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Dissertations / Theses on the topic 'Transition metal complexes - Spectra'

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Published: 4 June 2021

Last updated: 25 January 2023

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1

Wardell, E. M. "EXAFS studies on transition metal complexes." Thesis, University of Manchester, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.377729.

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2

Cartwright, P. S. "Synthetic and spectroscopic studies of transition metal complexes." Thesis, Bucks New University, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.380302.

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3

Greaves, Sarah Jennifer. "Transition metal O, O'-complexes : preparation, Raman spectra and electrochemistry." Thesis, Imperial College London, 1989. http://hdl.handle.net/10044/1/47454.

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4

Xie, Jin, and 解錦. "Synthesis, structures and spectroscopic properties of primary and secondary phosphine complexes of iron, ruthenium and osmiumporphyrins." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2007. http://hub.hku.hk/bib/B39556876.

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5

Dyer, Hellen Elizabeth. "New lanthanide complexes as polymerisation catalysts." Thesis, University of Oxford, 2009. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.560913.

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This Thesis describes the synthesis and characterisation of a series ofbisphenolate supported samarium borohydride, amide and zwitterionic rare earth complexes and their ability to effect the ring opening polymerisation (ROP) of cyclic esters and methylmethacrylate (MMA). Chapter 1 introduces ROP from both an industrial and an academic perspective and describes in detail the research in this area, with emphasis on rare earth initiators. The lanthanide elements and the bisphenolate ligand are also introduced. Chapter 2 describes the synthesis and characterisation ofbisphenolate supported samari

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6

Higgitt, Catherine L. "NMR studies of arene transition metal complexes : structure, dynamics and reactivity." Thesis, University of York, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.298537.

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7

Hedley, Gordon J. "Ultrafast photophysics of iridium complexes." Thesis, University of St Andrews, 2010. http://hdl.handle.net/10023/1981.

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This thesis presents ultrafast photophysical measurements on a number of phosphorescent iridium complexes and establishes relationships between the relaxation rates and the vibrational properties of the material. When ultrafast luminescence is measured on the peak of the phosphorescence spectrum and on its red-side, 230 fs and 3 ps decay time constants were observed in all materials studied, and this was attributed to population redistribution amongst the three electronic substates of the lowest triplet metal-ligand charge transfer (MLCT) state. The observation of luminescence at higher values

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8

Wong, Chun-yuen, and 黃駿弦. "Ruthenium-carbon bonding interaction synthesis and spectroscopic studies of ruthenium-acetylide, -carbene, -vinylidene and -allenylidene complexes." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2004. http://hub.hku.hk/bib/B31040858.

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9

Karunatilaka, Chandana. "Rotational Spectroscopy and Structures of Organometallic Compounds." Diss., The University of Arizona, 2007. http://hdl.handle.net/10150/193621.

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High-resolution pulsed beam Fourier Transform Microwave Spectroscopy (PBFTMS) technique has been used to investigate the rotational spectra, molecular structures and electronic charge distribution of organometallic and organic molecules. The thesis reports high-resolution rotational spectral findings for nine different asymmetric-top molecules in the singlet electronic ground state including: Cyclopentadienyltungstentricarbonylhydride, Bis-(cyclopentadienyl)tungstendihydride, Tetracarbonylethyleneosmium, two substituted Ferrocenes and an organic keto-enol tautomeric system, Z-2-Hydroxypyridin

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10

Essex, Sarah Jane. "Spectral intensities in planar copper(II) complexes." Thesis, University of Cambridge, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.239622.

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11

Knight, Cheryl Lynn. "Application of IR and NMR spectroscopy to certain complexes of 8-hydroxyquinoline and 8-aminoquinoline." Master's thesis, University of Cape Town, 1987. http://hdl.handle.net/11427/22001.

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The IR spectra of twenty-one transition metal complexes of 8-hydroxyquinoline over the range 700 - 50 cm⁻¹ are discussed in relation to their known or inferred structures. The complexes are of three types: (a) the bis(aquo) complexes of the first row transition metal(II) ions, [M(ox)₂(H₂O)₂] (M =Mn, Fe, Co, Ni, Cu, Zn); (b) the corresponding anhydrous complexes, [M(ox)₂]n (M=Mn, Co, Ni, Cu, Zn) and (c) the complexes of the metal(III) ions, [M(ox)₃] (M = Sc, V, Cr, Mn, Fe, Co, Ga, Rh and In). Deuterated 8-hydroxyquinoline was. synthesized by the Skraup synthesis and has been used to assist in t

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12

陳容芳 and Yung-fong Yvonne Cheng. "Resonance raman investigation of metal to ligand charge transfer transitions in selected inorganic complexes." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2001. http://hub.hku.hk/bib/B31224143.

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13

Xiao, Lan. "Etude physico-chimique de la complexation de divers ions metalliques (cu**(2+), ni**(2+) et co**(2+)) avec des dipeptides l-l contenant des chaines laterales non-coordinantes." Paris 7, 1988. http://www.theses.fr/1988PA077170.

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Stabilite des complexes en fonction de l'interaction des chaines laterales du dipeptide et le solvant. Mesures potentiometriques calorimetriques, caracterisation spectrometrique et structure moleculaire

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14

Tahiri, Mohamed. "Phtalocyanines de fer(i) et de fer(0) : synthese, structure et reactivite." Université Louis Pasteur (Strasbourg) (1971-2008), 1987. http://www.theses.fr/1987STR13043.

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Synthese et caracterisation d'une serie de complexes monoreduits de phtalocyanine de fer de type (fe pc r::(8))**(-) ou r=och::(3), ch::(3), h, cl et cn. On donne les structures par rx de composes monoanioniques et dianionique fe pc**(-) et fe pc**(2-). Proprietes chimiques de fe pc**(2-). De tels especes peuvent etre des modeles d'intermediaires formes dans la reaction de la phenylhydrazine sur la metmyoglobine ou dans le metabolisme de substrats suicides par cytochrome p450

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15

Faulmann, Christophe. "Conducteurs derives de metaux de transition : complexes moleculaires, polymeres, oxydes de cuivre." Toulouse 3, 1988. http://www.theses.fr/1988TOU30160.

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16

Ries, Michel. "Synthese et reactivite de clusters heterometalliques contenant le ligand assembleur ph : :(2)pch::(2)pph::(2)." Université Louis Pasteur (Strasbourg) (1971-2008), 1987. http://www.theses.fr/1987STR13208.

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17

Baillie, Gordon M. "Preparation, spectral and magnetic studies on some first row transition metal complexes and an investigation into their performance as colourants for poly(vinyl chloride)." Thesis, Edinburgh Napier University, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.385997.

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18

Arliguie, Thérèse. "Complexes du ruthenium hydrures et derives de l'hydrogene moleculaire : reactions de deshydrogenation inter et intramoleculaires." Toulouse 3, 1988. http://www.theses.fr/1988TOU30111.

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On etudie la reactivite chimique de complexes polyhudrures de ruthenium apres activation thermique ou photochimique. Certains complexes pentamethylcyclopentadienyl sont egalement prepares et etudies en spectroscopie rmn du proton

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19

Bouet, Gilles. "Etude structurale et analytique de complexes d'halogénures d'éléments 3D : mx::(2) (M = co,ni,cu; X = cl,br) et de diverses aldoximes furanniques." Angers, 1987. http://www.theses.fr/1987ANGE0009.

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Vingt-quatre nouveaux complexes d'halogénures de métaux 3 D : mx::(2) (m = co,ni,cu; x = cl,br) sont préparés et caractérisés. Leurs structures sont déterminées par diffraction des rayons X pour deux des composés et, à partir de celles-ci, pour l'ensemble des complexes grâce à la spectroscopie infrarouge et à la spectroscopie électronique. Le calcul des constantes de stabilité et des paramètres thermodynamiques correspondants par titrimétrie thermométrique est décrit.

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20

Edel, André. "Photochimie d'un complexe du cuivre (i) : etude dynamique et structurale par rmn de catenands et catenates." Université Louis Pasteur (Strasbourg) (1971-2008), 1987. http://www.theses.fr/1987STR13016.

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L'etude des proprietes photo-physiques et -chimiques du complexe cu(diphenylphenan)::(2)**(+) conduit au premier exemple d'un complexe de cu (i) realisant la photoreduction de l'eau sous irradiation en lumiere visible. Etude rmn de cu (cat-30)**(+) et cu (cat-27)**(+) montrant qu'ils presentent des proprietes topographiques identiques

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21

Gomes, de Lima Bernardes Miriam. "Réactivité de complexes organométalliques mono- et dinucléaires : synthèse de thiolato-composés du molybdène, du tungstène et du cobalt : étude de la formation de liaisons c-c dans la sphère de coordination du métal." Brest, 1986. http://www.theses.fr/1986BRES2008.

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Caracterisation des complexes ((c::(5)h::(5))(co)::(2) lwc(cf::(3)) = c(cf::(3))h) et (c::(5)h::(5))(co) lwc(o)c(cf::(3)) = c(cf::(3))h) (l=co,pr::(3),p(or)::(3)) synthese de complexes dinucleaires de mo et w. L'addition oxydante de dialkylsulfure a des derives biportes de mo(ii) et w(ii) a donne lieu a la formation de complexes thiolato triportes ((c::(5)h::(5))(co)m(mu -sr)::(3)m(co)(c::(5)h::(5)))tx**(-)

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22

Preuß, Andrea [Verfasser], Heinrich [Gutachter] Lang, Heinrich [Akademischer Betreuer] Lang, and Klaus-Dieter [Gutachter] Stöwe. "Synthesis and Characterization of Transition Metal Complexes as well as their Application in the Formation of Metal-based Materials and the Investigation of their (Spectro)Electrochemical Behavior / Andrea Preuß ; Gutachter: Heinrich Lang, Klaus-Dieter Stöwe ; Betreuer: Heinrich Lang." Chemnitz : Technische Universität Chemnitz, 2020. http://d-nb.info/1219665533/34.

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23

PETIT, JEAN-FRANCOIS. "Les squarates de lanthanoides : synthese, structure, comportement thermique et proprietes optiques, synthese et structure de dithiosquarates bimetalliques de nickel (ii) et de cerium (iii)." Toulouse 3, 1988. http://www.theses.fr/1988TOU30133.

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Cinq familles de composes isotypes ont ete identifiees en milieu aqueux. Etude radiocristallographique, comportement thermique dans differentes atmospheres, preparation du squarate de cerium anhydre et de trois nouvelles phases hydratees. Etude spectrometrique du derive de l'europium

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24

Ben, Nasr Chérif. "Complexation du nickel (II) et des lanthanides (III) par des phosphoramides bidentes : Application à l'extraction liquide-liquide." Nancy 1, 1986. http://www.theses.fr/1986NAN10032.

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Les composés de type (NME::(2))::(2)P(O)NRP(O)(NME::(2))::(2) complexent fortement lésions métalliques et peuvent être utilisés en tant qu'agents extractaires dans l'extraction liquide liquide. Synthèse systématique des complexes lanthanides-NDA. L'étude RMN a permis également de trier les contributions de contact et de pseudo-contact au déplacement paramagnétique des protons et des phosphores du ligand engagé dans le complexe et d'obtenir des informations concernant la structure des complexes en solution. Enfin, le problème de l'extraction liquide-liquide des lanthanides par le NIPA dans le n

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25

Barron, Andrew Ross. "Transition metal aluminohydride complexes." Thesis, Imperial College London, 1986. http://hdl.handle.net/10044/1/37935.

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26

Jasim, Naseralla. "Transition metal bifluoride complexes." Thesis, University of York, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.323538.

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27

Veighy, Clifford Robert. "Novel cyclopentadienyl transition metal complexes." Thesis, University of Southampton, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.327366.

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28

Zard, P. W. "Transition metal complexes with pyrimidinethiones." Thesis, Imperial College London, 1988. http://hdl.handle.net/10044/1/47322.

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29

Johnson, Donald Martin. "Cyanoscorpionates and Transition Metal Complexes." Digital Commons @ East Tennessee State University, 2010. https://dc.etsu.edu/etd/1725.

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The new dihydrobis(4-cyano-3-tert-butylpyrazolylborate) ligand has been synthesized. Isolated crystals of the thallium complex were collected and structurally characterized by X-ray diffraction. Transition metal complexes of the ligand are currently under investigation.

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30

Furenlid, Lars Ragnar. "X-ray absorption studies of metal-imidazole complexes." Diss., Georgia Institute of Technology, 1988. http://hdl.handle.net/1853/30042.

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31

Holder, Alan John. "Studies on transition metal macrocyclic complexes." Thesis, University of Edinburgh, 1987. http://hdl.handle.net/1842/10961.

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32

Cheung, Wai Man. "Transition metal complexes with dichalcogenoimidodiphosphinate ligands /." View abstract or full-text, 2007. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202007%20CHEUNG.

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33

Redfern, C. M. "Electronic structure of transition metal complexes." Thesis, University of Oxford, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.235094.

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34

Mobbs, B. E. "Arene transition metal complexes in synthesis." Thesis, University of Oxford, 1985. http://ora.ox.ac.uk/objects/uuid:4c7030d4-297e-4af8-a622-d5b4963fc0a3.

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This thesis deals with the applications of organopalladium and organochromium chemistry to the functionalisation of the benzopyran ring system, at a variety of oxidation levels. Section I demonstrates the functionalisation of 3-, 6-, and 8-bromochromones via palladium (0) insertion into the C-Br bond. The resultant arylpalladium species are shown to undergo addition to the least substituted end of a variety of olefins including methyl acrylate, acrylonitrile and styrene. Subsequent palladium-hydride elimination leads to overall palladium catalysed vinylation of the chromone and the synthesis o

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35

Bridgewater, Brian Michael. "Sterically hindered chiral transition metal complexes." Thesis, Durham University, 1998. http://etheses.dur.ac.uk/5022/.

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This thesis describes the synthesis, characterization and study of a series of organometallic compounds which all contain the same new ligand, l-phenyl-3-methyl-4,5,6,7-tetrahydroindenyl. The ligand forms a chiral complex once coordinated, and is relatively bulky when compared with ligands such as cyclopentadienyl or 4,5,6,7-tetrahydroindenyl.Chapter one of this thesis introduces cyclopentadienyl ligand chirality, cyclopentadienyl metal complex chirality and sterically demanding cyclopentadienyl systems. The synthesis and chemistry of tetrahydroindenes and some applications of chiral cyclopent

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36

Blunden, Ralph Benedict. "Novel early transition metal cyclopropenyl complexes." Thesis, University of Sussex, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.360552.

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37

Atkins, Andrew J. "Studies on transition metal macrocyclic complexes." Thesis, University of Edinburgh, 1993. http://hdl.handle.net/1842/11664.

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38

Usher, Peter I. "Electrochemical studies of transition metal complexes." Thesis, University of Edinburgh, 1995. http://hdl.handle.net/1842/11492.

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This thesis is concerned with the spectroscopic, electrochemical and spectroelectrochemical investigation of a range of transition metal species, all containing the ligand 2,2'-bipyridine (bpy). All the complexes studied exhibit rich electrochemistry and electronic absorption spectra. Chapter one details the electrochemical and spectroelectrochemical techniques used in this work, and presents a brief overview of the reasons why we study transition metal complexes in this manner. Chapter two is concerned with the solvent dependent behaviour of complexes of the form [M(bpy)<SUB>2</SUB>(CN)<SUB>2

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39

Reid, Gillian. "Studies on transition metal macrocyclic complexes." Thesis, University of Edinburgh, 1989. http://hdl.handle.net/1842/12853.

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40

Cooper, Glyn. "Photoelectron spectroscopy of transition metal complexes." Thesis, University of Oxford, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.670392.

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41

Chilton, Nicholas Frederick. "Magnetic anisotropy of transition metal complexes." Thesis, University of Manchester, 2015. https://www.research.manchester.ac.uk/portal/en/theses/magnetic-anisotropy-of-transition-metal-complexes(64b34057-8a7a-44db-a89a-22a233fdefb5).html.

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The study of magnetic anisotropy in molecular systems permeates the physical sciences and finds application in areas as diverse as biomedical imaging and quantum information processing. The ability to understand and subsequently to design improved agents requires a detailed knowledge of their fundamental operation. This work outlines the background theory of the electronic structure of magnetic molecules and provides examples, for elements across the Periodic Table, of how it may be employed to aid in the understanding of magnetically anisotropic molecules. The magnetic anisotropies of a serie

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42

Nazir, Ruqia. "Chemistry of transition metal fluoride complexes." Thesis, University of York, 2012. http://etheses.whiterose.ac.uk/2660/.

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Metal fluoride complexes that are extremely sensitive to air and water have been characterized by liquid injection field desorption/ionization (LIFDI) mass spectrometry. Dilute solutions of fluoride complexes of nickel, rhodium, titanium, zirconium, hafnium and ruthenium in toluene and tetrahydrofuran were examined by LIFDI methods on a time-of-flight mass spectrometer. All the spectra of nickel, titanium zirconium and hafnium complexes exhibited the molecular ion as base peak. The ruthenium and rhodium complexes showed loss of HF from the molecular ion as base peaks but the molecular ions wer

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43

Humphrey, Paul Andrew. "A study of transition metal complexes /." Title page, contents and summary only, 1990. http://web4.library.adelaide.edu.au/theses/09PH/09phh9262.pdf.

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44

葉漢基 and Hon-kay John Yip. "Spectroscopy, and photophysical and photochemical properties of metal-metal bonded complexes." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1992. http://hub.hku.hk/bib/B31233338.

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45

Olson, Michael David. "Pyrazolyl based ligands in transition metal complexes." Thesis, University of British Columbia, 1989. http://hdl.handle.net/2429/27610.

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Several uninegative/ multidentate pyrazolyl based ligands were synthesized [eg. HBPZ₃₋, HBpz”₃₋, MeGapz₃₋/ MeGapz” ₃₋, H2BpZ₂₋/ Me2Bpz₂₋/ Me2GapZ₂₋/ Me2Gapz"₂₋/ Me₂Gapz(OCH₂CH₂NH₂)⁻Me₂Gapz(OCH₂CH₂CH=CH₂)⁻ ; pz pyrazolyl/ pz" = 3, 5 dimethylpyrazolyl]. These ligands were reacted with the sterically hindered metal complex, HBpz*₃MCl (M = Co, Ni; pz* = 3-iPr-4-Br-pyrazolyl) and the mixed-ligand transition metal complexes of general formulae, HBpz*₃ML, were isolated. The X-ray crystal structure of one such complex, HBpz*₃Nipz"₃BH was determined showing a near octahedral arrangement of ligands abo

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46

Hyde, Timothy I. "Studies on transition metal tetraaza macrocyclic complexes." Thesis, University of Edinburgh, 1987. http://hdl.handle.net/1842/28273.

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47

Skinner, Michael E. G. "Transition metal complexes of diamide-diamine ligands." Thesis, University of Oxford, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.365390.

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48

Warner, P. "Asymmetric synthesis via transition metal acyl complexes." Thesis, University of Oxford, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.355823.

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49

Hyde, T. I. "Studies of transition metal tetraaza macrocyclic complexes." Thesis, University of Edinburgh, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.652780.

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A macrocyclic ligand can be regarded as a protecting group for a metal centre, controlling its stereochemical, electronic and redox properties. These properties were examined byulilizing ten 14 membered neutral macrocycles with varying ring substituents and donor groups. A study into the insertion of the platinum metals into four tetraaza 2, 6-pyridyl macrocycles with varying carbon and nitrogen alkylation was instituted. The single crystal X-ray structures of Pd(II), Rh(III), Ru(II) and Ir(III) metal inserted complexes were determined including the species [RuL<SUP>3</SUP>(CO)Cl]<SUP>+</SUP>

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50

Ball, R. J. "Redox-geometry relationships in transition metal complexes." Thesis, Queen's University Belfast, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.273126.

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