Relevant bibliographies by topics / Urea assisted combustion synthesis

Contents

  1. Journal articles
  2. Dissertations / Theses
  3. Book chapters
  4. Conference papers
  5. Reports

Academic literature on the topic 'Urea assisted combustion synthesis'

Author: Grafiati
Published: 5 June 2025
Last updated: 15 July 2025

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Journal articles on the topic "Urea assisted combustion synthesis"

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Sahu, Ranjan K., A. K. Ray, S. K. Das, A. J. Kailath, and L. C. Pathak. "Microwave-assisted combustion synthesis of Ni powder using urea." Journal of Materials Research 21, no. 7 (2006): 1664–73. http://dx.doi.org/10.1557/jmr.2006.0211.

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A novel microwave-assisted combustion method was used to prepare Ni powder. The method involves the combustion reaction of nickel nitrate and urea as a fuel in the microwave field. The initiation of the exothermic peak of the combustion reaction was found to vary as a function of urea content. The microwave-prepared Ni powder was characterized using x-ray diffraction (XRD), scanning electron microscopy, atomic force microscopy, Fourier transform infrared spectroscopy, thermogravimetric (TG) analysis, differential thermal analysis (DTA), and magnetic measurement. The XRD pattern revealed that the Ni powder crystallizes with the cubic phase when the molar ratio of fuel to nitrate is varied between 5:1 and 6:1. Above or below that molar ratio, NiO phase coexists as an impurity along with the Ni phase. The magnetization value of Ni measured at room temperature is 53.5 Am2/kg, which is close to the value observed for commercial Ni powder (55.0 Am2/kg). The mechanism for the formation of the Ni and NiO phase is discussed based on the infrared, TG, and DTA data. The method shows that highly pure Ni powder can be prepared using urea as a fuel and microwaves as a source of energy via the solution combustion method.
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D., Narsimulu, Nageswara Rao B., Venkateswarlu M., and Satyanarayana N. "Synthesis and characterization of spinel LiMn2O4 nanoparticles by urea assisted combustion synthesis." Journal of Indian Chemical Society Vol. 92, May 2015 (2015): 792–95. https://doi.org/10.5281/zenodo.5704127.

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Department of Physics, Pondicherry University, Pondicherry-605 014, India <em>E-mail </em>: nallanis2011@gmail.com R &amp; D, Amararaja Batteries, Tirupati-517 501, Andhra Pradesh, India Spinel LiMn<sub>2</sub>O<sub>4</sub> has been widely used as cathode material in lithium ion batteries because of its high energy density, low cost, high abundance, environmental friendliness etc. The application of LiMn<sub>2</sub>O<sub>4</sub> in high power applications is limited by its low rate capability. In order to overcome this problem, attempts have made through the reduction of particle size from micro to nano scale. The nanosize materials not only increase the electrode-electrolyte surface contact area but also shortens the diffusion lengths of both electrons and lithium ions. Synthesis process plays a key role in developing various nanostructured materials. In the present work, nanocrystalline LiMn<sub>2</sub>O<sub>4</sub> particles were prepared by urea assisted combustion process using citric acid and urea as fuels. Thermal behavior, phase analysis, structural co-ordination, surface morphology, specific surface area and electrical conductivity of prepared LiMn<sub>2</sub>O<sub>4</sub> particles were studied through TG/DTA, XRD, FTIR, SEM, BET-surface area analysis and impedance spectroscopy measurements, respectively1,2 .
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Rai, Alok Kumar, Sungjin Kim, Jihyeon Gim, Muhammad Hilmy Alfaruqi, Vinod Mathew, and Jaekook Kim. "Electrochemical lithium storage of a ZnFe2O4/graphene nanocomposite as an anode material for rechargeable lithium ion batteries." RSC Adv. 4, no. 87 (2014): 47087–95. http://dx.doi.org/10.1039/c4ra08414d.

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A graphene-based ZnFe<sub>2</sub>O<sub>4</sub> nanocomposite synthesized using urea-assisted auto combustion synthesis shows improved electrode performance probably due to strong bonding and hence improved intrinsic conductivity of ZnFe<sub>2</sub>O<sub>4</sub>.
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Chandel, Sakshee, Seulgi Lee, Sungjin Kim, et al. "Structural and electrochemical behavior of a NiMnO3/Mn2O3 nanocomposite as an anode for high rate and long cycle lithium ion batteries." New Journal of Chemistry 43, no. 33 (2019): 12916–22. http://dx.doi.org/10.1039/c9nj02800e.

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In this work, first time a pre-designed NiMnO<sub>3</sub>/Mn<sub>2</sub>O<sub>3</sub> nanocomposite is synthesized via a facile urea-assisted auto-combustion synthesis with the phase fraction ratio of ∼89% and ∼11%, respectively as an anode material for lithium-ion batteries.
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Jalota, Sahil, A. Cuneyt Tas, and Sarit B. Bhaduri. "Microwave-assisted synthesis of calcium phosphate nanowhiskers." Journal of Materials Research 19, no. 6 (2004): 1876–81. http://dx.doi.org/10.1557/jmr.2004.0230.

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Calcium phosphate [single-phase hydroxyapatite (HA), single-phase tricalcium phosphate (TCP), and biphasic HA-TCP] nanowhiskers and/or powders were produced by using a novel microwave-assisted “combustion synthesis (auto ignition)/molten salt synthesis” hybrid route. This work is an example of our “synergistic processing” philosophy combining these three technologies while taking advantage of their useful aspects. Aqueous solutions containing NaNO3, Ca(NO3)2·4H2O and KH2PO4 (with or without urea) were irradiated in a household microwave oven for 5 min at 600 watts of power. The as-synthesized precursors were then simply stirred in water at room temperature for 1 h to obtain the nanowhiskers or powders of the desired calcium phosphate bioceramics.
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KASAPOGLU, N., A. BAYKAL, Y. KOSEOGLU, and M. TOPRAK. "Microwave-assisted combustion synthesis of CoFe2O4 with urea, and its magnetic characterization." Scripta Materialia 57, no. 5 (2007): 441–44. http://dx.doi.org/10.1016/j.scriptamat.2007.04.042.

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Luiz, Thaís, Fabio Nakagomi, Reny Renzetti, and Guilherme Siqueira. "Nb2O5 nanoparticles obtained by microwave assisted combustion synthesis under different conditions." Processing and Application of Ceramics 15, no. 2 (2021): 128–35. http://dx.doi.org/10.2298/pac2102128l.

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The microwave assisted combustion synthesis (MACS) as a new, quick and low cost synthesis method was used for preparation of niobium pentoxide (Nb2O5) powders. The present paper investigated the effect of reactant concentrations (ammonium niobium oxalate, urea and ammonium nitrate) on the characteristics of Nb2O5 nanoparticles. Three samples were synthesized with stoichiometric ratio between the fuel and oxidant (C1), excess of oxidant (C2) and excess of fuel (C3). In all samples, Nb2O5 crystalline nanoparticles with irregular morphology were detected. The synthesis of nanoparticles with smaller diameter in the C2 and C3 samples was confirmed by greater values of band gap energy measured through UV-Visible diffuse reflectance spectroscopy (indicating quantum confinement) and by the Rietveld refinement of X-ray diffraction patterns. The results showed that the amounts of oxidant and fuel can change synthesis temperature, influencing the final characteristics of the particles, such as size and existent phases. In these cases the excess of oxidant and fuel in the C2 and C3 samples, respectively, decreases the average synthesis temperature and decelerates the particle growth and the formation of the monoclinic phase.
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Mishra, Girish C., Kabita Ku Satapathy, Sanjay J. Dhoble, and Rajiv S. Kher. "Urea assisted self combustion synthesis of CaAl2O4:Eu phosphor and its mechanoluminescence characterization." New J. Chem. 41, no. 5 (2017): 2193–97. http://dx.doi.org/10.1039/c6nj02514e.

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WEN, FENGYU. "SYNTHESIS AND ROOM TEMPERATURE FERROMAGNETIC PROPERTY OF COBALT DOPED ZINC OXIDE." Modern Physics Letters B 23, no. 14 (2009): 1799–804. http://dx.doi.org/10.1142/s021798490901996x.

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Nanocrystalline Co -doped ZnO ( Zn 1-x Co x O , x = 0.00, 0.05) powders have been successfully prepared by a microwave-assisted combustion method using Zn ( NO 3)2·6 H 2 O and Co ( NO 3)2·6 H 2 O as starting materials and urea as fuel. The as-prepared products were characterized by X-ray diffractometer (XRD), scanning electron microscope (SEM) and vibrating sample magnetometer (VSM). It was found that the combustion process took only a few minutes to obtain Zn 1-x Co x O powders. The field dependence of magnetization measurement at room temperature for the as-prepared Zn 0.95 Co 0.05 O powders exhibited the obvious ferromagnetic behavior.
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Lu, Yani, Xiangyu Ma, Jinping Ren, Jinke Kang, and Yatao Wang. "Exploration of the Reduction Diffusion Temperature for Different Phases of Samarium–Cobalt Magnetic Particles." Molecules 30, no. 9 (2025): 1975. https://doi.org/10.3390/molecules30091975.

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We report a method for synthesizing different phases of samarium–cobalt particles through microwave-assisted combustion combined with high-temperature reduction and diffusion, and identify the optimal temperature for forming the 1:5 phase using this approach. Initially, the samarium-to-cobalt ratio in a nitrate solution was determined. Using urea as both a reductant and fuel, samarium–cobalt oxides were synthesized via microwave-assisted combustion. The main components of the oxides were confirmed to be SmCoO3 and Co3O4. Subsequently, samarium–cobalt particles were synthesized at various diffusion temperatures. The results indicate that at 700 °C, the oxides were reduced to elemental Sm and Co. As the reduction temperature increased, the alloying of samarium and cobalt occurred, and the particle size gradually increased. At 900 °C, a pure 1:5 phase was formed, with particle sizes of approximately 800 nm, a coercivity of 35 kOe, and a maximum energy product of 14 MGOe. Based on the microwave-assisted combustion method, this study clarifies the transition temperatures of samarium–cobalt phases during the reduction and diffusion process, and further establishes the synthesis temperature for the 1:5 phase, providing new insights into the preparation and development of samarium–cobalt materials and potentially other rare earth materials.
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Dissertations / Theses on the topic "Urea assisted combustion synthesis"

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Cansin, Badan. "Microwave Assisted Synthesis Of Rare Earth Ions Doped Lanthanumorthoborate, Their Characterizations And Investigations Ofluminescence Properties." Master's thesis, METU, 2012. http://etd.lib.metu.edu.tr/upload/12614361/index.pdf.

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Lanthanum orthoborate (LaBO3) has aroused interest of scientists for many decades because of their remarkable properties and potential applications. They provide favorable magnetic properties for various applications. Additionally, they possess high VUV transparency and exceptional optical damage when they compose with rare earth elements. This study comprises the synthesis of pure lanthanum orthoborate, europium, dysprosium and terbium doped lanthanum orthoborate by two methods with v three fuels, citric acid, glycine and urea. LaBO3 has already been synthesized by various methods, however<br>in this work, two alternative roads are suggested, microwave assisted method and sol-gel microwave assisted method. The second task of the work is to find out the best luminescent product by altering the synthesis conditions, type of the doping material and the doping amount of the rare earth element. For the microwave assisted combustion method, urea was used as a fuel. After synthesis in the microwave oven, further heating up to 950&deg<br>C was performed. For the microwave assisted sol-gel method, citric acid and glycine were used. After obtaining the gel mixture, the product is synthesized in the microwave oven at 1200 W for ten minutes. For this route, again 950&deg<br>C heating for 2 hours was performed. Powder X-ray diffraction method was employed for the characterization of the material. The morphological properties of doped and un-doped materials were studied by SEM (Scanning Electron Microscope) and TEM (Transmission Electron Microscope). Besides, FT-IR (Fourier Transform Infra red) spectrometry analyses were performed to detect the differences in the bond structure and also to identify the corresponding bands. Luminescence studies were performed to detect the best emission intensities by using Fluorescence spectroscopy. The XRD patterns confirmed that lanthanum orthoborate production was successful by three precursors. The space group is Pnma, and the crystal system is orthorhombic with the unit cell dimensions<br>a= 5.8761(1)
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Chen, Chia-Ming, and 陳嘉民. "Preparation of phosphor powders using microwave assisted solution combustion synthesis method." Thesis, 2006. http://ndltd.ncl.edu.tw/handle/30680373239936951856.

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碩士<br>國立成功大學<br>化學工程學系碩博士班<br>94<br>Microwave heating technique is a high efficient heating way, and there are many advantages such as capable of achieving high temperature, rapid, and uniform heating, therefore, it has been used widely recently. In this thesis, the microwave-assisted the solution combustion method was used to prepare Zn2SiO4:Mn, Y2O3:Eu, Y3Al5O11:Ce, BaMgAl10O17:Eu phosphors which can emit different colors, respectively. The experimental parameters such as active ion concentration, firing temperature, the origin of reactant, fuel, firing atmosphere, the type of firing, will be discussed to find the essential factor and to research better phosphor and high efficient phosphors could be obtained. For Zn2SiO4:Mn, the results show that the highest luminescent intensity could be achieved after calcining at 1200℃(under nitrogen atmosphere) with 3 mol% Mn doped. For YAG, the highest luminescent intensity was at 1600℃ with 3.5% Ce doped. For Y2O3, the highest luminescent intensity was at 1200℃ with 15% Eu doped. As shown in XRD patterns, a high purity of BAM structure could be obtained when calcined at 1400℃and the crystalline increases with increasing temperature and reaches its maximum at 1650℃ under reducing atmosphere (5% H2 + 95% N2) with 6% Eu doped.
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Yang, Chuan-Kai, and 楊筌凱. "Synthesis of Hierarchical BiOBr Microspheres by Microwave-Assisted Hydrothermal Combustion for Photocatalytic Reactions." Thesis, 2013. http://ndltd.ncl.edu.tw/handle/92872934886708319736.

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碩士<br>逢甲大學<br>環境工程與科學學系<br>101<br>Semiconductor photocatalysts, such as TiO2 and ZnO, have been widely studied by many researchers. However, this type of photocatalyst can only be activated under UV light irradiation (λ < 400 nm) to create effective separation of electrons and holes, thereby facilitating the degradation of pollutants in the environment. Since UV light accounts for only a small portion of the solar spectrum, to fully harvest visible light bismuth oxyhalides, BiOX (X = Cl, Br, I), was chosen as a photocatalyst in this research and bismuth oxybromide could feature a unique layered structure, appropriate energy gap, favorable stability, and excellent photocatalytic performance. In this study, the microwave-assisted hydrothermal method was adopted. Using a reaction time and temperature of 10 min and 140 °C, respectively, 0.05 g of dispersant, and a synthetic solvent ratio of 75% EtOH: 25% EG can provide an optimal condition for synthesizing hierarchical BiOBr microspheres assembled by nanosheets. By employing several characterization analyses of as-synthesized photocatalyst (i.e., XRD, FE-SEM, FE-TEM, XPS, DRS, and BET), the crystal structure, elemental composition, and optical properties of the hierarchical BiOBr microspheres have been verified for the subsequent experiments regarding the photocatalytic degradation of tartaric acid. The catalyst materials were applied for the removal of tartaric acid, a model contaminant, in a synthetic solution by the process that combines heterogeneous catalysis with visible light photocatalysis. No degradation of tartaric acids was observed about 6 hours of visible light irradiation without using any BiOBr catalyst. However, upon the addition of BiOBr nanosheet microspheres, a considerable degradation was noted in 4 hours. The linear relationship between ln(C/C0) and time was utilized and it indicates that the degradation follows pseudo-first-order kinetics. According to the slopes of ln(C/C0) versus time, the first order rate constant was calculated for visible photocatalytic of tartaric acid at 8.31x10-4 min-1 with BiOBr, compared to 1.52x10-4 min-1 withour BiOBr. Furthermore, this photocatalyst has exhibited a high mineralization rate, high stability, and easy separation for recycling use, suggesting that BiOBr is a promising photocatalyst for the removal of organic pollutants in aqueous environemnt.
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Book chapters on the topic "Urea assisted combustion synthesis"

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Yilmaz, Esma, M. Seref Sonmez, Bora Derin, Filiz Cinar Sahin, and Onuralp Yucel. "Synthesis of Mn2O3 Nanopowders with Urea and Citric Acid by Solution Combustion Route." In TMS 2017 146th Annual Meeting & Exhibition Supplemental Proceedings. Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-51493-2_5.

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Jithin, P. V., and Joji Kurian. "Structural Study of Ethylene Glycol-Assisted Solution Combustion Synthesis of Strontium Doped LaMnO3." In Nanostructured Smart Materials. Apple Academic Press, 2021. http://dx.doi.org/10.1201/9781003130468-10.

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Jung, Young Mi, and Sang Woo Kim. "Microwave-Assisted Combustion Synthesis of α-Alumina and Magnesium Aluminate Spinel Nanocomposite Powders." In Solid State Phenomena. Trans Tech Publications Ltd., 2007. http://dx.doi.org/10.4028/3-908451-27-2.191.

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Meng, Qing Sen, Shao Ping Chen, Y. L. Shen, C. R. Liu, and Z. A. Munir. "Microstructure and Mechanical Properties of Graded Materials Prepared by Field-Activated and Pressure-Assisted Combustion Synthesis." In High-Performance Ceramics V. Trans Tech Publications Ltd., 2008. http://dx.doi.org/10.4028/0-87849-473-1.1876.

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Costa, A. C. F. M., D. A. Vieira, V. C. Diniz, H. L. Lira, D. R. Cornejo, and R. H. G. A. Kiminami. "Effect of Different Fuels on the Microwave-Assisted Combustion Synthesis of Ni0.5 Zn0.5 Fe1.95 Sm0.05 O4 Ferrites." In Ceramic Transactions Series. John Wiley & Sons, Inc., 2011. http://dx.doi.org/10.1002/9781118144442.ch17.

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Singh, Laxman, Dev Kumar Mahato, R. N. Rai, Ashok Kumar Gupta, and Youngil Lee. "Citric Acid–Assisted Inexpensive Semi-wet Combustion Synthesis and Characterization of Ultrafine LiFe0.95Ti0.05PO4 and LiFePO4 Polycrystalline Materials." In Nanocomposites. Jenny Stanford Publishing, 2022. http://dx.doi.org/10.1201/9781003314479-6.

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Ergin, Nuri, Gokhan Yoruk, and Ozkan Ozdemir. "Production of $$\mathrm{Ni}_{3}$$ Ni 3 Al and $$\mathrm{Ti}_{3}$$ Ti 3 Al Based Coating by Using Pressure Assisted Combustion Synthesis." In International Multidisciplinary Microscopy Congress. Springer International Publishing, 2014. http://dx.doi.org/10.1007/978-3-319-04639-6_4.

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Kharatyan, Suren L. "Chemically Assisted Combustion Synthesis." In Concise Encyclopedia of Self-Propagating High-Temperature Synthesis. Elsevier, 2017. http://dx.doi.org/10.1016/b978-0-12-804173-4.00028-4.

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"Salt-Assisted Solution Combustion Synthesis." In Combustion Synthesis: Novel Routes to Novel Materials, edited by Weifan Chen, Fengsheng Li, and Yuping Tong. BENTHAM SCIENCE PUBLISHERS, 2012. http://dx.doi.org/10.2174/978160805155711001010141.

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Manukyan, Khachatur V. "Template-Assisted Solution Combustion Synthesis." In Concise Encyclopedia of Self-Propagating High-Temperature Synthesis. Elsevier, 2017. http://dx.doi.org/10.1016/b978-0-12-804173-4.00153-8.

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Conference papers on the topic "Urea assisted combustion synthesis"

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Wu, M. M., Z. Y. Wen, Z. Z. Fan та Z. X. Lin. "GLYCINE-UREA-NITRATE COMBUSTION SYNTHESIS FOR γ- LiAlO2". У Proceedings of the 7th Asian Conference. WORLD SCIENTIFIC, 2000. http://dx.doi.org/10.1142/9789812791979_0106.

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Rahmawati, Mintarsih, Agus Purwanto, Hendri Widiyandari, et al. "Synthesis of NMC 111 via urea assisted solid state method." In PROCEEDINGS OF 2ND INTERNATIONAL CONFERENCE ON CHEMICAL PROCESS AND PRODUCT ENGINEERING (ICCPPE) 2019. AIP Publishing, 2020. http://dx.doi.org/10.1063/1.5140919.

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Widiyastuti, Adhi Setiawan, Heru Setyawan, et al. "Diffusion Flame Synthesis of Hydroxyapatite Nanoparticles using Urea Assisted Precursor Solution." In THE 4TH NANOSCIENCE AND NANOTECHNOLOGY SYMPOSIUM (NNS2011): An International Symposium. AIP, 2011. http://dx.doi.org/10.1063/1.3667244.

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Han, Y. X., H. Ling, and Y. F. Lu. "Laser-assisted combustion-flame synthesis of diamond films." In ICALEO® 2006: 25th International Congress on Laser Materials Processing and Laser Microfabrication. Laser Institute of America, 2006. http://dx.doi.org/10.2351/1.5060865.

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Pathak, Sanjay Kumar, Akshkumar Verma, and Ashish Verma. "Adjusting thermo-luminescence properties of ZnAl2O4:Eu, Dy phosphor by urea fuel combustion synthesis." In 3RD INTERNATIONAL CONFERENCE ON CONDENSED MATTER AND APPLIED PHYSICS (ICC-2019). AIP Publishing, 2020. http://dx.doi.org/10.1063/5.0001127.

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Pathak, Sanjay Kumar, Akshkumar Verma, and Ashish Verma. "Shifting optical-luminescence properties of ZnAl2O4:Eu, Dy phosphor by urea fuel combustion synthesis." In 3RD INTERNATIONAL CONFERENCE ON CONDENSED MATTER AND APPLIED PHYSICS (ICC-2019). AIP Publishing, 2020. http://dx.doi.org/10.1063/5.0001136.

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Aminikia, Behzad. "Synthesis of nano-crystalline TaC−TaB[sub 2] by microwave-assisted combustion synthesis." In 3RD INTERNATIONAL ADVANCES IN APPLIED PHYSICS AND MATERIALS SCIENCE CONGRESS. AIP, 2013. http://dx.doi.org/10.1063/1.4849226.

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Kumar, Anand. "Cellulose assisted combustion synthesis of nanomaterials for energy conversion applications." In 2018 IEEE 18th International Conference on Nanotechnology (IEEE-NANO). IEEE, 2018. http://dx.doi.org/10.1109/nano.2018.8706512.

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Chaudhari, Prashant, S. A. Acharya, S. S. Darunkar, and V. M. Gaikwad. "Microwave assisted combustion synthesis of nanocrystalline CoFe2O4 for LPG sensing." In ADVANCED MATERIALS AND RADIATION PHYSICS (AMRP-2015): 4th National Conference on Advanced Materials and Radiation Physics. AIP Publishing LLC, 2015. http://dx.doi.org/10.1063/1.4929193.

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Moiseev, N. V., A. P. Amosov, V. A. Novikov, A. A. Vikarchuk, and I. M. Sosnin. "Physics and chemistry of solution combustion synthesis of zinc oxide nanopowder from zinc nitrate-urea reagents." In INTERNATIONAL CONFERENCE ON PHYSICS AND CHEMISTRY OF COMBUSTION AND PROCESSES IN EXTREME ENVIRONMENTS (COMPHYSCHEM’20-21) and VI INTERNATIONAL SUMMER SCHOOL “MODERN QUANTUM CHEMISTRY METHODS IN APPLICATIONS”. AIP Publishing, 2020. http://dx.doi.org/10.1063/5.0034761.

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Reports on the topic "Urea assisted combustion synthesis"

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Klotz, Bradley R., Franklyn R. Kellogg, and Kyu C. Cho. Characterization and Consolidation of Tungsten Nanopowders Produced by Salt-Assisted Combustion Synthesis. Defense Technical Information Center, 2010. http://dx.doi.org/10.21236/ada532057.

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