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Dissertations / Theses on the topic 'Unsaturated ester'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Michaille, Sylvie. "Photolyse et photo-oxydation des polyesters insatures a l'etat solide." Clermont-Ferrand 2, 1987. http://www.theses.fr/1987CLF2D013.

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L'evolution photolytique et photo-oxydative des polyesters insatures, reticules ou non, exposes a une lumiere polychromatique de longueurs d'onde superieures a 300 nm, a ete etudiee par spectrophotometries ir, irtf, uv-visible. L'influence de chaque parametre d'elaboration a pu etre determinee: nature et concentration des diacides, nature des glycols, nature et concentration des agents reticulants, mode de reticulation. Les mecanismes mettent en jeu l'excitation primaire des groupes fumarates-maleates ou des groupes phtalates, et des reactions radicalaires rendent compte de l'apparition de pro

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2

Karila, Delphine. "Etude de la réaction d’esters ω-insaturés médiée par l’iode hypervalent et catalysée par le cuivre : développement d’une nouvelle réaction d’aminolactonisation. Application à la synthèse d’hétérocycles originaux fonctionnalisés". Thesis, Paris 11, 2011. http://www.theses.fr/2011PA112228.

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La réaction d’aziridination catalysée par les sels de cuivre permet de former des aziridines à partir d’oléfines en employant une source de nitrènes générée à partir de aryliminoiodanes.Le développement au laboratoire d’une version « one-pot » impliquant l’iodosylbenzène et un sulfonamide ainsi que l’emploi de l’iminoiodane N-Ses a rendu cette réaction plus attractive en synthèse.La première partie de ce travail a été consacrée à l’étude de la réactivité particulière des esters ω-insaturés dans les conditions d’aziridination. En effet, dans ces conditions, l’aziridine subit une ouverture intra

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3

Xu, Liqun. "Integrated analysis of liquid composite molding (LCM) processes." Connect to this title online, 2004. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=osu1095688597.

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Thesis (Ph. D.)--Ohio State University, 2004.<br>Title from first page of PDF file. Document formatted into pages; contains xix, 245 p.; also includes graphics. Includes bibliographical references (p. 233-245).

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4

Leeves, Nigel John. "Autoxidative degradation of unsaturated fatty acid esters." Thesis, Royal Holloway, University of London, 1985. http://repository.royalholloway.ac.uk/items/60dddc77-e1aa-4a11-8ee9-50abbfa8a499/1/.

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The autoxidative degradation of methyl cis-9-octadecenaote, methyl cis-9-cis-12-octadecadienoate and methyl cis-9-cis-12-cis-l5 octadecatrienoate promoted by both transition metal ions and photoinitiators produce volatile products. These were collected by cryogenic and chemical traps, then analysed by glc, HPLC and gc-ms. The major products so identified included; 3-heptanone, heptanal and octanal from methyl cis-9-octadecenoate, hexanal,2-hexenal and 2-heptenal from methyl cis-9-cis-12-octadecadienoate, and propanal, 1-penten-3-ol and 1-penten-3-one from methyl linolenate. Methyl octanoate wa

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5

Piras, Antioco. "Etude par résonnance magnétique nucléaire haute résolution en solution de la structure des polyesters insaturés." Paris 6, 1988. http://www.theses.fr/1988PA066483.

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Preparation et caracterisation par rmn a haute resolution d'alpha -omega -dihydroxy polyesters insatures modeles par rmn bidimensionnelle: mise en evidence de 3 types de branchements: cours, longs, cycliques. Preparation de polyesters lineaires par synthese en solution ou a partir de diacetates, reactions non adaptables industriellement sans modification des procedes; mise au point d'une technique de dosage de la reaction de saturation des produits industriels et etude des parametres influant sur cette reaction

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6

林正乾 and Ching-kin Lam. "Oxidation reaction of unsaturated long chain fatty esters: a sonochemical approach." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1995. http://hub.hku.hk/bib/B31212384.

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7

Lam, Ching-kin. "Oxidation reaction of unsaturated long chain fatty esters : a sonochemical approach /." [Hong Kong] : University of Hong Kong, 1995. http://sunzi.lib.hku.hk/hkuto/record.jsp?B14777460.

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8

Li, Ninglin. "Studies on the reduction of unsaturated thioesters using copper hydride." Click to view the E-thesis via HKUTO, 2010. http://sunzi.lib.hku.hk/hkuto/record/B44251324.

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9

Li, Ninglin, and 李宁琳. "Studies on the reduction of unsaturated thioesters using copper hydride." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2010. http://hub.hku.hk/bib/B44251324.

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10

Johnson, Brett Michael. "Stereoselective Olefin Cross-Metathesis of α,β,γ,δ-Unsaturated Phenyl Esters". Thesis, Boston College, 2015. http://hdl.handle.net/2345/bc-ir:104818.

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Thesis advisor: Amir H. Hoveyda<br>Chapter 1. Catalytic olefin metathesis has developed into a powerful tool in the arsenal of the synthetic chemist as a quick and reliable method to build complexity in biologically active molecules. One particular subset of this class of reactions, catalytic olefin cross-metathesis, has seen great strides within the last decade. Using recently reported well-defined catalysts, chemists have been able to synthesize olefins in a stereoselective fashion via this reaction in a laboratory setting. While many classes of Z olefins have succumbed to this transformatio

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11

Qin, Can. "Synthesis of Trisubstituted α,β-Unsaturated Esters through Catalytic Stereoretentive Cross-Metathesis:". Thesis, Boston College, 2021. http://hdl.handle.net/2345/bc-ir:109197.

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Thesis advisor: Amir H. Hoveyda<br>We have devised a broadly applicable catalytic cross-metathesis method for stereoretentive synthesis of Z- and E-trisubstituted α,β-unsaturated esters. Several new Mo-bisaryloxide complexes were prepared, and they showed superior efficiency in synthesizing the Z-trisubstituted enoates (vs. corresponding mono-aryloxide pyrrolide complexes). Synthetic utility of the method was demonstrated through several concise syntheses of bioactive triterpenoids and value-added derivatives of prenyl-containing compounds such as citronellal, citronellol, and geraniol, all of

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12

Rajagopal, Thivisa. "Synthesis of Single Isomer Trisubstituted Olefins from beta-chloro-alpha-iodo-alpha, beta-Unsaturated Esters and Alkynyl Esters." Thesis, University of Ottawa (Canada), 2010. http://hdl.handle.net/10393/28552.

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A convenient method to synthesize regiospecific and stereoselective trisubstituted olefins bearing three substitutents with various functionalities is disclosed. A unique olefin template such as (E)-beta-chloro-alpha-iodo-alpha,beta-unsaturated esters cross-couple with 9-alkyl-9-BBN to produce single isomer trisubstituted olefins using palladium-catalyzed Suzuki-Miyaura cross-coupling reaction. This methodology can be further expanded to introduce various alkyl groups at the beta-position. The mechanism is somewhat unusual as it involves two catalytic cycles with an allenoate intermediate to e

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13

Sanchez, Romero Oscar A. "Intramolecular cycloaddition of allylic esters of #beta#-azo-substituted #alpha#,#beta#-unsaturated acids." Thesis, University of Liverpool, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.328281.

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14

Derrien, Nolwenn. "Palladium catalysed carbonylation of terminal alkenes to α,β-unsaturated esters, &, Allylic C-H functionalisation of unsaturated hydrazine carboxylates to vinyl isoxasolidines". Thesis, Loughborough University, 2014. https://dspace.lboro.ac.uk/2134/14660.

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In the first part of the thesis, the aim was to devise a new simple catalytic system based on palladium to allow insertion of carbon monoxide in the presence of an alcohol into unsaturated systems with retention of the double bond to give an unsaturated ester. The process is known as oxidative carbonylation. To allow the process to become catalytic, the palladium needs to be reoxidised in situ. Optimal conditions for the catalytic system were developed and a wide range of substrates have been examined. Simple terminal alkenes and alkenes bearing functional group have been successfully carbonyl

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15

Strickler, Ricky R. "Sulfinyl chlorides as a source of enantioenriched Ã,ß-unsaturated sulfinate esters and sulfoxides." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2001. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp04/NQ56296.pdf.

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16

Sansone, John P. "The Kinetics of Epoxidation of A,B-Unsaturated Esters by Dimethyldioxirane: A Mechanistic Study." Digital Archive @ GSU, 2009. http://digitalarchive.gsu.edu/chemistry_theses/22.

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The epoxidation of a series of α,β-unsaturated esters by dimethyldioxirane was studied. Second order rate constants were determined under pseudo first order conditions. The epoxide of each ester upon full conversion was found to be the only isolable product. Second order rate constants for the cis-like ethyl tiglate showed a 4 fold increase over that of trans-like angelic methyl ester. The ester substituent was found to have little effect on overall rate constants. A comparison of a relatively strained cyclopentene carboxylate to the cyclohexene carboxylate showed a 2 fold increase in selectiv

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17

Habassi, Chefik. "Mise en evidence du phenomene d'agregation ionique dans les resines polyester neutralisees par des ions metalliques." Paris 6, 1988. http://www.theses.fr/1988PA066282.

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Etude de composes modeles, molecules de faible masse et oligomeres difonctionnels, neutralises et gonfles ou non par des solvants; diminution de la mobilite des chaines au voisinage des groupes -coomg et existence de plusieurs conformations dans les produits neutralises. Mise en evidence par saxs d'agregats ioniques de 5 a 10 a disperses dans la matrice constituee du polymere et du solvant de gonflement

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18

Garcia, Angela. "Kinetic modeling of oxygen absorption by unsaturated esters and linseed oil to be used as oxygen scavengers." Thesis, Paris, ENSAM, 2016. http://www.theses.fr/2016ENAM0001/document.

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Les capteurs d’oxygène sont le plus grand apport dans la technologie des emballages actifs parce qu’ils permettent de retarder la dégradation oxydante des aliments et ainsi éviter la perte de saveurs et le développement microbien au sein des aliments. Bien que le développement des emballages actes existe depuis les années 70 dans des pays producteur agricole, la recherche sur ces emballages reste encore embryonnaire, en particulier sur les critères techniques portant sur l’absorption d’oxygène de films. Cette thèse constitue une contribution sur l’étude des cinétiques d’absorption d’oxygène de

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19

Alberico, Dino. "Diels-Alder reactions of Ã,ß-unsaturated sulfinate esters for the preparation of poly hydroxy/mercapto compounds." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2001. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp04/MQ61867.pdf.

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20

Gaikwad, A. L. "β Activation of α , β- unsaturated esters for -C-C- bond formation reactions: applications in the synthesis of biological active compounds". Thesis(Ph.D.), CSIR-National Chemical Laboratory, Pune, 2011. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/3822.

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21

Curilazo, Ricardo. "Redução eletroquímica de 3,3\' - (1,X - fenileno) - bis - (2 - propenoatos de etila)." Universidade de São Paulo, 2006. http://www.teses.usp.br/teses/disponiveis/46/46135/tde-04092006-193506/.

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A redução eletroquímica de 3,3\'-(1,3- e 1,4-fenileno)-bis-(2-propenoatos de etila), sistemas diolefínicos cujas duplas ligações estão separadas por um anel benzênico, foi investigada em N,N-dimetilformamida (DMF) e acetonitrila (MeCN) e metanol/acetonitrila (MeOH/MeCN) (7:3) (v/v). As eletrólises a potencial controlado em DMF e MeCN conduziram a hidrodímeros cíclicos derivados da ciclopentanona com elevada estereosseletividade, análogos aos produtos formados a partir de ésteres do ácido cinâmico nas mesmas condições experimentais. Ao lado dos hidrodímeros, quantidades variáveis de produtos de

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22

Pianosi, Anthony. "Synthesis of Single Isomer Trisubstituted and Tetrasubstituted Olefins from E-β-Chloro-α-Iodo-α,β-Unsaturated Esters and Bergman Cycloaromatizations With and Without a Radical Trapping Agent". Thèse, Université d'Ottawa / University of Ottawa, 2011. http://hdl.handle.net/10393/20456.

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Optimized methods for the regioselective and stereospecific synthesis of both trisubstituted and tetrasubstituted olefins as single isomers from E-β-chloro-α-iodo-α,β-unsaturated esters have been developed from previous work done in the Ogilvie lab. These optimized methods have led to the synthesis of trans isomeric enediynes that can be photoisomerized to their respective cis isomers and subsequently undergo microwave-assisted Bergman cycloaromatizations. Furthermore, both cis and trans isomeric enediynes that have propargyl ether substituents have been found to be able to undergo photoacti

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23

Pedrozo, Eliane Corrêa. "Reações de ésteres ß,Y-insaturados com tálio(III) e de 1,2-di-hidronaftalenos com iodo(III)." Universidade de São Paulo, 2006. http://www.teses.usp.br/teses/disponiveis/46/46135/tde-28112006-144242/.

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Esta dissertação apresenta um estudo sobre a contração de anel de ésteres ß,y-insaturados promovida por trinitrato de tálio (TTN) e de 1,2-di-hidronaftalenos promovida por hidroxi(tosiloxi)iodobenzeno (HTIB), também conhecido como reagente de Koser. Ambos estudos visaram à síntese de indanos funcionalizados. A reação de uma série de ésteres ß,y-insaturados (por exemplo 2-(3,4-di-hidronaftalen-1-il)-proprionato de etila) com TTN em ácido acético forneceu os correspondentes produtos de contração, formando indanos em bons rendimentos. A presença de grupos doadores de elétrons na posição 6 no anel

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24

Grondin, Éric. "Exploration du potentiel biotechnologique des levures endémiques et indigènes de la Réunion et de Madagascar à produire des molécules d'arômes." Thesis, La Réunion, 2014. http://www.theses.fr/2014LARE0016.

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Depuis quelques décennies, la communauté scientifique s'intéresse de plus en plus à la recherche de nouvelles levures pour de nouvelles applications dans le domaine des biotechnologies blanches. De l'étude de la biodiversité à l'étude des propriétés métaboliques, les recherches visant à sélectionner de nouvelles levures avec des propriétés intéressantes pour l'industrie se sont intensifiées. Localisées dans le Sud-Ouest de l'océan Indien, les îles de La Réunion et de Madagascar sont aujourd'hui considérées comme des Hot Spot de la biodiversité. La grande diversité de plantes et de fruits tropi

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25

Feng, Chang Liao, and 張料峰. "On the Synthesis of Unsaturated Polyamide-ester/ Polysilisic Acid Hybird Materials and their Properties." Thesis, 2002. http://ndltd.ncl.edu.tw/handle/15817994169319935024.

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碩士<br>國立臺灣科技大學<br>纖維及高分子工程系<br>90<br>The transparent organic-inorganic hybrid materials, UPAE/NDMA/nPSA and UPAE/NDMA/M-nPSA were prepared through free radical polymerization of polysilicic acid (nPSA) and M-nPSA, modified nPSA through the reation of nPSA with 3-glycidylpropyl trimethoxylsilane(GPTS), respectively. The hydroxyl containing UPAE was obtained by the ring-opening reaction of diglycidyl ether of bisphenol (DGEBA) with 1.6-uexamethylene diamine：bissemimaleamide(HBSM) under the catalization of tetrethylammoniumbromide, while nPSA was prepared through hydrolysis and condensation of me

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26

Kao, Fan-Hsu, and 高凡敍. "Skeletal mechanisms relevant to the formation of unsaturated intermediates in combustion of methyl ester fuel surrogates." Thesis, 2016. http://ndltd.ncl.edu.tw/handle/95048303566045142529.

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碩士<br>國立中山大學<br>機械與機電工程學系研究所<br>104<br>In this study, a skeletal kinetic mechanisms for biodiesel fuel surrogates is developed for fuel oxidation that can overcome the barrier of incorporating detailed chemistry to computational fluid dynamics (CFD) for fuel combustion. This study begins from (1) assembling mechanisms which are able to predict experimentally measured methyl isobutyrate (MIB), polycyclic aromatic hydrocarbons (PAHs) and compound (C5H10) (2) generating a minimized skeletal mechanism for methyl butanoate (MB) oxidation. Using the path flux analysis method, the minimized skeletal

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27

孫珮珮. "The studies of the Intramolecular Free Radical Cyclization of Aldehyde and α,β－Unsaturated Ester Induced by Bu3SnH and SmI2". Thesis, 1993. http://ndltd.ncl.edu.tw/handle/16198905090017643334.

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28

Liu, Chia-hwuan, and 劉嘉樺. "Synthesis of nano-scale and submicron-scale acrylic type of core-shell rubber additives and unsaturated polyester, vinyl ester resin and their phase characteristics in styrene/ vinyl ester resin /additive ternary systems." Thesis, 2008. http://ndltd.ncl.edu.tw/handle/30744059045160366965.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>96<br>Acrylic type of core-shell rubbers (CSR) , with varied nano-scale and submicron-scale particle size and shell chemical composition, as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) and vinyl ester resin (VER) have been synthesized by two-stage seeded emulsion polymerizations . Three types of unsaturated polyester resin with different chemical structures, namely, MA-PG type, MA-PA-PG type, and vinyl ester resin (VER) ,have also been synthesized so that styrene (St) /UP /CSR ternary systems with different miscibility can be des

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Hsu, Shen-Yu, and 許勝裕. "Synthesis of nano-scale polymeric core-shell rubber additives by RAFT living free radical emulsion polymerizations for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2012. http://ndltd.ncl.edu.tw/handle/rd452n.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>100<br>Synthesis of s-CSR by RAFT polymerization via spontaneous phase inversion process and RAFT surfactant-free, batch emulsion polymerization as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) ,epoxy resin (EPR) and vinyl ester resin (VER) have been investigated . Two types of conventional unsaturated polyester resin with different chemical structures, namely, MA-PG type of UP and, MA-PA-PG type of UP, and vinyl ester resin (VER) ,have also been synthesized so that styrene (St) /UP(or VER) /CSR or EPR/DDM/CSR ternary systems with d

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Hsu, Yu-Lun, and 許毓倫. "Synthesis of nano-scale and submicron-scale polymeric core-shell rubber additives RAFT living free radical emulsion polymerizations for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2011. http://ndltd.ncl.edu.tw/handle/60122643389233776956.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>99<br>Synthesis of acrylic type of core-shell rubbers (gp-CSR) with varied nano-scale and submicron-scale particle size and shell chemical composition. And synthesis of s-CSR by RAFT polymerization via spontaneous phase inversion process and RAFT surfactant-free, batch emulsion polymerization as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) ,epoxy resin (EPR) and vinyl ester resin (VER) have been investigated. Two types of conventional nsaturated polyester resin with different chemical structures, namely, MA-PG type of UP and, MA-PA

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31

Chen, Yen-Po, and 陳彥博. "Synthesis of Nano-scale and Submicron-scale Reactive Microgel Particle as Low-profile Additives and Tougheners for Vinyl Ester Resins and Unsaturated Polyester Resins by Emulsion Polymerization." Thesis, 2019. http://ndltd.ncl.edu.tw/handle/vf45h8.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>107<br>In this paper, the traditional emulsion polymerization method is combined with the addition of surfactant and co- surfactant to synthesize nano-scale or submicron-scale reactive microgel (RM) particles as low-profile additives (LPA) and toughener for vinyl ester resin (VER) and unsaturated polyester (UP) resin. The bulk and solution polymerization were used to synthesize three kinds of traditional UP resins with different chemical structures, including Maleic anhydride (MA)-Phthalic anhydride (PA)-1, 2-Propanediol (PG) type, MA-PG type, MA-1,6-Hexanediol (HD)

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yeu-shiun, shieh, and 謝宇軒. "Synthesis of nano-scale inorganic silica gel/organic polymer core-shell particle as additives by RAFT living free radical polymerizations for unsaturated polyester, viny ester, and epoxy resins." Thesis, 2009. http://ndltd.ncl.edu.tw/handle/57494638192637782477.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>97<br>Abstract Synthesis of inorganic/organic core-shell particle (CSP) as low-profile additives for unsaturated polyester resins by RAFT living free radical polymerizations has been studied in this work. Before the RAFT polymerization, the chain transfer agent with a chemical structure of Z-C(=S)-S-R was synthesized first. The synthesized chain transfer agent was then characterized by using FTIR、1H-NMR and DSC to confirm its structure. The chain transfer agent (CTA), namely, BSPA, was bonded onto the inorganic silica particles. The silica-supported BSPA was then use

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Rao, Rui-Bo, and 饒瑞博. "Synthesis of nano-scale and submicron-scale polymeric core-shell rubber additives by conventional and RAFT living free radical emulsion polymerizations for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2013. http://ndltd.ncl.edu.tw/handle/73265497368200357799.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>101<br>Synthesis of s-CSR by RAFT polymerization viaspontaneous phase inversion process and RAFT surfactant-free, batch emulsion polymerizationas low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) ,epoxy resin (EPR) and vinyl ester resin (VER) have been investigated . Two types of conventional unsaturated polyester resin with different chemical structures, namely, MA-PG type of UP and, MA-PA-PG type of UP, and vinyl ester resin (VER) ,have also been synthesized so that styrene (St) /UP(or VER) /CSR or EPR/DDM/CSR ternary systems with dif

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DAI, MENG-SHIANG, and 戴夢祥. "Synthesis of nano-scale and submicron-scale polymeric core-shell rubber additives by conventional and RAFT living free radical emulsion polymerizations for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2010. http://ndltd.ncl.edu.tw/handle/34192836835901706631.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>98<br>Synthesis of acrylic type of core-shell rubbers (gp-CSR) with varied nano-scale and submicron-scale particle size and shell chemical composition. And synthesis of s-CSR by RAFT polymerization via spontaneous phase inversion process and RAFT surfactant-free, batch emulsion polymerization as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) ,epoxy resin (EPR) and vinyl ester resin (VER) have been investigated . Two types of conventional nsaturated polyester resin with different chemical structures, namely, MA-PG type of UP and, MA-P

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Tassia, Yuliana, and 許麗琪. "Effects of silane-grafted silica nanoparticles and montmorillonite clay on the volume shrinkage, internal pigmentability, mechanical properties and cured sample morphology for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2013. http://ndltd.ncl.edu.tw/handle/75680818314138415635.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>101<br>The synthesis of silane-grafted silica nanoparticles with different size (d = 15 and 30 nm) and montmorillonite clay (MMT) with the subsequent characterization of the grafting efficiency, grafting density, as well as the surface silanol groups conversion have been carried out. The silane coupling agents used for the treatment are γ-methacryloxy propyl trimethoxy silane (MPS) and γ-glycidyloxy propyl trimethoxy silane (GPS). The effects of those silane-modified silica nanoparticles and MMT on the volume shrinkage characteristics, internal pigmentability, mechan

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HUANG, CHUN-HAN, and 黃俊翰. "Synthesis of nano-scale and submicron-scale acrylic type of core-shell rubber additives by conventional and RAFT living free radical emulsion polymerizations for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2009. http://ndltd.ncl.edu.tw/handle/92235201378167177074.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>97<br>Synthesis of acrylic type of core-shell rubbers (CSR) with varied nano-scale and submicron-scale particle size and shell chemical composition, reactive microgel, CSR by RAFT surfactant-free, batch emulsion polymerization , and CSR by RAFT polymerization via spontaneous phase inversion process as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) ,epoxy resin (EPR) and vinyl ester resin (VER) have been investigated . Two types of conventional nsaturated polyester resin with different chemical structures, namely, MA-PG type of UP an

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Yaung, Chang-Rui, and 楊昌叡. "Synthesis of nano-scale and submicron-scale polymeric core-shell rubber and reactive microgel particle as low-profile additives and tougheners for unsaturated polyester and vinyl ester resins by conventional emulsion polymerizations." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/vrabgk.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>105<br>Synthesis of nano-scale or submicron-scale general prepose core-shell rubber (gp-CSR) and nano-scale reactive microgel particles (RM) by conventional emulsion polymerization with or without surfactant as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) and vinyl ester resin (VER) have been investigated. Two types of UP with different chemical structures, namely, MA-PG and MA-PA-PG, as well as epoxy resin (EPR) and vinyl ester resin (VER) with degree of polymerization (n) = 0.16, 2, and 5, have also been synthesized so that styre

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Lin, Chien-chen, and 林建辰. "Synthesis of nano-scale colloidal silica from elemental silicon by hydrolysis, and synthesis of nano-scale inorganic silica/organic polymer core-shell particle as additives by RAFT living free radical polymerizations for unsaturated polyester, vinyl ester." Thesis, 2010. http://ndltd.ncl.edu.tw/handle/40515457249652869763.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>98<br>In the synthesis of the Si-PMA, the nano-scale colloidal silica was obtained by the hydrolysis of elemental silicon. Then silica was reacted with 4-(chloromethyl)phenyltrimethoxysilane to produce benzyl chloride functionalized silica(Si-Cl) first, followed by reacting with BSPA to make BSPA-grafted silica particle (Si-BSPA). Later, Si-BSPA can be use as a media in Si-poly(methyl acrylate)(i.e. Si-PMA) via Reversible Addition-Fragmentation Chain Transfer (RAFT) polymerization. During RAFT polymerization, the CTA will become a dormant specimen which made the p

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Liu, Gu-Hao, and 劉家豪. "Synthesis of nano-scale colloidal silica from elemental silicon by hydrolysis, and synthesis of nano-scale inorganic silica/organic polymer core-shell particle as additives by RAFT living free radical polymerizations for unsaturated polyester, vinyl ester." Thesis, 2011. http://ndltd.ncl.edu.tw/handle/77493157132117376181.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>99<br>In the synthesis of the Si-PMA, the nano-scale colloidal silica was obtained by the hydrolysis of elemental silicon. Then silica was reacted with 4-(chloromethyl)phenyltrimethoxysilane to produce benzyl chloride functionalized silica(Si-Cl) first, followed by reacting with BSPA to make BSPA-grafted silica particle (Si-BSPA). Later, Si-BSPA can be use as a RAFT agent to make in Si-poly(methyl acrylate)(i.e. Si-PMA) via Reversible Addition-Fragmentation Chain Transfer (RAFT) polymerization. During RAFT polymerization, the CTA chain transfer agent would become a

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HSU, Ting-Yu, and 許廷宇. "Effects of nano-scale and submicron-scale core-shell rubber additives, inorganic silica gel/organic polymer core-shell particle, and montmorillonite clay on the cure kinetics and glass transition temperatures for unsaturated polyester, vinyl ester, and ep." Thesis, 2009. http://ndltd.ncl.edu.tw/handle/98969309854803471161.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>97<br>Abstract The effects of nano-scale and submicron-scale core shell rubbers (CSR) as low-profile additives (LPA), and inorganic silica gel/organic polymer core-shell particle,and silane treated montmorillonite clay (MMT) on the cure kinetics and glass transition temperatures for styrene/unsaturated polyester (or vinyl ester) /additive ternary systems and epoxy/curing agent /additive ternary systems have been investigated. The reaction kinetics for the ST/UP (or VER)/additive ternary system and epoxy/curing agent /additive ternary systems during the cure was measu

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Yeh, Kuan-Liang, and 葉冠良. "Synthesis of nano-scale and submicron-scale polymeric core-shell rubber and reactive microgel particle as low-profile additives and tougheners for unsaturated polyester and vinyl ester resins by conventional and RAFT living free radical emulsion polymerizations." Thesis, 2015. http://ndltd.ncl.edu.tw/handle/61222478300393758470.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>103<br>Synthesis of nano-scale specific core-shell rubber (s-CSR) by RAFT soapless emulsion polymerization via spontaneous phase inversion process and nano-scale or submicron-scale general prepose core-shell rubber (gp-CSR) by conventional emulsion polymerization with or without surfactant as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) and vinyl ester resin (VER) have been investigated. Two types of conventional UP with different chemical structures, namely, MA-PG and MA-PA-PG, EPR and VER with degree of polymerization (n) = 0.16,

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LIN, YI-CHUN, and 林怡均. "Synthesis of polymer-grafted graphene oxide and polymer-grafted thermally reduced graphene oxide with core-shell structure as low-profile additives and tougheners for unsaturated polyester and vinyl ester resins by RAFT living free radical solution polymerizations." Thesis, 2016. http://ndltd.ncl.edu.tw/handle/57903281759454807292.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>104<br>Synthesis of polymer grafted graphene oxide with core-shell structure (CSS) as low-profile additives (LPA) and tougheners for thermoset resins, and their effects on the cured sample morphology, volume shrinkage characteristics and mechanical properties for low-shrink vinyl ester resins (VER) during the cure were investigated. These CSS designated as GO-polymer, which contained graphene oxide(GO) as the core and organic polymer as the shell, were synthesized by the Z supported reversible addition-fragmentation chain transfer (RAFT) graft polymerization using S-

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ZHONG, YONG-HONG, and 鐘永宏. "Synthesis of nano-scale and submicron-scale polymeric core-shell rubber and reactive microgel particle as low-profile additives and tougheners for unsaturated polyester and vinyl ester resins by conventional and RAFT living free radical emulsion polymerizations." Thesis, 2016. http://ndltd.ncl.edu.tw/handle/35723558925110953842.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>104<br>Synthesis of nano-scale specific core-shell rubber (s-CSR) by RAFT soapless emulsion polymerization via spontaneous phase inversion process and nano-scale or submicron-scale general prepose core-shell rubber (gp-CSR) by conventional emulsion polymerization with or without surfactant as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP) and vinyl ester resin (VER) have been investigated. Two types of conventional UP with different chemical structures, namely, MA-PG and MA-PA-PG, EPR and VER with degree of polymerization (n) = 0.16,

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Nien, Chun-Yen, and 粘純嫣. "Synthesis of polymer-grafted graphene oxide and polymer-grafted thermally reduced graphene oxide with core-shell structure as low-profile additives and tougheners for unsaturated polyester and vinyl ester resins by RAFT living free radical solution polymerizations." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/kszmmz.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>105<br>Synthesis of polymer grafted graphene oxide with core-shell structure (CSS) as low-profile additives (LPA) and tougheners for thermoset resins, and their effects on the cured sample morphology, volume shrinkage characteristics and mechanical properties for low-shrink vinyl ester resins (VER) during the cure were investigated. These CSS designated as GO-polymer, which contained graphene oxide(GO) as the core and organic polymer as the shell, were synthesized by the Z supported reversible addition-fragmentation chain transfer (RAFT) graft polymerization using S-

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Lin, Yueh-ping, and 林悅蘋. "Effects of nano-scale and submicron-scale core-shell rubber additives, silane-grafted montmorillonite, and functionalized exfoliated graphene nanoplatelet on the cure kinetics, glass transition temperatures, and X-ray scattering characteristics for unsaturated polyester, and vinyl ester resins." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/80971795037713583188.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>102<br>The effects of three additives, including (1) nano-scale and submicron-scale core-shell rubber additive, (2) silane-grafted montmorillonite and (3) functionalized exfoliated grapheme nanoplatelet, on the cure kinetics, glass transition temperature and X-ray scattering characteristics for the Styrene(St)/Unsaturated polyester (or Vinyl ester resin)/additives ternary systems after the cure have been investigated. The scattering intensity of vinyl ester resin (VER) and unsaturated polyester (UP) with different structure in dilute styrene solution was measured by

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Chung, Meng-ju, and 鍾孟儒. "Synthesis of nano-scale and submicron-scale polymeric core-shell rubber and reactive microgel particle as low-profile additives and tougheners for unsaturated polyester, vinyl ester, and epoxy resins by conventional and RAFT living free radical emulsion polymerizations." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/42114206940228275707.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>102<br>Synthesis of nano-scale specific core-shell rubber (s-CSR) by RAFT polymerization viaspontaneous phase inversion process and nano-scale or submicron-scale general prepose core-shell rubber (gp-CSR) byconventional emulsion polymerization with or without surfactant as low-profile additives (LPA) and tougheners for unsaturated polyester resins (UP), epoxy resin (EPR) and vinyl ester resin (VER) have been investigated. Two types of conventional UP with different chemical structures, namely, MA-PG and MA-PA-PG, EPR and VER with degree of polymerization (n) = 0.11,

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Yu, Ya-ting, and 余雅婷. "Synthesis of nano-scale colloidal silica from elemental silicon by hydrolysis, and synthesis of nano-scale inorganicsilica/organic polymer core-shell particle as additives by RAFT living free radical polymerizations for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2013. http://ndltd.ncl.edu.tw/handle/74133996909570431842.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>101<br>In the synthesis of the SiO2-PBA-b-PMA and SiO2-PBA-b-P(MA-co-GMA), the nano-scale colloidal silica (15~60nm) was obtained by the hydrolysis of elemental silicon. Then silica was reacted with 4-(chloromethyl)phenyltrimethoxysilane to produce benzyl chloride functionalized silica(SiO2-Cl) first, followed by reacting with BSPA to make BSPA-grafted silica particle (SiO2-BSPA). Later, SiO2-BSPA can be used as a RAFT agent to make SiO2-PBA-b-PMA (or SiO2-PBA-b-P(MA-co-GMA)) via Reversible Addition -Fragmentation Chain Transfer (RAFT) polymerization. During RAFT po

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CHEN, YEN-TING, and 陳彥廷. "Synthesis of nano-scale colloidal silica from elemental silicon by hydrolysis, and synthesis of nano-scale inorganic silica/organic polymer core-shell particle as additives by RAFT living free radical polymerizations for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2012. http://ndltd.ncl.edu.tw/handle/qc863x.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>100<br>In the synthesis of the Si-PMA and Si-PBA-b-PMA, the nano-scale colloidal silica was obtained by the hydrolysis of elemental silicon. Then silica was reacted with 4-(chloromethyl)phenyltrimethoxysilane to produce benzyl chloride functionalized silica(Si-Cl) first, followed by reacting with BSPA to make BSPA-grafted silica particle (Si-BSPA). Later, Si-BSPA can be used as a RAFT agent to make Si-poly(methyl acrylate) (i.e. Si-PMA) and Si-PBA-b-PMA via Reversible Addition -Fragmentation Chain Transfer (RAFT) polymerization. During RAFT polymerization, the CTA c

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Huang, Hsin-Yao, and 黃新堯. "Effects of nano-scale core-shell rubber additives, inorganic silica /organic polymer core-shell particle, and montmorillonite clay on the cure kinetics, glass transition temperatures, volume shrinkage, mechanical properties and cured sample morphology for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2012. http://ndltd.ncl.edu.tw/handle/s6k57x.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>100<br>The effects of four additives, including (1) nano- scale core-shell rubber additive,(2) inorganic silica gel/organic polymer core-shell particle, (3) organic montmorillonite clay, on the cure kinetics, glass transition temperatures, cured sample morphology, volume shrinkage characteristics and mechanical properties of the Styrene(St)/ Unsaturated polyester (or Vinyl ester resin)/ additives ternary systems and Epoxy/curing agent /additive ternary systems after the cure have been investigated. The experimental results have been explained by integrated measurem

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Liu, Yi-Shan, and 劉伊珊. "Effects of nano- and submicron-scale core-shell rubber, inorganic/organic hybrid core-shell particle, and montmorillonite clay on cure kinetics, glass transition temperatures, volume shrinkage, mechanical properties and cured sample morphology for unsaturated polyester, vinyl ester, and epoxy resins." Thesis, 2013. http://ndltd.ncl.edu.tw/handle/46798222045048248037.

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碩士<br>國立臺灣科技大學<br>化學工程系<br>101<br>The effects of four additives, including (1) nano- scale core-shell rubber additive,(2) inorganic silica gel/organic polymer core-shell particle, (3) organic montmorillonite clay, on the cure kinetics, glass transition temperatures, cured sample morphology, volume shrinkage characteristics and mechanical properties of the Styrene(St)/ Unsaturated polyester (or Vinyl ester resin)/ additives ternary systems and Epoxy/curing agent /additive ternary systems after the cure have been investigated. The experimental results have been explained by integrated measurem

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