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Journal articles on the topic 'Trimethylsilane'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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1

Vuong, Thi. "(Trifluoromethyl)trimethylsilane." Synlett 23, no. 09 (2012): 1409–10. http://dx.doi.org/10.1055/s-0031-1290686.

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2

Krishnamoorthy, Sankarganesh, and G. Prakash. "Silicon-Based Reagents for Difluoromethylation and Difluoromethylenation Reactions." Synthesis 49, no. 15 (2017): 3394–406. http://dx.doi.org/10.1055/s-0036-1588489.

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There have been significant developments in the area of perfluoroalkyl group transfer using silicon reagents, specifically in nucleophilic trifluoromethylation. The mild and versatile activation conditions bestow significant synthetic prowess to the silicon reagents in the area of fluoroalkylations. Owing to the importance of difluoromethylene (CF2) containing compounds in pharmaceuticals, materials, and agrochemicals, several CF2 group transfer methods using related silicon reagents have been developed and studied in detail. This review summarizes the recent developments and trends in this a

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3

Wang, Fei, Lingchun Li, Chuanfa Ni, and Jinbo Hu. "Deoxygenative gem-difluoroolefination of carbonyl compounds with (chlorodifluoromethyl)trimethylsilane and triphenylphosphine." Beilstein Journal of Organic Chemistry 10 (February 6, 2014): 344–51. http://dx.doi.org/10.3762/bjoc.10.32.

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Background: 1,1-Difluoroalkenes cannot only be used as valuable precursors for organic synthesis, but also act as bioisosteres for enzyme inhibitors. Among various methods for their preparation, the carbonyl olefination with difluoromethylene phosphonium ylide represents one of the most straightforward methods. Results: The combination of (chlorodifluoromethyl)trimethylsilane (TMSCF2Cl) and triphenylphosphine (PPh3) can be used for the synthesis of gem-difluoroolefins from carbonyl compounds. Comparative experiments demonstrate that TMSCF2Cl is superior to (bromodifluoromethyl)trimethylsilane

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4

Sakurai, Hideki, Soichiro Kyushin та Yasuhiro Nakadaira. "(2-Cyanoallyl)trimethylsilane and (2-Cyanoethyl)trimethylsilane. Unique σπ Captodative Systems". Chemistry Letters 16, № 2 (1987): 297–300. http://dx.doi.org/10.1246/cl.1987.297.

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5

YOSHIDA, Yasuo. "((1-ethoxycyclopropyl)oxy) trimethylsilane." Journal of Synthetic Organic Chemistry, Japan 57, no. 12 (1999): 1116–17. http://dx.doi.org/10.5059/yukigoseikyokaishi.57.1116.

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6

Werstiuk, Nick Henry, and Wojciech Sokol. "Density functional theory computational study on Diels–Alder reactions of cyclopentadiene with selected vinylsilanes and methylenecyclopropane." Canadian Journal of Chemistry 89, no. 3 (2011): 409–14. http://dx.doi.org/10.1139/v10-167.

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Aimed at predicting relative reactivities, density functional theory (DFT) calculations were carried out on a series of Diels–Alder reactions involving silylvinyl derivatives reacting with cyclopentadiene as part of a synthetic research project. Using three reactions for which experimental rate data are available to calibrate our calculations, we computationally pinpointed the best synthetic route to bicyclo[2.2.1]hept-5-ene-2,2-diylbis(trimethylsilane) (1). The synthesis begins with the Diels–Alder reaction of cyclopentadiene (2) with commercially available (1-bromovinyl)trimethylsilane (6).

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7

Fraser, Stewart, and Simon Parsons. "(Chloromethyl)trimethylsilane at 160 K." Acta Crystallographica Section E Structure Reports Online 60, no. 4 (2004): o564—o565. http://dx.doi.org/10.1107/s1600536804005276.

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8

Trifonov, Alexey L., Artem A. Zemtsov, Vitalij V. Levin, Marina I. Struchkova, and Alexander D. Dilman. "Nucleophilic Difluoromethylation Using (Bromodifluoromethyl)trimethylsilane." Organic Letters 18, no. 14 (2016): 3458–61. http://dx.doi.org/10.1021/acs.orglett.6b01641.

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9

Jiao, C. Q., A. Garscadden, and P. D. Haaland. "Ionization of trimethylsilane, (CH3)3SiH." International Journal of Mass Spectrometry 184, no. 1 (1999): 83–88. http://dx.doi.org/10.1016/s1387-3806(98)14270-7.

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10

Yasuda, Hirotsugu, and Qingsong Yu. "Cathode glow polymerization of trimethylsilane." Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films 22, no. 3 (2004): 472. http://dx.doi.org/10.1116/1.1690776.

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11

Zhang, Yunxiao, Dongping Wu, and Zhiqiang Weng. "Synthesis of 1,2,2-trifluorovinyl sulphides and selenides from trifluorovinylation of organic thiocyanates and selenocyanates." Organic Chemistry Frontiers 4, no. 11 (2017): 2226–29. http://dx.doi.org/10.1039/c7qo00595d.

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12

Motoyoshiya, Jiro, Yusuke Masue, Yoshinori Nishi, and Hiromu Aoyama. "Synthesis of Hypericin via Emodin Anthrone Derived from a Two-fold Diels-Alder Reaction of 1,4-Benzoquinone." Natural Product Communications 2, no. 1 (2007): 1934578X0700200. http://dx.doi.org/10.1177/1934578x0700200113.

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The six-step synthesis of hypericin by the regioselective two-fold Diels-Alder reaction of 1,4-benzoquinone first with (1-methoxy-3-methylbuta-1,3-dienyloxy)trimethylsilane leading to 7-methyljuglone, and next with (1,3-dimethoxybuta-1,3-dienyloxy)trimethylsilane, to give emodin and its O-methylated derivative. The reduction of both compounds with tin(II) chloride in acidic media was accompanied by acid hydrolysis that produced emodin anthrone, whose oxidative dimerization with iron (III) chloride hydrate gave the bianthrone in high yield. The oxidation of the bianthrone in the presence of N-e

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13

Weikart, Christopher M., Masayo Miyama, and Hirotsugu K. Yasuda. "Surface Modification of Conventional Polymers by Depositing Plasma Polymers of Trimethylsilane and of Trimethylsilane + O2." Journal of Colloid and Interface Science 211, no. 1 (1999): 18–27. http://dx.doi.org/10.1006/jcis.1998.5963.

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14

Weikart, Christopher M., Masayo Miyama, and Hirotsugu K. Yasuda. "Surface Modification of Conventional Polymers by Depositing Plasma Polymers of Trimethylsilane and of Trimethylsilane + O2." Journal of Colloid and Interface Science 211, no. 1 (1999): 28–38. http://dx.doi.org/10.1006/jcis.1998.5964.

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15

Soethoudt, Job, Steven Crahaij, Thierry Conard, and Annelies Delabie. "Impact of SiO2 surface composition on trimethylsilane passivation for area-selective deposition." Journal of Materials Chemistry C 7, no. 38 (2019): 11911–18. http://dx.doi.org/10.1039/c9tc04091a.

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16

Panyam, Pradeep Kumar Reddy, Ramdas Sreedharan, and Thirumanavelan Gandhi. "Synthesis of topologically constrained naphthalimide appended palladium(ii)–N-heterocyclic carbene complexes – insights into additive controlled product selectivity." Organic & Biomolecular Chemistry 16, no. 23 (2018): 4357–64. http://dx.doi.org/10.1039/c8ob00616d.

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17

Yasuda, H. K., and Q. S. Yu. "Deposition of trimethylsilane in glow discharges." Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films 19, no. 3 (2001): 773–81. http://dx.doi.org/10.1116/1.1365137.

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18

Pajdowska, M., J. P. Hawranek, L. Sobczyk, and G. Bator. "Dielectric relaxation in liquid trimethylsilane carbonitrile." Journal of Molecular Liquids 32, no. 1 (1986): 1–10. http://dx.doi.org/10.1016/0167-7322(86)80008-3.

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19

Maiden, T. M. M., N. Mbelesi, P. A. Procopiou, S. Swanson, and J. P. A. Harrity. "A convergent strategy towards febrifugine and related compounds." Organic & Biomolecular Chemistry 16, no. 22 (2018): 4159–69. http://dx.doi.org/10.1039/c8ob00935j.

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We report a modular five step synthetic route to the febrifugines that employs 2-(chloromethyl)allyl-trimethylsilane as a conjunctive reagent for the coupling of the piperidine and quinazolinone groups.

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20

Zhang, Lin-Lin, Meng-Tian Li, Liang-Liang Shen, and Qin-Pei Wu. "Efficient Synthesis of 5-Trifluoromethylthio-1,2,3-Triazoles: One-Pot Multicomponent Reaction from Elemental Sulfur and TMSCF3." Synthesis 52, no. 02 (2019): 304–10. http://dx.doi.org/10.1055/s-0039-1690716.

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A sequential multistep reaction toward 5-trifluoromethylthio-1,2,3-triazoles has been established, starting from alkynes, organoazides, S8, and (trifluoromethyl)trimethylsilane (TMSCF3). This reaction features mild conditions, easy operation, and readily available substrates.

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21

Zhang, Zheng-Feng, and Ming-Der Su. "The mechanistic investigations of photochemical decarbonylations and oxidative addition reactions for M(CO)5 (M = Fe, Ru, Os) complexes." RSC Advances 9, no. 5 (2019): 2626–40. http://dx.doi.org/10.1039/c8ra07669c.

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22

Wu, Zhiwei, Fei Zhou, Qiang Ma, Qianzhi Wang, Zhifeng Zhou, and Lawrence Kwok-Yan Li. "Tribological and electrochemical properties of Cr–Si–C–N coatings in artificial seawater." RSC Advances 6, no. 80 (2016): 76724–35. http://dx.doi.org/10.1039/c6ra19243b.

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Cr–Si–C–N coatings were deposited on using unbalanced magnetron sputtering via adjusting trimethylsilane (TMS) flow. CrSiCN coatings exhibited low friction coefficient. The impedance modulus and phase value became high with increasing TMS flow.

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23

Takahashi, Kenjiro, Yusuke Ano, and Naoto Chatani. "Fluoride anion-initiated bis-trifluoromethylation of phenyl aromatic carboxylates with (trifluoromethyl)trimethylsilane." Chemical Communications 56, no. 78 (2020): 11661–64. http://dx.doi.org/10.1039/d0cc04826g.

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The fluoride anion-initiated reaction of phenyl aromatic carboxylates with (trifluoromethyl)trimethylsilane (Me<sub>3</sub>SiCF<sub>3</sub>) that results in the formation of O-silyl-protected 2-aryl-1,1,1,3,3,3-hexafluoroisopropanols is reported.

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24

Banert, Klaus, Manfred Hagedorn, Zhuang Wu, and Xiaoqing Zeng. "Synthesis, Characterization and Reactions of (Azidoethynyl)trimethylsilane." Molecules 20, no. 12 (2015): 21328–35. http://dx.doi.org/10.3390/molecules201219770.

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25

Hoffmeyer, H., O. Horie, P. Potzinger, and B. Reimann. "Reaction of atomic oxygen (3P) with trimethylsilane." Journal of Physical Chemistry 89, no. 13 (1985): 2901–5. http://dx.doi.org/10.1021/j100259a038.

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26

Voronkov, M. G., S. G. D’yachkova, V. I. Rakhlin, and I. P. Lebedeva. "(Organylsulfanyl)chloroacetylenes: VIII. Reaction with (diethylamino)trimethylsilane." Russian Journal of General Chemistry 76, no. 11 (2006): 1778–81. http://dx.doi.org/10.1134/s1070363206110193.

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27

Voronkov, M. G., A. E. Pestunovich, A. I. Albanov, and V. A. Kukhareva. "Reaction of bis(trimethylsiloxy)phosphine with trimethylsilane." Russian Journal of General Chemistry 79, no. 6 (2009): 1080–82. http://dx.doi.org/10.1134/s1070363209060061.

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28

Williams, David R., and Martin J. Walsh. "ChemInform Abstract: 1,1′-(Chloromethylene)bis[1,1,1]-trimethylsilane." ChemInform 43, no. 27 (2012): no. http://dx.doi.org/10.1002/chin.201227246.

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29

Grobe, Joseph, and Joachim Hegge. "Facile Aluminum Induced Synthesis of (Trifluoromethyl)trimethylsilane." Synlett 1995, no. 06 (1995): 641–42. http://dx.doi.org/10.1055/s-1995-5009.

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30

Rangou, Sofia, Sergey Shishatskiy, Volkan Filiz, and Volker Abetz. "Poly(vinyl trimethylsilane) and block copolymers of vinyl trimethylsilane with isoprene: Anionic polymerization, morphology and gas transport properties." European Polymer Journal 47, no. 4 (2011): 723–29. http://dx.doi.org/10.1016/j.eurpolymj.2010.10.024.

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31

de la Cruz, Ricardo A., Francisco X. Talamás, Alfredo Vázquez, and Joseph M. Muchowski. "Total synthesis of mycophenolic acid." Canadian Journal of Chemistry 75, no. 6 (1997): 641–45. http://dx.doi.org/10.1139/v97-078.

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A total synthesis of mycophenolic acid is reported. Diels–Alder reaction of [5-methoxy-3-(1-methoxypropenyl)-4,5-dihydrofuran-2-yloxy]-trimethylsilane with 3-benzenesulfinyl-5H-furan-2-one afforded the hexasubstituted nucleus. The side chain was constructed from the unveiled aldehyde. Keywords: mycophenolic acid, Diels–Alder reaction, pentasubstituted diene.

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32

Goldberg, Yu, R. Sturkovich, and E. Lukevics. "A Simple Sonochemical Synthesis of (3-Thienyl)trimethylsilane." Synthetic Communications 23, no. 9 (1993): 1235–38. http://dx.doi.org/10.1080/00397919308011208.

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33

Kawamoto, Takuo, Rosario S. So, Yoshihisa Masuda, and Atsuo Tanaka. "Efficient enzymatic synthesis of amide with (aminomethyl)trimethylsilane." Journal of Bioscience and Bioengineering 87, no. 5 (1999): 607–10. http://dx.doi.org/10.1016/s1389-1723(99)80122-4.

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34

Qi, Y., J. L. Sulak, W. G. Durrer, J. H. Craig, and P. W. Wang. "Initial adsorption of trimethylsilane on Ge(100) surfaces." Surface and Interface Analysis 26, no. 2 (1998): 113–20. http://dx.doi.org/10.1002/(sici)1096-9918(199802)26:2<113::aid-sia350>3.0.co;2-u.

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35

Fordyce, Euan A. F., Yi Wang, Thomas Luebbers, and Hon Wai Lam. "Copper-catalyzed silylation of cyclopropenes using (trifluoromethyl)trimethylsilane." Chemical Communications, no. 9 (2008): 1124. http://dx.doi.org/10.1039/b717568j.

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36

Qin, Ying-Ying, Xiao-Long Qiu, Yan-Yan Yang, Wei-Dong Meng, and Feng-Ling Qing. "Synthesis and Transformation of [Difluoro(phenylseleno)methyl]- trimethylsilane." Journal of Organic Chemistry 70, no. 22 (2005): 9040–43. http://dx.doi.org/10.1021/jo051119z.

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37

Lin, Y. S., and H. K. Yasuda. "Plasma polymerization of trimethylsilane in cascade arc discharge." Journal of Applied Polymer Science 66, no. 9 (1997): 1653–65. http://dx.doi.org/10.1002/(sici)1097-4628(19971128)66:9<1653::aid-app4>3.0.co;2-c.

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38

Supranovich, Vyacheslav I., Alexander D. Volodin, Alexander A. Korlyukov, Jinbo Hu, and Alexander D. Dilman. "Reaction of (bromodifluoromethyl)trimethylsilane with HMPA: Structural studies." Journal of Fluorine Chemistry 250 (October 2021): 109881. http://dx.doi.org/10.1016/j.jfluchem.2021.109881.

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39

Miele, Margherita, and Vittorio Pace. "(Difluoromethyl)trimethylsilane (TMSCHF2): A Useful Difluoromethylating Nucleophilic Source." Australian Journal of Chemistry 74, no. 8 (2021): 623. http://dx.doi.org/10.1071/ch21045.

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40

Su, Shih-Hao, та Ming-Der Su. "Mechanistic investigations of CO-photoextrusion and oxidative addition reactions of early transition-metal carbonyls: (η5-C5H5)M(CO)4(M = V, Nb, Ta)". Physical Chemistry Chemical Physics 18, № 24 (2016): 16396–403. http://dx.doi.org/10.1039/c6cp02471h.

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A model study of the photoactivation reactions of Si–H bonds in trimethylsilane by group 5 (η<sup>5</sup>-C<sub>5</sub>H<sub>5</sub>)M(CO)<sub>4</sub>(M = V, Nb and Ta;Rea-S0-M) complexes is undertaken using the M06-2X/Def2-SVPD level of theory.

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41

El-Agez, Taher M., David M. Wieliczka, Chris Moffitt, and Sofyan A. Taya. "Aging of Oxygen-Treated Trimethylsilane Plasma-Polymerized Films Using Spectroscopic Ellipsometry." Journal of Atomic, Molecular, and Optical Physics 2011 (September 29, 2011): 1–6. http://dx.doi.org/10.1155/2011/295304.

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Oxygen-treated trimethylsilane (TMS) plasma-polymerized films are investigated using rotating polarizer and analyzer ellipsometer. Aging process and composition of the samples are studied. Coordinated X-ray photoelectron spectroscopy (XPS) depth profiling studies on these films is presented for more detailed understanding of the aging process as well as the modeling of these films.

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42

Khasanov, Victor, Yuri Slizhov, Alexandra Makarycheva, and Anton Chumakov. "Analysis of the Oxygen-Containing Organic Substances of Natural Water Using Solid Phase Extraction of Distillates." Key Engineering Materials 670 (October 2015): 189–95. http://dx.doi.org/10.4028/www.scientific.net/kem.670.189.

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Analysis of organic acids in natural water samples using by the distillation followed by the SPE procedure at Strata-X and GC-MS of trimethylsilane derivatives. Influence of distillation and elution, as well as a cartridge housing material, on the compounds recovery was discussed. Data on organic acids in some natural samples are provided.

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43

Large-Radix, Sylvie, Thierry Billard, and Bernard R. Langlois. "Fluoride-assisted trifluoromethylation of aromatic thiones with (trifluoromethyl)trimethylsilane." Journal of Fluorine Chemistry 124, no. 2 (2003): 147–49. http://dx.doi.org/10.1016/s0022-1139(03)00203-3.

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44

Ma, Yibao, Meng Chen, John E. Jones, Andrew C. Ritts, Qingsong Yu, and Hongmin Sun. "Inhibition of Staphylococcus epidermidis Biofilm by Trimethylsilane Plasma Coating." Antimicrobial Agents and Chemotherapy 56, no. 11 (2012): 5923–37. http://dx.doi.org/10.1128/aac.01739-12.

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ABSTRACTBiofilm formation on implantable medical devices is a major impediment to the treatment of nosocomial infections and promotes local progressive tissue destruction.Staphylococcus epidermidisinfections are the leading cause of biofilm formation on indwelling devices. Bacteria in biofilms are highly resistant to antibiotic treatment, which in combination with the increasing prevalence of antibiotic resistance among human pathogens further complicates treatment of biofilm-related device infections. We have developed a novel plasma coating technology. Trimethylsilane (TMS) was used as a mon

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45

Matsukawa, S., S. Takahashi, and H. Takahashi. "TBD-Catalyzed Trifluoromethylation of Carbonyl Compounds with (Trifluoromethyl)trimethylsilane." Synthetic Communications 43, no. 11 (2013): 1523–29. http://dx.doi.org/10.1080/00397911.2011.644381.

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46

Singh, Rajendra P., and Jean'ne M. Shreeve. "Nucleophilic Trifluoromethylation Reactions of Organic Compounds with (Trifluoromethyl)trimethylsilane." Tetrahedron 56, no. 39 (2000): 7613–32. http://dx.doi.org/10.1016/s0040-4020(00)00550-0.

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47

Yu, Q. S., C. Huang, and H. K. Yasuda. "Glow characterization in direct current plasma polymerization of trimethylsilane." Journal of Polymer Science Part A: Polymer Chemistry 42, no. 5 (2004): 1042–52. http://dx.doi.org/10.1002/pola.11038.

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48

GROBE, J., and J. HEGGE. "ChemInform Abstract: Facile Aluminum Induced Synthesis of (Trifluoromethyl)trimethylsilane." ChemInform 26, no. 44 (2010): no. http://dx.doi.org/10.1002/chin.199544183.

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49

Kawano, Yoshikazu, Hidehiko Fujisawa, and Teruaki Mukaiyama. "Lewis Base-catalyzed Trifluoromethylation of Aldimines with (Trifluoromethyl)trimethylsilane." Chemistry Letters 34, no. 3 (2005): 422–23. http://dx.doi.org/10.1246/cl.2005.422.

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50

Hoffmann-Röder, Anja, Paul Seiler, and François Diederich. "Nucleophilic trifluoromethylation of cyclic imides using (trifluoromethyl)trimethylsilane CF3SiMe3." Org. Biomol. Chem. 2, no. 16 (2004): 2267–69. http://dx.doi.org/10.1039/b407555b.

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