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Journal articles on the topic 'Triphosgene'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Safaei-Ghomi, Javad, Abdolhamid Bamoniri, and Aboalfazl Abbaszadeh-Nooshabady. "A Convenient Procedure for the Preparation of Sulfonamidoureas Using Triphosgene." Zeitschrift für Naturforschung B 62, no. 5 (2007): 721–24. http://dx.doi.org/10.1515/znb-2007-0516.

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Abstract An efficient method for the preparation of sulfonamidourea using triphosgene in organic solvents is reported.Sulfonylhydrazides and acetylsulfanilylhydrazide were transformed into the corresponding intermediates using triphosgene in 1,4-dioxane/water or tetrahydrofuran as solvents.These intermediates were converted in situ into symmetrical and unsymmetrical sulfonamidoureas in high yields and shorter periods of time related to previous methods.

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2

Yuan, Yan-qin, Sheng-rong Guo, Hai-jun Gao, Yu-xin Gu, Zhe-fei Wang, and Yan Wang. "Triphosgene/Sodium Organosulfinate System: A General and Efficient Electrophilic Thiolation of Silylenol Ethers and Electron-Rich Heteroaromatics." Synlett 31, no. 18 (2020): 1838–42. http://dx.doi.org/10.1055/s-0040-1707299.

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AbstractAn efficient and practical approach to electrophilic thiolation was developed by using commercially available triphosgene as a reductant and the appropriate alkyl- or arylsulfinates, which were transformed in situ into electrophilic RSCl intermediates in the presence of triphosgene. This procedure represents a general and powerful approach for the synthesis of α-(trifluoromethyl)thio-substituted ketones and thiolated electron-rich heteroaromatic compounds.

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3

Villalpando, Andrés, Mirza A. Saputra, Thomas H. Tugwell, and Rendy Kartika. "Triphosgene–pyridine mediated stereoselective chlorination of acyclic aliphatic 1,3-diols." Chemical Communications 51, no. 81 (2015): 15075–78. http://dx.doi.org/10.1039/c5cc06365e.

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4

Rivero, I. A., R. Somanathan, and L. H. Hellberg. "OXIDATION OF ALCOHOLS USING TRIPHOSGENE." Organic Preparations and Procedures International 24, no. 3 (1992): 363–65. http://dx.doi.org/10.1080/00304949209355904.

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5

Cortez, R., I. A. Rivero, R. Somanathan, G. Aguirre, F. Ramirez, and E. Hong. "Synthesis of Quinazolinedione Using Triphosgene." Synthetic Communications 21, no. 2 (1991): 285–92. http://dx.doi.org/10.1080/00397919108020823.

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6

Eckert, Heiner, and Barbara Forster. "Triphosgene, a Crystalline Phosgene Substitute." Angewandte Chemie International Edition in English 26, no. 9 (1987): 894–95. http://dx.doi.org/10.1002/anie.198708941.

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7

Wei, Xiu-Zhi, Jianguo Liu, and Longlong Ma. "One-Pot Tandem Synthesis of Nitriles and Amides from Biomass Platform Compounds." Catalysis Research 2, no. 1 (2021): 1. http://dx.doi.org/10.21926/cr.2201004.

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In recent years, research on converting biomass platform compounds into high-value chemicals and pharmaceutical intermediates has garnered huge interest. Nitrile and amide groups are key structures in natural products and biologically active molecules. The direct conversion of biomass platform compounds into nitriles and amides will undoubtedly be an important guide for biomass utilization. In this paper, a facile and efficient triphosgene-assisted one-pot conversion for aldehydes and ketones into nitrile and amides is presented. Triphosgene is a phosgene alternative that contains both ester l

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8

Mifune, Yuto, Hiroyuki Nakamura, and Shinichiro Fuse. "A rapid and clean synthetic approach to cyclic peptides via micro-flow peptide chain elongation and photochemical cyclization: synthesis of a cyclic RGD peptide." Organic & Biomolecular Chemistry 14, no. 47 (2016): 11244–49. http://dx.doi.org/10.1039/c6ob02391f.

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9

Wang, Shao-Lin, Lin Zhong, and Qin-Hua Song. "A ratiometric fluorescent chemosensor for selective and visual detection of phosgene in solutions and in the gas phase." Chemical Communications 53, no. 9 (2017): 1530–33. http://dx.doi.org/10.1039/c6cc09361b.

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10

Liu, Jialei, Fuyang Huo, and Wenqing He. "Construction of a simple crosslinking system and its influence on the poling efficiency and oriental stability of organic electro-optic materials." RSC Advances 10, no. 11 (2020): 6482–90. http://dx.doi.org/10.1039/c9ra10813k.

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11

Kumar, Satish, and Sunil Kumar. "Analysis of Efficient Ratiometric Fluorescent Chemodosimeter for detection of Phosgene." Journal of Advances in Science and Technology 21, no. 1 (2024): 205–9. https://doi.org/10.29070/5hgmmb52.

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The study has been analysed the “Efficient ratiometric fluorescent chemodosimeter for detection of phosgene”. Nature has provided many outstanding examples of Molecular identification. Molecular recognition that biological situations and is seen in receptor-ligand, sugar-lectin, DNA-protein, antigen-antibody, and RNA-ribosome interactions. In this survey most design strategies for phosgene detection must rely on PET/ICT on mechanisms. Another relevant approach in the area of molecular recognition is the chemiosmotic method. For the replaced A new receptor, 3-oxime-4-hydroxy-1,8-naphthalic-N-bu

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12

Liu, Zhenhua, Tian Yu, Longhua Li, et al. "S-triggered Schmidt-type rearrangement of vinyl azides to access N-aryl-(trifluoromethylsulfinyl)acetamides." Organic Chemistry Frontiers 9, no. 5 (2022): 1241–46. http://dx.doi.org/10.1039/d1qo01516h.

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A novel S-induced Schmidt-type rearrangement of vinyl azides with CF3SO2Na is developed for synthesis of N-arylated 2-(trifluoromethylsulfinyl)acetamieds, which is mediated by triphosgene (BTC) under mild reaction conditions.

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13

E, Yongsheng, Ping Lv, and Fang Yang. "Study on Synthesizing Polycarbonate with Triphosgene." Journal of Physics: Conference Series 2194, no. 1 (2022): 012033. http://dx.doi.org/10.1088/1742-6596/2194/1/012033.

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Abstract Polycarbonate is a widely used thermoplastic engineering plastic with excellent properties. Using triphosgene and Bisphenol A as raw materials, polycarbonate is synthesized by interfacial polycondensation. The effects of catalyst dosage, molar ratio of raw material, reaction temperature and reaction time on the molecular weight of the product are investigated, and the optimal reaction conditions are obtained. The structure of the product is verified by infrared absorption spectroscopy. The rotary viscometer measures the intrinsic viscosity of the sample and calculates the viscosity av

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14

Trotzki, Ronald, Matthias Nüchter, and Bernd Ondruschka. "Microwave assisted phosgenation – alcoholysis using triphosgene." Green Chem. 5, no. 3 (2003): 285–90. http://dx.doi.org/10.1039/b210895j.

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15

BRACHER, F., and T. LITZ. "ChemInform Abstract: Bis(trichloromethyl)carbonate (“Triphosgene”)." ChemInform 26, no. 51 (2010): no. http://dx.doi.org/10.1002/chin.199551294.

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16

Stalder, R., A. Mavrinskiy, C. Grand, et al. "Electrochromic and liquid crystalline polycarbonates based on telechelic oligothiophenes." Polymer Chemistry 6, no. 8 (2015): 1230–35. http://dx.doi.org/10.1039/c4py01551g.

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The triphosgene carbonate synthesis is adapted towards an alternating main-chain rod/coil polycarbonate based on a telechelic sexithiophene oligomer, yielding an electrochromic material displaying morphological behaviour typical of a liquid-crystalline polymer.

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17

K. Patil, Umesh, Sayujjata R. Vaidya, and Balaji R. Madje. "Novel Process for Preparation of Oxazolonone, Benzoxazolonone." Oriental Journal Of Chemistry 39, no. 1 (2023): 212–15. http://dx.doi.org/10.13005/ojc/390126.

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Synthesis of oxazolonone, benzoxazolononeby using amino hydroxy compound, alkyl haloformate, trialkylamine and DMF as solvents. Herein used simple carbonylation agent such as alkylhaloformate instead of phosgene and Triphosgene. Developed novel and simple synthesis method.

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18

Alkhathlan, H. Z., M. A. Al-Saad, H. M. Al-Hazimi, K. A. Al-Farhan, and A. A. Mousa. "Synthesis and X-ray Crystal Structures of Novel Spiro 1,3-benzoxazine Dimers." Journal of Chemical Research 2002, no. 10 (2002): 473–74. http://dx.doi.org/10.3184/030823402103170619.

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Novel spiro 1,3-benzoxazine dimers are obtained when hydrazones of 2-hydroxyacetophenone are treated with triphosgene. An X-ray crystal structure, and the NMR and mass spectra of these new compounds, are reported and discussed.

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19

Bi, Wen-Zhu, Yang Geng, Wen-Jie Zhang, et al. "Highly sensitive and selective detection of triphosgene with a 2-(2′-hydroxyphenyl)benzimidazole derived fluorescent probe." RSC Advances 13, no. 44 (2023): 30771–76. http://dx.doi.org/10.1039/d3ra06061f.

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A C4′ amino substituted 2-(2′-hydroxyphenyl)benzimidazole probe (4-AHBI) was designed and synthesized for highly selective and sensitive detection of triphosgene with low detection limit (0.08 nM) over range of 0–0.5 μM.

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20

Cao, Gui Rong, Xue Yan Zhao, and Rui Jie Xiao. "Study on Synthesis of Nitrophenyl Isocyanates Using Triphosgene." Advanced Materials Research 550-553 (July 2012): 1039–42. http://dx.doi.org/10.4028/www.scientific.net/amr.550-553.1039.

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In this paper, triphosgene respectively reacting with o-nitrophenyl aniline, m-nitrophenyl aniline and p-nitrophenyl aniline to synthesize corresponding isocyanates. The effects of reactants molar ratio, reaction time and reaction temperature on the yield were investigated. As a result, using 1,2-dichloroethane as reaction solvent, the optimum molar ratio of the three kinds of nitroaniline and triphosgene were all 2.5:1, the optimum reaction time of synthesis of o-nitrophenyl isocyanate, m-nitrophenyl isocyanate and p-nitrophenyl isocyanate respectively was 6h, 5.5h and 5h; the optimum reactio

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21

Isik, Murat. "Synthesis of a β-Nitrile-BODIPY from its β-Aldoxime Through Dehydration by Triphosgene: Comparative Spectroscopic Characterization". INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY 34, № 04 (2024): 447. https://doi.org/10.59467/ijhc.2024.34.447.

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A high yielding (84%) transformation of a β-aldoxime-Boron dipyrromethenes (BODIPY) to its β-nitrile was achieved through a dehydration reaction employing in situ generated phosgene (from triphosgene and triethylamine). The two new organic dyes were comparatively and comprehensively characterized by 1H and 13C nuclear magnetic resonance, high-resolution mass spectrometry, infrared spectroscopy, Ultraviolet-vis absorption, and fluorescence emission spectroscopy (both steady-state and time-correlated). The significantly reduced emission and shorter excited-state lifetimes of β-oxime- BODIPY, com

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22

Ghorbani-Choghamarani, Arash, and Gouhar Azadi. "Triphosgene and its Application in Organic Synthesis." Current Organic Chemistry 20, no. 27 (2016): 2881–93. http://dx.doi.org/10.2174/1385272820666160630124216.

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23

Menguy, Laurence, Bruno Drouillat, and François Couty. "Reaction of N -alkyl azetidines with triphosgene." Tetrahedron Letters 56, no. 47 (2015): 6625–28. http://dx.doi.org/10.1016/j.tetlet.2015.10.036.

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24

THATIKONDA, NARENDER REDDY, NAGA SESHA SAI PAVAN KUMAR CHEBOLU, MAHENDAR BUDDE, and JAYATHIRTHA RAO VAIDYA. "Triphosgene mediated chlorination of Baylis–Hillman adducts." Journal of Chemical Sciences 124, no. 2 (2012): 513–19. http://dx.doi.org/10.1007/s12039-012-0243-3.

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25

CORTEZ, R., I. A. RIVERO, R. SOMANATHAN, G. AGUIRRE, F. RAMIREZ, and E. HONG. "ChemInform Abstract: Synthesis of Quinazolinedione Using Triphosgene." ChemInform 22, no. 48 (2010): no. http://dx.doi.org/10.1002/chin.199148176.

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26

RIVERO, I. A., R. SOMANATHAN, and L. H. HELLBERG. "ChemInform Abstract: Oxidation of Alcohols Using Triphosgene." ChemInform 24, no. 6 (2010): no. http://dx.doi.org/10.1002/chin.199306093.

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27

Fan, Xuesen, Xinying Zhang, and Yongmin Zhang. "Samarium diiodide mediated regeneration of 1,2-benzene diamine and preparation of benzimidazolin-2-ones from 2,1,3-benzothiadiazoles." Journal of Chemical Research 2005, no. 1 (2005): 21–22. http://dx.doi.org/10.3184/0308234053431095.

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On treatment with SmI2 in THF and in the presence of methanol, 2,1,3-benzothiadiazoles underwent reductive N–S bond cleavage leading to 1,2-benzenediamines in high yields. Without methanol but in the presence of triphosgene, benzimidazolin-2-ones were obtained in moderate yields under mild conditions.

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28

Alkhathlan, H. Z., M. A. Al-Saad, H. M. Al-Hazimi, K. A. Al-Farhan, and A. A. Mousa. "Quinazoline, Pyrazolo[1,5-c]Quinazoline and Spiro Quinazoline Dimers from the Reaction of 2-Aminoacetophenone Hydrazones with Triphosgene." Journal of Chemical Research 2002, no. 12 (2002): 587–88. http://dx.doi.org/10.3184/030823402103170952.

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The reaction of hydrazones of 2-aminoacetophenone with triphosgene in dichloromethane or benzene in the presence of triethylamine gave quinazolines, pyrazolo[1,5-c]quinazoline and spiro quinazoline dimers. The latter compounds are being reported for the first time. In addition, a 4,4-disubstituted quinazoline derivative is prepared and its x-ray crystal structure is reported.

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29

Ishikawa, Tsutomu, Tatsuru Saito, and Makoto Yoshida. "Triphosgene: A Versatile Reagent for Bischler-Napieralski Reaction." HETEROCYCLES 54, no. 1 (2001): 437. http://dx.doi.org/10.3987/com-00-s(i)44.

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30

Miyata, Okiko, Masafumi Ueda, Yuika Nishida, and Norihiko Takeda. "Triphosgene-Mediated Chlorolactamization and Aminolactamization of Homoallylic Amines." HETEROCYCLES 95, no. 2 (2017): 787. http://dx.doi.org/10.3987/com-16-s(s)42.

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31

Chaskar, A. C., S. Yewale, R. Bhagat, and B. P. Langi. "Triphosgene: An Efficient Catalyst for Synthesis of Isothiocyanates." Synthetic Communications 38, no. 12 (2008): 1972–75. http://dx.doi.org/10.1080/00397910801997744.

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32

Eckert, Heiner. "ChemInform Abstract: Phosgenation Reactions with Phosgene from Triphosgene." ChemInform 43, no. 26 (2012): no. http://dx.doi.org/10.1002/chin.201226233.

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33

Rajyashree, Chakravorty, Sirohi Reenu, and Kishore D. "A green chemistry approach to the synthesis of isatoic anhydrides from anthranilic acid derivatives." Journal of Indian Chemical Society Vol. 83, May 2006 (2006): 519–21. https://doi.org/10.5281/zenodo.5819435.

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Department of Chemistry. Banasthali Vidyapith, Banasthali-304 022, Rajasthan. India <em>E-mail </em>: kishoredharma@yahoo.co.in Fax: 91-01438-228365 <em>Manuscript received 7 November 2005, accepted 21 February 2006</em> An efricient one pot synthesis of isatoic anhydrides (2a-g) from anthranilic acid derivatives (la-g) using triphosgene over basic alumina, under solvent free conditions with microwave heating is described.

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34

Shi, Daqing, Guolan Dou, and Zheng-Yi Li. "Synthesis of 3-Aryl-3,4-Dihydroquinazolin-2(1H)-Ones with the Aid of Low-Valent Titanium Reagent (TiCl4-Sm)." Journal of Chemical Research 2007, no. 9 (2007): 545–47. http://dx.doi.org/10.3184/030823407x248306.

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A short and facile synthesis of a series of 3-aryl-3,4-dihydroquinazolin-2(1H)-ones was accomplished in good yields via the novel reductive cyclisation of 2-nitrobenzylamines with bis(trichloromethyl)carbonate (triphosgene) promoted by TiCl4/Sm system. The structures of the products were characterised by IR, 1H NMR and elemental analysis and the structure of 3a was confirmed by X-ray diffraction analysis.

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35

Alexander, Petr, Antonín Holý, and Milena Masojídková. "Preparation of 9-(2-Phosphonomethoxyethyl)adenine Esters as Potential Prodrugs." Collection of Czechoslovak Chemical Communications 59, no. 8 (1994): 1853–69. http://dx.doi.org/10.1135/cccc19941853.

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Esters of 9-(2-phosphonomethoxyethyl)adenine with substituted aliphatic alcohols were prepared as potential prodrugs. Activation of the phosphonate moiety with dimethylchloromethyleneammonium chloride, generated by reaction of thionyl chloride or triphosgene with dimethylformamide, proved to be the method of choice. The esters were also prepared by alkylation of the phosphonate group with dimethylformamide dialkyl acetals or a mixture of the appropriate alcohol with dimethylformamide dineopentylacetal.

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36

Vijay, Natarajan, Gopal Balamurugan, Peter Jerome, and Tae Hwan Oh. "One-step synthesis of a sparkling fluorescent chemodosimeter: Selective and sensitive detection of triphosgene and application in tracing triphosgene in soil." Journal of Photochemistry and Photobiology A: Chemistry 454 (September 2024): 115722. http://dx.doi.org/10.1016/j.jphotochem.2024.115722.

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37

Movassagh, Barahman, and Mohammad Soleiman-Beigi. "Convenient Route to Thiocarbonates from Alcohols, Thiols, and Triphosgene." Synthetic Communications 40, no. 23 (2010): 3467–71. http://dx.doi.org/10.1080/00397910903457258.

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38

Kricheldorf, Hans R., Sigrid Böhme, Gert Schwarz, and Claus-L. Schultz. "Cyclic Polycarbonates by Polycondensation of Bisphenol A with Triphosgene†." Macromolecules 37, no. 5 (2004): 1742–48. http://dx.doi.org/10.1021/ma0301348.

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39

Villalpando, Andrés, Caitlan E. Ayala, Christopher B. Watson, and Rendy Kartika. "Triphosgene–Amine Base Promoted Chlorination of Unactivated Aliphatic Alcohols." Journal of Organic Chemistry 78, no. 8 (2013): 3989–96. http://dx.doi.org/10.1021/jo400341n.

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40

Qingmin, Wang, and Huang Runqiu. "Two convenient new syntheses of ferrocenoyl chloride by triphosgene." Journal of Organometallic Chemistry 604, no. 2 (2000): 287–89. http://dx.doi.org/10.1016/s0022-328x(00)00182-0.

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41

Xu, Yingzhou, Dufen Hu, Hui Zheng, David Mei, and Zhaobo Gao. "Regioselective bromination of arenes mediated by triphosgene-oxidized bromide." Tetrahedron 75, no. 39 (2019): 130539. http://dx.doi.org/10.1016/j.tet.2019.130539.

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42

Krishnaswamy, D., B. M. Bhawal, and A. R. A. S. Deshmukh. "Triphosgene, an efficient acid activator for the Staudinger reaction." Tetrahedron Letters 41, no. 3 (2000): 417–19. http://dx.doi.org/10.1016/s0040-4039(99)02074-2.

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43

Zhou, Yuhan, Runjun Gong, and Weirong Miao. "New Method of SynthesizingN‐Alkoxycarbonyl‐N‐arylamide with Triphosgene." Synthetic Communications 36, no. 18 (2006): 2661–66. http://dx.doi.org/10.1080/00397910600764675.

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44

Banwell, Martin G., Mark J. Coster, Michael J. Harvey, and John Moraes. "Selective Cleavage ofN-Benzyl-Protected Secondary Amines by Triphosgene." Journal of Organic Chemistry 68, no. 2 (2003): 613–16. http://dx.doi.org/10.1021/jo0263622.

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45

Rivero, I. A., S. Heredia, and A. Ochoa. "ESTERIFICATION OF AMINO ACIDS AND MONO ACIDS USING TRIPHOSGENE." Synthetic Communications 31, no. 14 (2001): 2169–75. http://dx.doi.org/10.1081/scc-100104468.

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46

Ayala, Caitlan E., Andres Villalpando, Alex L. Nguyen, Gregory T. McCandless, and Rendy Kartika. "Chlorination of Aliphatic Primary Alcohols via Triphosgene–Triethylamine Activation." Organic Letters 14, no. 14 (2012): 3676–79. http://dx.doi.org/10.1021/ol301520d.

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47

Qing-Min, Wang, Cheng Jun-Ran, and Huang Run-Qiu. "New reactions ofN-T-butyl-N-benzoylhydrazine with triphosgene." Journal of Heterocyclic Chemistry 40, no. 1 (2003): 195–97. http://dx.doi.org/10.1002/jhet.5570400130.

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48

Thatikonda, Narender Reddy, Naga Sesha Saipavan Kumar Chebolu, Mahendar Budde, and Jayathirtha Rao Vaidya. "ChemInform Abstract: Triphosgene Mediated Chlorination of Baylis-Hillman Adducts." ChemInform 43, no. 33 (2012): no. http://dx.doi.org/10.1002/chin.201233084.

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49

Yi, Wen Bin, Fang Luan, Jian Min Xiu, Lv Qi Jiang, and Chun Cai. "Triphosgene as a Safe and Environment-Friendly Carbonylation Reagent for the Preparation of 2-Benzimidazolone." Advanced Materials Research 955-959 (June 2014): 651–55. http://dx.doi.org/10.4028/www.scientific.net/amr.955-959.651.

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2-Benzimidazolone and their derivatives which have a wide range of biological and pharmaceutical activity are important intermediates for organic synthesis. Reported synthetic methods mostly involved unfriendly materials like phosgene, dimethyl carbonate and urea. This paper developed a novel method for the synthesis of 2-benzimidazolone by the reaction of o-phenylendiamine with triphosgene (BTC) instead of phosgene. BTC is a safer solid and easier to handle compared to phosgene. BTC can greatly reduce risks to both human health and the environment.

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50

Han, Ki-Jong, and Misoo Kim. "Direct Synthesis of Weinreb Amides from Carboxylic Acids Using Triphosgene." Letters in Organic Chemistry 4, no. 1 (2007): 20–22. http://dx.doi.org/10.2174/157017807780037441.

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