by a ligand coupling mechanism. For this reason, by using chiral lead(IV) compounds, it may be possible to achieve a transfer of asymmetry in the bond formation reaction. A variety of achiral and

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44

Moran, Wesley James. "Novel uses of conjunctive reagents in organic synthesis." Thesis, University of Sheffield, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.401207.

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45

Hays, David S. (David Scott) 1970. "The development of organotin reagents for organic synthesis." Thesis, Massachusetts Institute of Technology, 1998. http://hdl.handle.net/1721.1/47483.

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46

MacCoss, Rachel Nicola. "Applications of solid-supported reagents for organic synthesis." Thesis, University of Cambridge, 2005. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.614821.

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47

Wheatley, Andrew Edward Henry. "The role of organolithium reagents in organic synthesis." Thesis, University of Cambridge, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.624976.

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48

Bream, Robert Nicholas. "Multi-step organic synthesis using solid-supported reagents." Thesis, University of Cambridge, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.619764.

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49

Jude, Hershel Jr. "Synthesis and Characterization of Two-Electron Platinum Reagents." University of Cincinnati / OhioLINK, 2004. http://rave.ohiolink.edu/etdc/view?acc_num=ucin1077290152.

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Jude, Jr Hershel. "Synthesis and characterization of two-eletron platinum reagents." Cincinnati, Ohio : University of Cincinnati, 2004. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=ucin1077290152.

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