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Journal articles on the topic 'Thiadiazole-5-carbaldehyde'

Author: Grafiati

Published: 4 June 2025

Last updated: 1 August 2025

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1

Begum, Noor Shahina, D. E. Vasundhara, G. D. Kolavi, and I. M. Khazi. "2-Ethyl-6-(4-methoxyphenyl)imidazo[2,1-b][1,3,4]thiadiazole-5-carbaldehyde." Acta Crystallographica Section E Structure Reports Online 63, no. 4 (2007): o1955—o1957. http://dx.doi.org/10.1107/s1600536807012639.

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2

L'Abbé, Gerrit, Els Vanderstede, Wim Dehaen, Pieter Delbeke, and Suzanne Toppet. "Ring transformations of 5-chloro-1,2,3-thiadiazole-4-carbaldehyde with amines, hydrazines and hydroxylamine." J. Chem. Soc., Perkin Trans. 1, no. 3 (1991): 607–10. http://dx.doi.org/10.1039/p19910000607.

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3

Sowmya, A., G. N. Anil Kumar, Sujeet Kumar, and Subhas S. Karki. "Crystal structure, quantum chemical and Hirshfeld surface analysis of substituted imidazo-thiadiazole-5-carbaldehyde." Chemical Data Collections 17-18 (December 2018): 431–41. http://dx.doi.org/10.1016/j.cdc.2018.11.002.

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4

Mukesh, Bugalia, B. Puranik Sangamesh, Saraswat Rohit, Jhajharia Mahesh, and Sharma Prashant. "Design, One-pot Synthesis and Biological Evaluation of Imidazo[2,1-b] [1,3,4] Thiadiazole Derivatives for their Anti- Tubercular and Anti-Fungal Activity." International Multispeciality Journal of Health 6, no. 7 (2020): 14–24. https://doi.org/10.5281/zenodo.4095236.

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<strong>Abstract</strong><strong>—</strong> In the present designed work, we have synthesized imidazo[2,1-b][1,3,4]thiadiazole derivatives <strong>(6a1-a6 to 6d1-d6) </strong>by reaction of compound <strong>3 </strong>with appropriate α-haloaryl ketones produce substituted imidazo thiadiazole derivatives <strong>(4a-d)</strong>. In the next step, these compounds <strong>(4a–d) </strong>undergoes the Vilsmeier reaction to introduce formyl group on the substituted arylimidazo[2,1-b][1,3,4]thiadiazole derivatives to form carbaldehyde derivatives <strong>(5a–d) </strong>and

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5

Sowmya, A., G. N. Anil Kumar, Sujeet Kumar, and Subhas S. Karki. "The crystal structure of 6-(4-chlorophenyl)-2-(4-methylbenzyl)imidazo[2,1-b][1,3,4]thiadiazole-5-carbaldehyde." Acta Crystallographica Section E Crystallographic Communications 72, no. 10 (2016): 1460–62. http://dx.doi.org/10.1107/s2056989016014754.

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In the title imidazo[2,1-b][1,3,4]thiadiazole derivative, C19H14ClN3OS, the 4-methylbenzyl and chlorophenyl rings are inclined to the planar imidazo[2,1-b][1,3,4]thiadiazole moiety (r.m.s. deviation = 0.012 Å) by 64.5 (1) and 3.7 (1)°, respectively. The molecular structure is primarily stabilized by a strong intramolecular C—H...O hydrogen bond, leading to the formation of a pseudo-seven-memberedS(7) ring motif, and a short intramolecular C—H...N contact forming anS(5) ring motif. In the crystal, molecules are linked by pairs of C—H...S hydrogen bonds, forming inversion dimers. The dimers are

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6

Banu, Afshan, Ravi S. Lamani, I. M. Khazi, and Noor Shahina Begum. "Synthesis and Crystal Structure of 2-(4-Fluorobenzyl)-6-Phenylimidazo[2,1-b][1,3,4]Thiadiazole-5-Carbaldehyde." Molecular Crystals and Liquid Crystals 533, no. 1 (2010): 141–51. http://dx.doi.org/10.1080/15421406.2010.526556.

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7

L'ABBE, G., E. VANDERSTEDE, W. DEHAEN, P. DELBEKE, and S. TOPPET. "ChemInform Abstract: Ring Transformations of 5-Chloro-1,2,3-thiadiazole-4-carbaldehyde with Amines, Hydrazines and Hydroxylamine." ChemInform 22, no. 24 (2010): no. http://dx.doi.org/10.1002/chin.199124148.

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8

Hashem, Aya B., Olfat A. Nief, and Abdulkader M. Noori. "Synthesis, Characterization, and Antimicrobial Evaluation of Thiadiazole Derivatives Derived from 2-Amino-5-Thio-1,3,4-Thiadiazole." Iraqi Journal of Industrial Research 11, no. 2 (2024): 87–96. http://dx.doi.org/10.53523/ijoirvol11i2id402.

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This manuscript introduces a series of novel Schiff base and heterocyc-licring compounds, focusing on derivatives of 1,3-oxazepine and thiazo-lidinone.The derivative (2-Hydroxy-N-(5-mercapto-[1,3,4] thiadiazol-2-yl)-2-phenyl-acetamide was created by reacting ethyl mandelate ester[M1] and 2-amino-5-thio-1,3,4-thiadiazole compound to produce new compound [M2] and after that, compound [M2] was reacted with hydrazine hydrate 99% in dry DMF solvent, yielding the compound (N-(5-Hydrazino-[1,3,4]thiadiazol-2-yl)-2-hydroxy-2-phenyl-acetamide [M3]. In contrast , the Schiff base compound [M4] were synth

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9

Vasundhara, D. E., C. R. Girija, G. D. Kolavi, V. S. Hegde, and I. M. Khazi. "Synthesis, spectroscopy and crystal structure of 2-ethyl-6-(4-nitro-phenyl)imidazo[2,1-b][1,3,4]thiadiazole-5-carbaldehyde." Journal of Chemical Research 2006, no. 5 (2006): 286–88. http://dx.doi.org/10.3184/030823406777411070.

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10

Shaalan, Naser, Waleed Madhloom Khalaf, and Shatha Mahdi. "Preparation and Characterization of New Tetra-Dentate N<sub>2</sub>O<sub>2</sub> Schiff Base with Some of Metal Ions Complexes." Indonesian Journal of Chemistry 22, no. 1 (2021): 62. http://dx.doi.org/10.22146/ijc.66118.

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This study describes preparation a new series of tetra-dentate N2O2 dinuclear complexes Cr(III), Co(II)and Cu(II) of the Schiff base 2-[5-(2-hydroxy-phenyl)-1,3,4-thiadiazol-2-ylimino]-methyl-naphthalen-1-ol], (LH2) derived from 1-hydroxy-naphthalene-2-carbaldehyde with 2-amino-5-(2-hydroxy-phenyl)-1,3,4-thiadiazole. These ligands were characterized by FT-IR, UV-Vis, Mass spectra, elemental analysis, and 1H-NMR. All prepared complexes have been characterized by conductance measurement, magnetic susceptibility, electronic spectra, infrared spectrum, thermal Analysis (TGA), and metal analysis by

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11

Begum, Noor Shahina, D. E. Vasundhara, C. R. Girija, G. D. Kolavi, V. S. Hegde, and I. M. Khazi. "Synthesis, spectroscopic and crystal structure analysis of a compound with pharmocophoric substituent: 2-cyclohexyl-6-(2-oxo-2H-chromen-3-yl)- imidazo[2,1-b][1,3,4]thiadiazole-5-carbaldehyde." Journal of Chemical Crystallography 37, no. 3 (2007): 193–98. http://dx.doi.org/10.1007/s10870-006-9159-4.

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12

N. Ayyash, Ahmed, Entesar J. Fadhil, and Zainab H. Mohammad. "Synthesis of Novel Bioactive compounds of 5-arylidene-2-imino-thiazolidin-4-ones as Antimicrobial agents." Research Journal of Pharmacy and Technology, September 28, 2022, 4187–91. http://dx.doi.org/10.52711/0974-360x.2022.00702.

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In this study, a variety of 3,3'-(pyrazine-2,3-diyldi-1,3,4-thiadiazole-5,2-diyl)bis[2-imino-5-(5-substitutedpyridine-2-yl)-1,3-thiazolidin-4-one] derivatives have been synthesized with good yields starting by reaction of pyrazine-2,3-dicarboxylic acid and thiosemicarbazide. The resulted compound 2-amino-1,3,4-thiadiazole was treated with chloroacetic acid to give the corresponding chloroacetamide which further refluxed with potassium thiocyanate. The condensation of the product 2-imino-1,3-thiazolidin-4-one with different 5-substitutedpyridine-2-carbaldehyde produced the titled compounds. An

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13

Sagar, Kunigal S., Karthik Kumara, Banu SH, Neratur K. Lokanath, Manikyanahalli N. Kumara, and Kempegowda Mantelingu. "Microwave‐Assisted Synthesis and Characterization of Some Aldehyde Derivatives of Imidazo[2,1‐b][1,3,4]thiadiazole: Crystal Structure Insights, In‐Silico and Biological Studies." ChemistrySelect 8, no. 47 (2023). http://dx.doi.org/10.1002/slct.202302877.

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AbstractThe microwave‐assisted synthesis, crystallographic studies, in‐silico docking and the evaluation of in‐vitro biological activities of 2‐(3,4‐dimethoxy)‐6‐(substituted phenyl)‐ imidazo[2,1‐b][1,3,4]thiadiazole‐5‐carbaldehydes is represented here. Single‐crystal X‐ray diffraction experiments were used to identify the crystal structure of the 6‐(4‐chlorophenyl)‐2‐(3,4‐dimethoxybenzyl)imidazo[2,1‐b][1,3,4]thiadiazole‐5‐carbaldehyde. Using fingerprint plots, Hirshfeld surface analysis was used to confirm the contributions of distinct intermolecular interactions in the development of the cry

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14

Begum, Noor Shahina, D. E. Vasundhara, C. R. Girija, G. D. Kolavi, V. S. Hegde, and I. M. Khazi. "Synthesis, Spectroscopy and Crystal Structure of 2-Ethyl-6-(4-nitrophenyl)imidazo[2,1-b] [1,3,4]thiadiazole-5-carbaldehyde." ChemInform 37, no. 40 (2006). http://dx.doi.org/10.1002/chin.200640132.

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15

Srour, Aladdin M., Mohamed N. El-Bayaa, Mervat M. Omran, Marwa M. Sharaky, and Wael A. ElSayed. "Synthesis and Cytotoxic Properties of New Substituted Glycosides- Indole Conjugates as Apoptosis Inducers in Cancer Cells." Anti-Cancer Agents in Medicinal Chemistry 20 (September 29, 2020). http://dx.doi.org/10.2174/1871520620666200929155246.

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Background & Objective: Glycosyl heterocycles, being as nucleoside analogs with modified glycon and hybrid heterocycle motifs, are of considerable interest and thus the targeted compounds were synthesized via convenient and efficient approach. Methods: New indolyl-thiadiazolyl thioglycosides scaffolds were synthesized starting with the reaction of indole-3-carbaldehyde with 2- aminothiadiazole-5-thiole followed by glycosylation and deprotection. Likewise, new molecular hybrids comprising indole, thiadiazole, triazole and glycosyl moieties were synthesized utilizing click chemistry strategy

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