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Journal articles on the topic 'T3P®'

Author: Grafiati

Published: 5 June 2025

Last updated: 2 August 2025

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1

Harsha, Kachigere B., and Kanchugarkoppal S. Rangappa. "One-step approach for the synthesis of functionalized quinoxalines mediated by T3P®–DMSO or T3P® via a tandem oxidation–condensation or condensation reaction." RSC Advances 6, no. 62 (2016): 57154–62. http://dx.doi.org/10.1039/c6ra03078e.

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An easy and efficient (T3P®)–DMSO or T3P® mediated oxidation–condensation or condensation reaction for the synthesis of quinoxalines from the different arrays of condensing partners and ortho-phenylene diamines (o-PDs) in one step has been reported.

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2

Behera, Manoranjan, C. Balakrishna, Venu Kandula, Ramakrishna Gudipati, Satyanarayana Yennam, and P. Devi. "An Efficient Microwave-Assisted Propylphosphonic Anhydride (T3P®)-Mediated One-Pot Chromone Synthesis via Enaminones." Synlett 29, no. 08 (2018): 1087–91. http://dx.doi.org/10.1055/s-0036-1591898.

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An efficient synthesis of 4H-chromene-4-ones via enamino ketones, with cyclization by using T3P® under microwave heating is described. This is the first report for the synthesis of chromones by using T3P®. Significant features of this method include short reaction times and high-purity products.

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3

Varga, Valentina, Péter Ábrányi-Balogh, and Mátyás Milen. "Synthesis of Naphthoxazinones in a One-Pot Two-Step Manner by the Application of Propylphosphonic Anhydride (T3P®)." Chemistry 2, no. 2 (2020): 600–612. http://dx.doi.org/10.3390/chemistry2020037.

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A sequential one-pot two-step protocol has been elaborated for the synthesis of naphthoxazinones from 2-naphthol, methyl carbamate, and aromatic aldehydes. First, a three-component reaction was optimized with the dehydrating additive propylphosphonic anhydride (T3P®), resulting in 1-carbamatoalkyl 2-naphthols in good to excellent yields. Following the successful multicomponent approach, intramolecular acylation was performed at high temperature, again with the contribution of T3P®, resulting in naphthoxazinone derivatives in moderate yields. These two steps were optimized together in one-pot a

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4

Balakrishna, C., Ramakrishna Gudipati, Venu Kandula, Satyanarayana Yennam, P. Uma Devi, and Manoranjan Behera. "T3P® mediated domino C(sp2)–H sulfenylation/annulation of enaminones and methylsulfinyls for the synthesis of chromone thioether derivatives." New Journal of Chemistry 43, no. 6 (2019): 2458–63. http://dx.doi.org/10.1039/c8nj05554h.

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5

Cheruku, Srinivas, Sandhya C. Nagarakere, Makanahalli P. Sunilkumar, et al. "An expedient, efficient and solvent-free synthesis of T3P®-mediated amidation of benzhydrols with poorly reactive N-nucleophiles under MW irradiation." New Journal of Chemistry 46, no. 9 (2022): 4421–26. http://dx.doi.org/10.1039/d1nj04502d.

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An expedient, efficient, economical, environmentally benign, and solvent free amidation protocol of benzhydrols with less reactive nitrogen nucleophiles assisted by propylphosphonic anhydride (T3P®) under microwave irradiation has been developed.

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6

Gowda, Darshini, Kachigere B. Harsha, Veeresha Gowda Shalini, Shobith Rangappa, and Kanchugarakoppal S. Rangappa. "Microwave assisted one-pot access to pyrazolo quinolinone and tetrahydroisoxazolo quinolinone derivatives via T3P®-DMSO catalysed tandem oxidative–condensation reaction." RSC Advances 13, no. 40 (2023): 28362–70. http://dx.doi.org/10.1039/d3ra05235d.

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A new strategic approach for the synthesis of two important annulated pyrazolo quinolinone and tetrahydroisoxazolo quinolinone derivatives has been reported for the first time from the alcohols using T3P®-DMSO as a catalyst.

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7

Mattellone, Alexia, Dario Corbisiero, Paolo Cantelmi, et al. "Fast Solution-Phase and Liquid-Phase Peptide Syntheses (SolPSS and LPPS) Mediated by Biomimetic Cyclic Propylphosphonic Anhydride (T3P®)." Molecules 28, no. 20 (2023): 7183. http://dx.doi.org/10.3390/molecules28207183.

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The growing applications of peptide-based therapeutics require the development of efficient protocols from the perspective of an industrial scale-up. T3P® (cyclic propylphosphonic anhydride) promotes amidation in the solution-phase through a biomimetic approach, similar to the activation of carboxylic moiety catalyzed by ATP-grasp enzymes in metabolic pathways. The T3P® induced coupling reaction was applied in this study to the solution-phase peptide synthesis (SolPPS). Peptide bond formation occurred in a few minutes with high efficiency and no epimerization, generating water-soluble by-produ

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8

Gajda, Tadeusz, Łukasz Janczewski, Anna Gajda, Sebastian Frankowski, and Tomasz Goszczyński. "T3P® – A Benign Desulfurating Reagent in the Synthesis of Isothiocyanates." Synthesis 50, no. 05 (2017): 1141–51. http://dx.doi.org/10.1055/s-0036-1591842.

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A number of alkyl, aryl and bifunctional isothiocyanates are obtained in moderate to high yields (41–94%) in a two-step, one-pot reaction of the parent primary amines or their salts with carbon disulfide, followed by reaction of the thus formed dithiocarbamates with T3P® (propane phosphonic acid anhydride) as a new and efficient desulfurating agent.

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9

Jablonkai, Erzsébet, Réka Henyecz, Mátyás Milen, János Kóti, and György Keglevich. "T3P®-assisted esterification and amidation of phosphinic acids." Tetrahedron 70, no. 44 (2014): 8280–85. http://dx.doi.org/10.1016/j.tet.2014.09.021.

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10

Kandula, Venu, Ramakrishna Gudipati, Anindita Chatterjee, Satyanarayana Yennam, and Manoranjan Behera. "An Efficient Method for the Preparation of N-Formamides using Propylphosphonic Anhydride (T3P®)." SynOpen 02, no. 02 (2018): 0176–79. http://dx.doi.org/10.1055/s-0036-1591584.

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The synthesis of N-formamides from aromatic amines and formic acid using propylphosphonic anhydride (T3P®) as a green coupling reagent is described. By using this method, aryl, heteroaryl and fluorinated aryl-containing formamides were synthesized in high yield and purity. The significant features of this method include easy work up, high purity and reduced toxicity of the reaction.

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11

Waghmare, Anirudha A., Rama Mohan Hindupur, and Hari N. Pati. "Propylphosphonic anhydride (T3P®): An expedient reagent for organic synthesis." Review Journal of Chemistry 4, no. 2 (2014): 53–131. http://dx.doi.org/10.1134/s2079978014020034.

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12

Tortoioli, Simone, Linda Bannwart, and Stefan Abele. "Metal-Free Amidation of Acids with Formamides and T3P®." Synthesis 48, no. 13 (2016): 2069–78. http://dx.doi.org/10.1055/s-0035-1561427.

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13

Zarei, Maaroof. "Convenient Propylphosphonic Anhydride (T3P®)-Mediated Synthesis of β-Sultams". Mendeleev Communications 23, № 1 (2013): 39–40. http://dx.doi.org/10.1016/j.mencom.2013.01.014.

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14

Milen, Mátyás, Péter Ábrányi-Balogh, Réka Kangyal, András Dancsó, Dávid Frigyes та György Keglevich. "T3P®-Mediated One-Pot Synthesis of Bis(α-aminophosphonates)". Heteroatom Chemistry 25, № 4 (2014): 245–55. http://dx.doi.org/10.1002/hc.21170.

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15

Reddy, Sirigireddy Sudharsan, Bhoomireddy Rajendra Prasad Reddy та Peddiahgari Vasu Govardhana Reddy. "Propylphosphonic anhydride (T3P®) catalyzed one-pot synthesis of α-aminonitriles". Chinese Chemical Letters 26, № 6 (2015): 739–43. http://dx.doi.org/10.1016/j.cclet.2015.03.021.

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16

Jablonkai, Erzsebet, Reka Henyecz, Matyas Milen, Janos Koti, and Gyoergy Keglevich. "ChemInform Abstract: T3P®-Assisted Esterification and Amidation of Phosphinic Acids." ChemInform 46, no. 14 (2015): no. http://dx.doi.org/10.1002/chin.201514248.

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17

Denißen, Melanie, Alexander Kraus, Guido J. Reiss, and Thomas J. J. Müller. "One-pot syntheses of blue-luminescent 4-aryl-1H-benzo[f]isoindole-1,3(2H)-diones by T3P® activation of 3-arylpropiolic acids." Beilstein Journal of Organic Chemistry 13 (November 3, 2017): 2340–51. http://dx.doi.org/10.3762/bjoc.13.231.

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In situ activation of 3-arylpropiolic acids with T3P® (n-propylphosphonic acid anhydride) initiates a domino reaction furnishing 4-arylnaphtho[2,3-c]furan-1,3-diones in excellent yields. Upon employing these anhydrides as reactive intermediates blue-luminescent 4-aryl-1H-benzo[f]isoindole-1,3(2H)-diones are formed by consecutive pseudo three-component syntheses in a one-pot fashion. The Stokes shifts correlate excellently with the Hammett–Taft σR parameter indicating an extended degree of resonance stabilization in the vibrationally relaxed excited singlet state.

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18

Mann, Lea, Markus Lang, Philipp Schulze та ін. "Racemization-free synthesis of Nα-2-thiophenoyl-phenylalanine-2-morpholinoanilide enantiomers and their antimycobacterial activity". Amino Acids 53, № 8 (2021): 1187–96. http://dx.doi.org/10.1007/s00726-021-03044-1.

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AbstractNα-2-thiophenoyl-d-phenylalanine-2-morpholinoanilide (MMV688845, IUPAC: N-(1-((2-morpholinophenyl)amino)-1-oxo-3-phenylpropan-2-yl)thiophene-2-carboxamide) from the Pathogen Box® library (Medicines for Malaria Ventures, MMV) is a promising lead compound for antimycobacterial drug development. Two straightforward synthetic routes to the title compound starting from phenylalanine or its Boc-protected derivative are reported. Employing Boc-phenylalanine as starting material and the T3P® and PyBOP® amide coupling reagents enables racemization-free synthesis, avoiding the need for subsequen

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19

Al Musaimi, Othman, Richard Wisdom, Peter Talbiersky, Beatriz G. De La Torre, and Fernando Albericio. "Propylphosphonic Anhydride (T3P®) as Coupling Reagent for Solid‐Phase Peptide Synthesis." ChemistrySelect 6, no. 11 (2021): 2649–57. http://dx.doi.org/10.1002/slct.202100123.

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20

Wen, Xiaoan, Jamal El Bakali, Rebecca Deprez-Poulain, and Benoit Deprez. "Efficient propylphosphonic anhydride (®T3P) mediated synthesis of benzothiazoles, benzoxazoles and benzimidazoles." Tetrahedron Letters 53, no. 19 (2012): 2440–43. http://dx.doi.org/10.1016/j.tetlet.2012.03.007.

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21

Milen, Mátyás, Péter Ábrányi-Balogh, András Dancsó, Dávid Frigyes, László Pongó та György Keglevich. "T3P®-promoted Kabachnik–Fields reaction: an efficient synthesis of α-aminophosphonates". Tetrahedron Letters 54, № 40 (2013): 5430–33. http://dx.doi.org/10.1016/j.tetlet.2013.07.145.

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22

Zarei, Maaroof. "ChemInform Abstract: Convenient Propylphosphonic Anhydride (T3P®)-Mediated Synthesis of β-Sultams". ChemInform 44, № 22 (2013): no. http://dx.doi.org/10.1002/chin.201322098.

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23

Desroses, Matthieu, Krzysztof Wieckowski, Marc Stevens, and Luke R. Odell. "A microwave-assisted, propylphosphonic anhydride (T3P®) mediated one-pot Fischer indole synthesis." Tetrahedron Letters 52, no. 34 (2011): 4417–20. http://dx.doi.org/10.1016/j.tetlet.2011.06.053.

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24

Augustine, John, Agnes Bombrun, Ashis Mandal, Padma Alagarsamy, Rajendra Atta, and Panneer Selvam. "Propylphosphonic Anhydride (T3P®)-Mediated One-Pot Rearrangement of Carboxylic Acids to Carbamates." Synthesis 2011, no. 09 (2011): 1477–83. http://dx.doi.org/10.1055/s-0030-1259964.

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25

Reddy, Sirigireddy Sudharsan, Bhoomireddy Rajendra Prasad Reddy та Peddiahgari Vasu Govardhana Reddy. "ChemInform Abstract: Propylphosphonic Anhydride (T3P®) Catalyzed One-Pot Synthesis of α-Aminonitriles." ChemInform 46, № 41 (2015): no. http://dx.doi.org/10.1002/chin.201541079.

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26

Desroses, Matthieu, Marie-Caroline Jacques-Cordonnier, Sabin Llona-Minguez, et al. "A Convenient Microwave-Assisted Propylphosphonic Anhydride (T3P®) Mediated One-Pot Pyrazolone Synthesis." European Journal of Organic Chemistry 2013, no. 26 (2013): 5879–85. http://dx.doi.org/10.1002/ejoc.201300380.

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27

Milen, Matyas, Peter Abranyi-Balogh, Andras Dansco, David Frigyes, Laszlo Pongo та Gyoergy Keglevich. "ChemInform Abstract: T3P®-Promoted Kabachnik-Fields Reaction: An Efficient Synthesis of α-Aminophosphonates." ChemInform 45, № 4 (2014): no. http://dx.doi.org/10.1002/chin.201404191.

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28

Wen, Xiaoan, Jamal El Bakali, Rebecca Deprez-Poulain, and Benoit Deprez. "ChemInform Abstract: Efficient Propylphosphonic Anhydride (®T3P) Mediated Synthesis of Benzothiazoles, Benzoxazoles and Benzimidazoles." ChemInform 43, no. 35 (2012): no. http://dx.doi.org/10.1002/chin.201235137.

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29

Popovics-Tóth, Nóra, Kármen Emőke Szabó, and Erika Bálint. "Study of the Three-Component Reactions of 2-Alkynylbenzaldehydes, Aniline, and Dialkyl Phosphites—The Significance of the Catalyst System." Materials 14, no. 20 (2021): 6015. http://dx.doi.org/10.3390/ma14206015.

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New, practical approaches for the synthesis of α-amino (2-alkynylphenyl)-methylphosphonates and 1,2-dihydroisoquinolin-1-ylphosphonates were developed. By the propylphosphonic anhydride (T3P®)-mediated Kabachnik–Fields reaction of 2-alkynylbenzaldehydes, aniline, and dialkyl phosphites, α-amino (2-alkynylphenyl)-methylphosphonates were obtained selectively in high yields. The method developed is a simple operation and did not require a chromatographic separation since the products could be isolated from the reaction mixture by a simple extraction. At the same time, 2,3-disubstituted-1,2-dihydr

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30

Jablonkai, Erzsébet, Mátyás Milen, László Drahos, and György Keglevich. "Esterification of five-membered cyclic phosphinic acids under mild conditions using propylphosphonic anhydride (T3P®)." Tetrahedron Letters 54, no. 44 (2013): 5873–75. http://dx.doi.org/10.1016/j.tetlet.2013.08.082.

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31

Cheruku, Srinivas, Chaithra Nagaraju, Poornima Shetty, et al. "An efficient synthesis of medicinally important indole based triarylmethanes by using propylphosphonic anhydride (T3P®)." Synthetic Communications 50, no. 10 (2020): 1486–94. http://dx.doi.org/10.1080/00397911.2020.1743319.

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32

Desroses, Matthieu, Krzysztof Wieckowski, Marc Stevens, and Luke R. Odell. "ChemInform Abstract: A Microwave-Assisted, Propylphosphonic Anhydride (T3P®) Mediated One-Pot Fischer Indole Synthesis." ChemInform 42, no. 48 (2011): no. http://dx.doi.org/10.1002/chin.201148116.

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33

Augustine, John Kallikat, Agnes Bombrun, Ashis Baran Mandal, Padma Alagarsamy, Rajendra Nath Atta, and Panneer Selvam. "ChemInform Abstract: Propylphosphonic Anhydride (T3P®)-Mediated One-Pot Rearrangement of Carboxylic Acids to Carbamates." ChemInform 42, no. 34 (2011): no. http://dx.doi.org/10.1002/chin.201134080.

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34

Desroses, Matthieu, Marie-Caroline Jacques-Cordonnier, Sabin Llona-Minguez, et al. "ChemInform Abstract: A Convenient Microwave-Assisted Propylphosphonic Anhydride (T3P®) Mediated One-Pot Pyrazolone Synthesis." ChemInform 45, no. 7 (2014): no. http://dx.doi.org/10.1002/chin.201407129.

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35

Al Musaimi, Othman, Richard Wisdom, Peter Talbiersky, Beatriz G. De La Torre, and Fernando Albericio. "Cover Picture: Propylphosphonic Anhydride (T3P®) as Coupling Reagent for Solid‐Phase Peptide Synthesis (11/2021)." ChemistrySelect 6, no. 11 (2021): 2648. http://dx.doi.org/10.1002/slct.202100729.

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36

Jida, Mouhamad, and Benoit Deprez. "Friedländer synthesis of polysubstituted quinolines and naphthyridines promoted by propylphosphonic anhydride (T3P®) under mild conditions." New Journal of Chemistry 36, no. 4 (2012): 869. http://dx.doi.org/10.1039/c2nj21043f.

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37

Sharath Kumar, Kothanahally S., Toreshettahally R. Swaroop, Kachigere B. Harsha, Kereyagalahally H. Narasimhamurthy, and Kanchugarakoppal S. Rangappa. "T3P®-DMSO mediated one pot cascade protocol for the synthesis of 4-thiazolidinones from alcohols." Tetrahedron Letters 53, no. 42 (2012): 5619–23. http://dx.doi.org/10.1016/j.tetlet.2012.08.020.

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38

Sureshbabu, Vommina, T. Vishwanatha, and Nageswara Panguluri. "Propanephosphonic Acid Anhydride (T3P®) - A Benign Reagent for Diverse Applications Inclusive of Large-Scale Synthesis." Synthesis 45, no. 12 (2013): 1569–601. http://dx.doi.org/10.1055/s-0033-1338989.

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39

Müller, Thomas, Lucilla Levi, and Sven Scheuren. "A Novel N-Benzylation of Phenothiazine with Benzyl Alcohols Activated by n-Propylphosphonic Acid Anhydride (T3P®)." Synthesis 46, no. 22 (2014): 3059–66. http://dx.doi.org/10.1055/s-0034-1378541.

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40

Sambaiah, M., Ramakrishna Gudipati, K. Shiva Kumar, Satyanarayana Yennam, and Manoranjan Behera. "An efficient method for the preparation of N-formyl-imide via amidine using propylphosphonic anhydride (T3P®)." Tetrahedron Letters 57, no. 3 (2016): 403–6. http://dx.doi.org/10.1016/j.tetlet.2015.12.046.

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41

Augustine, John Kallikat, Agnes Bombrun, and Srinivasa Venkatachaliah. "An efficient catalytic method for the Friedländer annulation mediated by peptide coupling agent propylphosphonic anhydride (T3P®)." Tetrahedron Letters 52, no. 50 (2011): 6814–18. http://dx.doi.org/10.1016/j.tetlet.2011.10.048.

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42

Zarei, Maaroof. "An efficient and green method for the synthesis of 2-azetidinones mediated by propylphosphonic anhydride (T3P®)." Monatshefte für Chemie - Chemical Monthly 145, no. 9 (2014): 1495–99. http://dx.doi.org/10.1007/s00706-014-1217-6.

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43

Pinzón Martín, Sandra Milena, Ricardo Fierro Medina, Carlos Arturo Iregui Castro, Zuly Jenny Rivera Monroy, and Javier Eduardo García Castañeda. "Novel Synthesis of N-Glycosyl Amino Acids Using T3P®: Propylphosphonic Acid Cyclic Anhydride as Coupling Reagent." International Journal of Peptide Research and Therapeutics 24, no. 2 (2017): 291–98. http://dx.doi.org/10.1007/s10989-017-9614-4.

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44

Hazai, Viktor, Tímea Szabó, Balázs Volk, and Mátyás Milen. "Propylphosphonic anhydride (T3P®)-mediated three-component synthesis of hexahydrodibenzo[b,e][1,4]diazepin-1-one derivatives." Chemistry of Heterocyclic Compounds 56, no. 2 (2020): 237–40. http://dx.doi.org/10.1007/s10593-020-02650-3.

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45

Jablonkai, Erzsebet, Matyas Milen, Laszlo Drahos, and Gyoergy Keglevich. "ChemInform Abstract: Esterification of Five-Membered Cyclic Phosphinic Acids under Mild Conditions Using Propylphosphonic Anhydride (T3P®)." ChemInform 45, no. 10 (2014): no. http://dx.doi.org/10.1002/chin.201410200.

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46

Madau, Mathieu, Didier Le Cerf, Virginie Dulong, and Luc Picton. "Hyaluronic Acid Functionalization with Jeffamine® M2005: A Comparison of the Thermo-Responsiveness Properties of the Hydrogel Obtained through Two Different Synthesis Routes." Gels 7, no. 3 (2021): 88. http://dx.doi.org/10.3390/gels7030088.

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Hyaluronic acid (HA) of different molar masses (respectively 38,000, 140,000 and 1,200,000 g.mol−1) have been functionalized with a commercial poly(etheramine), Jeffamine® M2005, in order to devise physical thermo-responsive hydrogels. Two routes have been studied, involving the use of either water for the first one or of N,N′-Dimethylformamide (DMF), a polar aprotic solvent, for the second one. In the case of the water route, the reaction was performed using a mixture of N-(3-Dimethylaminopropyl)-N′-ethylcarbodiimide (EDC) and N-hydroxysuccinimide (NHS) as coupling reagents. The reaction was

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47

Augustine, John Kallikat, Agnes Bombrun, Wolfgang H. B. Sauer, and Pujari Vijaykumar. "Highly efficient and chemoselective acetalization and thioacetalization of aldehydes catalyzed by propylphosphonic anhydride (®T3P) at room temperature." Tetrahedron Letters 53, no. 37 (2012): 5030–33. http://dx.doi.org/10.1016/j.tetlet.2012.07.052.

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48

Basavaprabhu, N. Narendra, Ravi S. Lamani, and Vommina V. Sureshbabu. "T3P® (propylphosphonic anhydride) mediated conversion of carboxylic acids into acid azides and one-pot synthesis of ureidopeptides." Tetrahedron Letters 51, no. 22 (2010): 3002–5. http://dx.doi.org/10.1016/j.tetlet.2010.04.002.

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49

Jida, Mouhamad, and Benoit Deprez. "ChemInform Abstract: Friedlaender Synthesis of Polysubstituted Quinolines and Naphthyridines Promoted by Propylphosphonic Anhydride (T3P®) under Mild Conditions." ChemInform 43, no. 37 (2012): no. http://dx.doi.org/10.1002/chin.201237148.

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50

Basavaprabhu, Basavaprabhu, T. M. Vishwanatha, Nageswara Rao Panguluri, and Vommina V. Sureshbabu. "ChemInform Abstract: Propanephosphonic Acid Anhydride (T3P®) - A Benign Reagent for Diverse Applications Inclusive of Large-Scale Synthesis." ChemInform 44, no. 32 (2013): no. http://dx.doi.org/10.1002/chin.201332249.

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