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Journal articles on the topic 'Time domain NMR'

Author: Grafiati

Published: 9 March 2023

Last updated: 31 July 2025

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1

Litvinov, Victor, and Yongfeng Men. "Time-domain NMR in polyolefin research." Polymer 256 (September 2022): 125205. http://dx.doi.org/10.1016/j.polymer.2022.125205.

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2

Todt, Harald, Wolfgang Burk, Gisela Guthausen, Andreas Guthausen, Andreas Kamlowski, and Dieter Schmalbein. "Quality control with time-domain NMR." European Journal of Lipid Science and Technology 103, no. 12 (2001): 835–40. http://dx.doi.org/10.1002/1438-9312(200112)103:12<835::aid-ejlt835>3.0.co;2-p.

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3

Bielecki, A., D. B. Zax, A. M. Thayer, J. M. Millar, and A. Pines. "Time Domain Zero Field NMR and NQR." Zeitschrift für Naturforschung A 41, no. 1-2 (1986): 440–44. http://dx.doi.org/10.1515/zna-1986-1-286.

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Field cycling methods are described for the time domain measurement of nuclear quadrupolar and dipolar spectra in zero applied field. Since these techniques do not involve irradiation in zero field, they offer significant advantages in terms of resolution, sensitivity at low frequency, and the accessible range of spin lattice relaxation times. Sample data are shown which illustrate the high sensitivity and resolution attainable. Comparison is made to other field cycling methods, and an outline of basic instrumental requirements is given.

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4

Webber, John Beausire Wyatt, and Pavel Demin. "Digitally Based Precision Time-Domain Spectrometer for NMR Relaxation and NMR Cryoporometry." Micro 3, no. 2 (2023): 404–33. http://dx.doi.org/10.3390/micro3020028.

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NMR Relaxation (NMRR) is an extremely useful quantitative technique for material science, particularly for studying polymers and porous materials. NMR Cryoporometry (NMRC) is a powerful technique for the measurement of pore-size distributions and total porosities. This paper discusses the use, capabilities and application of a newly developed compact NMR time-domain relaxation spectrometer suitable for studying both solid and liquid samples (Mk3 NMR Relaxation spectrometer & Cryoporometer, Lab-Tools (nano-science), Ramsgate, Kent, UK. (2019)). This highly compact precision NMR Spectrometer

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5

Pedroso, João, João Camporez, Luciana Belpiede, Rafaela Pinto, José Cipolla-Neto, and Jose Donato. "Evaluation of Hepatic Steatosis in Rodents by Time-Domain Nuclear Magnetic Resonance." Diagnostics 9, no. 4 (2019): 198. http://dx.doi.org/10.3390/diagnostics9040198.

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Devices that analyze body composition of rodents by time-domain nuclear magnetic resonance (TD-NMR) are becoming popular in research centers that study metabolism. Theoretically, TD-NMR devices can also evaluate lipid content in isolated tissues. However, the accuracy of TD-NMR to determine hepatic steatosis in the liver of small laboratory animals has not been evaluated in detail. We observed that TD-NMR was able to detect increased lipid content in the liver of rats consuming high-fat diet (HFD) for 12 weeks and in genetically obese (Lepob/ob and Leprdb/db) mice. The lipid content determined

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6

Le Botlan, D., F. Casseron, and F. Lantier. "Polymorphism of sugars studied by time domain NMR." Analusis 26, no. 5 (1998): 198–204. http://dx.doi.org/10.1051/analusis:1998135.

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7

Romano, Rocco, Maria Teresa Santini, and Pietro Luigi Indovina. "A Time-Domain Algorithm for NMR Spectral Normalization." Journal of Magnetic Resonance 146, no. 1 (2000): 89–99. http://dx.doi.org/10.1006/jmre.2000.2102.

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8

Nascimento, Paloma Andrade Martins, Paulo Lopes Barsanelli, Ana Paula Rebellato, Juliana Azevedo Lima Pallone, Luiz Alberto Colnago, and Fabíola Manhas Verbi Pereira. "Time-Domain Nuclear Magnetic Resonance (TD-NMR) and Chemometrics for Determination of Fat Content in Commercial Products of Milk Powder." Journal of AOAC INTERNATIONAL 100, no. 2 (2017): 330–34. http://dx.doi.org/10.5740/jaoacint.16-0408.

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Abstract This study shows the use of time-domain (TD)-NMR transverse relaxation (T2) data and chemometrics in the nondestructive determination of fat content for powdered food samples such as commercial dried milk products. Most proposed NMR spectroscopy methods for measuring fat content correlate free induction decay or echo intensities with the sample's mass. The need for the sample's mass limits the analytical frequency of NMR determination, because weighing the samples is an additional step in this procedure. Therefore, the method proposed here is based on a multivariate model of T2 decay,

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9

Rodrigues, Elton J. R., Pedro J. O. Sebastião, and Maria I. B. Tavares. "1H time domain NMR real time monitoring of polyacrylamide hydrogels synthesis." Polymer Testing 60 (July 2017): 396–404. http://dx.doi.org/10.1016/j.polymertesting.2017.04.028.

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10

Nikolskaya, Ekaterina, Petri Janhunen, Mikko Haapalainen, and Yrjö Hiltunen. "Solids Content of Black Liquor Measured by Online Time-Domain NMR." Applied Sciences 9, no. 10 (2019): 2169. http://dx.doi.org/10.3390/app9102169.

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Black liquor, a valuable by-product of the pulp production process, is used for the recovery of chemicals and serves as an energy source for the pulp mill. Before entering the recovery unit, black liquor runs through several stages of evaporation, wherein the solids content (SC) can be used to control the evaporation effectiveness. In the current study, the time-domain nuclear magnetic resonance (TD-NMR) technique was applied to determine the SC of black liquor. The TD-NMR system was modified for flowing samples, so that the black liquor could be pumped through the system, followed by the meas

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11

Rodrigues, Elton Jorge da Rocha, Maxwell de Paula Cavalcante, and Maria Inês Bruno Tavares. "Time domain NMR evaluation of poly(vinyl alcohol) xerogels." Polímeros 26, no. 3 (2016): 221–27. http://dx.doi.org/10.1590/0104-1428.2093.

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12

Witek, M., H. Peemoeller, J. Szymońska, and B. Blicharska. "Investigation of Starch Hydration by 2D Time Domain NMR." Acta Physica Polonica A 109, no. 3 (2006): 359–64. http://dx.doi.org/10.12693/aphyspola.109.359.

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13

Onuki, Yoshinori. "Usefulness of Time-Domain NMR in Characterizing Pharmaceutical Properties." Journal of the Society of Powder Technology, Japan 61, no. 10 (2024): 612–21. https://doi.org/10.4164/sptj.61.612.

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14

Coggins, Brian E., and Pei Zhou. "Sampling of the NMR time domain along concentric rings." Journal of Magnetic Resonance 184, no. 2 (2007): 207–21. http://dx.doi.org/10.1016/j.jmr.2006.10.002.

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15

Kazimierczuk, Krzysztof, Anna Zawadzka, and Wiktor Koźmiński. "Optimization of random time domain sampling in multidimensional NMR." Journal of Magnetic Resonance 192, no. 1 (2008): 123–30. http://dx.doi.org/10.1016/j.jmr.2008.02.003.

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16

Ghosh, Arindam, Yibing Wu, Yunfen He, and Thomas Szyperski. "Theory of mirrored time domain sampling for NMR spectroscopy." Journal of Magnetic Resonance 213, no. 1 (2011): 46–57. http://dx.doi.org/10.1016/j.jmr.2011.08.037.

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17

Rössler, Ernst. "Two-dimensional exchange NMR analysed in the time domain." Chemical Physics Letters 128, no. 3 (1986): 330–34. http://dx.doi.org/10.1016/0009-2614(86)80350-5.

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18

TODT, H., G. GUTHAUSEN, W. BURK, D. SCHMALBEIN, and A. KAMLOWSKI. "Water/moisture and fat analysis by time-domain NMR." Food Chemistry 96, no. 3 (2006): 436–40. http://dx.doi.org/10.1016/j.foodchem.2005.04.032.

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19

Rosen, M. E. "Selective Detection in NMR by Time-Domain Digital Filtering." Journal of Magnetic Resonance, Series A 107, no. 1 (1994): 119–25. http://dx.doi.org/10.1006/jmra.1994.1057.

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20

Xin, Gao, Zhou Fan, Fu Zongying, and Zhou Yongdong. "A study of pine resin in softwood by 1D and 2D time-domain NMR." Holzforschung 74, no. 9 (2020): 839–52. http://dx.doi.org/10.1515/hf-2019-0001.

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AbstractTime-domain nuclear magnetic resonance (TD-NMR) is widely used in the investigation of wood-water relationship. However, some ambiguities between the NMR signals and the components in wood remain unresolved, particularly the effect of pine resin on NMR signals. To clarify these ambiguities and increase the use of TD-NMR in wood research, different sample treatment methods were studied, including air-drying, low-temperature vacuum-drying, diethyl ether extraction and moisture isothermal adsorption. The corresponding one-dimensional (1D) T1, T2 and two-dimensional (2D) T1-T2 correlation

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21

Besghini, Denise, Michele Mauri, and Roberto Simonutti. "Time Domain NMR in Polymer Science: From the Laboratory to the Industry." Applied Sciences 9, no. 9 (2019): 1801. http://dx.doi.org/10.3390/app9091801.

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Highly controlled polymers and nanostructures are increasingly translated from the lab to the industry. Together with the industrialization of complex systems from renewable sources, a paradigm change in the processing of plastics and rubbers is underway, requiring a new generation of analytical tools. Here, we present the recent developments in time domain NMR (TD-NMR), starting with an introduction of the methods. Several examples illustrate the new take on traditional issues like the measurement of crosslink density in vulcanized rubber or the monitoring of crystallization kinetics, as well

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22

Webber, John Beausire Wyatt. "Updates on an Even More Compact Precision NMR Spectrometer and a Wider Range V-T Probe, for General Purpose NMR and for NMR Cryoporometric Nano- to Micro-Pore Measurements." Micro 4, no. 3 (2024): 509–29. http://dx.doi.org/10.3390/micro4030032.

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There is an increasing need for compact low-cost NMR apparatus that can be used on the laboratory bench and in the field. There are four main usage variants of usage: (a) time-domain apparatus, particularly for physical measurements; (b) frequency-domain apparatus, particularly for chemical analysis, (c) NMR Cryoporometry apparatus for measuring pore-size distributions; and (d) MRI apparatus for imaging. For all of these, variable temperature capability may be vital. We have developed compact low-cost apparatus targeted at these applications. We discuss a hand-held NMR Spectrometer, and three

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23

Li, Jingyu, and Erni Ma. "Characterization of Water in Wood by Time-Domain Nuclear Magnetic Resonance Spectroscopy (TD-NMR): A Review." Forests 12, no. 7 (2021): 886. http://dx.doi.org/10.3390/f12070886.

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This review summarizes the development of the experimental technique and analytical method for using TD-NMR to study wood-water interactions in recent years. We briefly introduce the general concept of TD-NMR and magnetic resonance imaging (MRI), and demonstrate their applications for characterizing the following aspects of wood-water interactions: water state, fiber saturation state, water distribution at the cellular scale, and water migration in wood. The aim of this review is to provide an overview of the utilizations and future research opportunities of TD-NMR in wood-water relations. It

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24

Pakoulev, Andrei V., Mark A. Rickard, Kent A. Meyer, et al. "Mixed Frequency/Time Domain Optical Analogues of Heteronuclear Multidimensional NMR." Journal of Physical Chemistry A 110, no. 10 (2006): 3352–55. http://dx.doi.org/10.1021/jp057339y.

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25

Schwartz, Leslie J. "A step-by-step picture of pulsed (time domain) NMR." Journal of Chemical Education 65, no. 9 (1988): 752. http://dx.doi.org/10.1021/ed065p752.

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26

Schwartz, Leslie. "A step by step picture of pulsed (time domain) NMR." Journal of Chemical Education 65, no. 11 (1988): 959. http://dx.doi.org/10.1021/ed065p959.

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27

Shao, Xiaolong, Wen Xu, Shuihong Xu, Changrui Xing, Chao Ding, and Qin Liu. "Time-Domain NMR Applied to Sitophilus zeamais Motschulsky/Wheat Detection." Journal of Agricultural and Food Chemistry 67, no. 45 (2019): 12565–75. http://dx.doi.org/10.1021/acs.jafc.9b04007.

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28

Digennaro, Frank S., and David Cowburn. "Parametric estimation of time-domain NMR signals using simulated annealing." Journal of Magnetic Resonance (1969) 96, no. 3 (1992): 582–88. http://dx.doi.org/10.1016/0022-2364(92)90343-6.

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29

Lemmerling, Philippe, Leentje Vanhamme, Rocco Romano, and Sabine Van Huffel. "A Subspace Time-Domain Algorithm for Automated NMR Spectral Normalization." Journal of Magnetic Resonance 157, no. 2 (2002): 190–99. http://dx.doi.org/10.1006/jmre.2002.2598.

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30

Rutledge, D. N., A. S. Barros, and F. Gaudard. "ANOVA and factor analysis applied to time domain NMR signals." Magnetic Resonance in Chemistry 35, no. 13 (1997): S13—S21. http://dx.doi.org/10.1002/(sici)1097-458x(199712)35:133.0.co;2-p.

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31

Segar, Jeffrey L., Kirthikaa Balapattabi, John J. Reho, Connie C. Grobe, Colin M. L. Burnett, and Justin L. Grobe. "Quantification of body fluid compartmentalization by combined time-domain nuclear magnetic resonance and bioimpedance spectroscopy." American Journal of Physiology-Regulatory, Integrative and Comparative Physiology 320, no. 1 (2021): R44—R54. http://dx.doi.org/10.1152/ajpregu.00227.2020.

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The measurement of fluid compartmentalization, or the distribution of fluid volume between extracellular (ECF) and intracellular (ICF) spaces, historically requires complicated, burdensome, and often terminal methodologies that do not permit repeated or longitudinal experiments. New technologies including time-domain nuclear magnetic resonance (TD-NMR)-based methods allow for highly accurate measurements of total body water (TBW) within minutes in a noninvasive manner, but do not permit dissection of ECF versus ICF reservoirs. In contrast, methods such as bioimpedance spectroscopy (BIS) allow

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32

Igreja Nascimento Mitre, Cirlei, Bruna Ferreira Gomes, Elaine Paris, Carlos Manuel Silva Lobo, Christina Roth, and Luiz Alberto Colnago. "Use of Time Domain Nuclear Magnetic Resonance Relaxometry to Monitor the Effect of Magnetic Field on the Copper Corrosion Rate in Real Time." Magnetochemistry 8, no. 4 (2022): 40. http://dx.doi.org/10.3390/magnetochemistry8040040.

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The corrosion of metals is a major problem of modern societies, demanding new technologies and studies to understand and minimize it. Here we evaluated the effect of a magnetic field (B) on the corrosion of copper in aqueous HCl solution under open circuit potential. The corrosion product, Cu2+, is a paramagnetic ion and its concentration in the solution was determined in real time in the corrosion cell by time-domain NMR relaxometry. The results show that the magnetic field (B = 0.23 T) of the time-domain NMR instrument reduces the corrosion rate by almost 50%, in comparison to when the corro

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33

Garcia, Rodrigo Henrique dos Santos, Jefferson Gonçalves Filgueiras, Luiz Alberto Colnago, and Eduardo Ribeiro de Azevedo. "Real-Time Monitoring Polymerization Reactions Using Dipolar Echoes in 1H Time Domain NMR at a Low Magnetic Field." Molecules 27, no. 2 (2022): 566. http://dx.doi.org/10.3390/molecules27020566.

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1H time domain nuclear magnetic resonance (1H TD-NMR) at a low magnetic field becomes a powerful technique for the structure and dynamics characterization of soft organic materials. This relies mostly on the method sensitivity to the 1H-1H magnetic dipolar couplings, which depend on the molecular orientation with respect to the applied magnetic field. On the other hand, the good sensitivity of the 1H detection makes it possible to monitor real time processes that modify the dipolar coupling as a result of changes in the molecular mobility. In this regard, the so-called dipolar echoes technique

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34

Slijkerman, W. F. J., W. J. Looyestijn, P. Hofstra, and J. P. Hofman. "Processing of Multi-Acquisition NMR Data." SPE Reservoir Evaluation & Engineering 3, no. 06 (2000): 492–97. http://dx.doi.org/10.2118/68408-pa.

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Summary Crucial issues in formation evaluation are the determination of porosity, permeability, hydrocarbon volumes, and net-to-gross ratio. Nuclear magnetic resonance (NMR) logging provides measurements that are directly related to these parameters. The NMR response of fluids contained in pores is governed by their T2- and T1-relaxation times, diffusion coefficient, and whether or not they wet the rock. In the case where fluids possess a sufficiently large contrast in these properties and NMR data have been acquired with suitably chosen acquisition parameters (i.e., wait times and/or inter-ec

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35

Webber, J. Beau W. "Some Applications of a Field Programmable Gate Array Based Time-Domain Spectrometer for NMR Relaxation and NMR Cryoporometry." Applied Sciences 10, no. 8 (2020): 2714. http://dx.doi.org/10.3390/app10082714.

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NMR Relaxation (NMRR) is an extremely useful quantitative technique for material science, particularly for studying polymers and porous materials. NMR Cryoporometry (NMRC) is a powerful technique for the measurement of pore-size distributions and total porosities. This paper discusses the use, capabilities and application of a newly available compact NMR time-domain relaxation spectrometer, the Lab-Tools Mk3 NMR Relaxometer & Cryoporometer [Lab-Tools (nano-science), Ramsgate, Kent, UK (2019)]. Being Field Programmable Gate Array based means that it is unusually compact, which makes it part

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36

Fritzsching, Keith J., Yizhuo Yang, Emily M. Pogue, Joseph B. Rayman, Eric R. Kandel, and Ann E. McDermott. "Micellar TIA1 with folded RNA binding domains as a model for reversible stress granule formation." Proceedings of the National Academy of Sciences 117, no. 50 (2020): 31832–37. http://dx.doi.org/10.1073/pnas.2007423117.

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TIA1, a protein critical for eukaryotic stress response and stress granule formation, is structurally characterized in full-length form. TIA1 contains three RNA recognition motifs (RRMs) and a C-terminal low-complexity domain, sometimes referred to as a “prion-related domain” or associated with amyloid formation. Under mild conditions, full-length (fl) mouse TIA1 spontaneously oligomerizes to form a metastable colloid-like suspension. RRM2 and RRM3, known to be critical for function, are folded similarly in excised domains and this oligomeric form of apo fl TIA1, based on NMR chemical shifts.

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37

Declerck, Arnout, Veronique Nelis, Sabine Danthine, Koen Dewettinck, and Paul Van der Meeren. "Characterisation of Fat Crystal Polymorphism in Cocoa Butter by Time-Domain NMR and DSC Deconvolution." Foods 10, no. 3 (2021): 520. http://dx.doi.org/10.3390/foods10030520.

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The polymorphic state of edible fats is an important quality parameter in fat research as well as in industrial applications. Nowadays, X-ray diffraction (XRD) is the most commonly used method to determine the polymorphic state. However, quantification of the different polymorphic forms present in a sample is not straightforward. Differential Scanning Calorimetry (DSC) is another method which provides information about fat crystallization processes: the different peaks in the DSC spectrum can be coupled to the melting/crystallisation of certain polymorphs. During the last decade, nuclear magne

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38

Almeida, Luisa Souza, Jaqueline Carneiro, and Luiz Alberto Colnago. "Time domain NMR for polymorphism characterization: Current status and future perspectives." International Journal of Pharmaceutics 669 (January 2025): 125027. https://doi.org/10.1016/j.ijpharm.2024.125027.

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39

Nikolskaya, Ekaterina, and Yrjö Hiltunen. "Time-Domain NMR in Characterization of Liquid Fuels: A Mini-Review." Energy & Fuels 34, no. 7 (2020): 7929–34. http://dx.doi.org/10.1021/acs.energyfuels.0c01464.

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40

Clayden, N. J., R. J. Lehnert, and S. Turnock. "Factor analysis of time domain NMR data: crystallinity of poly(tetrafluoroethene)." Analytica Chimica Acta 344, no. 3 (1997): 261–69. http://dx.doi.org/10.1016/s0003-2670(97)00058-5.

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41

Clayden, N. J. "Factor analysis of simulated time domain NMR data for semicrystalline polymers." Analytica Chimica Acta 356, no. 1 (1997): 27–33. http://dx.doi.org/10.1016/s0003-2670(97)00517-5.

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42

Rutledge, D. N. "Characterisation of water in agro-food products by time domain-NMR." Food Control 12, no. 7 (2001): 437–45. http://dx.doi.org/10.1016/s0956-7135(01)00060-3.

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43

Nordon, Alison, Paul J. Gemperline, Colin A. McGill, and David Littlejohn. "Quantitative Analysis of Low-Field NMR Signals in the Time Domain." Analytical Chemistry 73, no. 17 (2001): 4286–94. http://dx.doi.org/10.1021/ac0102866.

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44

Gesmar, Henrik, and Jens J. Led. "Spectral estimation of complex time-domain NMR signals by linear prediction." Journal of Magnetic Resonance (1969) 76, no. 1 (1988): 183–92. http://dx.doi.org/10.1016/0022-2364(88)90215-6.

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45

van Duynhoven, John, Isabelle Dubourg, Gert-Jan Goudappel, and Eli Roijers. "Determination of MG and TG phase composition by time-domain NMR." Journal of the American Oil Chemists' Society 79, no. 4 (2002): 383–88. http://dx.doi.org/10.1007/s11746-002-0493-7.

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46

Labbé, Nicole, Bernard De Jéso, Jean-Claude Lartigue, Gérard Daudé, Michel Pétraud, and Max Ratier. "Time-domain 1H NMR characterization of the liquid phase in greenwood." Holzforschung 60, no. 3 (2006): 265–70. http://dx.doi.org/10.1515/hf.2006.043.

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Abstract The time domain of 1H NMR spectroscopy allows straightforward editing of the T 2 relaxation profiles in maritime pine wood. A new method from the Carr-Purcell-Meiboom-Gill sequence is proposed to measure the amount and distribution of water in wood, as well as the location of major dissolved organic materials. A general calibration model giving reliable and precise identification of these parameters is described. The method presented for editing T 2 relaxation profiles (obtained by the Contin program) may be helpful in solving practical drying and gluing problems in the wood industry.

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47

Oleskevich, D. A., N. Ghahramany, W. P. Weglarz, and H. Peemoeller. "Interfacial Spin–Spin Coupling in Wood by 2D Time-Domain NMR." Journal of Magnetic Resonance, Series B 113, no. 1 (1996): 1–8. http://dx.doi.org/10.1006/jmrb.1996.0148.

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48

Geil, B., F. Fujara, and H. Sillescu. "2H NMR Time Domain Analysis of Ultraslow Reorientations in Supercooled Liquids." Journal of Magnetic Resonance 130, no. 1 (1998): 18–26. http://dx.doi.org/10.1006/jmre.1997.1284.

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49

Linke, Christina, Gisela Guthausen, Eckhard Flöter, and Stephan Drusch. "Solid Fat Content Determination of Dispersed Lipids by Time-Domain NMR." European Journal of Lipid Science and Technology 120, no. 4 (2018): 1700132. http://dx.doi.org/10.1002/ejlt.201700132.

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50

Gomes, Bruna, Carlos Lobo, and Luiz Colnago. "Monitoring Electrochemical Reactions in Situ with Low Field NMR: A Mini-Review." Applied Sciences 9, no. 3 (2019): 498. http://dx.doi.org/10.3390/app9030498.

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The number of applications of time domain NMR using low-field spectrometers in research and development has been steadily increasing in recent years with applications ranging from quality control of industrial products to the study of physical and chemical properties of a wide array of solid and liquid samples to, most recently, electrochemical studies. In this mini-review we summarize the progress that has been achieved in the coupling between time domain NMR (using low-field spectrometers) and electrochemistry and how the challenges that this coupling poses have been overcome over the years.

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