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Journal articles on the topic 'Thiodiglycol'

Author: Grafiati

Published: 4 June 2021

Last updated: 29 July 2025

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1

Samuilov, A. Ya, E. I. Galeeva, A. V. Kulikov, I. N. Bakirova, and Ya D. Samuilov. "Thiodiglycol-based oligomers." Russian Journal of Applied Chemistry 80, no. 12 (2007): 2093–96. http://dx.doi.org/10.1134/s1070427207120170.

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2

Brozena, Ann, David E. Tevault, and Katherine Irwin. "Vapor Pressure of Thiodiglycol." Journal of Chemical & Engineering Data 59, no. 2 (2014): 307–11. http://dx.doi.org/10.1021/je400978j.

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3

Reddy, Gunda, Michael A. Major, and Glenn J. Leach. "Toxicity Assessment of Thiodiglycol." International Journal of Toxicology 24, no. 6 (2005): 435–42. http://dx.doi.org/10.1080/10915810500368878.

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Sulfur mustard (HD) undergoes hydrolysis to form various products such as thiodiglycol (TG) in biological and environmental systems. TG is a precursor in the production of HD and it is also considered as a “Schedule 2” compound (dual-use chemicals with low to moderate commercial use and high-risk precursors). Several toxicological studies on TG were conducted to assess environmental and health effects. The oral LD50 values were >5000 mg/kg in rats. It was a mild skin and moderate ocular irritant and was not a skin sensitizer in animals. It was not mutagenic in Ames Salmonella, Escherichia c

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4

Morrison, Kelsey A., and Brian H. Clowers. "Non-contact detection of thiodiglycol vapors and associated degradation products using atmospheric flow tube mass spectrometry." Analyst 146, no. 10 (2021): 3263–72. http://dx.doi.org/10.1039/d0an01793k.

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5

Veriansyah, Bambang, Jae-Duck Kim, and Jong-Chol Lee. "Supercritical Water Oxidation of Thiodiglycol." Industrial & Engineering Chemistry Research 44, no. 24 (2005): 9014–19. http://dx.doi.org/10.1021/ie050482t.

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6

Lee, K. Patrick, and Herbert E. Allen. "Environmental transformation mechanisms of thiodiglycol." Environmental Toxicology and Chemistry 17, no. 9 (1998): 1720–26. http://dx.doi.org/10.1002/etc.5620170911.

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7

Houpt, John T., Lee C. B. Crouse, Richard A. Angerhofer, Glenn J. Leach, and Gunda Reddy. "Developmental Toxicity of Thiodiglycol in Sprague-Dawley Rats." International Journal of Toxicology 26, no. 4 (2007): 365–71. http://dx.doi.org/10.1080/10915810701461993.

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Thiodiglycol (TG), a hydrolysis product of sulfur mustard (HD), is a potential contaminant of soil and water at certain military sites. To establish developmental toxicity criteria for TG, an oral developmental toxicity study was conducted in Sprague-Dawley rats. Neat thiodiglycol (99.9 %) was administered orally to mated female rats from gestation days (GDs) 5 through 19. The day of positive mating was considered day 0. A pilot study was conducted with TG at dose levels 250, 500, 1000, 2000, or 5000 mg/kg to select suitable doses for the main study. In the main study, three groups of rats (25

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8

Popiel, Stanisław, Jakub Nawała, Daniel Dziedzic, Martin Söderström, and Paula Vanninen. "Determination of Mustard Gas Hydrolysis Products Thiodiglycol and Thiodiglycol Sulfoxide by Gas Chromatography-Tandem Mass Spectrometry after Trifluoroacetylation." Analytical Chemistry 86, no. 12 (2014): 5865–72. http://dx.doi.org/10.1021/ac500656g.

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9

Adão, Maria Helena, Benilde Saramago, and Anabela C. Fernandes. "Estimation of the Surface Tension Components of Thiodiglycol." Langmuir 14, no. 15 (1998): 4198–203. http://dx.doi.org/10.1021/la970878c.

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10

Singh, Beer, G. K. Prasad, M. V. S. Suryanarayana, and S. Banerjee. "The reaction of thiodiglycol on metal-impregnated carbon." Carbon 39, no. 14 (2001): 2131–42. http://dx.doi.org/10.1016/s0008-6223(01)00031-8.

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11

Lee, T. s., S. H. Chan, W. A. Weigand, and W. E. Bentley. "Biocatalytic Transformation of [(2-Hydroxyethyl)thio]acetic Acid and Thiodiglycolic Acid from Thiodiglycol by Alcaligenes xylosoxydans ssp. xylosoxydans (SH91)." Biotechnology Progress 16, no. 3 (2000): 363–67. http://dx.doi.org/10.1021/bp000044b.

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12

Bakirova, I. N., E. I. Galeeva, and A. Ya Samuilov. "The regularities of polyurethane foam chemical degradation with thiodiglycol." Russian Journal of General Chemistry 82, no. 9 (2012): 1546–51. http://dx.doi.org/10.1134/s1070363212090162.

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13

Angerhofer, Richard A., Mark W. Michie, Glenn J. Leach, Mark S. Johnson, and Gunda Reddy. "Oral Toxicity Evaluation of Thiodiglycol in Sprague-Dawley Rats." International Journal of Toxicology 33, no. 5 (2014): 393–402. http://dx.doi.org/10.1177/1091581814547541.

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Thiodiglycol (TDG) is the main product of sulfur mustard hydrolysis and is an environmental contaminant. Subacute and subchronic oral toxicity studies with TDG were conducted in Sprague-Dawley rats. Neat TDG was administered by gavage at doses of 157, 313, 625, 1250, 2500, 5000, and 9999 mg/kg/d, 5 days per week, for 14 days. In the 14-day study, decreased body weight and food consumption were observed at 5000 mg/kg/d. In the 90-day study, rats received neat TDG at doses of 50, 500, or 5000 mg/kg/d for 5 days per week. A fourth group served as a sham control. Individual body weight and food co

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14

Lachance, R., J. Paschkewitz, J. DiNaro, and J. W. Tester. "Thiodiglycol hydrolysis and oxidation in sub- and supercritical water." Journal of Supercritical Fluids 16, no. 2 (1999): 133–47. http://dx.doi.org/10.1016/s0896-8446(99)00025-x.

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15

Beck, Nicola V., Wendy A. Carrick, David B. Cooper, and Bob Muir. "Extraction of thiodiglycol from soil using pressurised liquid extraction." Journal of Chromatography A 907, no. 1-2 (2001): 221–27. http://dx.doi.org/10.1016/s0021-9673(00)01037-2.

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16

Riches, James, Robert W. Read, and Robin M. Black. "Analysis of the sulphur mustard metabolites thiodiglycol and thiodiglycol sulphoxide in urine using isotope-dilution gas chromatography–ion trap tandem mass spectrometry." Journal of Chromatography B 845, no. 1 (2007): 114–20. http://dx.doi.org/10.1016/j.jchromb.2006.07.065.

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17

Siasios, G., and ERT Tiekink. "Preparation, Spectroscopic Characterization and X-Ray Structure of [Dicyclohexylphosphinyl-N-methyl(thioformamide)]gold(I) Chloride: Au[Cy2P(O)C(S)N(H)Me]Cl." Australian Journal of Chemistry 48, no. 4 (1995): 757. http://dx.doi.org/10.1071/ch9950757.

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The reaction of [AuCl4]- with Cy2P(O)C(S)N(H)Me in the presence of thiodiglycol affords the air-stable adduct Au[Cy2P(O)C(S)N(H)Me] Cl which features a linear gold atom geometry defined by a chloride atom and a sulfur atom derived from a monodentate thioformamide ligand. The pale-green crystals are monoclinic, space group P21, with unit cell dimensions a 18.507(4), b 12.204(2), c 18.513(6) Ǻ, β 117.69(2)°, Z 8; the structure was refined to final R 0.042, 4106 reflections being used.

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18

Mohammadi, Abbas, and Mehdi Barikani. "Synthesis and characterization of superparamagnetic Fe3O4 nanoparticles coated with thiodiglycol." Materials Characterization 90 (April 2014): 88–93. http://dx.doi.org/10.1016/j.matchar.2014.01.021.

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19

Garcia-Ruiz, V., L. E. Martin-Otero, and A. Puyet. "Transformation of Thiodiglycol by Resting Cells of Alcaligenes xylosoxydans PGH10." Biotechnology Progress 18, no. 2 (2002): 252–56. http://dx.doi.org/10.1021/bp010190x.

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20

Alexeenko, L. P., and V. N. Orekhovich. "STABILIZATION OF THE FINAL PRODUCT IN THE SAKAGUCHI REACTION BY THIODIGLYCOL." International Journal of Protein Research 2, no. 1-4 (2009): 241–46. http://dx.doi.org/10.1111/j.1399-3011.1970.tb01681.x.

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21

Vahidi, Mehdi, and Mohammad Shokouhi. "Experimental solubility of carbon dioxide and hydrogen sulfide in 2,2′-thiodiglycol." Journal of Chemical Thermodynamics 133 (June 2019): 202–7. http://dx.doi.org/10.1016/j.jct.2019.02.024.

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22

Lee, Tsu-Shun, William A. Weigand, and William E. Bentley. "Observations of metabolite formation and variable yield in thiodiglycol biodegradation process." Applied Biochemistry and Biotechnology 63-65, no. 1 (1997): 743–57. http://dx.doi.org/10.1007/bf02920472.

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23

Galeeva, E. I., and I. N. Bakirova. "Chemical degradation of elastic foamed polyurethanes under the action of thiodiglycol." Russian Journal of Applied Chemistry 80, no. 10 (2007): 1741–44. http://dx.doi.org/10.1134/s1070427207100291.

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24

Kumar, Rakesh, Linxiang Wang, and Lina Zhang. "Structure and mechanical properties of soy protein materials plasticized by Thiodiglycol." Journal of Applied Polymer Science 111, no. 2 (2008): 970–77. http://dx.doi.org/10.1002/app.29136.

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25

Jakubowski, E. M., C. L. Woodard, M. M. Mershon, and T. W. Dolzine. "Quantification of thiodiglycol in urine by electron ionization gas chromatography—mass spectrometry." Journal of Chromatography B: Biomedical Sciences and Applications 528 (January 1990): 184–90. http://dx.doi.org/10.1016/s0378-4347(00)82374-9.

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26

Jakubowski, E. M., F. R. Sidell, R. A. Evans, et al. "QUANTIFICATION OF THIODIGLYCOL IN HUMAN URINE AFTER AN ACCIDENTAL SULFUR MUSTARD EXPOSURE." Toxicology Methods 10, no. 2 (2000): 143–50. http://dx.doi.org/10.1080/10517230050083375.

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27

T.-S., Lee, Chan S.-H., Weigand W., and Bentley W. "A metabolic model for thiodiglycol degradation: capacity constraint leads to byproduct accumulation." Bioprocess and Biosystems Engineering 24, no. 1 (2001): 33–38. http://dx.doi.org/10.1007/s004490100228.

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28

Irvine, David A., James P. Earley, Daniel P. Cassidy, and Steven P. Harvey. "Biodegradation of sulfur mustard hydrolysate in the sequencing batch reactor." Water Science and Technology 35, no. 1 (1997): 67–74. http://dx.doi.org/10.2166/wst.1997.0014.

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The United States Army is currently examining chemical neutralization followed by biodegradation for disposal of the chemical warfare agent sulfur mustard. The acidic hydrolysis of sulfur mustard (“mustard gas”, 2,2′-dichlorodiethyl sulfide), yields a detoxified and biodegradable product typically containing from 80 to 95% thiodiglycol. The hydrolyzed product was typically amended with 1,450 mg/L of ammonium chloride (NH4Cl), 280 mg/L of potassium phosphate monobasic (KH2PO4), and mineral salts and fed to aerobic Sequencing Batch Reactors (SBRs). The SBRs were operated with 3-5 hour aerated Fi

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29

Pham, Minh-Quan K., Steven P. Harvey, William A. Weigand, and William E. Bentley. "Reactor comparisons for the biodegradation of thiodiglycol, a product of mustard gas hydrolysis." Applied Biochemistry and Biotechnology 57-58, no. 1 (1996): 779–89. http://dx.doi.org/10.1007/bf02941758.

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30

Sines, Brian J., Eric W. Teather, Steven P. Harvey, and William A. Weigand. "Investigation of biological reactor designs for treatment of methanol and thiodiglycol waste streams." Applied Biochemistry and Biotechnology 45-46, no. 1 (1994): 881–95. http://dx.doi.org/10.1007/bf02941857.

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31

Dudley, Billy F., Alan A. Brimfield, and Gary W. Winston. "Oxidation of thiodiglycol (2,2?-thiobis-ethanol) by alcohol dehydrogenase: Comparison of human isoenzymes." Journal of Biochemical and Molecular Toxicology 14, no. 5 (2000): 244–51. http://dx.doi.org/10.1002/1099-0461(2000)14:5<244::aid-jbt3>3.0.co;2-4.

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32

Rawat, Bachan S., and Indar B. Gulati. "Studies on the extraction of aromatics with sulpholane and its combination with thiodiglycol." Journal of Chemical Technology and Biotechnology 31, no. 1 (2007): 25–32. http://dx.doi.org/10.1002/jctb.503310106.

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33

Leong, W. Y., E. H. Teo, C. H. Lim, and Y. L. Tan. "Efficiency of adsorbents for removal of organosulphur compounds in water." Water Science and Technology 38, no. 6 (1998): 139–46. http://dx.doi.org/10.2166/wst.1998.0246.

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Four carbonaceous adsorbents - Ambersorb XEN-563, Carbochem LQ830, Carbochem LQ1000 and Morganite FY5 - were evaluated in terms of adsorptive capacity for organosulphur compounds (thiodiglycol, ethyl 2-hydroxyethylsulphide, 1,4-thioxane, ethyl vinylsulphide) in water. The adsorption isotherms in single-solute and multi-component systems were fitted to Freundlich isotherms which give a first-cut estimation of the adsorptive capacities and breakthrough times. All four adsorbents demonstrated decreasing adsorptive capacity with increasing polarity of the adsorbates. Morganite FY5 and Ambersorb XE

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34

Wils, E. R. J., A. G. Hulst, A. L. de Jong, A. Verweij, and H. L. Borer. "Analysis of Thiodiglycol in Urine of Victims of an Alleged Attack with Mustard Gas." Journal of Analytical Toxicology 9, no. 6 (1985): 254–57. http://dx.doi.org/10.1093/jat/9.6.254.

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35

Koryagina, N. L., E. I. Savel’eva, N. S. Khlebnikova, and A. S. Radilov. "Determination of Thiodiglycol and Its Oxide in Biomedical Samples by Gas Chromatography–Mass Spectrometry." Journal of Analytical Chemistry 73, no. 13 (2018): 1209–16. http://dx.doi.org/10.1134/s1061934818130075.

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36

Bassi, Leila El, Naoya Shinzato, Tomoyuki Namihira, Hirosuke Oku, and Toru Matsui. "Biodegradation of thiodiglycol, a hydrolyzate of the chemical weapon Yperite, by benzothiophene-desulfurizing bacteria." Journal of Hazardous Materials 167, no. 1-3 (2009): 124–27. http://dx.doi.org/10.1016/j.jhazmat.2008.12.097.

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37

Doster, Douglas E., and Melodee Zentner. "Separation of thiodiglycol polyethers and related compounds by reversed-phase high-performance liquid chromatography." Journal of Chromatography A 461 (January 1989): 293–303. http://dx.doi.org/10.1016/s0021-9673(00)94296-1.

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38

Gómez-Caballero, Esther, Roberto Martínez-Álvarez, and Miguel A. Sierra. "Unexpected Reaction Pathways Leading to Thiodiglycol During the Degradation of Long-Chain Sulfur Mustards." Journal of Organic Chemistry 83, no. 20 (2018): 12432–39. http://dx.doi.org/10.1021/acs.joc.8b01670.

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39

JIANG, DAHONG, and MIN HUANG. "Selective synthesis of thiodiglycol dicarboxylic acid esters via p-TsOH/C-catalysed direct esterification." Journal of Chemical Sciences 124, no. 5 (2012): 1087–90. http://dx.doi.org/10.1007/s12039-012-0296-3.

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40

Huang, Xingqi, Ting Zhao, Chunxiao Yan, Yanren Jin, Yue Wu, and Lingxuan Zhang. "Decontamination performance of air filter paper impregnated with zirconium hydroxide on sulfur mustard." E3S Web of Conferences 267 (2021): 02063. http://dx.doi.org/10.1051/e3sconf/202126702063.

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Using zirconium hydroxide as a decontaminant, a kind of self-decontaminating air filter paper that can effectively degrade HD was successfully prepared by impregnating. The morphology and filtration efficiency of the filter paper before and after immersing were compared. The filtration efficiency increased linearly and slowly, with the regression equation: η=0.0001L+99.971. The liquid-solid decontamination reaction of HD on zirconium hydroxide powder and self-decontaminating filter paper conformed to the kinetic of quasi-first-order reaction and found that half-lives were 0.4 h and 2.1 h respe

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41

FARQUHARSON, STUART, and FRANK E. INSCORE. "A SERS-BASED ANALYZER FOR POINT AND CONTINUOUS WATER MONITORING OF CHEMICAL AGENTS AND THEIR HYDROLYSIS PRODUCTS." International Journal of High Speed Electronics and Systems 17, no. 04 (2007): 719–28. http://dx.doi.org/10.1142/s0129156407004928.

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Protection of military personnel and civilians from water supplies poisoned by chemical warfare agents (CWAs) requires an analyzer that has sufficient sensitivity (μg/L, ppb), specificity (differentiate the CWA from its hydrolysis products), and speed (less than 10 minutes) to be of value. In an effort to meet these requirements, we have been investigating the ability of surface-enhanced Raman spectroscopy (SERS) to detect cyanide and sulfur mustard in water. In our work, we have developed a novel SERS-active material that consists of a porous glass with trapped metal particles. Previously, we

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42

Sokołowski, Mieczysław S., Leszek Konopski, and Zlatko Fröbe. "Detection of Lewisite-2 in the Presence of Alcohols and/or Thiodiglycol in Aqueous Matrices." Phosphorus, Sulfur, and Silicon and the Related Elements 183, no. 7 (2008): 1630–40. http://dx.doi.org/10.1080/10426500701708137.

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43

Sathe, Manisha, Shruti Srivastava, S. Merwyn, G. S. Agarwal, and M. P. Kaushik. "Competitive immunochromatographic assay for the detection of thiodiglycol sulfoxide, a degradation product of sulfur mustard." Analyst 139, no. 20 (2014): 5118–26. http://dx.doi.org/10.1039/c4an00720d.

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44

Petetin, L., F. Berger, A. Chambaudet, and R. Planade. "Detection of thiodiglycol vapours using tin dioxide-based gas sensors: study of the interaction mechanism." Sensors and Actuators B: Chemical 78, no. 1-3 (2001): 166–73. http://dx.doi.org/10.1016/s0925-4005(01)00808-5.

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45

Dell’Amico, E., S. Bernasconi, L. Cavalca, C. Magni, B. Prinsi, and V. Andreoni. "New insights into the biodegradation of thiodiglycol, the hydrolysis product of Yperite (sulfur mustard gas)." Journal of Applied Microbiology 106, no. 4 (2009): 1111–21. http://dx.doi.org/10.1111/j.1365-2672.2008.04074.x.

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46

Capacio, Benedict R., J. Richard Smith, Michael T. DeLion, et al. "Monitoring Sulfur Mustard Exposure by Gas Chromatography-Mass Spectrometry Analysis of Thiodiglycol Cleaved from Blood Proteins." Journal of Analytical Toxicology 28, no. 5 (2004): 306–10. http://dx.doi.org/10.1093/jat/28.5.306.

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47

Ohsawa, Isaac, Mieko Kanamori-Kataoka, Kouichiro Tsuge, and Yasuo Seto. "Determination of thiodiglycol, a mustard gas hydrolysis product by gas chromatography–mass spectrometry after tert-butyldimethylsilylation." Journal of Chromatography A 1061, no. 2 (2004): 235–41. http://dx.doi.org/10.1016/j.chroma.2004.10.087.

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48

Kuvichkina, T. N., I. T. Ermakova, and A. N. Reshetilov. "Strain Alcaligenes xylosoxydans subsp. denitrificans TD2 as the basis of a biosensor for determination of thiodiglycol." Microbiology 81, no. 6 (2012): 750–51. http://dx.doi.org/10.1134/s0026261712060082.

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49

Wils, E. R. J., A. G. Hulst, and J. van Laar. "Analysis of Thiodiglycol in Urine of Victims of an Alleged Attack with Mustard Gas, Part II." Journal of Analytical Toxicology 12, no. 1 (1988): 15–19. http://dx.doi.org/10.1093/jat/12.1.15.

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50

Jiang, Dahong, and Min Huang. "ChemInform Abstract: Selective Synthesis of Thiodiglycol Dicarboxylic Acid Esters via p-TsOH/C-Catalyzed Direct Esterification." ChemInform 44, no. 8 (2013): no. http://dx.doi.org/10.1002/chin.201308043.

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